Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
Cas:13078-21-2
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Cas:13078-21-2
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Cas:13078-21-2
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inquiryFINETECH INDUSTRY LIMITED is a LONDON based CRO company providing drug discovery & development services to worldwide clients. FINETECH INDUSTRY LIMITED supplies the ETHYL 2-METHOXYPHENOXYACETATE, CAS:13078-21-2 with the most competitive price and the
Ethyl2-(2-methoxyphenoxy)acetate Application:99
Cas:13078-21-2
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inquiryhigh purity Application:Drug intermediates Materials intermediates and active molecules
Conditions | Yield |
---|---|
With potassium carbonate In acetone Reflux; | 99% |
Stage #1: 2-methoxy-phenol With potassium carbonate In acetone at 20℃; for 0.25h; Inert atmosphere; Stage #2: ethyl bromoacetate In acetone at 0℃; for 8h; Inert atmosphere; Reflux; | 90% |
Stage #1: 2-methoxy-phenol With potassium carbonate In acetone at 20℃; for 0.25h; Stage #2: ethyl bromoacetate In acetone at 20 - 65℃; | 90% |
ethanol
(2-methoxyphenoxy)acetic acid
ethyl 2-(2-methoxyphenoxy)acetate
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid at 20℃; | 92% |
With toluene-4-sulfonic acid for 5h; Heating; |
chloroacetic acid ethyl ester
2-methoxy-phenol
ethyl 2-(2-methoxyphenoxy)acetate
Conditions | Yield |
---|---|
With ethanol; sodium | |
With potassium carbonate; potassium iodide In acetone | |
With potassium carbonate In acetone for 15h; Heating; |
1-(3,4-dimethoxyphenyl)-2-(methoxyphenoxy)propane-1,3-diol
ethyl 2-(2-methoxyphenoxy)acetate
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: sodium formate / water / 15 h / 110 °C 2: potassium carbonate / acetonitrile View Scheme | |
Multi-step reaction with 3 steps 1: water / 15 h / 110 °C 2: zinc; formic acid / water / 7 h / 110 °C / Sealed tube 3: potassium carbonate / acetonitrile View Scheme | |
Multi-step reaction with 3 steps 1: zinc / water / 7 h / 100 °C / Sealed tube 2: zinc; formic acid / water / 7 h / 110 °C / Sealed tube 3: potassium carbonate / acetonitrile View Scheme |
ethyl 2-(2-methoxyphenoxy)acetate
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: zinc; formic acid / water / 7 h / 110 °C / Sealed tube 2: potassium carbonate / acetonitrile View Scheme |
1-(4-hydroxyphenyl)-2-(2-methoxyphenoxy)propane-1,3-diol
ethyl 2-(2-methoxyphenoxy)acetate
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: formic acid; sodium formate / water / 110 °C 2: potassium carbonate / acetonitrile View Scheme |
ethyl 2-(2-methoxyphenoxy)acetate
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: nano-Pd1Ni4 /MIL-100(Fe) / water / 6 h / 130 °C / Inert atmosphere 2.1: potassium carbonate / acetone / 0.25 h / 20 °C 2.2: 20 - 65 °C View Scheme |
2-(2-methoxyphenoxy)-acetophenone
ethyl 2-(2-methoxyphenoxy)acetate
