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Dayang Chem (Hangzhou) Co.,Ltd.

As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch

2-n-hexylcyclopentanone

Cas:13074-65-2

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

inquiry

Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply 2-hexylcyclopentan-1-one

Cas:13074-65-2

Min.Order:1

Negotiable

Type:Other

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Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

2-Hexyl-1-cyclopentanone

Cas:13074-65-2

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

inquiry

Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Pharmaceutical Grade CAS 13074-65-2 with competitive price

Cas:13074-65-2

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

inquiry

Qingdao Beluga Import and Export Co., LTD

2-N-HEXYLCYCLOPENTANONE CAS:13074-65-2 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic i

2-N-HEXYLCYCLOPENTANONE CAS:13074-65-2

Cas:13074-65-2

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

Cyclopentanone,2-hexyl-

Cas:13074-65-2

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

Cyclopentanone,2-hexyl-

Cas:13074-65-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

2-Hexylcyclopentanone manufacturer

Cas:13074-65-2

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

inquiry

Henan Tianfu Chemical Co., Ltd.

Our company was built in 2009 with an ISO certificate.In the past 6 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O

13074-65-2 2-N-HEXYLCYCLOPENTANONE

Cas:13074-65-2

Min.Order:1 Kilogram

FOB Price: $1000.0

Type:Lab/Research institutions

inquiry

GIHI CHEMICALS CO.,LIMITED

Lower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe

2-Hexylcyclopentanone

Cas:13074-65-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Kono Chem Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou

Hexylcyclopentanone; 98%

Cas:13074-65-2

Min.Order:0

Negotiable

Type:Other

inquiry

Henan Allgreen Chemical Co.,Ltd

high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea

2-Hexylcyclopentanone

Cas:13074-65-2

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

BOC Sciences

We leverage our wide spectrum of business in the fields of development, manufacturing, marketing, and distribution to help you make best-informed decisions tailored to your evolving needs for premium chemicals. Our complete suite of CRO services sp

DIHYDRO ISOJASMONE

Cas:13074-65-2

Min.Order:1 Gram

Negotiable

Type:Trading Company

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Antimex Chemical Limied

Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali

Cyclopentanone,2-hexyl-

Cas:13074-65-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Fandachem Co.,Ltd

2-HEXYLCYCLOPENTANONEAppearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express

2-HEXYLCYCLOPENTANONE

Cas:13074-65-2

Min.Order:0

Negotiable

Type:Other

inquiry

Henan Kanbei Chemical Co.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

2-N-HEXYLCYCLOPENTANONE

Cas:13074-65-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hebei Quanhe Biotechnology Co. LTD

1. Timely and efficient service to ensure communication with customers2. Produce products of different specifications and sizes according to your requirements.3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures sta

2-N-HEXYLCYCLOPENTANONE

Cas:13074-65-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Shanghai Yuanye Bio-Technology Co., Ltd.

Known for its best quality and competitve price, this chemicals we offered is widely appreciated by our customers.Appearance:White powder Storage:keep sealed and keep from direct light Package:According client's requirements Application:pharmaceutica

2-Hexylcyclopentanone manufacturer

Cas:13074-65-2

Min.Order:0

Negotiable

Type:Trading Company

inquiry

ZHEJIANG JIUZHOU CHEM CO.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

2-N-HEXYLCYCLOPENTANONE

Cas:13074-65-2

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Bide Pharmatech Ltd

Our mission is to provide high-quality and innovative products to our customers. By offering a broad range of products, custom synthesis and personalized services, Bide can help scientists speeding up their research in the chemical and pharmaceutical

2-Hexylcyclopentanone

Cas:13074-65-2

Min.Order:0

Negotiable

Type:Other

inquiry

Amadis Chemical Co., Ltd.

1.Professional synthesis laboratory and production base. 2.Strong synthesis team and service team. 3.Professional data management system. 4.We provide the professional test date and product information ,ex. HNMR ,CNMR,FNMR, HPLC/G

2-Hexylcyclopentanone

Cas:13074-65-2

Min.Order:10 Milligram

Negotiable

Type:Lab/Research institutions

inquiry

Shaanxi Mingqi Chemical Co., Ltd

Known for its best quality and competitve price, this chemicals we offered is widely appreciated by our customers. Our advantages:1, High quality with competitive price:1) Standard:BP/USP/EP/Enterprise standard2) All Purity≥99%3) We are manufacturer

2-Hexylcyclopentanone manufacturer

Cas:13074-65-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hubei Norna Technology Co., Ltd.

