Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
Cas:13036-02-7
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:13036-02-7
Min.Order:5 Kiloliter
FOB Price: $1.2 / 5.0
Type:Manufacturers
inquiryOur Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con
Cas:13036-02-7
Min.Order:1 Kilogram
FOB Price: $1.0 / 10.0
Type:Trading Company
inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:13036-02-7
Min.Order:1 Kilogram
FOB Price: $139.0 / 210.0
Type:Trading Company
inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
Cas:13036-02-7
Min.Order:10 Kilogram
Negotiable
Type:Trading Company
inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:13036-02-7
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryDimethyl 5-hydroxyisophthalate CAS:13036-02-7 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality or
Cas:13036-02-7
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:13036-02-7
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Cas:13036-02-7
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryBest quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:13036-02-7
Min.Order:0 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Cas:13036-02-7
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:13036-02-7
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquiryWe are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov
Cas:13036-02-7
Min.Order:100 Gram
FOB Price: $100.0 / 2000.0
Type:Lab/Research institutions
inquirySuperior quality, moderate price & quick delivery. Appearance:white powder Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:10g/bag,or as your request Application:Used for Pesticide intermediates Transport
Cas:13036-02-7
Min.Order:1 Gram
Negotiable
Type:Trading Company
inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providing h
Cas:13036-02-7
Min.Order:0
Negotiable
Type:Other
inquiryOur company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung, LG, Merck, Thermo Fisher Scientific and so o
Cas:13036-02-7
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryProduct name: Dimethyl 5-Hydroxyisophthalate CAS No.:13036-02-7 Molecule Formula:C10H10O5 Molecule Weight:210.18 Purity: 99% Package:25kg/drum Description:White crystalline powder Manufacture Standards:Enterprise Standard TESTING
Cas:13036-02-7
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
Cas:13036-02-7
Min.Order:1 Kilogram
FOB Price: $18.0 / 20.0
Type:Trading Company
inquiryZhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed
Cas:13036-02-7
Min.Order:1 Kilogram
FOB Price: $2.0
Type:Lab/Research institutions
inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
Cas:13036-02-7
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryADVANTAGE 1.Professional: More than 10 years chemical exporting experience. We have produced chemical more than fifteen years, 95% products are for export . More than 10 years chemical exporting experience. Good and stabilized factory price. 2.Reaso
Cas:13036-02-7
Min.Order:1 Kilogram
FOB Price: $1.0
Type:Lab/Research institutions
inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
Cas:13036-02-7
Min.Order:1 Metric Ton
FOB Price: $1.5
Type:Trading Company
inquiryWe are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp
Cas:13036-02-7
Min.Order:1 Metric Ton
FOB Price: $1.0
Type:Trading Company
inquiryStock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
Cas:13036-02-7
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryLower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
Cas:13036-02-7
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
R & D enterprises have their own stock in stockAppearance:To be subject to the object Package:Customized Application:pharmaceutical intermediates Transportation:Air Port:Shanghai;Guangzhou
Jinhua huayi chemical co., ltd. is dedicated to the development, production and marketing of chemicals. On the basis of equality and mutual benefit, and under the principle of customer first, credit first, quality first, we are ready to join hands
Cas:13036-02-7
Min.Order:100 Gram
Negotiable
Type:Lab/Research institutions