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: sodium tetrahydroborate / methanol / 4 h / 25 °C 2.1: nano-Pd1Ni4 /MIL-100(Fe) / water / 6 h / 130 °C / Inert atmosphere 3.1: potassium carbonate / acetone / 0.25 h / 20 °C 3.2: 20 - 65 °C View Scheme |
ethyl 2-(2-methoxyphenoxy)acetate
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: sodium tetrahydroborate / methanol / 4 h / 25 °C 2.1: nano-Pd1Ni4 /MIL-100(Fe) / water / 6 h / 150 °C / Inert atmosphere 3.1: potassium carbonate / acetone / 0.25 h / 20 °C 3.2: 20 - 65 °C View Scheme |
2-(2-methoxyphenoxy)-1-(4-methoxyphenyl)ethan-1-one
ethyl 2-(2-methoxyphenoxy)acetate
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: sodium tetrahydroborate / methanol / 4 h / 25 °C 2.1: nano-Pd1Ni4 /MIL-100(Fe) / water / 6 h / 150 °C / Inert atmosphere 3.1: potassium carbonate / acetone / 0.25 h / 20 °C 3.2: 20 - 65 °C View Scheme |
ethyl 2-(2-methoxyphenoxy)acetate
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: nano-Pd1Ni4 /MIL-100(Fe) / water / 6 h / 150 °C / Inert atmosphere 2.1: potassium carbonate / acetone / 0.25 h / 20 °C 2.2: 20 - 65 °C View Scheme |
ethyl 2-(2-methoxyphenoxy)acetate
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: nano-Pd1Ni4 /MIL-100(Fe) / water / 6 h / 150 °C / Inert atmosphere 2.1: potassium carbonate / acetone / 0.25 h / 20 °C 2.2: 20 - 65 °C View Scheme |
guaiacylglycerol-β-guaiacyl ether
ethyl 2-(2-methoxyphenoxy)acetate
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: sodium t-butanolate; oxygen / tert-butyl alcohol / 16 h / 30 °C / 760.05 Torr / Green chemistry 2.1: potassium carbonate / acetone / 0.5 h / Reflux 2.2: 12 h / Reflux View Scheme |
ethyl 2-(2-methoxyphenoxy)acetate
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / 0 - 60 °C 2.1: sodium t-butanolate; oxygen / tert-butyl alcohol / 16 h / 30 °C / 760.05 Torr / Green chemistry 3.1: potassium carbonate / acetone / 0.5 h / Reflux 3.2: 12 h / Reflux View Scheme |
ethyl 2-(2-methoxyphenoxy)acetate
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / 0 - 60 °C 2.1: sodium t-butanolate; oxygen / tert-butyl alcohol / 16 h / 30 °C / 760.05 Torr / Green chemistry 3.1: potassium carbonate / acetone / 0.5 h / Reflux 3.2: 12 h / Reflux View Scheme |
2-(2-methoxyphenoxy)-1-phenylpropane-1,3-diol
ethyl 2-(2-methoxyphenoxy)acetate
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: sodium t-butanolate; oxygen / tert-butyl alcohol / 16 h / 30 °C / 760.05 Torr / Green chemistry 2.1: potassium carbonate / acetone / 0.5 h / Reflux 2.2: 12 h / Reflux View Scheme |
ethyl 2-(2-methoxyphenoxy)acetate
(2-methoxyphenoxy)acetic acid
Conditions | Yield |
---|---|
With potassium hydroxide In methanol; water at 20℃; Inert atmosphere; | 99% |
With sodium hydroxide; water In methanol | |
With potassium hydroxide In ethanol; water at 20℃; for 1.5h; | |
With water; sodium hydroxide In ethanol at 20℃; for 4h; |
ethyl 2-(2-methoxyphenoxy)acetate
benzaldehyde
Conditions | Yield |
---|---|