Our Services 1.TOP 10 Chemical enterprises in China 2.Over 10 years of experience 3.Wholly owned production plant (12002) 4.Sales to more than 120 countries 5.200 products with competitive price

2-Hexylcyclopentanone distributor Buy 13074-65-2

Cas:13074-65-2

Min.Order:1 Gram

Negotiable

Type:Trading Company

inquiry

Jilin haofei import and export trade Co.,Ltd

Price, service, company and transport advantage: 1. Best service, place of origin China, high quality, and reasonable price. 2. It's customers' right to choose the package (EMS, DHL, FEDEX, UPS). 3. It's customers' right

CSR160805-20693 CAS NO.13074-65-2

Cas:13074-65-2

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Yinghao Pharm Co.,Ltd.

Yinghao Pharm products include: leader molecule, heterocyclic compounds,chiral compounds, photoelectric materials, biochemical reagents etc. For example:benzene, pyrimidine, boricacid,pyridine, pyrazole, imidazole, pyrrole, fluorine and other derivat

2-N-HEXYLCYCLOPENTANONE

Cas:13074-65-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Share Chemical Co., Ltd

At Share Chemical Company, we scrupulously abide by our policy of “Excellent Quality at a Reasonable Price”. We strive to satisfy all of our customers by providing the finest quality products supported by the finest in customer servi

2-n-Hexylcyclopentanone

Cas:13074-65-2

Min.Order:1 Gram

Negotiable

Type:Other

inquiry

Nanjing Norris Pharm Technology Co., Ltd.

R & D enterprises have their own stock in stockAppearance:To be subject to the object Package:Customized Application:pharmaceutical intermediates Transportation:Air Port:Shanghai;Guangzhou

2-Hexylcyclopentanone

Cas:13074-65-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Chemical Technology Co.,LTD

1. Production capacity: we have three production base with high-tech production equipment and instruments, equipped with professional production personnel, meet your requirements.2. Quality assurance: we have a first-class testing equipment and testi

2-N-HEXYLCYCLOPENTANONE

Cas:13074-65-2

Min.Order:0

Negotiable

Type:Other

inquiry

Shanghai united Scientific Co.,Ltd.

United Scientific Company Located in Shanghai of China , is a competitive player in the global specialty and fine chemical market. Fenghua has both the expertise and flexibility to produce a wide range of chemicals. Focusing on developing the innovat

Cyclopentanone,2-hexyl-

Cas:13074-65-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Finetech Industry Limited

FINETECH INDUSTRY LIMITED is a LONDON based CRO company providing drug discovery & development services to worldwide clients. FINETECH INDUSTRY LIMITED supplies the 2-N-HEXYLCYCLOPENTANONE, CAS:13074-65-2 with the most competitive price and the best

2-N-HEXYLCYCLOPENTANONE

Cas:13074-65-2

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Synthetic route

1-hexene
592-41-6

1-hexene

cyclopentanone
120-92-3

cyclopentanone

2-hexylcyclopentanone
13074-65-2

2-hexylcyclopentanone

Conditions
ConditionsYield
With tert.-butylhydroperoxide at 150 - 160℃; under 12000.9 - 13501.1 Torr;68%
With di-tert-butyl peroxide at 130℃; for 6.5h;43.5%
With 7-azaindoline; chlorobis(cyclooctene)rhodium(I) dimer; tert-Octylamine; toluene-4-sulfonic acid; [1,3-bis(2,4,6-trimethylphenyl)imidazol]-2-ylidene In water at 130℃; for 48h; Catalytic behavior; regioselective reaction;
With di-tert-butyl peroxide at 140 - 160℃; Autoclave;
2-hexylidenecyclopentanone
17373-89-6

2-hexylidenecyclopentanone

2-hexylcyclopentanone
13074-65-2

2-hexylcyclopentanone

Conditions
ConditionsYield
With hydrogen; palladium on activated charcoal
Ir(CO)(PPh3)2Cl at 240℃;
1-hexene
592-41-6

1-hexene

lithium cyclopent-1-enolate
37160-52-4

lithium cyclopent-1-enolate

2-hexylcyclopentanone
13074-65-2

2-hexylcyclopentanone

Conditions
ConditionsYield
Yield given. Multistep reaction;
(2-Hexyl-cyclopent-1-enylsulfanyl)-benzene
58567-72-9

