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Cas:13074-65-2
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inquiry2-N-HEXYLCYCLOPENTANONE CAS:13074-65-2 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic i
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inquiryLower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
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inquiry2-HEXYLCYCLOPENTANONEAppearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
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inquiry1. Timely and efficient service to ensure communication with customers2. Produce products of different specifications and sizes according to your requirements.3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures sta
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inquiryKnown for its best quality and competitve price, this chemicals we offered is widely appreciated by our customers.Appearance:White powder Storage:keep sealed and keep from direct light Package:According client's requirements Application:pharmaceutica
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inquiryFINETECH INDUSTRY LIMITED is a LONDON based CRO company providing drug discovery & development services to worldwide clients. FINETECH INDUSTRY LIMITED supplies the 2-N-HEXYLCYCLOPENTANONE, CAS:13074-65-2 with the most competitive price and the best
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide at 150 - 160℃; under 12000.9 - 13501.1 Torr; | 68% |
With di-tert-butyl peroxide at 130℃; for 6.5h; | 43.5% |
With 7-azaindoline; chlorobis(cyclooctene)rhodium(I) dimer; tert-Octylamine; toluene-4-sulfonic acid; [1,3-bis(2,4,6-trimethylphenyl)imidazol]-2-ylidene In water at 130℃; for 48h; Catalytic behavior; regioselective reaction; | |
With di-tert-butyl peroxide at 140 - 160℃; Autoclave; |
2-hexylidenecyclopentanone
2-hexylcyclopentanone
Conditions | Yield |
---|---|
With hydrogen; palladium on activated charcoal | |
Ir(CO)(PPh3)2Cl at 240℃; |
Conditions | Yield |
---|---|
Yield given. Multistep reaction; |
(2-Hexyl-cyclopent-1-enylsulfanyl)-benzene
2-hexylcyclopentanone
Conditions | Yield |
---|---|
With water; titanium tetrachloride; acetic acid |
1-Trimethylsiloxy-2-n-hexylcyclopenten
2-hexylcyclopentanone
Conditions | Yield |
---|---|
(hydrolysis); | |
With hydrogenchloride |
1-bromo-hexane
2-cyclopentylidene-1,1-dimethylhydrazine
2-hexylcyclopentanone
Conditions | Yield |
---|---|
With potassium dihydrogenphosphate; n-butyllithium; phosphonic Acid 1.) THF, -30 deg C, 1 h, 2.) 25 deg C, 2 h, 3.) 25 deg C, overnight; Yield given. Multistep reaction; |
2-hexylcyclopentanone
Conditions | Yield |
---|---|
With ethanol; nickel Hydrogenation; |
2-hexylcyclopentanone
Conditions | Yield |
---|---|
With ethanol; nickel Hydrogenation; |
2-hexylcyclopentanone
Conditions | Yield |
---|---|
Hydrogenation; |
cyclopentanone
2-hexylcyclopentanone
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 2: 1.) n-BuLi, 3.) KH2OP4, H3PO3 / 1.) THF, -30 deg C, 1 h, 2.) 25 deg C, 2 h, 3.) 25 deg C, overnight View Scheme |
hexanal
2-hexylcyclopentanone
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: (i) aq. KOH, (ii) oxalic acid 2: H2 / Pd-C View Scheme | |
Multi-step reaction with 2 steps 1: (i) benzene, (ii) aq. HCl 2: Ir(CO)(PPh3)2Cl / 240 °C View Scheme |
2-Hexyl-2-methyl-1-oxa-spiro[2.2]pentane
2-hexylcyclopentanone
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: (i) LiNEt2, (ii) /BRN= 1209232/ 2: 330 °C 3: aq. HCl View Scheme |