Stage #1: ethyl 2-(2-methoxyphenoxy)acetate With lithium diisopropyl amide In tetrahydrofuran at -78℃; for 2.5h; Stage #2: benzaldehyde In tetrahydrofuran at -78℃; for 2.5h; | 85% |
With lithium diisopropyl amide In tetrahydrofuran; hexane at -78℃; for 1.5h; | 53.4% |
With n-butyllithium; diisopropylamine In tetrahydrofuran at -78℃; for 1h; Inert atmosphere; |
3-methoxy-4-(phenylmethoxy)benzaldehyde
ethyl 2-(2-methoxyphenoxy)acetate
Conditions | Yield |
---|---|
With lithium diisopropyl amide In tetrahydrofuran at -78℃; | 84% |
ethyl 2-(2-methoxyphenoxy)acetate
1-(3,4-dimethoxyphenyl)ethanone
ethyl-3-(3,4-dimethoxyphenyl)-3-hydroxy-2-(2-methoxyphenoxy)-3-methylpropanoate
Conditions | Yield |
---|---|
Stage #1: ethyl 2-(2-methoxyphenoxy)acetate With n-butyllithium; diisopropylamine In tetrahydrofuran; hexane at -78 - 0℃; for 0.583333h; Inert atmosphere; Stage #2: 1-(3,4-dimethoxyphenyl)ethanone In tetrahydrofuran; hexane at -78℃; for 0.25h; Inert atmosphere; | 83% |
ethyl 2-(2-methoxyphenoxy)acetate
3,4,5-trimethoxy-benzaldehyde
Conditions | Yield |
---|---|
Stage #1: ethyl 2-(2-methoxyphenoxy)acetate With n-butyllithium; diisopropylamine In tetrahydrofuran at -78℃; for 1h; Aldol Condensation; Stage #2: 3,4,5-trimethoxy-benzaldehyde In tetrahydrofuran at -78℃; for 3h; | 76% |
ethyl 2-(2-methoxyphenoxy)acetate
4-methoxy-benzaldehyde
Conditions | Yield |
---|---|
Stage #1: ethyl 2-(2-methoxyphenoxy)acetate With n-butyllithium; diisopropylamine In tetrahydrofuran at -78℃; for 1h; Aldol Condensation; Stage #2: 4-methoxy-benzaldehyde In tetrahydrofuran at -78℃; for 3h; | 70% |
ethyl 2-(2-methoxyphenoxy)acetate
ortho-anisoxyacetic acid hydrazide
Conditions | Yield |
---|---|
With hydrazine hydrate In ethanol for 12h; Heating; | 65% |
With hydrazine hydrate In ethanol for 3h; Heating; |
ethyl 2-(2-methoxyphenoxy)acetate
4-(benzyloxy)-3,5-dimethoxybenzaldehyde
1-<3,5-Dimethoxyphenyl-4-(phenylmethoxy)phenyl>-2-carbethoxy-2-(2-methoxyphenoxy)ethanol
Conditions | Yield |
---|---|
Stage #1: ethyl 2-(2-methoxyphenoxy)acetate With n-butyllithium; diisopropylamine In tetrahydrofuran; hexane at -78℃; for 1h; Stage #2: 4-(benzyloxy)-3,5-dimethoxybenzaldehyde In tetrahydrofuran; hexane at -78℃; for 3h; | 56% |
ethyl 2-(2-methoxyphenoxy)acetate
3,4-dimethoxy-benzaldehyde
ethyl 3-(3,4-dimethoxyphenyl)-3-hydroxy-2-(2-methoxyphenoxy)propanoate
Conditions | Yield |
---|---|
With lithium diisopropyl amide In tetrahydrofuran; hexane at -78℃; for 1.5h; | 52.9% |
Stage #1: ethyl 2-(2-methoxyphenoxy)acetate With lithium diisopropyl amide In tetrahydrofuran at -78℃; for 1h; Inert atmosphere; Stage #2: 3,4-dimethoxy-benzaldehyde In tetrahydrofuran at 45℃; for 2h; Inert atmosphere; | 40% |
Stage #1: ethyl 2-(2-methoxyphenoxy)acetate With lithium diisopropyl amide In tetrahydrofuran at -78℃; for 1.16667h; Inert atmosphere; Stage #2: 3,4-dimethoxy-benzaldehyde In tetrahydrofuran at -78℃; for 2h; Inert atmosphere; | 37% |
ethyl 2-(2-methoxyphenoxy)acetate
3,4-dimethoxy-benzaldehyde
Conditions | Yield |
---|---|
