Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
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inquiryAS No: 117445-22-4 Product name: Boc-3-Aminomethylbenzoic acid Appearance: White powder Purity: 97% Color: White Molecular Formula: C13H17NO4 Molecular Weight: 251.28 Appearance: white powder Storage:Store in cool and dry place, away fr
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inquiryBoc-3-Aminomethylbenzoic acid CAS:117445-22-4 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality o
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquiryOur Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
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inquiryA substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
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inquiryWe are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov
Cas:117445-22-4
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inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
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inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
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inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
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inquiryWe product this chemical more than 10 years . We are very experience to export it to many countries, Our superior & stable quality , competitive price gain warm reception from our customers. Specification : Boc-3-Aminomethylbenzoic acid CA
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inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
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inquiryAppearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
High quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use
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inquiryWe are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp
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inquiryStock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
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inquiryThe process is mature and can be mass produced to 100 kg, with good quality and purity up to 99%.The product has a large stock and can be supplied stably. Package:bottle Application:Drug R&D Transportation:Sealed drying(25℃) Port:ShangHai
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inquiryLower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
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inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
1.A strong technical force and advanced processing equipments. The quality of the products has been strictly inspected and all kinds of index have reached or exceeded domestic and international standards.2. Now we have established long-term stable re
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inquiryhigh qualityAppearance:white crystalline powder Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
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inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:Beijing or Guangzhou
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inquiry1.Our services:A.Supply sampleB.The packing also can be according the customers` requirmentC.Any inquiries will be replied within 24 hoursD.we provide Commerical Invoice, Packing List, Bill of loading, COA , Health certificate and Origin certificate.
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inquirybulk productiongoods in stockswe have the best competitive price in the marketmeantime,we are committed to service to our every customer Chemsigma International Co.,Ltd. is a chemical manufacturer, specialize in custom synthesis and organic chemical
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inquiryAnsciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
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inquiryBoc-3-aminomethylbenzoic acid Application:Boc-3-aminomethylbenzoic acid
2-(tert-Butoxycarbonyloxyimino)-2-phenylacetonitrile
3-aminomethylbenzoic acid
3-(tert-butoxycarbonylamino-methyl)benzoic acid
Conditions | Yield |
---|---|