2-(1-Trimethylsiloxycyclopropyl)oct-1-en
2-hexylcyclopentanone
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 0 h / 330 °C 2: (hydrolysis) View Scheme | |
Multi-step reaction with 2 steps 1: 330 °C 2: aq. HCl View Scheme |
[1-(1-Methylene-heptyl)-cyclopropylsulfanyl]-benzene
2-hexylcyclopentanone
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 350 °C 2: TiCl4, AcOH, H2O View Scheme |
2-(1-Phenylsulfanyl-cyclopropyl)-octan-2-ol
2-hexylcyclopentanone
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: SOCl2, Py 2: 350 °C 3: TiCl4, AcOH, H2O View Scheme |
hexyl-methyl-ketone
2-hexylcyclopentanone
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: (i) KOH, (ii) Et2NLi, (iii) /BRN= 1209232/ 2: 0 h / 330 °C 3: (hydrolysis) View Scheme |
Conditions | Yield |
---|---|
With hydrogen at 140℃; under 26252.6 Torr; for 6.66667h; Autoclave; | 75 %Chromat. |
2-hexylcyclopentanone
A
(6S)-6-hexyltetrahydropyran-2-one
B
(R)-2-n-hexylcyclopentanone
Conditions | Yield |
---|---|
With YP-Gal; cyclomaltooctaose; engineered bakers' yeast cell culture at 30℃; for 60h; Baeyer-Villiger oxidation; | A 88% B 78% |
chloro-trimethyl-silane
2-hexylcyclopentanone
1-Trimethylsiloxy-2-n-hexylcyclopenten
Conditions | Yield |
---|---|
With pyridine; sodium iodide In acetonitrile | 87% |
With pyridine; sodium iodide In acetonitrile |
2-hexylcyclopentanone
6-hexyltetrahydro-2H-pyran-2-one
Conditions | Yield |
---|---|
With MoOBr3; dihydrogen peroxide; acetic anhydride; acetic acid at 50 - 70℃; for 6h; | 86% |
With urea hydrogen peroxide adduct; acetic acid at 60℃; under 750.075 Torr; for 6h; Baeyer-Villiger oxidation; | 78% |
With Candida antarctica lipase; dihydrogen peroxide; n-tetradecanoic acid In toluene for 144h; | 73% |
2-hexylcyclopentanone
A
2-(n-hexyl)-2-cyclopenten-1-one
B
2-chloro-2-hexylcyclopentanone
Conditions | Yield |
---|---|
With sulfuryl dichloride In tetrachloromethane for 1h; temp.: RT to 40 deg C; | A n/a B 78% |
2-hexylcyclopentanone
ethylene glycol
6-hexyl-1,4-dioxaspiro[4.4]nonane
Conditions | Yield |
---|---|
With GdPO4*(MoO2)0.5PMo12O40 In toluene Reflux; Dean-Stark; | 61.8% |
With P0.17Mo2.4CoBr0.27O6.8 In 5,5-dimethyl-1,3-cyclohexadiene at 130℃; for 6h; | 57% |
2-hexylcyclopentanone
A
2-(n-hexyl)-2-cyclopenten-1-one
B
(E)-2-n-hexylidenecyclopentanone
Conditions | Yield |
---|---|
With CuCl2*2H2O In ethanol; water Heating; 2:1 molar ratio of salt to ketone; | A 56% B n/a |
With CuCl2*2H2O In ethanol; water Heating; | A 56% B n/a |
2-hexylcyclopentanone
3,4-dimethoxy-benzaldehyde
5-hexyl-2-veratrylidene-cyclopentanone
Conditions | Yield |
---|---|
With potassium hydroxide |
2-hexylcyclopentanone
2-(n-hexyl)-2-cyclopenten-1-one
Conditions | Yield |
---|---|
With N-Bromosuccinimide; aniline 1) CCl4, reflux, 3 h, 2) rt, 15 h; Yield given. Multistep reaction; | |
Multi-step reaction with 2 steps 1: 78 percent / sulfuryl chloride / CCl4 / 1 h / temp.: RT to 40 deg C 2: 94 percent Chromat. / 0.5 h / 60 °C / 15 Torr View Scheme |
2-hexylcyclopentanone
A
(R)-6-hexyl-tetrahydro-2H-pyran-2-one
B
(6S)-6-hexyltetrahydropyran-2-one
Conditions | Yield |
---|---|
In water at 30℃; for 1.5h; pH 7.1; NADPH-dependent biotransformation by partially purified monooxygenase from (+)-camphor grown Ps. putida NCIMB 10007; further monooxygenases; Yield given. Yields of byproduct given. Title compound not separated from byproducts; | |
