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Dayang Chem (Hangzhou) Co.,Ltd.

As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch

2-Amino-5-iodobenzonitrile

Cas:132131-24-9

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

inquiry

Xi'an Xszo Chem Co., Ltd.

1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s

High Quality 99% Benzonitrile, 2-amino-5-iodo- 132131-24-9 ISO Producer

Cas:132131-24-9

Min.Order:1 Gram

FOB Price: $0.1

Type:Manufacturers

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Hebei yanxi chemical co.,LTD.

hebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developm

2-Amino-5-iodobenzonitrile CAS NO.132131-24-9

Cas:132131-24-9

Min.Order:1 Metric Ton

FOB Price: $1.0 / 3.0

Type:Trading Company

inquiry

Henan Tianfu Chemical Co., Ltd.

2-AMINO-5-IODOBENZONITRILE Basic information Product Name: 2-AMINO-5-IODOBENZONITRILE Synonyms: 2-AMINO-5-IODOBENZONITRILE;2-Cyano-4-iodoaniline CAS: 132131-24-9

132131-24-9

Cas:132131-24-9

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Hebei Nengqian Chemical Import and Export Co., LTD

Our advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva

2-AMINO-5-IODOBENZONITRILE

Cas:132131-24-9

Min.Order:1 Kilogram

FOB Price: $9.0 / 99.0

Type:Trading Company

inquiry

Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Pharmaceutical Grade CAS 132131-24-9 with competitive price

Cas:132131-24-9

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

inquiry

Wuhan Han Sheng New Material Technology Co.,Ltd

Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We

Hot Sell Factory Supply Raw Material CAS 132131-24-9 2-AMINO-5-IODOBENZONITRILE

Cas:132131-24-9

Min.Order:10 Kilogram

Negotiable

Type:Trading Company

inquiry

Hebei Sankai Chemical Technology Co., Ltd

1. Product advantages ♦ High purity, all above 98.5%, no impurities after the dissolution ♦ We will test each batch to ensure quality ♦ OEM and private brand services designed for free ♦ Various cap colors available &diam

2-AMINO-5-IODOBENZONITRILE CAS132131-24-9

Cas:132131-24-9

Min.Order:1 Kilogram

FOB Price: $7.0 / 10.0

Type:Trading Company

inquiry

Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

Benzonitrile, 2-amino-5-iodo- 132131-24-9

Cas:132131-24-9

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Qingdao Beluga Import and Export Co., LTD

2-AMINO-5-IODOBENZONITRILE CAS:864070-44-0 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organ

2-AMINO-5-IODOBENZONITRILE CAS:864070-44-0

Cas:132131-24-9

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

Benzonitrile, 2-amino-5-iodo-

Cas:132131-24-9

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Lonwin Chemical Group Limited

2-AMINO-5-IODOBENZONITRILE CAS: 132131-24-9 Specification Test Item Standard: USP Identification IR spectrum similar to that of RS HPLC retention time similar to that of RS Rela

Factory supply 2-AMINO-5-IODOBENZONITRILE

Cas:132131-24-9

Min.Order:1 Kilogram

Negotiable

Type:Other

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

Benzonitrile, 2-amino-5-iodo-

Cas:132131-24-9

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

SHANGHAI T&W PHARMACEUTICAL CO., LTD.

A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc

132131-24-9

Cas:132131-24-9

Min.Order:4 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

Benzonitrile, 2-amino-5-iodo-

Cas:132131-24-9

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

High quality 2-amino-5-iodobenzonitrile

Cas:132131-24-9

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

inquiry

SHANGHAI SYSTEAM BIOCHEM CO., LTD

We are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov

Buy Actavis

Cas:132131-24-9

Min.Order:100 Gram

FOB Price: $100.0 / 2000.0

Type:Lab/Research institutions

inquiry

Hebei Kunsui Technology Co., Ltd.