(2-Hexyl-cyclopent-1-enylsulfanyl)-benzene

2-hexylcyclopentanone
13074-65-2

2-hexylcyclopentanone

Conditions
ConditionsYield
With water; titanium tetrachloride; acetic acid
1-Trimethylsiloxy-2-n-hexylcyclopenten
39834-30-5

1-Trimethylsiloxy-2-n-hexylcyclopenten

2-hexylcyclopentanone
13074-65-2

2-hexylcyclopentanone

Conditions
ConditionsYield
(hydrolysis);
With hydrogenchloride
1-bromo-hexane
111-25-1

1-bromo-hexane

2-cyclopentylidene-1,1-dimethylhydrazine
14090-60-9

2-cyclopentylidene-1,1-dimethylhydrazine

2-hexylcyclopentanone
13074-65-2

2-hexylcyclopentanone

Conditions
ConditionsYield
With potassium dihydrogenphosphate; n-butyllithium; phosphonic Acid 1.) THF, -30 deg C, 1 h, 2.) 25 deg C, 2 h, 3.) 25 deg C, overnight; Yield given. Multistep reaction;
(+-)-1-hexyl-cyclopenten-(2)-one-(5)

(+-)-1-hexyl-cyclopenten-(2)-one-(5)

2-hexylcyclopentanone
13074-65-2

2-hexylcyclopentanone

Conditions
ConditionsYield
With ethanol; nickel Hydrogenation;
1-hexyl-cyclopenten-(1)-one-(5)

1-hexyl-cyclopenten-(1)-one-(5)

2-hexylcyclopentanone
13074-65-2

2-hexylcyclopentanone

Conditions
ConditionsYield
With ethanol; nickel Hydrogenation;
1-hexylidene-cyclopentanone-(2)

1-hexylidene-cyclopentanone-(2)

2-hexylcyclopentanone
13074-65-2

2-hexylcyclopentanone

Conditions
ConditionsYield
Hydrogenation;
cyclopentanone
120-92-3

cyclopentanone

2-methyl-phenethyl magnesium chloride

2-methyl-phenethyl magnesium chloride

2-hexylcyclopentanone
13074-65-2

2-hexylcyclopentanone

Conditions
ConditionsYield
Multi-step reaction with 2 steps
2: 1.) n-BuLi, 3.) KH2OP4, H3PO3 / 1.) THF, -30 deg C, 1 h, 2.) 25 deg C, 2 h, 3.) 25 deg C, overnight
View Scheme
hexanal
66-25-1

hexanal

2-hexylcyclopentanone
13074-65-2

2-hexylcyclopentanone

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: (i) aq. KOH, (ii) oxalic acid
2: H2 / Pd-C
View Scheme
Multi-step reaction with 2 steps
1: (i) benzene, (ii) aq. HCl
2: Ir(CO)(PPh3)2Cl / 240 °C
View Scheme
2-Hexyl-2-methyl-1-oxa-spiro[2.2]pentane
39834-28-1

2-Hexyl-2-methyl-1-oxa-spiro[2.2]pentane

2-hexylcyclopentanone
13074-65-2

2-hexylcyclopentanone

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: (i) LiNEt2, (ii) /BRN= 1209232/
2: 330 °C
3: aq. HCl
View Scheme
2-(1-Trimethylsiloxycyclopropyl)oct-1-en
39834-29-2

2-(1-Trimethylsiloxycyclopropyl)oct-1-en

2-hexylcyclopentanone
13074-65-2

2-hexylcyclopentanone

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 0 h / 330 °C
2: (hydrolysis)
View Scheme
Multi-step reaction with 2 steps
1: 330 °C
2: aq. HCl
View Scheme
[1-(1-Methylene-heptyl)-cyclopropylsulfanyl]-benzene
58567-67-2

[1-(1-Methylene-heptyl)-cyclopropylsulfanyl]-benzene

2-hexylcyclopentanone
13074-65-2

2-hexylcyclopentanone

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 350 °C
2: TiCl4, AcOH, H2O
View Scheme
2-(1-Phenylsulfanyl-cyclopropyl)-octan-2-ol
63365-75-3

