As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
Cas:13036-50-5
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inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
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Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiry2-CHLORO-4-PHENYLPYRIMIDINE CAS:13036-50-5 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organ
Cas:13036-50-5
Min.Order:1 Gram
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Type:Lab/Research institutions
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:13036-50-5
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin
Cas:13036-50-5
Min.Order:1 Kilogram
FOB Price: $1.0 / 10.0
Type:Trading Company
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:13036-50-5
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquiry2-CHLORO-4-PHENYLPYRIMIDINE Basic information Product Name: 2-CHLORO-4-PHENYLPYRIMIDINE Synonyms: 2-chloro-4-phenyl-pyrimidin;2-CHLORO-4-PHENYLPYRIMIDINE;Pyrimidine, 2-chloro-4-phenyl-;2-Chloro-4-phenylpyrimidine95% CAS: 13036-50-5 MF: C1
Cas:13036-50-5
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryWe Huarong Pharm can provide Customized Synthesis & Process R&D & APIs and intermediates Production & Quality Research & Registration Application, especially our GMP validation service which complies with SFDA, FDA, WHO and EU EMPA. O
Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
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inquiryLower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
Cas:13036-50-5
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Type:Lab/Research institutions
inquiryR & D enterprises have their own stock in stockAppearance:To be subject to the object Package:Customized Application:pharmaceutical intermediates Transportation:Air Port:Shanghai;Guangzhou
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:Beijing or Guangzhou
Cas:13036-50-5
Min.Order:0
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Type:Lab/Research institutions
inquiryShanghai Finebiotech Co.,Ltd.was established in 2020, which providing professional chemical services. As a customer-oriented company, we have distinguished ourself from others in providing worldwide customers with cost-effective and efficient service
1.Our services:A.Supply sampleB.The packing also can be according the customers` requirmentC.Any inquiries will be replied within 24 hoursD.we provide Commerical Invoice, Packing List, Bill of loading, COA , Health certificate and Origin certificate.
Cas:13036-50-5
Min.Order:0
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Type:Lab/Research institutions
inquiryAnsciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
Cas:13036-50-5
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryWe are committed to providing our customers with the best products and services at the most competitive prices.Appearance:off-white powder Storage:Room temperature with sealed well Package:according to the clients requirement Application:Use as prima
2-CHLORO-4-PHENYLPYRIMIDINEAppearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
Cas:13036-50-5
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryGood Quality Package:1kg/bag Application:Medical or chemical Transportation:Air/Train/Sea Port:Shenzhen
factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
Best Seller, High Quality, Competitive Price, Fast Delivery, Quick ResponseAppearance:powder, or liquid Storage:Stored in room temperature, ventilated place Package:Bottle, barrel, cargo, container, etc. Application:Pharmaceuticals, intermediates, AP
1.Professional synthesis laboratory and production base. 2.Strong synthesis team and service team. 3.Professional data management system. 4.We provide the professional test date and product information ,ex. HNMR ,CNMR,FNMR, HPLC/G
Cas:13036-50-5
Min.Order:10 Milligram
Negotiable
Type:Lab/Research institutions
inquiryOur Advantage 1.Best quality with competitive price. 2.Quick shipping,delivery on time. 3.We have a pharmaceutical raw material production plant and a reagent R&D center. 4.Support multiple trading methods and payment.We support wire transfer
Cas:13036-50-5
Min.Order:1 Kilogram
FOB Price: $6.8 / 8.6