1. A strong scientific research team . 2. Stable quality (with a complete scientific research center and testing center to ensure the quality stability of each batch of products). 3. Rich export experience (with practical experience in exporting to m

Organic Intermediate 2-Amino-5-iodobenzonitrile Powder CAS 132131-24-9

Cas:132131-24-9

Min.Order:1 Kilogram

FOB Price: $8.2 / 8.8

Type:Trading Company

inquiry

Zibo Dorne chemical technology co. LTD

Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,

2-Amino-5-iodobenzonitrile

Cas:132131-24-9

Min.Order:1 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Jiangsu Qianyu Molecular Technology Co., LTD.

Our Advantages A. International Top level TechnologyOur company owned biomedicine experts are famous at home and abroad with rich experience in research and development in the field of efficient chiral functional molecules research and development an

Buy Top Purity 2-AMINO-5-IODOBENZONITRILE

Cas:132131-24-9

Min.Order:0

Negotiable

Type:Trading Company

inquiry

EAST CHEMSOURCES LIMITED

factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B

Buy Actavis

Cas:132131-24-9

Min.Order:1 Kilogram

FOB Price: $18.0 / 20.0

Type:Trading Company

inquiry

TAIZHOU ZHENYU BIOTECHNOLOGY CO., LTD

Zhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed

2-AMINO-5-IODOBENZONITRILE

Cas:132131-24-9

Min.Order:1 Kilogram

FOB Price: $2.0

Type:Lab/Research institutions

inquiry

Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

Buy Actavis

Cas:132131-24-9

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

KAISA GROUP INC

1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer

Buy Actavis

Cas:132131-24-9

Min.Order:1 Metric Ton

FOB Price: $1.5

Type:Trading Company

inquiry

Golden Pharma Co., Limited

GOLDEN PHARMA CO.,LIMITED.is a professional pharmaceutical company,our team have more than 20years expereince in pharmaceutical production and sales. we are a professional technical enterprise specializing in the R & D, production,QA regulation

2-AMINO-5-IODOBENZONITRILE

Cas:132131-24-9

Min.Order:1 Kilogram

Negotiable

Type:Other

inquiry

Bluecrystal chem-union

We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp

Buy Actavis

Cas:132131-24-9

Min.Order:1 Metric Ton

FOB Price: $1.0

Type:Trading Company

inquiry

Changzhou Anchor Biological Technology Co., Ltd.

Our company is engaged in customizing the benzene ring and pyridine derivative organic intermediates, and the quantity is flexible according to customer's needs. It mainly provides high-quality intermediates for domestic and foreign pharmaceutical an

2-Amino-5-iodobenzonitrile Manufacturer/High quality/Best price/In stock CAS NO.132131-24-9

Cas:132131-24-9

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hebei Mojin Biotechnology Co.,Ltd

We produce carbomer by our own factory,carbomer 940 is our best seller.It is used for cosmetic and medical.And we also become agent for lubrizol.Our carbomer 940 get high viscosity and good transparency.The price will depond on the market,surely supp

2-AMINO-5-IODOBENZONITRILE

Cas:132131-24-9

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Win-Win chemical Co.Ltd

Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai

2-Amino-5-iodobenzonitrile cas no. 132131-24-9 97%

Cas:132131-24-9

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

GIHI CHEMICALS CO.,LIMITED

Lower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe

Benzonitrile, 2-amino-5-iodo-

Cas:132131-24-9

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Synthetic route

anthranilic acid nitrile
1885-29-6

anthranilic acid nitrile

5-iodoanthranilonitrile
132131-24-9

5-iodoanthranilonitrile

Conditions
ConditionsYield
With K(ICl2) In methanol; water at 20℃; for 2h;93%
With ammonium iodide; dihydrogen peroxide; acetic acid at 20℃; for 12h;92.6%
With ammonium iodide; dihydrogen peroxide; acetic acid at 20℃; for 12h;92.6%
N-iodo-succinimide
516-12-1