2-(1-Phenylsulfanyl-cyclopropyl)-octan-2-ol

2-hexylcyclopentanone
13074-65-2

2-hexylcyclopentanone

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: SOCl2, Py
2: 350 °C
3: TiCl4, AcOH, H2O
View Scheme
hexyl-methyl-ketone
111-13-7

hexyl-methyl-ketone

2-hexylcyclopentanone
13074-65-2

2-hexylcyclopentanone

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: (i) KOH, (ii) Et2NLi, (iii) /BRN= 1209232/
2: 0 h / 330 °C
3: (hydrolysis)
View Scheme
hexanal
66-25-1

hexanal

cyclopentanone
120-92-3

cyclopentanone

2-hexylcyclopentanone
13074-65-2

2-hexylcyclopentanone

Conditions
ConditionsYield
With hydrogen at 140℃; under 26252.6 Torr; for 6.66667h; Autoclave;75 %Chromat.
2-hexylcyclopentanone
13074-65-2

2-hexylcyclopentanone

A

(6S)-6-hexyltetrahydropyran-2-one
108861-13-8

(6S)-6-hexyltetrahydropyran-2-one

B

(R)-2-n-hexylcyclopentanone
214335-64-5

(R)-2-n-hexylcyclopentanone

Conditions
ConditionsYield
With YP-Gal; cyclomaltooctaose; engineered bakers' yeast cell culture at 30℃; for 60h; Baeyer-Villiger oxidation;A 88%
B 78%
chloro-trimethyl-silane
75-77-4

chloro-trimethyl-silane

2-hexylcyclopentanone
13074-65-2

2-hexylcyclopentanone

1-Trimethylsiloxy-2-n-hexylcyclopenten
39834-30-5

1-Trimethylsiloxy-2-n-hexylcyclopenten

Conditions
ConditionsYield
With pyridine; sodium iodide In acetonitrile87%
With pyridine; sodium iodide In acetonitrile
2-hexylcyclopentanone
13074-65-2

2-hexylcyclopentanone

6-hexyltetrahydro-2H-pyran-2-one
710-04-3

6-hexyltetrahydro-2H-pyran-2-one

Conditions
ConditionsYield
With MoOBr3; dihydrogen peroxide; acetic anhydride; acetic acid at 50 - 70℃; for 6h;86%
With urea hydrogen peroxide adduct; acetic acid at 60℃; under 750.075 Torr; for 6h; Baeyer-Villiger oxidation;78%
With Candida antarctica lipase; dihydrogen peroxide; n-tetradecanoic acid In toluene for 144h;73%
2-hexylcyclopentanone
13074-65-2

2-hexylcyclopentanone

A

2-(n-hexyl)-2-cyclopenten-1-one
95-41-0

2-(n-hexyl)-2-cyclopenten-1-one

B

2-chloro-2-hexylcyclopentanone
83593-56-0

2-chloro-2-hexylcyclopentanone

Conditions
ConditionsYield
With sulfuryl dichloride In tetrachloromethane for 1h; temp.: RT to 40 deg C;A n/a
B 78%
2-hexylcyclopentanone
13074-65-2

2-hexylcyclopentanone

ethylene glycol
107-21-1

ethylene glycol

6-hexyl-1,4-dioxaspiro[4.4]nonane
87735-16-8

6-hexyl-1,4-dioxaspiro[4.4]nonane

Conditions
ConditionsYield
With GdPO4*(MoO2)0.5PMo12O40 In toluene Reflux; Dean-Stark;61.8%
With P0.17Mo2.4CoBr0.27O6.8 In 5,5-dimethyl-1,3-cyclohexadiene at 130℃; for 6h;57%
2-hexylcyclopentanone
13074-65-2

2-hexylcyclopentanone

A

2-(n-hexyl)-2-cyclopenten-1-one
95-41-0

2-(n-hexyl)-2-cyclopenten-1-one

B

(E)-2-n-hexylidenecyclopentanone
103517-11-9

(E)-2-n-hexylidenecyclopentanone

Conditions
ConditionsYield
With CuCl2*2H2O In ethanol; water Heating; 2:1 molar ratio of salt to ketone;A 56%
B n/a
With CuCl2*2H2O In ethanol; water Heating;A 56%
B n/a
2-hexylcyclopentanone
13074-65-2