In water at 30℃; for 1.5h; pH 7.1; Yield given. Yields of byproduct given. Title compound not separated from byproducts; |
Conditions | Yield |
---|---|
at 0 - 10℃; Erwaermen des Reaktionsprodukts mit 5prozent ig. wss. Schwefelsaeure auf dem Dampfbad; |
2-hexylcyclopentanone
5-Hexyl-bicyclo[3.1.0]hexan-1-ol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: NaI; pyridine / acetonitrile 2: Et2Zn / hexane 3: ClSiMe3; methanol / 0.25 h / 20 °C View Scheme | |
Multi-step reaction with 3 steps 1: 87 percent / NaI, pyridine / acetonitrile 2: 90 percent / Et2Zn / hexane / 0.25 h / 25 °C 3: MeOH, Me3SiCl / 0.25 h / 25 °C View Scheme |
2-hexylcyclopentanone
(5-Hexyl-bicyclo[3.1.0]hex-1-yloxy)-trimethyl-silane
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: NaI; pyridine / acetonitrile 2: Et2Zn / hexane View Scheme | |
Multi-step reaction with 2 steps 1: 87 percent / NaI, pyridine / acetonitrile 2: 90 percent / Et2Zn / hexane / 0.25 h / 25 °C View Scheme |
2-hexylcyclopentanone
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: 87 percent / NaI, pyridine / acetonitrile 2: 90 percent / Et2Zn / hexane / 0.25 h / 25 °C 3: MeOH, Me3SiCl / 0.25 h / 25 °C 4: DMAP / CH2Cl2 / 2 h / 25 °C 5: NaOH / methanol / 4 h / 60 °C View Scheme | |
Multi-step reaction with 3 steps 1: 87 percent / NaI, pyridine / acetonitrile 2: 90 percent / Et2Zn / hexane / 0.25 h / 25 °C 3: NaOH / methanol / 4 h / 60 °C View Scheme |
2-hexylcyclopentanone
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: 87 percent / NaI, pyridine / acetonitrile 2: 90 percent / Et2Zn / hexane / 0.25 h / 25 °C 3: MeOH, Me3SiCl / 0.25 h / 25 °C 4: DMAP / CH2Cl2 / 2 h / 25 °C 5: NaOH / methanol / 4 h / 60 °C View Scheme | |
Multi-step reaction with 3 steps 1: 87 percent / NaI, pyridine / acetonitrile 2: 90 percent / Et2Zn / hexane / 0.25 h / 25 °C 3: NaOH / methanol / 4 h / 60 °C View Scheme |
2-hexylcyclopentanone
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: 87 percent / NaI, pyridine / acetonitrile 2: 90 percent / Et2Zn / hexane / 0.25 h / 25 °C 3: MeOH, Me3SiCl / 0.25 h / 25 °C 4: DMAP / CH2Cl2 / 2 h / 25 °C 5: 1.) Lipozyme, t-BuOMe, 1-propanol, 2.) Et3N / 1.) 36 deg C, 8 h, 2.) 25 deg C, 18 h View Scheme |
2-hexylcyclopentanone
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: 87 percent / NaI, pyridine / acetonitrile 2: 90 percent / Et2Zn / hexane / 0.25 h / 25 °C 3: MeOH, Me3SiCl / 0.25 h / 25 °C 4: DMAP / CH2Cl2 / 2 h / 25 °C 5: 1.) Lipozyme, t-BuOMe, 1-propanol, 2.) Et3N / 1.) 36 deg C, 8 h, 2.) 25 deg C, 18 h View Scheme |
2-hexylcyclopentanone
Chloro-acetic acid 5-hexyl-bicyclo[3.1.0]hex-1-yl ester
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 87 percent / NaI, pyridine / acetonitrile 2: 90 percent / Et2Zn / hexane / 0.25 h / 25 °C 3: MeOH, Me3SiCl / 0.25 h / 25 °C 4: DMAP / CH2Cl2 / 2 h / 25 °C View Scheme |
2-hexylcyclopentanone
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 87 percent / NaI, pyridine / acetonitrile 2: 90 percent / Et2Zn / hexane / 0.25 h / 25 °C 3: MeOH, Me3SiCl / 0.25 h / 25 °C 4: 1.) DMAP, 2.) Lipozyme, t-BuOMe, 1-propanol / 1.) CHCl2, 25 deg C, 2 h, 2.) 36 deg C, 8 h View Scheme |
2-hexylcyclopentanone
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 87 percent / NaI, pyridine / acetonitrile 2: 90 percent / Et2Zn / hexane / 0.25 h / 25 °C 3: MeOH, Me3SiCl / 0.25 h / 25 °C 4: 1.) DMAP, 2.) Lipozyme, t-BuOMe, 1-propanol / 1.) CHCl2, 25 deg C, 2 h, 2.) 36 deg C, 8 h View Scheme |
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