N-iodo-succinimide

anthranilic acid nitrile
1885-29-6

anthranilic acid nitrile

5-iodoanthranilonitrile
132131-24-9

5-iodoanthranilonitrile

Conditions
ConditionsYield
In DMF (N,N-dimethyl-formamide) at 20℃; for 18h;73%
N-(2-cyano-4-iodo-phenyl)-2,2,2-trifluoro-acetamide

N-(2-cyano-4-iodo-phenyl)-2,2,2-trifluoro-acetamide

5-iodoanthranilonitrile
132131-24-9

5-iodoanthranilonitrile

Conditions
ConditionsYield
With potassium carbonate In methanol at 20℃; for 12h;
N-(2,4-diiodo-phenyl)-2,2,2-trifluoro-acetamide
878133-06-3

N-(2,4-diiodo-phenyl)-2,2,2-trifluoro-acetamide

5-iodoanthranilonitrile
132131-24-9

5-iodoanthranilonitrile

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: dimethylformamide / 0.5 h / 100 °C
2: aq. K2CO3 / methanol / 12 h / 20 °C
View Scheme
2,4-diiodoaniline
533-70-0

2,4-diiodoaniline

5-iodoanthranilonitrile
132131-24-9

5-iodoanthranilonitrile

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: dimethylformamide / 0.5 h / 20 °C
2: dimethylformamide / 0.5 h / 100 °C
3: aq. K2CO3 / methanol / 12 h / 20 °C
View Scheme
p-aminoiodobenzene
540-37-4

p-aminoiodobenzene

5-iodoanthranilonitrile
132131-24-9

5-iodoanthranilonitrile

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: ICl / dimethylformamide / 0.5 h / 20 °C
2: dimethylformamide / 0.5 h / 20 °C
3: dimethylformamide / 0.5 h / 100 °C
4: aq. K2CO3 / methanol / 12 h / 20 °C
View Scheme
anthranilic acid nitrile
1885-29-6

anthranilic acid nitrile

A

5-iodoanthranilonitrile
132131-24-9

5-iodoanthranilonitrile

B

3-iodo-2-aminobenzonitrile
114344-67-1

3-iodo-2-aminobenzonitrile

Conditions
ConditionsYield
With dihydrogen peroxide; acetic acid; potassium iodide In water at 20℃; for 24h;
Iodine monochloride
7790-99-0

Iodine monochloride

anthranilic acid nitrile
1885-29-6

anthranilic acid nitrile

5-iodoanthranilonitrile
132131-24-9

5-iodoanthranilonitrile

Conditions
ConditionsYield
In acetic acid at 25 - 35℃; for 3h;
5-iodoanthranilonitrile
132131-24-9

5-iodoanthranilonitrile

N,N-dimethyl-formamide
68-12-2, 33513-42-7

N,N-dimethyl-formamide

N’-(2-cyano-4-iodophenyl)-N,N-dimethyl formamidine
903597-10-4

N’-(2-cyano-4-iodophenyl)-N,N-dimethyl formamidine

Conditions
ConditionsYield
In N,N-dimethyl acetamide at 110℃; for 2h; Product distribution / selectivity; Heating / reflux;100%
at 70 - 75℃; for 2h;
5-iodoanthranilonitrile
132131-24-9

5-iodoanthranilonitrile

N,N-dimethyl-formamide dimethyl acetal
4637-24-5

N,N-dimethyl-formamide dimethyl acetal

(E)-N'-(2-cyano-4-iodophenyl)-N,N-dimethylformamidine

(E)-N'-(2-cyano-4-iodophenyl)-N,N-dimethylformamidine

Conditions
ConditionsYield
at 120℃; for 2h;100%
at 90℃; for 1h;98%
at 90℃; for 1h;1.2 g
5-iodoanthranilonitrile
132131-24-9