2-hexylcyclopentanone

3,4-dimethoxy-benzaldehyde
120-14-9

3,4-dimethoxy-benzaldehyde

5-hexyl-2-veratrylidene-cyclopentanone
102600-88-4

5-hexyl-2-veratrylidene-cyclopentanone

Conditions
ConditionsYield
With potassium hydroxide
2-hexylcyclopentanone
13074-65-2

2-hexylcyclopentanone

2-(n-hexyl)-2-cyclopenten-1-one
95-41-0

2-(n-hexyl)-2-cyclopenten-1-one

Conditions
ConditionsYield
With N-Bromosuccinimide; aniline 1) CCl4, reflux, 3 h, 2) rt, 15 h; Yield given. Multistep reaction;
Multi-step reaction with 2 steps
1: 78 percent / sulfuryl chloride / CCl4 / 1 h / temp.: RT to 40 deg C
2: 94 percent Chromat. / 0.5 h / 60 °C / 15 Torr
View Scheme
2-hexylcyclopentanone
13074-65-2

2-hexylcyclopentanone

A

(R)-6-hexyl-tetrahydro-2H-pyran-2-one
108861-12-7

(R)-6-hexyl-tetrahydro-2H-pyran-2-one

B

(6S)-6-hexyltetrahydropyran-2-one
108861-13-8

(6S)-6-hexyltetrahydropyran-2-one

2-Hexyl-cyclopentanone

2-Hexyl-cyclopentanone

2-Hexyl-cyclopentanone

2-Hexyl-cyclopentanone

Conditions
ConditionsYield
In water at 30℃; for 1.5h; pH 7.1; NADPH-dependent biotransformation by partially purified monooxygenase from (+)-camphor grown Ps. putida NCIMB 10007; further monooxygenases; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
In water at 30℃; for 1.5h; pH 7.1; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
sulfuric acid
7664-93-9

sulfuric acid

2-hexylcyclopentanone
13074-65-2

2-hexylcyclopentanone

K2S2O8

K2S2O8

K2SO4

K2SO4

6-hexyltetrahydro-2H-pyran-2-one
710-04-3

6-hexyltetrahydro-2H-pyran-2-one

Conditions
ConditionsYield
at 0 - 10℃; Erwaermen des Reaktionsprodukts mit 5prozent ig. wss. Schwefelsaeure auf dem Dampfbad;
2-hexylcyclopentanone
13074-65-2

2-hexylcyclopentanone

5-Hexyl-bicyclo[3.1.0]hexan-1-ol
229638-73-7

5-Hexyl-bicyclo[3.1.0]hexan-1-ol

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: NaI; pyridine / acetonitrile
2: Et2Zn / hexane
3: ClSiMe3; methanol / 0.25 h / 20 °C
View Scheme
Multi-step reaction with 3 steps
1: 87 percent / NaI, pyridine / acetonitrile
2: 90 percent / Et2Zn / hexane / 0.25 h / 25 °C
3: MeOH, Me3SiCl / 0.25 h / 25 °C
View Scheme
2-hexylcyclopentanone
13074-65-2

2-hexylcyclopentanone

(5-Hexyl-bicyclo[3.1.0]hex-1-yloxy)-trimethyl-silane
211234-63-8

(5-Hexyl-bicyclo[3.1.0]hex-1-yloxy)-trimethyl-silane

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: NaI; pyridine / acetonitrile
2: Et2Zn / hexane
View Scheme
Multi-step reaction with 2 steps
1: 87 percent / NaI, pyridine / acetonitrile
2: 90 percent / Et2Zn / hexane / 0.25 h / 25 °C
View Scheme
2-hexylcyclopentanone
13074-65-2

2-hexylcyclopentanone

(-)-2-hexyl-2-methylcyclopentanone

(-)-2-hexyl-2-methylcyclopentanone

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: 87 percent / NaI, pyridine / acetonitrile
2: 90 percent / Et2Zn / hexane / 0.25 h / 25 °C
3: MeOH, Me3SiCl / 0.25 h / 25 °C
4: DMAP / CH2Cl2 / 2 h / 25 °C
5: NaOH / methanol / 4 h / 60 °C
View Scheme
Multi-step reaction with 3 steps
1: 87 percent / NaI, pyridine / acetonitrile
2: 90 percent / Et2Zn / hexane / 0.25 h / 25 °C
3: NaOH / methanol / 4 h / 60 °C
View Scheme
2-hexylcyclopentanone
13074-65-2

