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Hangzhou JINLAN Pharm-Drugs Technology Co., Ltd

Jinlan Pharm-Drugs Technology Co.,Limited (with its export company Hangzhou Royall Import & Export Co.,Ltd.)is located in Hangzhou, Zhejiang Province. Neighboring Ningbo port, Shanghai port, Hangzhou Xiaoshan Int’l Airport and Shanghai Pu

13290-96-5/Dimethyl 5-nitroisophthalate

Cas:13290-96-5

Min.Order:1 Gram

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Type:Manufacturers

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Zhejiang Haizhou Pharmaceutical Co., Ltd.

Specifciaiton: In-house; Certification: ISO 9001; US FDA and EDQM Approved Plant; Appearance:White Storage:Preserve in tight containers Application:Contrast agent Port:Shanghai, Ningbo, etc.

Dimethyl 5-nitroisophthalate

Cas:13290-96-5

Min.Order:50 Gram

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Type:Trading Company

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Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality Dimethyl5-Nitroisophthalate supplier in China

Cas:13290-96-5

Min.Order:1 Metric Ton

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Jinan Finer Chemical Co., Ltd

Product informations Product Name Dimethyl 5-nitroisophthalate CAS No. 13290-96-5 Appearance White crystalline powder Assay ≥99%

Dimethyl 5-nitroisophthalate

Cas:13290-96-5

Min.Order:1 Gram

FOB Price: $8.0

Type:Lab/Research institutions

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply Dimethyl 5-nitroisophthalate

Cas:13290-96-5

Min.Order:1

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Type:Other

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COLORCOM LTD.

Colorcom is a global leader in industrial chemical manufacturing and is continuously innovating and transforming to exceed client expectations and industry standards. Colorcom prides itself on superior customer and technical focus, while focusing on

Dimethyl 5-Nitroisophthalate

Cas:13290-96-5

Min.Order:1 Metric Ton

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Type:Manufacturers

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Dayang Chem (Hangzhou) Co.,Ltd.

DayangChem exported this product to many countries and regions at best price in China. If you are looking for the product’s supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product specifica

Dimethyl 5-nitroisophthalate

Cas:13290-96-5

Min.Order:1 Kilogram

FOB Price: $2.0

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Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

5-Nitroisophthalic acid dimethyl ester

Cas:13290-96-5

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

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Hubei DiBo chemical co., LTD

Name:Dimethyl 5-nitroisophthalate CAS NO: 13290-96-5 Grade:Medical scientific research and export Molecular formula:C10H9NO6 Molecular weight:239.18 Product Quality 12 years of chemical raw materials Mature operation of the industry System

Dimethyl 5-nitroisophthalate/cas:13290-96-5/Raw material spot

Cas:13290-96-5

Min.Order:25 Kilogram

FOB Price: $1.0 / 2.0

Type:Other

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Henan Tianfu Chemical Co., Ltd.

Our company engages in Sodium Tripolyphosphate (STPP) and Sodium Hexametabphosphate (SHMP) production; development of noble metal catalysts, synthesis of electronic chemical materials and general chemicals Imp&Exp trading business. The company

TIANFU-CHEM - Dimethyl 5-nitroisophthalate

Cas:13290-96-5

Min.Order:1 Kilogram

FOB Price: $1000.0

Type:Lab/Research institutions

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Leader Biochemical Group

About Product Details Item Specification Test Results Appearance White crystalline powder Conform

China Biggest factory Supply High Quality Dimethyl 5-nitroisophthalate 13290-96-5

Cas:13290-96-5

Min.Order:1 Kilogram

FOB Price: $1.0 / 5.0

Type:Lab/Research institutions

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Hebei Nengqian Chemical Import and Export Co., LTD

Our advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva

Dimethyl 5-nitroisophthalate

Cas:13290-96-5

Min.Order:1 Kilogram

FOB Price: $9.0 / 99.0

Type:Trading Company

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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Top Purity CAS 13290-96-5 with fast shipping

Cas:13290-96-5

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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Wuhan Han Sheng New Material Technology Co.,Ltd

Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We

Low Price Dimethyl 5-Nitroisophthalate CAS 13290-96-5 in Stock

Cas:13290-96-5

Min.Order:10 Kilogram

Negotiable

Type:Trading Company

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LIDE PHARMACEUTICALS LIMITED

Advantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&amp

Dimethyl 5-nitroisophthalate/ LIDE PHARMA- Factory supply / Best price

Cas:13290-96-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Henan Sinotech Import&Export Corporation