5-iodoanthranilonitrile

N,N-dimethyl-formamide dimethyl acetal
4637-24-5

N,N-dimethyl-formamide dimethyl acetal

N’-(2-cyano-4-iodophenyl)-N,N-dimethyl formamidine
903597-10-4

N’-(2-cyano-4-iodophenyl)-N,N-dimethyl formamidine

Conditions
ConditionsYield
at 120℃; for 2h;100%
at 120℃; for 2h;100%
With acetic acid In toluene at 35℃; for 0.5h;89.3%
With acetic acid at 35℃; for 0.5h;89.3%
With acetic acid In toluene at 35℃; for 0.5h;89.3%
ortho-bromophenylacetic acid
18698-97-0

ortho-bromophenylacetic acid

5-iodoanthranilonitrile
132131-24-9

5-iodoanthranilonitrile

2-(2-bromophenyl)-N-(2-cyano-4-iodophenyl)acetamide

2-(2-bromophenyl)-N-(2-cyano-4-iodophenyl)acetamide

Conditions
ConditionsYield
Stage #1: ortho-bromophenylacetic acid With thionyl chloride In dichloromethane for 4h; Reflux;
Stage #2: 5-iodoanthranilonitrile In toluene for 16h; Reflux;
99%
5-formylfurane-2-boronic acid
27329-70-0

5-formylfurane-2-boronic acid

5-iodoanthranilonitrile
132131-24-9

5-iodoanthranilonitrile

2-amino-5-[(5-formyl)furan-2-yl]benzonitrile

2-amino-5-[(5-formyl)furan-2-yl]benzonitrile

Conditions
ConditionsYield
With palladium 10% on activated carbon; triethylamine In methanol; 1,2-dimethoxyethane at 20 - 45℃; for 3h; Suzuki Coupling;98.6%
5-formylfurane-2-boronic acid
27329-70-0

5-formylfurane-2-boronic acid

toluene-4-sulfonic acid
104-15-4

toluene-4-sulfonic acid

5-iodoanthranilonitrile
132131-24-9

5-iodoanthranilonitrile

2-amino-5-[(5-formyl)furan-2-yl]benzonitrile p-toluenesulfonic acid

2-amino-5-[(5-formyl)furan-2-yl]benzonitrile p-toluenesulfonic acid

Conditions
ConditionsYield
Stage #1: 5-formylfurane-2-boronic acid; 5-iodoanthranilonitrile With palladium 10% on activated carbon; triethylamine In methanol; 1,2-dimethoxyethane at 20 - 45℃; for 3h;
Stage #2: toluene-4-sulfonic acid In water at 60℃;
96%
(E)-N'-(3-chloro-4-((3-fluorobenzyl)oxy)phenyl)-N-(3-chloro-4-((3-fluorobenzyl)oxy)phenyl)formamidine

(E)-N'-(3-chloro-4-((3-fluorobenzyl)oxy)phenyl)-N-(3-chloro-4-((3-fluorobenzyl)oxy)phenyl)formamidine

5-iodoanthranilonitrile
132131-24-9

5-iodoanthranilonitrile

N-(3-chloro-4-(3-fluorobenzyloxy)phenyl)-6-iodoquinazolin-4-amine
231278-20-9

N-(3-chloro-4-(3-fluorobenzyloxy)phenyl)-6-iodoquinazolin-4-amine

Conditions
ConditionsYield
With toluene-4-sulfonic acid In toluene at 110℃; for 5h;92.2%
cyclohexanone
108-94-1

cyclohexanone

5-iodoanthranilonitrile
132131-24-9

5-iodoanthranilonitrile

9-amino-7-iodo-1,2,3,4-tetrahydroacridine
252357-65-6

9-amino-7-iodo-1,2,3,4-tetrahydroacridine

Conditions
ConditionsYield
Stage #1: cyclohexanone; 5-iodoanthranilonitrile With zinc(II) chloride at 145 - 150℃; for 0.5h; Condensation;
Stage #2: With sodium hydroxide In water at 60℃; for 1h; Hydrolysis;
91%
With sodium hydroxide; zinc(II) chloride Multistep reaction;
Stage #1: cyclohexanone; 5-iodoanthranilonitrile With zinc(II) chloride at 140℃; Condensation;
Stage #2: With sodium hydroxide Addition;
guanidine hydrochloride
50-01-1