Type:Trading Company
inquiryPrice, service, company and transport advantage: 1. Best service, place of origin China, high quality, and reasonable price. 2. It's customers' right to choose the package (EMS, DHL, FEDEX, UPS). 3. It's customers' right
Cas:13036-50-5
Min.Order:0
Negotiable
Type:Trading Company
inquiryStrong R&D strength and team We have a R&D team with around 30 R&D personnel.All of our employees have chemical backgrounds and have worked in the chemical industry for many years.Our laboratory can synthesize target products with wei
HuBei ipure is a diversified product production and operation enterprise, with API, pharma intermediates, and other fine chemicals as well as R&D and pigments development and sales as one of the large enterprises, with more than 130 acres of pl
Cas:13036-50-5
Min.Order:1 Gram
FOB Price: $1.0
Type:Trading Company
inquiryproductName Pyrimidine,2-chloro-4-phenyl- Synonyms 2-Chloro-4… Package:Aluminum foil bag or according to custom's requirement Application:Organic intermediates Transportation:Ship it by express. Port:China
Cas:13036-50-5
Min.Order:1 Gram
Negotiable
Type:Trading Company
inquiry1. Production capacity: we have three production base with high-tech production equipment and instruments, equipped with professional production personnel, meet your requirements.2. Quality assurance: we have a first-class testing equipment and testi
Conditions | Yield |
---|---|
With tetrabutylammomium bromide; sodium carbonate In ethanol; water at 70℃; for 10h; Catalytic behavior; Suzuki-Miyaura Coupling; | 87% |
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In ethanol; toluene for 4h; Inert atmosphere; Reflux; | 86% |
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In ethanol; toluene for 4h; Inert atmosphere; Reflux; | 86% |
Conditions | Yield |
---|---|
With di-tert-butyl(methyl)phosphonium tetrafluoroborate salt; palladium diacetate; potassium carbonate In 1,4-dioxane at 100℃; for 18h; Inert atmosphere; | 84% |
2,6-Dichloropyrimidine
phenylboronic acid
A
2-chloro-4-phenylpyrimidine
B
2,4-diphenylpyrimidine
Conditions | Yield |
---|---|
With sodium carbonate; tetrakis(triphenylphosphine) palladium(0) In methanol; benzene for 4h; Phenylation; Heating; | A 80% B 10% |
2,6-Dichloropyrimidine
phenylzinc(II) bromide
2-chloro-4-phenylpyrimidine
Conditions | Yield |
---|---|
tetrakis(triphenylphosphine) palladium(0) In tetrahydrofuran at 50℃; | 64% |
tetrakis(triphenylphosphine) palladium(0) In tetrahydrofuran at 50℃; | |
tetrakis(triphenylphosphine) palladium(0) In tetrahydrofuran at 50℃; |
2,6-Dichloropyrimidine
tributylphenylstannane
2-chloro-4-phenylpyrimidine
Conditions | Yield |
---|---|
With bis-triphenylphosphine-palladium(II) chloride In N,N-dimethyl-formamide at 80℃; for 10h; | 60% |
N-(1-phenylethylidene)cyanamide
N,N-dimethyl-formamide
2-chloro-4-phenylpyrimidine
Conditions | Yield |
---|---|
Stage #1: N,N-dimethyl-formamide With trichlorophosphate at 20℃; for 0.166667h; Vilsmeier Reaction; Stage #2: N-(1-phenylethylidene)cyanamide at 20 - 130℃; for 1.5h; | 60% |
2-chloropyrimidine
phenylmagnesium chloride
2-chloro-4-phenylpyrimidine
Conditions | Yield |
---|---|
In tetrahydrofuran at 25℃; for 8h; | 49% |
Conditions | Yield |
---|---|
With manganese(III) triacetate dihydrate In ethanol at 170℃; for 0.166667h; Microwave irradiation; regioselective reaction; | 48% |
2-Amino-4-phenylpyrimidine 1-Oxide
A
2-chloro-4-phenylpyrimidine
B
2-chloro-4-phenylpyrimidine 1-oxide
Conditions | Yield |
---|---|
With hydrogenchloride; sodium nitrite at 0℃; for 2h; | A 12% B 46% |
With hydrogenchloride; lithium chloride; sodium nitrite In acetic acid | A 12% B 46% |
4-phenylpyrimidin-2-amine
A
2-chloro-4-phenylpyrimidine
B
2-hydroxy-4-phenylpyrimidine
Conditions | Yield |
---|---|
With hydrogenchloride; lithium chloride; sodium nitrite In acetic acid | A 35% B 20% |
4-phenyl-1H-pyrimidin-2-one
2-chloro-4-phenylpyrimidine
Conditions | Yield |
---|---|
With trichlorophosphate |
2,4-dichloro-6-phenyl-pyrimidine
2-chloro-4-phenylpyrimidine
Conditions | Yield |
---|---|
With ammonia; zinc |
4-phenylpyrimidin-2-amine
A
2-chloro-4-phenylpyrimidine
B
2-hydroxy-4-phenylpyrimidine
C
5-bromo-2-amino-4-phenylpyrimidine
Conditions | Yield |