inquiryAcmec is a leading manufacturer and supplier of biochemical reagents and life science products. We have over 40,000 items in stock (real-time inventory) and offer discounted prices to registered members of the online store ( www.acmec.com.cn ) Appea
Cas:13036-02-7
Min.Order:1 bottle
Negotiable
Type:Lab/Research institutions
inquiryConditions | Yield |
---|---|
With thionyl chloride Heating; | 100% |
With thionyl chloride for 1.5h; Heating; | 100% |
With sulfuric acid | 100% |
5-Hydroxyisophthalic acid
Dimethyl 5-hydroxyisophthalate
Conditions | Yield |
---|---|
100% | |
With boron trifluoride diethyl etherate In methanol Reflux; | 78% |
With sulfuric acid In methanol | |
With sulfuric acid In methanol | |
With hydrogenchloride In methanol |
5-Hydroxyisophthalic acid
2,2-dimethoxy-propane
Dimethyl 5-hydroxyisophthalate
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In methanol at 60℃; for 12h; Inert atmosphere; | 96% |
With toluene-4-sulfonic acid In methanol at 60℃; | 79% |
3,5-bis(methoxycarbonyl)phenyl trifluoromethanesulfonate
Dimethyl 5-hydroxyisophthalate
Conditions | Yield |
---|---|
With tetraethylammonium hydroxide In 1,4-dioxane at 20℃; for 1h; | 95% |
Conditions | Yield |
---|---|
With potassium hydrogencarbonate In N,N-dimethyl-formamide at 40℃; | 95% |
5-Hydroxyisophthalic acid
diazomethyl-trimethyl-silane
Dimethyl 5-hydroxyisophthalate
Conditions | Yield |
---|---|
In methanol; hexane; ethyl acetate; toluene | 59% |
Conditions | Yield |
---|---|
In methanol; ethyl acetate; toluene | 59% |
Conditions | Yield |
---|---|
Stage #1: Chelidamic acid With thionyl chloride Reflux; Stage #2: methanol at 0 - 20℃; for 2h; | 29% |
methanol
Dimethyl 5-hydroxyisophthalate
Dimethyl 5-hydroxyisophthalate
Conditions | Yield |
---|---|
With trifluoroacetic acid In chloroform-d1 for 1h; |
methanol
5-Hydroxybenzene-1,3-dicarbonyl dichloride
Dimethyl 5-hydroxyisophthalate
5-Hydroxyisophthalic acid
A
Dimethyl 5-hydroxyisophthalate
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: SOCl2 / dimethylformamide; tetrahydrofuran / 3 h / Heating View Scheme |
Dimethyl 5-hydroxyisophthalate
Conditions | Yield |
---|---|
With sulfuric acid In methanol; water |
di-tert-butyl dicarbonate
2-(N-tert-butoxycarbonylamino)ethanol
diethylazodicarboxylate
Dimethyl 5-hydroxyisophthalate
Conditions | Yield |
---|---|
With hydrogenchloride; sodium hydrogencarbonate; triphenylphosphine; trifluoroacetic acid In tetrahydrofuran; dichloromethane; ethyl acetate |
methanol
5-hydroxy-isopththalic acid monomethyl ester
Dimethyl 5-hydroxyisophthalate
Conditions | Yield |
---|---|
With thionyl chloride at 20℃; Schlenk technique; |
Dimethyl 5-hydroxyisophthalate
Conditions | Yield |
---|---|
With water-d2; sodium; platinum on activated charcoal at 140℃; under 7500.6 Torr; for 144h; | 100% |
With water-d2; sodium; platinum on activated charcoal at 140℃; under 7500.6 Torr; for 144h; Yield given; |
Dimethyl 5-hydroxyisophthalate
allyl bromide
dimethyl 5-(prop-2-en-1-yloxy)benzene-1,3-dicarboxylate
Conditions | Yield |
---|---|
With potassium carbonate In acetone Heating / reflux; | 100% |
Stage #1: Dimethyl 5-hydroxyisophthalate With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 2h; Inert atmosphere; Stage #2: allyl bromide In N,N-dimethyl-formamide at 90℃; for 9h; Inert atmosphere; | 100% |
With caesium carbonate In N,N-dimethyl-formamide for 1h; | 99% |
Dimethyl 5-hydroxyisophthalate
methyl iodide
dimethyl 5-methoxyisophthalate
Conditions | Yield |
---|---|
With potassium carbonate In acetone at 20℃; | 100% |
With potassium carbonate In acetone Heating; | 95% |
With potassium carbonate In acetonitrile Reflux; | 94% |
Dimethyl 5-hydroxyisophthalate
3,5-bis(hydroxymethyl)phenol
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In tetrahydrofuran for 3h; Heating; | 100% |
Stage #1: Dimethyl 5-hydroxyisophthalate With lithium aluminium tetrahydride In tetrahydrofuran at -30 - 20℃; Stage #2: With hydrogenchloride In tetrahydrofuran; water; acetonitrile at 0 - 10℃; Product distribution / selectivity; | 99% |
With lithium aluminium tetrahydride In tetrahydrofuran Inert atmosphere; | 99% |
Dimethyl 5-hydroxyisophthalate
benzyl bromide
dimethyl 5-(benzyloxy)isophthalate