guanidine hydrochloride

5-iodoanthranilonitrile
132131-24-9

5-iodoanthranilonitrile

2,4-diamino-6-iodoquinazoline
132131-20-5

2,4-diamino-6-iodoquinazoline

Conditions
ConditionsYield
With sodium ethanolate In ethanol at 80 - 150℃; for 26h;90%
(methoxymethylidene)dimethylammonium methyl sulfate
21511-55-7, 34643-89-5

(methoxymethylidene)dimethylammonium methyl sulfate

5-iodoanthranilonitrile
132131-24-9

5-iodoanthranilonitrile

N’-(2-cyano-4-iodophenyl)-N,N-dimethyl formamidine
903597-10-4

N’-(2-cyano-4-iodophenyl)-N,N-dimethyl formamidine

Conditions
ConditionsYield
With sodium methylate In toluene at 20℃; for 9h;86.9%
5-iodoanthranilonitrile
132131-24-9

5-iodoanthranilonitrile

N,N-dimethyl-formamide
68-12-2, 33513-42-7

N,N-dimethyl-formamide

6-Iodo-1H-quinazoline-2,4-dione
16353-27-8

6-Iodo-1H-quinazoline-2,4-dione

Conditions
ConditionsYield
With zinc(II) chloride at 200℃; for 5h; sealed tube;80%
acetic anhydride
108-24-7

acetic anhydride

5-iodoanthranilonitrile
132131-24-9

5-iodoanthranilonitrile

2-cyano-4-iodoacetanilide

2-cyano-4-iodoacetanilide

Conditions
ConditionsYield
In acetic acid Heating;79%
5-iodoanthranilonitrile
132131-24-9

5-iodoanthranilonitrile

2-cyano-4-iodobenzenediazonium tetrafluoroborate

2-cyano-4-iodobenzenediazonium tetrafluoroborate

Conditions
ConditionsYield
With tert.-butylnitrite; boron trifluoride diethyl etherate In tetrahydrofuran at -20 - 5℃; for 0.5h;77%
5-iodoanthranilonitrile
132131-24-9

5-iodoanthranilonitrile

4-bromo-benzaldehyde
1122-91-4

4-bromo-benzaldehyde

phenylboronic acid
98-80-6

phenylboronic acid

2-(4-bromophenyl)-6-iodo-4-phenylquinazoline

2-(4-bromophenyl)-6-iodo-4-phenylquinazoline

Conditions
ConditionsYield
With potassium fluoride; 5,5'-dimethyl-2,2'-bipyridine; bis(acetylacetonato)palladium(II); trifluorormethanesulfonic acid In N,N-dimethyl-formamide at 80℃; for 48h; Sealed tube; Schlenk technique;76%
(E)-N'-(1-(3-fluorobenzyl)-1H-indol-5-yl)-N,N-dimethylformamide

(E)-N'-(1-(3-fluorobenzyl)-1H-indol-5-yl)-N,N-dimethylformamide

5-iodoanthranilonitrile
132131-24-9

5-iodoanthranilonitrile

N-(1-(3-fluorobenzyl)-1H-indazol-5-yl)-6-iodoquinazolin-4-amine
231278-79-8

N-(1-(3-fluorobenzyl)-1H-indazol-5-yl)-6-iodoquinazolin-4-amine

Conditions
ConditionsYield
With acetic acid In 5,5-dimethyl-1,3-cyclohexadiene for 10h; Reflux;75.63%
4-fluoroboronic acid
1765-93-1