With triethylamine | 75% |
3-aminomethylbenzoic acid
3-(tert-butoxycarbonylamino-methyl)benzoic acid
Conditions | Yield |
---|---|
With di-tert-butyl dicarbonate; triethylamine In 1,4-dioxane; water | 68% |
2-(tert-Butoxycarbonyloxyimino)-2-phenylacetonitrile
3-(aminomethyl)benzoic acid hydrochloride
3-(tert-butoxycarbonylamino-methyl)benzoic acid
Conditions | Yield |
---|---|
With triethylamine In water Ambient temperature; | 64% |
methyl 3-(((tert-butoxycarbonyl)amino)methyl)benzoate
3-(tert-butoxycarbonylamino-methyl)benzoic acid
Conditions | Yield |
---|---|
Stage #1: methyl 3-(((tert-butoxycarbonyl)amino)methyl)benzoate With water; lithium hydroxide In tetrahydrofuran at 25 - 50℃; for 4h; Stage #2: With acetic acid In ethyl acetate | 44% |
Stage #1: methyl 3-(((tert-butoxycarbonyl)amino)methyl)benzoate With water; lithium hydroxide In tetrahydrofuran at 50℃; for 4h; Stage #2: With acetic acid | 44% |
di-tert-butyl dicarbonate
3-aminomethylbenzoic acid
3-(tert-butoxycarbonylamino-methyl)benzoic acid
Conditions | Yield |
---|---|
With sodium hydroxide In 1,4-dioxane | |
With sodium hydrogencarbonate In 1,4-dioxane; water |
3-Cyanobenzoic acid
3-(tert-butoxycarbonylamino-methyl)benzoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: NH3 / Raney Ni / ethanol / 51714.8 Torr 2: aq. NaOH / dioxane View Scheme | |
Multi-step reaction with 2 steps 1: 64 percent / H2, conc. HCl / 10percent Pd/C / ethanol / 38 h 2: 64 percent / Et3N / H2O / Ambient temperature View Scheme | |
Multi-step reaction with 2 steps 1: 95 percent / hydrogen / Pd/C 2: 75 percent / triethylamine View Scheme |
3-Cyanobenzoic acid
di-tert-butyl dicarbonate
3-(tert-butoxycarbonylamino-methyl)benzoic acid
Conditions | Yield |
---|---|
palladium on carbon In ethanol |
dichloromethane
3-Cyanobenzoic acid
di-tert-butyl dicarbonate
3-(tert-butoxycarbonylamino-methyl)benzoic acid
Conditions | Yield |
---|---|
palladium In methanol; ethanol |
3-bromomethylbenzoic acid
3-(tert-butoxycarbonylamino-methyl)benzoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: thionyl chloride / 1 h / 25 °C / Reflux 2: N,N-dimethyl-formamide / 12 h / 85 °C 3: hydrazine hydrate / methanol / 4 h / 25 °C / Reflux 4: sodium hydrogencarbonate / ethyl acetate; water / 1.17 h / pH 8 5: water; lithium hydroxide / tetrahydrofuran / 4 h / 25 - 50 °C View Scheme | |
Multi-step reaction with 5 steps 1: thionyl chloride / 1 h / 25 °C / Reflux 2: N,N-dimethyl-formamide / 12 h / 85 °C 3: hydrazine hydrate / methanol / 4 h / Reflux 4: sodium hydrogencarbonate / ethyl acetate; water / 1.17 h / pH 8 5: water; lithium hydroxide / tetrahydrofuran / 4 h / 50 °C View Scheme |
m-Toluic acid
3-(tert-butoxycarbonylamino-methyl)benzoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1: N-Bromosuccinimide / 2,2'-azobis(isobutyronitrile) / tetrachloromethane / 3 h / 25 °C / Reflux 2: thionyl chloride / 1 h / 25 °C / Reflux 3: N,N-dimethyl-formamide / 12 h / 85 °C 4: hydrazine hydrate / methanol / 4 h / 25 °C / Reflux 5: sodium hydrogencarbonate / ethyl acetate; water / 1.17 h / pH 8 6: water; lithium hydroxide / tetrahydrofuran / 4 h / 25 - 50 °C View Scheme | |
Multi-step reaction with 6 steps 1: N-Bromosuccinimide / 2,2'-azobis(isobutyronitrile) / tetrachloromethane / 3 h / 25 °C / Reflux 2: thionyl chloride / 1 h / 25 °C / Reflux 3: N,N-dimethyl-formamide / 12 h / 85 °C 4: hydrazine hydrate / methanol / 4 h / Reflux 5: sodium hydrogencarbonate / ethyl acetate; water / 1.17 h / pH 8 6: water; lithium hydroxide / tetrahydrofuran / 4 h / 50 °C View Scheme |
3-methoxycarbonylbenzyl bromide
3-(tert-butoxycarbonylamino-methyl)benzoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: N,N-dimethyl-formamide / 12 h / 85 °C 2: hydrazine hydrate / methanol / 4 h / 25 °C / Reflux 3: sodium hydrogencarbonate / ethyl acetate; water / 1.17 h / pH 8 4: water; lithium hydroxide / tetrahydrofuran / 4 h / 25 - 50 °C View Scheme | |
Multi-step reaction with 4 steps 1: N,N-dimethyl-formamide / 12 h / 85 °C 2: hydrazine hydrate / methanol / 4 h / Reflux 3: sodium hydrogencarbonate / ethyl acetate; water / 1.17 h / pH 8 4: water; lithium hydroxide / tetrahydrofuran / 4 h / 50 °C View Scheme |