Stage #1: ethyl 2-(2-methoxyphenoxy)acetate With n-butyllithium; N-ethyl-N,N-diisopropylamine In tetrahydrofuran; hexane at -78℃; for 1.16667h; Inert atmosphere; Stage #2: 3,4-dimethoxy-benzaldehyde In tetrahydrofuran; hexane at -78℃; for 2h; Inert atmosphere; optical yield given as %de; | 52% |
Stage #1: ethyl 2-(2-methoxyphenoxy)acetate With n-butyllithium; diisopropylamine In tetrahydrofuran at -78℃; for 1h; Aldol Condensation; Stage #2: 3,4-dimethoxy-benzaldehyde In tetrahydrofuran at -78℃; for 3h; |
ethyl 2-(2-methoxyphenoxy)acetate
3,4,5-trimethoxy-benzaldehyde
Conditions | Yield |
---|---|
Stage #1: ethyl 2-(2-methoxyphenoxy)acetate With lithium diisopropyl amide In tetrahydrofuran at -78℃; for 1.16667h; Inert atmosphere; Stage #2: 3,4,5-trimethoxy-benzaldehyde In tetrahydrofuran at -78℃; for 2h; Inert atmosphere; | 42% |
Stage #1: ethyl 2-(2-methoxyphenoxy)acetate With lithium diisopropyl amide In tetrahydrofuran Stage #2: 3,4,5-trimethoxy-benzaldehyde In tetrahydrofuran at -78 - 20℃; | |
With lithium diisopropyl amide |
ethyl 2-(2-methoxyphenoxy)acetate
4-(benzyloxy)-3,5-dimethoxybenzaldehyde
ethyl 3-(4-(benzyloxy)-3,5-dimethoxyphenyl)-3-hydroxy-2-(2-methoxyphenoxy)propanoate
Conditions | Yield |
---|---|
Stage #1: ethyl 2-(2-methoxyphenoxy)acetate With lithium diisopropyl amide In tetrahydrofuran at -78℃; for 1.16667h; Inert atmosphere; Stage #2: 4-(benzyloxy)-3,5-dimethoxybenzaldehyde In tetrahydrofuran at -78℃; for 2h; Inert atmosphere; | 41% |
With lithium diisopropyl amide In tetrahydrofuran at -70℃; Addition; | |
With lithium diisopropyl amide In tetrahydrofuran at -78℃; |
ethyl 2-(2-methoxyphenoxy)acetate
ortho-anisaldehyde
Conditions | Yield |
---|---|
With lithium diisopropyl amide In tetrahydrofuran; hexane at -78℃; for 1.5h; | 38.4% |
ethyl 2-(2-methoxyphenoxy)acetate
3-methoxy-benzaldehyde
Conditions | Yield |
---|---|
With lithium diisopropyl amide In tetrahydrofuran; hexane at -78℃; for 1.5h; | 38.4% |
ethyl 2-(2-methoxyphenoxy)acetate
3,4-dimethoxy-benzaldehyde
Conditions | Yield |
---|---|
Stage #1: ethyl 2-(2-methoxyphenoxy)acetate With lithium diisopropyl amide In tetrahydrofuran at -78℃; for 1.5h; Stage #2: 3,4-dimethoxy-benzaldehyde In tetrahydrofuran at -78℃; for 3h; Stage #3: With water In tetrahydrofuran | A 6% B 34% |
With lithium diisopropyl amide | A n/a B n/a |
Stage #1: ethyl 2-(2-methoxyphenoxy)acetate With sodium hexamethyldisilazane In tetrahydrofuran at -78℃; for 0.166667h; Stage #2: 3,4-dimethoxy-benzaldehyde In tetrahydrofuran at -78 - 20℃; for 2h; Overall yield = 42 %; Overall yield = 1.59 g; |
3-methoxy-4-(phenylmethoxy)benzaldehyde
ethyl 2-(2-methoxyphenoxy)acetate
Conditions | Yield |
---|---|
Stage #1: ethyl 2-(2-methoxyphenoxy)acetate With n-butyllithium; N-ethyl-N,N-diisopropylamine In tetrahydrofuran; hexane at -78℃; for 1.16667h; Inert atmosphere; Stage #2: 3-methoxy-4-(phenylmethoxy)benzaldehyde In tetrahydrofuran; hexane at -78℃; for 2h; Inert atmosphere; optical yield given as %de; diastereoselective reaction; | A 30% B n/a |