4-fluoroboronic acid

benzaldehyde
100-52-7

benzaldehyde

5-iodoanthranilonitrile
132131-24-9

5-iodoanthranilonitrile

4-(4-fluorophenyl)-6-iodo-2-phenylquinazoline

4-(4-fluorophenyl)-6-iodo-2-phenylquinazoline

Conditions
ConditionsYield
With potassium fluoride; 5,5'-dimethyl-2,2'-bipyridine; bis(acetylacetonato)palladium(II); trifluorormethanesulfonic acid In N,N-dimethyl-formamide at 80℃; for 48h; Sealed tube; Schlenk technique;72%
5-iodoanthranilonitrile
132131-24-9

5-iodoanthranilonitrile

bis(pinacol)diborane
73183-34-3

bis(pinacol)diborane

2‐amino‐5‐(4,4,5,5‐tetramethyl‐1,3,2‐dioxaborolan‐2‐yl)benzonitrile
934426-22-9

2‐amino‐5‐(4,4,5,5‐tetramethyl‐1,3,2‐dioxaborolan‐2‐yl)benzonitrile

Conditions
ConditionsYield
With potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride In N,N-dimethyl-formamide at 80℃; for 4h;69%
With potassium acetate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2 In N,N-dimethyl-formamide at 80℃; for 4h;69%
benzaldehyde
100-52-7

benzaldehyde

5-iodoanthranilonitrile
132131-24-9

5-iodoanthranilonitrile

phenylboronic acid
98-80-6

phenylboronic acid

6-iodo-2,4-diphenylquinazoline

6-iodo-2,4-diphenylquinazoline

Conditions
ConditionsYield
With potassium fluoride; 5,5'-dimethyl-2,2'-bipyridine; bis(acetylacetonato)palladium(II); trifluorormethanesulfonic acid In N,N-dimethyl-formamide at 80℃; for 48h; Sealed tube; Schlenk technique;68%
4-methyl-benzaldehyde
104-87-0

4-methyl-benzaldehyde

5-iodoanthranilonitrile
132131-24-9

5-iodoanthranilonitrile

phenylboronic acid
98-80-6

phenylboronic acid

6-iodo-4-phenyl-2-(p-tolyl)quinazoline

6-iodo-4-phenyl-2-(p-tolyl)quinazoline

Conditions
ConditionsYield
With potassium fluoride; 5,5'-dimethyl-2,2'-bipyridine; bis(acetylacetonato)palladium(II); trifluorormethanesulfonic acid In N,N-dimethyl-formamide at 80℃; for 48h; Sealed tube; Schlenk technique;67%
2-(methoxycarbonyl)benzenediazonium tetrafluoroborate
342-54-1

2-(methoxycarbonyl)benzenediazonium tetrafluoroborate

5-iodoanthranilonitrile
132131-24-9

5-iodoanthranilonitrile

acetonitrile
75-05-8

acetonitrile

10-iodo-6-methyl-13H-quinazolino[3,4-a]quinazolin-13-one

10-iodo-6-methyl-13H-quinazolino[3,4-a]quinazolin-13-one

Conditions
ConditionsYield
at 80℃; for 5h; Sealed tube;66%
7-(PHENYLSULFONYL)-1H-INDOLE-2-CARBOXYLIC acid
666859-79-6

7-(PHENYLSULFONYL)-1H-INDOLE-2-CARBOXYLIC acid

5-iodoanthranilonitrile
132131-24-9

5-iodoanthranilonitrile

N-(2-CYANO-4-IODOPHENYL)-7-(PHENYLSULFONYL)-1H-INDOLE-2-carboxamide

N-(2-CYANO-4-IODOPHENYL)-7-(PHENYLSULFONYL)-1H-INDOLE-2-carboxamide

Conditions
ConditionsYield
Stage #1: 7-(PHENYLSULFONYL)-1H-INDOLE-2-CARBOXYLIC acid With oxalyl dichloride In DMF (N,N-dimethyl-formamide); dichloromethane at 20℃; for 3h;
Stage #2: 5-iodoanthranilonitrile In pyridine; dichloromethane at 20℃;
65%
4-Chlorophenylboronic acid
1679-18-1