Alias: 5-Nitro Isophthalic acid dimethyl ester; Dimethyl 5-nitrobenzene-1,3-dicarboxylate; 5-Nitroisophthalic acid dimethyl ester; Dimethyl 5-Nitrophthalate; Dimethyl 5-nitroisophthalate; 5-NIPA DME; 2,4-dimethyl-5-nitrobenzene-1,3-dicarboxylate;

Dimethyl 5-nitroisophthalate

Cas:13290-96-5

Min.Order:5 Metric Ton

FOB Price: $1.0 / 2.0

Type:Other

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Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

Dimethyl 5-nitroisophthalate 13290-96-5

Cas:13290-96-5

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Qingdao Beluga Import and Export Co., LTD

Dimethyl 5-nitroisophthalate CAS:13290-96-5 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality orga

Dimethyl 5-nitroisophthalate CAS:13290-96-5

Cas:13290-96-5

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

Dimethyl 5-nitroisophthalate

Cas:13290-96-5

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

Dimethyl 5-nitroisophthalate

Cas:13290-96-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Xiamen Hisunny Chemical Co.,Ltd

Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia

Dimethyl 5-nitroisophthalate

Cas:13290-96-5

Min.Order:0

Negotiable

Type:Manufacturers

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Taixing Joxin Bio-tec Co.,Ltd.

CAS-No. 13290-96-5 Molecular Formula: C10H9NO6 Molecular Weight:239.19 SYNONYMS Dimethyl 5-nitrobenzene-1,3-dicarboxylate; 5-Nitroisophthalic acid dimethyl ester;

Dimethyl 5-nitroisophthalate

Cas:13290-96-5

Min.Order:0 Metric Ton

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Type:Lab/Research institutions

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Zhengzhou Yuanli Biological Technology Co., Ltd.

Advantages: 1. owerful R & D team; 2. Mature technical support 3.Best quality in your requirement 4. Competitive price in china market . 5. The ability of quantized production,from grams to tons; 6. Efficient and safe logistic plans for c

High purtiy Dimethyl 5-nitroisophthalate ; In stock

Cas:13290-96-5

Min.Order:1 Gram

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Type:Lab/Research institutions

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Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

Dimethyl 5-nitroisophthalate

Cas:13290-96-5

Min.Order:0 Metric Ton

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Type:Lab/Research institutions

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Afine Chemicals Limited

Company Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments

5-NITROBENZENE-1,3-DICARBOXYLIC ACID

Cas:13290-96-5

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

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Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

Dimethyl 5-nitroisophthalate

Cas:13290-96-5

Min.Order:0

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Type:Lab/Research institutions

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Shaanxi Cuicheng Biomedical Technology Co., Ltd.

Why Choose Us: 1. Factory direct sales, so we can provide the competitive price and high quality product base on 8 years of production and R&D experience. 2. It is available in stock for quick shipment.Products could be packaged according to cu

Dimethyl 5-nitroisophthalate

Cas:13290-96-5

Min.Order:1 Gram

Negotiable

Type:Other

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Chemlyte Solutions

Chemlyte Solutions believe that customers and suppliers deserve much more than what traditional distributors can offer. To grow in today s fast-paced and increasingly competitive market it is essential to be able to quickly adapt to market forces eff

Featured products 5-Nitroisophthalic acid dimethyl ester

Cas:13290-96-5

Min.Order:100 Gram

Negotiable

Type:Other

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Shanghai Massive Chemical Technology Co., Ltd.

Massive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and

Dimethyl 5-nitroisophthalate/Manufacturer/High quality/Best price

Cas:13290-96-5

Min.Order:1 Gram

FOB Price: $1.0

Type:Lab/Research institutions

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Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

High quality Dimethyl5-Nitroisophthalate

Cas:13290-96-5

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

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Synthetic route

methanol
67-56-1

methanol

5-nitrobenzene-1,3-dicarboxylic acid
618-88-2

5-nitrobenzene-1,3-dicarboxylic acid

dimethyl 5-nitroisophthalate
13290-96-5

dimethyl 5-nitroisophthalate

Conditions
ConditionsYield
With sulfuric acid for 3h; Inert atmosphere; Reflux;98%
With hydrogenchloride
dimethyl Isophthalate
1459-93-4

dimethyl Isophthalate

dimethyl 5-nitroisophthalate
13290-96-5

dimethyl 5-nitroisophthalate

Conditions
ConditionsYield
With iron(III) chloride; Nitrogen dioxide; ozone In 1,2-dichloro-ethane at 5℃; for 1.5h; Product distribution; Further Variations:; Solvents; Reagents;92%
With sulfur dioxide; dinitrogen pentoxide 1.) -78 to -11 deg C, 2 h, 2.) -11 deg C, 2 h;90%
With sulfuric acid; sulfur trioxide; nitric acid
5-nitrobenzene-1,3-dicarboxylic acid
618-88-2