2-hexylcyclopentanone

(+)-2-hexyl-2-methylcyclopentanone

(+)-2-hexyl-2-methylcyclopentanone

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: 87 percent / NaI, pyridine / acetonitrile
2: 90 percent / Et2Zn / hexane / 0.25 h / 25 °C
3: MeOH, Me3SiCl / 0.25 h / 25 °C
4: DMAP / CH2Cl2 / 2 h / 25 °C
5: NaOH / methanol / 4 h / 60 °C
View Scheme
Multi-step reaction with 3 steps
1: 87 percent / NaI, pyridine / acetonitrile
2: 90 percent / Et2Zn / hexane / 0.25 h / 25 °C
3: NaOH / methanol / 4 h / 60 °C
View Scheme
2-hexylcyclopentanone
13074-65-2

2-hexylcyclopentanone

((1R,5R)-5-Hexyl-bicyclo[3.1.0]hex-1-yloxy)-trimethyl-silane

((1R,5R)-5-Hexyl-bicyclo[3.1.0]hex-1-yloxy)-trimethyl-silane

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: 87 percent / NaI, pyridine / acetonitrile
2: 90 percent / Et2Zn / hexane / 0.25 h / 25 °C
3: MeOH, Me3SiCl / 0.25 h / 25 °C
4: DMAP / CH2Cl2 / 2 h / 25 °C
5: 1.) Lipozyme, t-BuOMe, 1-propanol, 2.) Et3N / 1.) 36 deg C, 8 h, 2.) 25 deg C, 18 h
View Scheme
2-hexylcyclopentanone
13074-65-2

2-hexylcyclopentanone

((1S,5S)-5-Hexyl-bicyclo[3.1.0]hex-1-yloxy)-trimethyl-silane

((1S,5S)-5-Hexyl-bicyclo[3.1.0]hex-1-yloxy)-trimethyl-silane

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: 87 percent / NaI, pyridine / acetonitrile
2: 90 percent / Et2Zn / hexane / 0.25 h / 25 °C
3: MeOH, Me3SiCl / 0.25 h / 25 °C
4: DMAP / CH2Cl2 / 2 h / 25 °C
5: 1.) Lipozyme, t-BuOMe, 1-propanol, 2.) Et3N / 1.) 36 deg C, 8 h, 2.) 25 deg C, 18 h
View Scheme
2-hexylcyclopentanone
13074-65-2

2-hexylcyclopentanone

Chloro-acetic acid 5-hexyl-bicyclo[3.1.0]hex-1-yl ester
211234-74-1

Chloro-acetic acid 5-hexyl-bicyclo[3.1.0]hex-1-yl ester

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: 87 percent / NaI, pyridine / acetonitrile
2: 90 percent / Et2Zn / hexane / 0.25 h / 25 °C
3: MeOH, Me3SiCl / 0.25 h / 25 °C
4: DMAP / CH2Cl2 / 2 h / 25 °C
View Scheme
2-hexylcyclopentanone
13074-65-2

2-hexylcyclopentanone

Chloro-acetic acid (1R,5R)-5-hexyl-bicyclo[3.1.0]hex-1-yl ester

Chloro-acetic acid (1R,5R)-5-hexyl-bicyclo[3.1.0]hex-1-yl ester

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: 87 percent / NaI, pyridine / acetonitrile
2: 90 percent / Et2Zn / hexane / 0.25 h / 25 °C
3: MeOH, Me3SiCl / 0.25 h / 25 °C
4: 1.) DMAP, 2.) Lipozyme, t-BuOMe, 1-propanol / 1.) CHCl2, 25 deg C, 2 h, 2.) 36 deg C, 8 h
View Scheme
2-hexylcyclopentanone
13074-65-2

2-hexylcyclopentanone

Chloro-acetic acid (1S,5S)-5-hexyl-bicyclo[3.1.0]hex-1-yl ester

Chloro-acetic acid (1S,5S)-5-hexyl-bicyclo[3.1.0]hex-1-yl ester

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: 87 percent / NaI, pyridine / acetonitrile
2: 90 percent / Et2Zn / hexane / 0.25 h / 25 °C
3: MeOH, Me3SiCl / 0.25 h / 25 °C
4: 1.) DMAP, 2.) Lipozyme, t-BuOMe, 1-propanol / 1.) CHCl2, 25 deg C, 2 h, 2.) 36 deg C, 8 h
View Scheme

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