4-Chlorophenylboronic acid

benzaldehyde
100-52-7

benzaldehyde

5-iodoanthranilonitrile
132131-24-9

5-iodoanthranilonitrile

4-(4-chlorophenyl)-6-iodo-2-phenylquinazoline

4-(4-chlorophenyl)-6-iodo-2-phenylquinazoline

Conditions
ConditionsYield
With potassium fluoride; 5,5'-dimethyl-2,2'-bipyridine; bis(acetylacetonato)palladium(II); trifluorormethanesulfonic acid In N,N-dimethyl-formamide at 80℃; for 48h; Sealed tube; Schlenk technique;65%
5-iodoanthranilonitrile
132131-24-9

5-iodoanthranilonitrile

2-naphthylmethylzinc chloride

2-naphthylmethylzinc chloride

2-amino-5-(2'-naphthylmethyl)benzonitrile
378791-67-4

2-amino-5-(2'-naphthylmethyl)benzonitrile

Conditions
ConditionsYield
dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2 In tetrahydrofuran for 0.5h; Heating;63%
5-iodoanthranilonitrile
132131-24-9

5-iodoanthranilonitrile

(2-chlorobenzyl)zinc(II) chloride
312624-11-6

(2-chlorobenzyl)zinc(II) chloride

2-amino-5-(2'-chlorobenzyl)benzonitrile
378791-55-0

2-amino-5-(2'-chlorobenzyl)benzonitrile

Conditions
ConditionsYield
dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2 In tetrahydrofuran for 0.5h; Heating;62%
5-iodoanthranilonitrile
132131-24-9

5-iodoanthranilonitrile

(2-methoxybenzyl)zinc(II) chloride
312693-15-5

(2-methoxybenzyl)zinc(II) chloride

2-amino-5-(2'-methoxybenzyl)benzonitrile
378791-60-7

2-amino-5-(2'-methoxybenzyl)benzonitrile

Conditions
ConditionsYield
dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2 In tetrahydrofuran for 0.5h; Heating;61%
4-methylphenylboronic acid
5720-05-8

4-methylphenylboronic acid

benzaldehyde
100-52-7

benzaldehyde

5-iodoanthranilonitrile
132131-24-9

5-iodoanthranilonitrile

6-iodo-2-phenyl-4-(p-tolyl)quinazoline

6-iodo-2-phenyl-4-(p-tolyl)quinazoline

Conditions
ConditionsYield
With potassium fluoride; 5,5'-dimethyl-2,2'-bipyridine; bis(acetylacetonato)palladium(II); trifluorormethanesulfonic acid In N,N-dimethyl-formamide at 80℃; for 48h; Sealed tube; Schlenk technique;61%
5-iodoanthranilonitrile
132131-24-9

5-iodoanthranilonitrile

(4-chlorobenzyl)zinc(II) chloride

(4-chlorobenzyl)zinc(II) chloride

2-amino-5-(4'-chlorobenzyl)benzonitrile

2-amino-5-(4'-chlorobenzyl)benzonitrile

Conditions
ConditionsYield
dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2 In tetrahydrofuran for 0.5h; Heating;59%
5-iodoanthranilonitrile
132131-24-9

5-iodoanthranilonitrile

3,5-dimethoxybenzylzinc chloride

3,5-dimethoxybenzylzinc chloride

2-amino-5-(3',5'-dimethoxybenzyl)benzonitrile

2-amino-5-(3',5'-dimethoxybenzyl)benzonitrile

Conditions
ConditionsYield
dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2 In tetrahydrofuran for 0.5h; Heating;59%

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