3-(tert-butoxycarbonylamino-methyl)benzoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: sodium hydrogencarbonate / ethyl acetate; water / 1.17 h / pH 8 2: water; lithium hydroxide / tetrahydrofuran / 4 h / 25 - 50 °C View Scheme | |
Multi-step reaction with 2 steps 1: sodium hydrogencarbonate / ethyl acetate; water / 1.17 h / pH 8 2: water; lithium hydroxide / tetrahydrofuran / 4 h / 50 °C View Scheme |
3-(1, 3-Dioxo-1,3-dihydro-isoindol-2-ylmethyl)-benzoic acid methyl ester
3-(tert-butoxycarbonylamino-methyl)benzoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: hydrazine hydrate / methanol / 4 h / 25 °C / Reflux 2: sodium hydrogencarbonate / ethyl acetate; water / 1.17 h / pH 8 3: water; lithium hydroxide / tetrahydrofuran / 4 h / 25 - 50 °C View Scheme | |
Multi-step reaction with 3 steps 1: hydrazine hydrate / methanol / 4 h / Reflux 2: sodium hydrogencarbonate / ethyl acetate; water / 1.17 h / pH 8 3: water; lithium hydroxide / tetrahydrofuran / 4 h / 50 °C View Scheme |
3-(tert-butoxycarbonylamino-methyl)benzoic acid
trifluoroacetic acid
3-(aminomethyl)benzoic acid trifluoroacetate
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 1h; | 100% |
2-methylphenethylamine
3-(tert-butoxycarbonylamino-methyl)benzoic acid
3-aminomethyl-N-(2-o-tolyl-ethyl)-benzamide
Conditions | Yield |
---|---|
With benzotriazol-1-ol; 1,2-dichloro-ethane In ethyl acetate; N,N-dimethyl-formamide | 93% |
3-(tert-butoxycarbonylamino-methyl)benzoic acid
1,1-dimethylethyl {[3-(hydroxymethyl)phenyl]methyl}carbamate
Conditions | Yield |
---|---|
Stage #1: 3-(tert-butoxycarbonylamino-methyl)benzoic acid With 4-methyl-morpholine; isobutyl chloroformate In tetrahydrofuran at 0℃; for 0.166667h; Stage #2: With sodium tetrahydroborate In methanol for 0.5h; | 93% |
Stage #1: 3-(tert-butoxycarbonylamino-methyl)benzoic acid With dimethylsulfide borane complex In tetrahydrofuran at 25℃; for 2h; Stage #2: With ammonium chloride In tetrahydrofuran | 86% |
Stage #1: 3-(tert-butoxycarbonylamino-methyl)benzoic acid With dimethylsulfide borane complex In tetrahydrofuran at 25℃; for 2h; Cooling with ice; Stage #2: With ammonium chloride In tetrahydrofuran | 86% |
With dimethylsulfide borane complex In tetrahydrofuran at 20℃; for 24h; Inert atmosphere; | 74% |
With dimethyl sulfide borane In tetrahydrofuran at 20℃; for 3h; |
2-amino-5-methyl-4,5,6,7-tetrahydrothiazolo[5,4-c]pyridine
3-(tert-butoxycarbonylamino-methyl)benzoic acid
[3-(5-methyl-4,5,6,7-tetrahydro-thiazolo[5,4-c]pyridin-2-ylcarbamoyl)-benzyl]-carbamic acid tert-butyl ester
Conditions | Yield |
---|---|
With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; | 90% |
N-(3,5-dichlorobenzyl)-1-(4-fluorophenyl)methanamine
3-(tert-butoxycarbonylamino-methyl)benzoic acid
tert-butyl 3-((3,5-dichlorobenzyl)(4-fluorobenzyl)carbamoyl)benzylcarbamate
Conditions | Yield |
---|---|
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In N,N-dimethyl-formamide at 20℃; for 20h; | 89% |
3-(tert-butoxycarbonylamino-methyl)benzoic acid
Conditions | Yield |
---|---|
With 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In N,N-dimethyl-formamide at 20℃; for 16h; | 89% |
benzyl bromide
3-(tert-butoxycarbonylamino-methyl)benzoic acid
Conditions | Yield |
---|---|
Stage #1: 3-(tert-butoxycarbonylamino-methyl)benzoic acid With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 0.333333h; Stage #2: benzyl bromide In N,N-dimethyl-formamide at 20℃; for 6h; | 88% |
With caesium carbonate In N,N-dimethyl-formamide |
(4-nitrophenyl)(phenyl)methanone oxime
3-(tert-butoxycarbonylamino-methyl)benzoic acid
Boc-Mamb-Ox
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In dichloromethane Ambient temperature; | 79% |
With dmap; dicyclohexyl-carbodiimide | 52% |
dimethyl amine
3-(tert-butoxycarbonylamino-methyl)benzoic acid
Conditions | Yield |
---|---|
Stage #1: 3-(tert-butoxycarbonylamino-methyl)benzoic acid With 1,1'-carbonyldiimidazole In tetrahydrofuran for 3h; Stage #2: dimethyl amine In tetrahydrofuran at 60℃; for 16h; | 77% |
N-propylcyclohexylamine
3-(tert-butoxycarbonylamino-methyl)benzoic acid
C22H34N2O3
Conditions | Yield |
---|---|