ethyl 2-(2-methoxyphenoxy)acetate
4-methoxy-benzaldehyde
Conditions | Yield |
---|---|
Stage #1: ethyl 2-(2-methoxyphenoxy)acetate With lithium diisopropyl amide In tetrahydrofuran at -78℃; for 1.16667h; Inert atmosphere; Stage #2: 4-methoxy-benzaldehyde In tetrahydrofuran at -78℃; for 2h; Inert atmosphere; | 28% |
With lithium diisopropyl amide In tetrahydrofuran; hexane at -78℃; for 1.5h; |
ethyl 2-(2-methoxyphenoxy)acetate
4-benzoyloxy-3-methoxybenzaldehyde
Conditions | Yield |
---|---|
Stage #1: ethyl 2-(2-methoxyphenoxy)acetate With n-butyllithium; N-ethyl-N,N-diisopropylamine In tetrahydrofuran at -78℃; Stage #2: 4-benzoyloxy-3-methoxybenzaldehyde In tetrahydrofuran at -78℃; for 3h; | A 25% B 20% |
ethyl 2-(2-methoxyphenoxy)acetate
benzyl chloride
Ethyl β-hydroxy-3-methoxy-α-(2-methoxyphenoxy)-4-(phenylmethoxy)benzenepropanoate
Conditions | Yield |
---|---|
With tetrabutylammomium bromide; sodium chloride; sodium hydroxide In water; toluene at 90℃; for 2h; Reflux; | A 2% B 3% |
ethyl 2-(2-methoxyphenoxy)acetate
2-(2-methoxyphenoxy)acetamide
Conditions | Yield |
---|---|
With ammonia |
ethyl 2-(2-methoxyphenoxy)acetate
N,N-diethylethylenediamine
N,N-Diethyl-N'-<(2-methoxy-phenoxy)-acetyl>-ethylendiamin
3-methoxy-4-(phenylmethoxy)benzaldehyde
ethyl 2-(2-methoxyphenoxy)acetate
Ethyl β-hydroxy-3-methoxy-α-(2-methoxyphenoxy)-4-(phenylmethoxy)benzenepropanoate
Conditions | Yield |
---|---|
With lithium diisopropyl amide 1.) THF, -75 deg C, 2.) THF, -75 deg C; Yield given. Multistep reaction; | |
With lithium diisopropyl amide In tetrahydrofuran at -78℃; |
ethyl 2-(2-methoxyphenoxy)acetate
4-(benzyloxy)-3,5-dimethoxybenzaldehyde
1-<3,5-Dimethoxyphenyl-4-(phenylmethoxy)phenyl>-2-carbethoxy-2-(2-methoxyphenoxy)ethanol
1-<3,5-Dimethoxyphenyl-4-(phenylmethoxy)phenyl>-2-carbethoxy-2-(2-methoxyphenoxy)ethanol
Conditions | Yield |
---|---|
With lithium diisopropyl amide 1.) THF, -75 dg C, 2.) THF, -75 deg C; Yield given. Multistep reaction. Yields of byproduct given; | |
With lithium diisopropyl amide 1.) THF, -75 deg C, 2.) THF, -75 deg C; Yield given. Multistep reaction. Yields of byproduct given; |
ethyl 2-(2-methoxyphenoxy)acetate
3,4-dimethoxy-benzaldehyde
1-(3,4-Dimethoxyphenyl)-2-carbethoxy-2-(2-methoxyphenoxy)ethanol
Conditions | Yield |
---|---|
With lithium diisopropyl amide 1.) THF, -75 deg C, 2.) THF, -75 deg C, 90 min; Yield given. Multistep reaction; | |
Stage #1: ethyl 2-(2-methoxyphenoxy)acetate With lithium diisopropyl amide In tetrahydrofuran at -78 - 20℃; Stage #2: 3,4-dimethoxy-benzaldehyde In tetrahydrofuran |
ethyl 2-(2-methoxyphenoxy)acetate
(2-Methoxy-phenoxy)-acethydroxamsaeure
Conditions | Yield |
---|---|
With hydroxylamine; sodium methylate In methanol |
3-methoxy-4-(phenylmethoxy)benzaldehyde
ethyl 2-(2-methoxyphenoxy)acetate
Conditions | Yield |
---|---|
With lithium diisopropyl amide In tetrahydrofuran at -70℃; Addition; | |
With lithium diisopropyl amide In tetrahydrofuran at -78℃; |
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