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Conditions | Yield |
---|---|
In solid byproducts: LiCl; under N2; Li2O and metal halide ground together, added to glass ampoule, sealed under vacuum, sonicated (ultrasound) for 10 min, wrapped in glss wool, placed in oven at 450°C for 10 h; removed from oven, allowed to cool to room temp., trituration with THF for 10 h, ppt. and cloudy THF layer formed, evapn.of THF filtrate produced Li salt; or metal oxides washed with H2O for 10 min to remove Li salt; | 85% |
cobalt(II) acetate
cobalt(II) oxide
Conditions | Yield |
---|---|
In benzyl alcohol other Radiation; dispersed, microwave heating for 30-1200 s; XRD; | 60.8% |
In solid byproducts: H2O, CO2, CO; Co(CH3CO2)2 was thermodestructed at 260°C; | |
In neat (no solvent) N2 atmosphere; heating (300 - 400°C); detd. by powder X-ray diffraction; |
cobaltocene
tetraphenylborate anion
1,5-dicyclooctadiene
A
cobalt(II) oxide
B
(η5-cyclopentadienyl)-η4-cycloocta-1,5-dienecobalt(I)
E
cobalt
Conditions | Yield |
---|---|
With C5H5Na In tetrahydrofuran; water; pentane under N2, CoBr2*DME, NaCp, CoCp2 and COD mixed in THF in molar ratio of2/2.06/0.5/1.16 (CoCp2 added at -80°C prior to NaCp), warmed to room temp. during 3 h, evapd., pentane ext. passed through Al2O3/4% H2O and CuCl powder; concd., cooled to -80°C, CpCoCOD filtered off; CuCl washed with water, CoCp2(1+) pptd. with BPh4(1-) from aq. soln., filtered off; pentane-insol. residue treated with water, Co and CoO mixt. filtered, Co(2+) determined complexometrically; | A n/a B 45.3% C n/a D n/a E n/a |
With C5H5Na In tetrahydrofuran; water; pentane under N2, CoBr2*DME, NaCp, CoCp2 and COD mixed in THF in molar ratio of2/2.06/0.5/1.16 (CoCp2 added at -80°C after NaCp), warmed to room temp. during 3 h, evapd., pentane ext. passed through Al2O3/4% H2O andCuCl powder; concd., cooled to -80°C, CpCoCOD filtered off; CuCl washed with water, CoCp2(1+) pptd. with BPh4(1-) from aq. soln., filtered off; pentane-insol. residue treated with water, Co and CoO mixt. filtered, Co(2+) determined complexometrically; | A n/a B 43% C n/a D n/a E n/a |
With C5H5Na In tetrahydrofuran; water; pentane under N2, CoBr2*DME, NaCp, CoCp2 and COD mixed in THF in molar ratio of2/2.06/0.5/1.16 (CoCp2 added at 0°C prior to NaCp at -80°C), warmed to room temp. during 3 h, evapd., pentane ext. passed throughAl2O3/4% H2O and CuCl powder; concd., cooled to -80°C, CpCoCOD filtered off; CuCl washed with water, CoCp2(1+) pptd. with BPh4(1-) from aq. soln., filtered off; pentane-insol. residue treated with water, Co and CoO mixt. filtered, Co(2+) determined complexometrically; | A n/a B 37.5% C n/a D n/a E n/a |
With C5H5Na In tetrahydrofuran; water; pentane under N2, CoBr2*DME, NaCp, CoCp2 and COD mixed in THF in molar ratio of2/3/0.5/1.16, warmed to room temp. during 3 h, evapd., pentane ext. passed through Al2O3/4% H2O and CuCl powder; concd., cooled to -80°C, CpCoCOD filtered off; CuCl washed with water, CoCp2(1+) pptd. with BPh4(1-) from aq. soln., filtered off; pentane-insol. residue treated with water, Co and CoO mixt. filtered, Co(2+) determined complexometrically; | A n/a B 11.5% C n/a D n/a E n/a |