Stage #1: 3-(tert-butoxycarbonylamino-methyl)benzoic acid With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide for 0.333333h; Stage #2: N-propylcyclohexylamine In N,N-dimethyl-formamide for 1h; | 76% |
1,1-diphenyltetrahydro-1H-oxazolo[3,4-α]pyrazin-3(5H)-one
3-(tert-butoxycarbonylamino-methyl)benzoic acid
Conditions | Yield |
---|---|
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In acetonitrile at 20℃; for 15h; | 75% |
3-(tert-butoxycarbonylamino-methyl)benzoic acid
5-amino-m-xylylenebis(phosphonic acid) tetramethyl ester
Conditions | Yield |
---|---|
With 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; N-ethyl-N,N-diisopropylamine In dichloromethane; ethyl acetate at 20℃; for 16h; | 73% |
4-(dimethylaminomethyl)aniline
3-(tert-butoxycarbonylamino-methyl)benzoic acid
[3-(4-dimethylaminomethylphenylcarbamoyl)benzyl]carbamic acid tert-butyl ester
Conditions | Yield |
---|---|
With 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In N,N-dimethyl-formamide | 69% |
Stage #1: 4-(dimethylaminomethyl)aniline; 3-(tert-butoxycarbonylamino-methyl)benzoic acid With 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In N,N-dimethyl-formamide for 48h; Stage #2: In dichloromethane |
N-(p-toluenesulfonyl)aziridine
3-(tert-butoxycarbonylamino-methyl)benzoic acid
Conditions | Yield |
---|---|
With mesitylenecarboxylic acid; palladium diacetate; caesium carbonate at 50℃; for 24h; Sealed tube; | 67% |
3-(tert-butoxycarbonylamino-methyl)benzoic acid
Conditions | Yield |
---|---|
Stage #1: β-dihydronaltrexamine; 3-(tert-butoxycarbonylamino-methyl)benzoic acid With HATU In N,N-dimethyl-formamide at 20℃; for 0.0833333h; Inert atmosphere; Stage #2: With N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; for 2h; Inert atmosphere; | 66% |
3-(tert-butoxycarbonylamino-methyl)benzoic acid
Conditions | Yield |
---|---|
With 1-hydroxy-pyrrolidine-2,5-dione; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide at 20℃; for 18h; | 59% |
1-(2-aminoethyl)pyrrolidine
3-(tert-butoxycarbonylamino-methyl)benzoic acid
[3-(2-pyrrolidin-1-yl-ethylcarbamoyl)-benzyl]-carbamic acid tert-butyl ester
Conditions | Yield |
---|---|
With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine In N,N-dimethyl-formamide at 20℃; for 15h; | 58% |
3-(tert-butoxycarbonylamino-methyl)benzoic acid
methyl iodide
Nα-(tert-butyloxycarbonyl)-Nα-methyl-m-(aminomethyl)benzoic acid
Conditions | Yield |
---|---|
With silver(l) oxide In N,N-dimethyl-formamide at 45℃; for 42h; | 53% |
4-(1,3,2-dithiocycloarsenic-2-yl)aniline
3-(tert-butoxycarbonylamino-methyl)benzoic acid
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In dichloromethane at 20℃; for 4h; | 50% |
1-(3'-ethyl-6-fluorobiphenyl-2-yl)-5-methoxy-1-(piperidin-4-yl)pentan-1-ol
3-(tert-butoxycarbonylamino-methyl)benzoic acid
tert-butyl 3-(4-(1-(3'-ethyl-6-fluorobiphenyl-2-yl)-1-hydroxy-5-methoxypentyl)piperidine-1-carbonyl)benzylcarbamate
Conditions | Yield |
---|---|
With benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 25℃; for 20h; | 42% |
BOC-glycine
Boc-Arg(Tos)-OH
Boc-Asp(O-cyclohexyl)-OH
3-(tert-butoxycarbonylamino-methyl)benzoic acid
Conditions | Yield |
---|---|
solid-phase synthesis using p-nitrobenzophenone oxime resin; Yield given. Multistep reaction; |
BOC-glycine
Boc-Arg(Tos)-OH
Boc-Asp(O-cyclohexyl)-OH
3-(tert-butoxycarbonylamino-methyl)benzoic acid
Conditions | Yield |
---|---|
solid-phase synthesis using p-nitrobenzophenone oxime resin; Yield given. Multistep reaction; |
BOC-glycine
Boc-Arg(Tos)-OH
Boc-Asp(O-cyclohexyl)-OH
3-(tert-butoxycarbonylamino-methyl)benzoic acid
Conditions | Yield |
---|---|
solid-phase synthesis using p-nitrobenzophenone oxime resin; Yield given. Multistep reaction; |
3-(tert-butoxycarbonylamino-methyl)benzoic acid
3-{[(tert-butoxycarbonyl)amino]methyl}cyclohexanecarboxylic acid
Conditions | Yield |
---|---|
With hydrogen; acetic acid; platinum(IV) oxide under 2585.7 Torr; |
3-(tert-butoxycarbonylamino-methyl)benzoic acid
Conditions | Yield |
---|---|
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane; N,N-dimethyl-formamide for 0.166667h; |
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