---|---|
With sulfuric acid; sodium nitrite In water at 0 - 5℃; Product distribution; Mechanism; other acids; other temepratures; |
2-Amino-4-phenylpyrimidine 1-Oxide
A
2-chloro-4-phenylpyrimidine
B
2-chloro-4-phenylpyrimidine 1-oxide
C
5-chloro-2-amino-4-phenylpyrimidine 1-oxide
D
5-bromo-2-amino-4-phenylpyrimidine 1-oxide
Conditions | Yield |
---|---|
With sulfuric acid; sodium nitrite In water at 0 - 5℃; Product distribution; Mechanism; other acids; other temepratures; |
2-chloro-4-phenylpyrimidine
Conditions | Yield |
---|---|
With 2,3-dicyano-5,6-dichloro-p-benzoquinone In tetrahydrofuran; diethyl ether for 0.0833333h; Ambient temperature; Yield given; |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: diethyl ether / 1 h / 1.) -30 deg C, 30 min, 2.) 0 deg C, 30 min 2: 2,3-dichloro-5,6-dicyanobenzoquinone / diethyl ether; tetrahydrofuran / 0.08 h / Ambient temperature View Scheme |
4-phenylpyrimidin-2-amine
2-chloro-4-phenylpyrimidine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: aqueous H2SO4; aqueous NaNO2 2: POCl3 View Scheme |
6-phenyluracil
2-chloro-4-phenylpyrimidine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: POCl3 2: zinc-powder; aq.-ethanolic NH3 View Scheme |
2-methylthio-6-phenyl-3,4-dihydropyrimidin-4-one
2-chloro-4-phenylpyrimidine
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: aqueous H2SO4 / 140 - 150 °C 2: POCl3 3: zinc-powder; aq.-ethanolic NH3 View Scheme |
3-Oxo-3-phenylpropanal
2-chloro-4-phenylpyrimidine
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: pyridine 2: aqueous H2SO4; aqueous NaNO2 3: POCl3 View Scheme |
Conditions | Yield |
---|---|
With bunazosin In tetrahydrofuran at -78 - 0℃; for 3h; |
acetophenone oxime
2-chloro-4-phenylpyrimidine
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: triethylamine / dichloromethane / 0 °C 2.1: fac-tris(2-(4'-tert-butyl)phenylpyridine)iridium(III); tetrakis(acetonitrile)copper(I)tetrafluoroborate; 1,10-Phenanthroline / chlorobenzene / 24 h / 25 °C / Inert atmosphere; Sealed tube; Irradiation 3.1: trichlorophosphate / 0.17 h / 20 °C 3.2: 1.5 h / 20 - 130 °C View Scheme |
2-chloro-4-phenylpyrimidine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: fac-tris(2-(4'-tert-butyl)phenylpyridine)iridium(III); tetrakis(acetonitrile)copper(I)tetrafluoroborate; 1,10-Phenanthroline / chlorobenzene / 24 h / 25 °C / Inert atmosphere; Sealed tube; Irradiation 2.1: trichlorophosphate / 0.17 h / 20 °C 2.2: 1.5 h / 20 - 130 °C View Scheme |
acetophenone
2-chloro-4-phenylpyrimidine
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: hydroxylamine hydrochloride; sodium acetate / methanol / 75 °C 2.1: triethylamine / dichloromethane / 0 °C 3.1: fac-tris(2-(4'-tert-butyl)phenylpyridine)iridium(III); tetrakis(acetonitrile)copper(I)tetrafluoroborate; 1,10-Phenanthroline / chlorobenzene / 24 h / 25 °C / Inert atmosphere; Sealed tube; Irradiation 4.1: trichlorophosphate / 0.17 h / 20 °C 4.2: 1.5 h / 20 - 130 °C View Scheme |
2-chloro-4-phenylpyrimidine
4-phenyl-1H-pyrimidin-2-one
Conditions | Yield |
---|---|
With hydrogenchloride at 100℃; for 1h; | 100% |
With hydrogenchloride In water Reflux; | 55% |
With hydrogenchloride In water for 1h; Reflux; | |
With hydrogenchloride In water for 1h; Reflux; |
2-chloro-4-phenylpyrimidine
Conditions | Yield |
---|---|
Stage #1: 2-chloro-4-phenylpyrimidine; (±)-trans-methyl 2-(((6-(5-(aminomethyl)-1-methyl-1H-1,2,3-triazol-4-yl)-2-methylpyridin-3-yl)oxy)methyl)cyclobutanecarboxylate With N-ethyl-N,N-diisopropylamine In butan-1-ol at 180℃; for 1.33333h; Stage #2: With lithium hydroxide monohydrate; water In tetrahydrofuran; methanol at 20℃; | 97% |
2-chloro-4-phenylpyrimidine
2-fluoro-4-phenylpyrimidine
Conditions | Yield |
---|---|
With 18-crown-6 ether; tetramethlyammonium chloride; cesium fluoride In acetonitrile at 60℃; for 16h; Glovebox; | 97% |
With tetramethylammonium fluoride In dimethyl sulfoxide at 80℃; for 24h; Inert atmosphere; Sealed tube; | 90% |
1-methyl-piperazine
2-chloro-4-phenylpyrimidine
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 90℃; for 1.5h; Inert atmosphere; | 95% |
In N,N-dimethyl-formamide at 90℃; for 1.5h; Inert atmosphere; | 95% |
In ethanol for 0.5h; Heating; |