With C5H5Na In hexane; water; pentane under N2, CoBr2*DME, NaCp, CoCp2 and COD mixed in molar ratio of 2/3/0.5/1.16 in hexane at -80°C, warmed to room temp. during 3 h, evapd., pentane ext. passed through Al2O3/4% H2O and CuCl powder; concd., cooled to -80°C, CpCoCOD filtered off; CuCl washed with water, CoCp2(1+) pptd. with BPh4(1-) from aq. soln., filtered off; pentane-insol. residue treated with water, Co and CoO mixt. filtered, Co(2+) determined complexometrically; | A n/a B 8.6% C n/a D n/a E n/a |
cobaltocene
tetraphenylborate anion
cyclopentadienyllithium
1,5-dicyclooctadiene
A
cobalt(II) oxide
B
(η5-cyclopentadienyl)-η4-cycloocta-1,5-dienecobalt(I)
E
cobalt
Conditions | Yield |
---|---|
In tetrahydrofuran; water; pentane under N2, CoBr2*DME, LiCp, CoCp2 and COD mixed in THF in molar ratio of2/2.06/0.5/1.16, warmed to room temp. during 3 h, evapd., pentane ext. passed through Al2O3/4% H2O and CuCl powder; concd., cooled to -80°C, CpCoCOD filtered off; CuCl washed with water, CoCp2(1+) pptd. with BPh4(1-) from aq. soln., filtered off; pentane-insol. residue treated with water, Co and CoO mixt. filtered, Co(2+) determined complexometrically; | A n/a B 18% C n/a D n/a E n/a |
Conditions | Yield |
---|---|
In neat (no solvent) 1700°C;; | 14.6% |
In neat (no solvent) 1700°C;; | 14.6% |
In neat (no solvent) byproducts: Co3O4; less than 500°C, 1Torr O2;; |
cobalt(II) oxide
Conditions | Yield |
---|---|
at 20 - 800℃; | 13.5% |
Conditions | Yield |
---|---|
In neat (no solvent) byproducts: H2SO4; decompn.;; | |
In neat (no solvent) byproducts: H2SO4; decompn.;; |
cobalt(II) oxide
Conditions | Yield |
---|---|
With methane In neat (no solvent) reduction at 450°C;; | |
In solid calcination (1050°C, N2 (low p(O2)) atmosphere); | |
In neat (no solvent) heating to 1200°C in vacuum;; |
Conditions | Yield |
---|---|
In solid byproducts: O2; heating Co2O3 to 1000°C under air; |
Conditions | Yield |
---|---|
In neat (no solvent) byproducts: H2O; furnace heating (rate 4.5°C/min); gas chromy., X-ray diffraction; |
Conditions | Yield |
---|---|
In neat (no solvent) (Ar); In2O3 and Co reacted in 1:1 or 1:2 or 2:1 molar ratio; powdered inmortar; sealed under vacuum in quartz ampoule; heated to 723 K and with 0.5 K/h to 973 K; maintained for 7 days; cooled to 0.8 K/h to 473 K; le ft standing at room temp.; |
Conditions | Yield |
---|---|
In neat (no solvent) Kinetics; 300-400°C, p(H2O)=5-60 atm; drying (room temp.); X-ray diffraction; |
Conditions | Yield |
---|---|
In neat (no solvent) Kinetics; 300°C, p(H2O)=5 atm; drying (room temp.); X-ray diffraction; |
Conditions | Yield |
---|---|
at red heat;; | |
equilibrium;; | |
equilibrium;; |
Conditions | Yield |
---|---|
In neat (no solvent) Kinetics; byproducts: O2; heating up to 600°C (in air); |
cobalt(II) oxide
Conditions | Yield |
---|---|
In neat (no solvent) byproducts: H2O; multi stage react. on heating; sample placed in sample pan and heated gradually from 298 to 1200 K at 10 K/min under flowing air at rate of 100 mL/min; detn. by TG; | |
In solid Co salt was heated at 823 K for 6 h; | |
With CH3OCH2CH2OH In water mixt. stirred for 5 h; aged at room temp. for 8 h; film deposited by spin coating on SiO2 substrate; XRD; |
A