Conditions | Yield |
---|---|
With potassium carbonate In dimethyl sulfoxide; acetone for 22h; Reflux; | 100% |
With potassium carbonate In acetone at 20℃; for 18h; Heating / reflux; | 100% |
potassium carbonate In water; N,N-dimethyl-formamide | 96% |
Isobutyl bromide
Dimethyl 5-hydroxyisophthalate
dimethyl 5-(isobutyloxy)isophthalate
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 40℃; for 20h; | 99.5% |
With potassium carbonate; potassium iodide In N,N-dimethyl-formamide at 60℃; for 72h; Inert atmosphere; | 94% |
Dimethyl 5-hydroxyisophthalate
tert-butyldimethylsilyl chloride
dimethyl 5-{[(1,1-dimethylethyl)dimethylsilyl]oxy}benzene-1,3-dicarboxylate
Conditions | Yield |
---|---|
With dmap; triethylamine In dichloromethane at 25℃; for 16h; | 99% |
With 1H-imidazole In N,N-dimethyl-formamide at 20℃; for 18h; Inert atmosphere; | 97% |
With 1H-imidazole In dichloromethane at 0 - 20℃; | 95% |
trifluoromethylsulfonic anhydride
Dimethyl 5-hydroxyisophthalate
3,5-bis(methoxycarbonyl)phenyl trifluoromethanesulfonate
Conditions | Yield |
---|---|
With pyridine In dichloromethane at 0℃; for 0.333333h; Substitution; | 99% |
With pyridine In dichloromethane at 0℃; for 24h; Inert atmosphere; | 83% |
With pyridine In dichloromethane at 0℃; for 24h; Inert atmosphere; | 83% |
Dimethyl 5-hydroxyisophthalate
propargyl bromide
5-(prop-2-ynyloxy)isophthalic acid dimethyl ester
Conditions | Yield |
---|---|
Stage #1: Dimethyl 5-hydroxyisophthalate With potassium carbonate In N,N-dimethyl-formamide at 60℃; for 1h; Stage #2: propargyl bromide In N,N-dimethyl-formamide at 20 - 25℃; | 99% |
With potassium carbonate In N,N-dimethyl-formamide at 20℃; | 98% |
Stage #1: Dimethyl 5-hydroxyisophthalate In N,N-dimethyl-formamide for 0.166667h; Cooling with ice; Stage #2: propargyl bromide In N,N-dimethyl-formamide; toluene at 20℃; for 4h; | 96% |
Dimethyl 5-hydroxyisophthalate
[3,5-bis[[3,5-bis[[3,5-bis(phenylmethoxy)phenyl]methoxy]phenyl]methoxy]phenyl]methyl alcohol
Conditions | Yield |
---|---|
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 0 - 20℃; Mitsunobu coupling; | 99% |
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 0 - 20℃; for 12.1667h; Mitsunobu Displacement; Inert atmosphere; | 99% |
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 0 - 50℃; for 12.1667h; Mitsunobu Displacement; Inert atmosphere; Schlenk technique; | 99% |
Dimethyl 5-hydroxyisophthalate
chloromethyl methyl ether
dimethyl 5-(methoxymethoxy)isophthalate
Conditions | Yield |
---|---|
Stage #1: Dimethyl 5-hydroxyisophthalate With sodium hydride In tetrahydrofuran; mineral oil for 0.5h; Cooling with ice; Inert atmosphere; Stage #2: chloromethyl methyl ether In tetrahydrofuran; mineral oil at 20℃; Cooling with ice; Inert atmosphere; | 99% |
Stage #1: Dimethyl 5-hydroxyisophthalate With sodium hydride In tetrahydrofuran; mineral oil for 0.5h; Inert atmosphere; Schlenk technique; Stage #2: chloromethyl methyl ether In tetrahydrofuran; mineral oil at 20℃; for 3h; Inert atmosphere; Schlenk technique; | 99% |
Stage #1: Dimethyl 5-hydroxyisophthalate With sodium hydride In tetrahydrofuran; mineral oil for 0.5h; Cooling with ice; Inert atmosphere; Schlenk technique; Stage #2: chloromethyl methyl ether In tetrahydrofuran; mineral oil at 20℃; for 3h; Cooling with ice; Inert atmosphere; Schlenk technique; | 99% |
Conditions | Yield |
---|---|
Stage #1: Dimethyl 5-hydroxyisophthalate With lithium hydride In N,N-dimethyl-formamide at 20℃; for 0.0833333h; solid phase reaction; Stage #2: C9H9Cl2OPol With tetra-(n-butyl)ammonium iodide In N,N-dimethyl-formamide at 60℃; solid phase reaction; | 99% |
Conditions | Yield |
---|---|
Stage #1: Dimethyl 5-hydroxyisophthalate With lithium hydride In N,N-dimethyl-formamide at 20℃; for 0.0833333h; solid phase reaction; Stage #2: C25H23Cl4O3Pol With tetra-(n-butyl)ammonium iodide In N,N-dimethyl-formamide at 60℃; solid phase reaction; | 99% |
Conditions | Yield |
---|---|
Stage #1: Dimethyl 5-hydroxyisophthalate With lithium hydride In N,N-dimethyl-formamide at 20℃; for 0.0833333h; solid phase reaction; Stage #2: bromomethyl resin With tetra-(n-butyl)ammonium iodide In N,N-dimethyl-formamide at 60℃; solid phase reaction; | 99% |