2-chloro-4-phenylpyrimidine
2-Cyclopropyl-4,5-dihydro-1H-imidazol
C16H16N4
Conditions | Yield |
---|---|
With palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl In toluene at 100℃; Buchwald-Hartwig arylation; Inert atmosphere; | 92% |
2-chloro-4-phenylpyrimidine
2-(4-(benzyloxy)phenyl)-4-phenylpyrimidine
Conditions | Yield |
---|---|
With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate; lithium hydroxide In 1,4-dioxane; water at 80℃; for 0.5h; Suzuki-Miyaura cross-coupling; Inert atmosphere; | 89% |
2-chloro-4-phenylpyrimidine
Conditions | Yield |
---|---|
With potassium hexamethylsilazane In tetrahydrofuran at 100℃; for 16h; Inert atmosphere; Schlenk technique; Sealed tube; Green chemistry; | 89% |
2-chloro-4-phenylpyrimidine
2-hydroxy-4-phenylpyrimidine
Conditions | Yield |
---|---|
With acetylhydroxamic acid; potassium carbonate In dimethyl sulfoxide at 80℃; for 12h; Sealed tube; | 87% |
With hydrogenchloride; water at 100℃; for 1h; | |
With hydrogenchloride; water at 100℃; for 1h; |
2-chloro-4-phenylpyrimidine
4-nitrophenylboronic acid
2-(4-nitrophenyl)-4-phenylpyrimidine
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); sodium carbonate In water; acetonitrile at 90℃; | 84% |
Conditions | Yield |
---|---|
With palladium diacetate; triphenylphosphine In tetrahydrofuran for 18h; Reflux; | 83% |
2-chloro-4-phenylpyrimidine
sodium methylate
2-methoxy-4-phenylpyrimidine
Conditions | Yield |
---|---|
for 4h; Heating; | 80% |
2-chloro-4-phenylpyrimidine
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In acetonitrile at 95℃; for 16h; Inert atmosphere; | 80% |
2-chloro-4-phenylpyrimidine
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In acetonitrile at 95℃; for 16h; Inert atmosphere; | 79% |
2-chloro-4-phenylpyrimidine
4-aminophenylacetic acid
2-(4-(4-phenylpyrimidin-2-ylamino)phenyl)acetic acid
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In tetrahydrofuran; water at 160℃; for 10h; Microwave irradiation; in a seal tube; | 77% |
2-chloro-4-phenylpyrimidine
2-amino-1-(morpholin-4-yl)ethanone hydrochloride
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In acetonitrile at 100℃; for 12h; Inert atmosphere; Sealed tube; | 74.5% |
2-chloro-4-phenylpyrimidine
1-butyn-4-ol
2-but-3-ynyloxy-4-phenylpyrimidine
Conditions | Yield |
---|---|
Stage #1: 3-Butyn-1-ol With sodium hydride In tetrahydrofuran at 0℃; for 1h; Stage #2: 2-chloro-4-phenylpyrimidine In tetrahydrofuran at 20℃; | 71% |
2-chloro-4-phenylpyrimidine
m-aminobenzenesulfonamide
Conditions | Yield |
---|---|
With acetic acid In butan-1-ol at 110℃; for 21h; | 70% |
With trifluoroacetic acid In isopropyl alcohol for 18h; Sealed tube; Heating; | 39% |
2-chloro-4-phenylpyrimidine
2-amino-N,N-dimethylpropanamide hydrochloride
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In acetonitrile at 100℃; for 16h; Inert atmosphere; | 69% |
2-chloro-4-phenylpyrimidine
(2-phenylvinyl)tributylstannane
Conditions | Yield |
---|---|
With bis-triphenylphosphine-palladium(II) chloride In N,N-dimethyl-formamide at 100℃; for 10h; | 68% |
2-chloro-4-phenylpyrimidine
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In acetonitrile at 110℃; for 16h; Inert atmosphere; | 68% |
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate In toluene for 12h; Inert atmosphere; Heating; | 65% |
2-chloro-4-phenylpyrimidine
2-amino-N,N-dimethyl-acetamide hydrochloride
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In acetonitrile at 100℃; for 16h; Inert atmosphere; | 63% |
2-chloro-4-phenylpyrimidine
4-(2-(2-pyridinyl)ethenyl)phenol
Conditions | Yield |
---|---|
With copper; caesium carbonate In N,N-dimethyl-formamide at 110℃; for 6h; Inert atmosphere; | 63% |
2-Amino-4-methylpyridine
2-chloro-4-phenylpyrimidine
N-(4-methylpyridin-2-yl)-4-phenylpyrimidin-2-amine
Conditions | Yield |
---|---|
With potassium phosphate; tris-(dibenzylideneacetone)dipalladium(0); 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene In 1,4-dioxane at 160℃; for 6h; Buchwald-Hartwig reaction; Inert atmosphere; | 62% |
2-chloro-4-phenylpyrimidine
N-(4-aminophenyl)-4-methoxybenzenesulfonamide
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid at 80℃; | 62% |
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