cobalt(II) oxide
Conditions | Yield |
---|---|
In not given a soln. containing 2 moles Co(NO3)2*6H2O and 1 mole Mn(NO3)2*6H2O is evaporated and the residue heated at 850 °C;; product mixture obtained;; |
Co(N-(6-methyl-2-pyridyl)salicylaldimine)2
cobalt(II) oxide
Conditions | Yield |
---|---|
With sodium hydroxide In water 60°C; |
Conditions | Yield |
---|---|
In solid 354+/-3°C; | |
In neat (no solvent, solid phase) 354+/-3°C; |
Conditions | Yield |
---|---|
In solid 356+/-1°C; | |
In neat (no solvent, solid phase) 356+/-1°C; |
Conditions | Yield |
---|---|
In melt Electrolysis; (N2); at 650-700.degreeC; voltages 3-5 V; current 1 A; 99.7 mol. % PO3(1-) in the melt; graphite anode and cathode or platinum anode and silver cathode; elem. anal.; | 100% |
Conditions | Yield |
---|---|
In melt Electrolysis; (N2); at 650-700.degreeC; voltages 3-5 V; current 1 A; 97.6 mol. % PO3(1-) in the melt; graphite anode and cathode or platinum anode and silver cathode; elem. anal.; | A 95% B 5% |
Conditions | Yield |
---|---|
In melt Electrolysis; (N2); at 650-700°C; voltages 3-5 V; current 1 A; graphite electrodes; 95 mol.% metaarsenite in the melt; | A 10% B 90% |
Conditions | Yield |
---|---|
In melt Electrolysis; (N2); at 650-700.degreeC; voltages 3-5 V; current 1 A; 99.3 mol. % PO3(1-) in the melt; graphite anode and cathode or platinum anode and silver cathode; elem. anal.; | A 88% B 12% |
In melt Electrolysis; (N2); at 650-700.degreeC; voltages 3-5 V; current 1 A; 99.0 mol. % PO3(1-) in the melt; graphite anode and cathode or platinum anode and silver cathode; elem. anal.; | A 50% B 50% |
Conditions | Yield |
---|---|
With O2 In further solvent(s) dione as solvent, reflux for 24 h under O2; cooling to room temp., evapn. in vac., extn. with acetone, evapn. at room temp. in air or in vac., sublimation, recrystn. from EtOH, elem. anal.; | 85% |
Conditions | Yield |
---|---|
at 350℃; for 72h; Sealed tube; | 82.35% |
Conditions | Yield |
---|---|
In water High Pressure; mixt. of MoO3, CoO suspended in H2O; pH value of soln. before hydrothermal treatment was 4.1; mixt. put into Teflon-lined autoclave and heated in a forced convection oven at 453 K under autogenous pressure for 1 ds or heated at 423 K; filtered; washed (H2O); dried in air at room temp.; monitored by X-ray diffraction; | 81.6% |
Conditions | Yield |
---|---|
In water High Pressure; mixt. of MoO3, CoO suspended in H2O; pH value of soln. before hydrothermal treatment was 4.1; mixt. put into Teflon-lined autoclave and heated in a forced convection oven at 453 K under autogenous pressure for 3 ds; filtered; washed (H2O); dried in air at room temp.; monitored by X-ray diffraction; elem. anal.; | 73.8% |
cobalt(II) oxide
3,3’,5,5’-tetracarboxydiphenylmethane
water
N,N-dimethyl-formamide
Conditions | Yield |
---|---|
In water; N,N-dimethyl-formamide High Pressure; mixt. of CoO, acid, DMF and H2O was heated in reactor at 105°C for 3 d; cooled to room temp. at rate 10°C/h; elem. anal.; | 72% |
cobalt(II) oxide
phosphoric acid
oxalic acid dihydrate
1,4-diaminobutane
Conditions | Yield |
---|---|
In water at 170℃; for 168h; Autoclave; | 70.2% |
Conditions | Yield |
---|---|