Conditions | Yield |
---|---|
With 18-crown-6 ether; potassium carbonate In tetrahydrofuran | 99% |
Dimethyl 5-hydroxyisophthalate
[3,5-Bis-(3,5-bis-benzyloxy-benzyloxy)-phenyl]-methanol
C59H52O11
Conditions | Yield |
---|---|
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 0 - 50℃; for 12.1667h; Mitsunobu Displacement; Inert atmosphere; Schlenk technique; | 99% |
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 20℃; Mitsunobu Displacement; |
Dimethyl 5-hydroxyisophthalate
1-dodecylbromide
Conditions | Yield |
---|---|
With potassium carbonate In acetone for 48h; Reflux; | 99% |
With potassium carbonate In N,N-dimethyl-formamide at 70℃; for 24h; | 68% |
With potassium carbonate In N,N-dimethyl-formamide at 85℃; for 24h; |
1-bromo-octane
Dimethyl 5-hydroxyisophthalate
dimethyl 5-octyloxyl-1,3-benzenedicarboxylyate
Conditions | Yield |
---|---|
With potassium carbonate In DMF (N,N-dimethyl-formamide) at 120℃; for 4h; | 98.6% |
With potassium carbonate; potassium iodide In N,N-dimethyl-formamide at 80℃; for 48h; Inert atmosphere; | 93% |
With potassium carbonate In N,N-dimethyl-formamide at 110℃; for 1h; Inert atmosphere; | 90% |
Dimethyl 5-hydroxyisophthalate
1,3-bis{[3,5-bis(tert-butyl)benzyl]oxy}-5-(bromomethyl)benzene
dimethyl 5-(3,5-bis(3,5-di(tert-butyl)phenylmethoxy)phenylmethoxy)isophthalate
Conditions | Yield |
---|---|
With 18-crown-6 ether; tetra-(n-butyl)ammonium iodide; potassium carbonate In acetone Heating; | 98% |
1,4-dibromo-butane
Dimethyl 5-hydroxyisophthalate
1,4-bis(3,5-bis(methoxycarbonyl)phenoxy)butane
Conditions | Yield |
---|---|
With 18-crown-6 ether; potassium carbonate In acetonitrile at 60℃; for 48h; | 98% |
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 48h; | 75% |
With tetra-(n-butyl)ammonium iodide; sodium hydride In tetrahydrofuran for 3h; Heating; | 64% |
Dimethyl 5-hydroxyisophthalate
2,5,8,11-tetraoxatridecan-13-ol tosylate
dimethyl 5-(2,5,8,11-tetraoxatridecan-13-yloxy)isophthalate
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile for 16h; Heating; | 98% |
Conditions | Yield |
---|---|
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 0 - 20℃; Mitsunobu coupling; | 98% |
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 0 - 20℃; for 12.1667h; Mitsunobu Displacement; Inert atmosphere; | 98% |
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 0 - 50℃; for 12.1667h; Mitsunobu Displacement; Inert atmosphere; Schlenk technique; | 98% |
Dimethyl 5-hydroxyisophthalate
benzyl bromide
[5-(benzyloxy)-1,3-phenylene]dimethanol
Conditions | Yield |
---|---|
With potassium carbonate In tetrahydrofuran; water; N,N-dimethyl-formamide | 98% |
Dimethyl 5-hydroxyisophthalate
benzyl chloride
dimethyl 5-(benzyloxy)isophthalate
Conditions | Yield |
---|---|
Stage #1: Dimethyl 5-hydroxyisophthalate With potassium carbonate In acetone; acetonitrile for 0.5h; Reflux; Stage #2: benzyl chloride In acetone; acetonitrile Reflux; | 98% |
Conditions | Yield |
---|---|
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 0 - 50℃; for 12.1667h; Mitsunobu Displacement; Inert atmosphere; Schlenk technique; | 98% |
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 20℃; Mitsunobu Displacement; |
1,4-bis(bromomethyl)benzene
Dimethyl 5-hydroxyisophthalate
5,5′-(1,4-phenylenebis(methylene))bis(oxy)diisophthalate
Conditions | Yield |
---|---|
With dibenzo-18-crown-6; potassium carbonate In tetrahydrofuran at 70℃; for 24h; | 97% |
With dibenzo-18-crown-6; potassium carbonate In tetrahydrofuran at 70℃; for 24h; | 97% |
With 18-crown-6 ether; potassium carbonate In tetrahydrofuran at 65℃; for 24h; Etherification; | 90% |
With potassium carbonate |
Conditions | Yield |
---|---|
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 0 - 20℃; Mitsunobu coupling; | 97% |
Dimethyl 5-hydroxyisophthalate
methanesulfonyl chloride
dimethyl 5-(methylsulfonyloxy)isophthalate
Conditions | Yield |
---|---|
With triethylamine In ethyl acetate at 0 - 20℃; for 0.166667h; Green chemistry; | 97% |
With pyridine In dichloromethane at 20℃; | 93% |
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