With Na2CO3 In melt Electrolysis; (N2); at 650-700°C; voltages 3-5 V; current 1 A; graphite electrodes; 95 mol.% metaantimonate in the melt; | A 70% B 29% |
Conditions | Yield |
---|---|
In water High Pressure; mixing C5H3N(CO2H)2, CoO, Tb compd., H2O in steel vessel, heating to 180°C for 3 d, cooling to room temp. (1.5°C/h); isolation of crystals, washing with H2O and Et2O, elem. anal.; | 70% |
Conditions | Yield |
---|---|
With hydrogenchloride In water at 230℃; for 72h; Autoclave; | 68% |
Conditions | Yield |
---|---|
In neat (no solvent) at 160℃; Autoclave; | 67.2% |
cobalt(II) oxide
Conditions | Yield |
---|---|
In water under N2; addn. of CoO to Ir compd. in water, stirred for 10 min at 80°C, then addn. of CoBr2, stirring at 80°C for 4 h; filtered, filtrate allowed to stand at room temp. for 2 d, crystn., collected by filtration; elem. anal.; | 66% |
Conditions | Yield |
---|---|
In water High Pressure; mixing C5H3N(CO2H)2, CoO, Eu compd., H2O in steel vessel, heating to 180°C for 3 d, cooling to room temp. (1.5°C/h); isolation of crystals, washing with H2O and Et2O, elem. anal.; | 65% |
Conditions | Yield |
---|---|
In water High Pressure; mixing C5H3N(CO2H)2, CoO, Pr compd., H2O in steel vessel, heating to 180°C for 3 d, cooling to room temp. (1.5°C/h); isolation of crystals, washing with H2O and Et2O, elem. anal.; | 63% |
Conditions | Yield |
---|---|
In water High Pressure; mixing C5H3N(CO2H)2, CoO, Yb compd., H2O in steel vessel, heating to 180°C for 3 d, cooling to room temp. (1.5°C/h); isolation of crystals, washing with H2O and Et2O, elem. anal.; | 62% |
Conditions | Yield |
---|---|
In water High Pressure; mixing C5H3N(CO2H)2, CoO, Sm compd., H2O in steel vessel, heating to 180°C for 3 d, cooling to room temp. (1.5°C/h); isolation of crystals, washing with H2O and Et2O, elem. anal.; | 60% |
Conditions | Yield |
---|---|
In water High Pressure; mixing C5H3N(CO2H)2, CoO, Dy compd., H2O in steel vessel, heating to 180°C for 3 d, cooling to room temp. (1.5°C/h); isolation of crystals, washing with H2O and Et2O, elem. anal.; | 60% |
cobalt(II) oxide
copper(l) iodide
hydrogen iodide
potassium iodide
Conditions | Yield |
---|---|
In methanol at 20 - 145℃; for 168h; Autoclave; | 60% |
Conditions | Yield |
---|---|
In water at 580℃; for 168h; Sealed tube; Autoclave; | A n/a B 50% |
cobalt(II) oxide
citric acid
[(zinc(II))(cobalt(II))(citric acid(-3H))(bromide)]
Conditions | Yield |
---|---|
In melt High Pressure; mixt. of CoO (0.680 mmol), ZnBr2 (7.370 mmol) and citric acid (31.302 mmol) heated in Teflon-lined stainless steel reactor at 170°C for 6d, slowly cooled to room temp.; ppt. sepd., washed with H2O and EtOH, dried in air; elem. anal.; | 40.25% |
Conditions | Yield |
---|---|
at 580℃; under 1500150 Torr; Autoclave; | 40% |
cobalt(II) oxide
citric acid
zinc(II) chloride
[(zinc(II))(cobalt(II))(citric acid(-3H))(chloride)]
Conditions | Yield |
---|---|
In melt High Pressure; mixt. of CoO (0.680 mmol), ZnCl2 (7.330 mmol) and citric acid (31.302 mmol) heated in Teflon-lined stainless steel reactor at 170°C for 6d, slowly cooled to room temp.; ppt. sepd., washed with H2O and EtOH, dried in air; elem. anal.; | 36.29% |
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