5-nitrobenzene-1,3-dicarboxylic acid

dimethyl 5-nitroisophthalate
13290-96-5

dimethyl 5-nitroisophthalate

Conditions
ConditionsYield
With thionyl chloride In methanol at 0 - 80℃; for 6h; Inert atmosphere;90%
With hydrogenchloride
With sulfuric acid In methanol; water; toluene
5-nitro-1,3-benzenedicarbonylchloride
13438-30-7

5-nitro-1,3-benzenedicarbonylchloride

dimethyl 5-nitroisophthalate
13290-96-5

dimethyl 5-nitroisophthalate

Conditions
ConditionsYield
In methanol
dimethyl 5-aminoisophthalate
99-27-4

dimethyl 5-aminoisophthalate

dimethyl 5-nitroisophthalate
13290-96-5

dimethyl 5-nitroisophthalate

Conditions
ConditionsYield
With oxone In dichloromethane; water for 6h; Inert atmosphere;
dimethyl 5-nitroisophthalate
13290-96-5

dimethyl 5-nitroisophthalate

serinol
534-03-2

serinol

N,N'-bis-(2-hydroxy-1-hydroxymethylethyl)-5-nitroisophthalamide
60166-97-4

N,N'-bis-(2-hydroxy-1-hydroxymethylethyl)-5-nitroisophthalamide

Conditions
ConditionsYield
In methanol at 20℃; for 48h; Reflux;99%
dimethyl 5-nitroisophthalate
13290-96-5

dimethyl 5-nitroisophthalate

ethylenediamine
107-15-3

ethylenediamine

N,N'-bis-(2-amino-ethyl)-5-nitro-isophthalamide

N,N'-bis-(2-amino-ethyl)-5-nitro-isophthalamide

Conditions
ConditionsYield
at 0℃; for 24h;96.8%
dimethyl 5-nitroisophthalate
13290-96-5

dimethyl 5-nitroisophthalate

dimethyl 5-aminoisophthalate
99-27-4

dimethyl 5-aminoisophthalate

Conditions
ConditionsYield
With formic acid; triethylamine chemoselective reaction;95%
With ammonium sulfide
With hydrogenchloride; methanol; zinc
dimethyl 5-nitroisophthalate
13290-96-5

dimethyl 5-nitroisophthalate

ethanolamine
141-43-5

ethanolamine

N,N’-bis(2-hydroxyethyl)-5-nitroisophthaldiamide
88116-47-6

N,N’-bis(2-hydroxyethyl)-5-nitroisophthaldiamide

Conditions
ConditionsYield
In methanol at 70 - 75℃; for 70h;94%
dimethyl 5-nitroisophthalate
13290-96-5

dimethyl 5-nitroisophthalate

propan-1-ol-3-amine
156-87-6

propan-1-ol-3-amine

N,N’-bis(3-hydroxypropyl)-5-nitroisophthalamide

N,N’-bis(3-hydroxypropyl)-5-nitroisophthalamide

Conditions
ConditionsYield
In methanol at 70 - 75℃; for 70h;92%
3-Amino-1,2-propanediol
616-30-8, 13552-31-3

3-Amino-1,2-propanediol

dimethyl 5-nitroisophthalate
13290-96-5

dimethyl 5-nitroisophthalate

5-nitro-N,N'-bis-(2,3-dihydroxypropyl)isophthalamide
76820-34-3

5-nitro-N,N'-bis-(2,3-dihydroxypropyl)isophthalamide

Conditions
ConditionsYield
In methanol at 70 - 75℃; for 70h;91%
In methanol85%
With sodium methylate In methanol for 80h;
With sodium methylate In methanol at 25 - 30℃; for 2h; Temperature; Solvent;
With sodium methylate In methanol at 20 - 50℃;
dimethyl 5-nitroisophthalate
13290-96-5

dimethyl 5-nitroisophthalate

dimethyl 5-(N,N-dimethylamino)isophthalate
2718-64-1

dimethyl 5-(N,N-dimethylamino)isophthalate

Conditions
ConditionsYield
With formaldehyd; hydrogen; propionic acid; aluminum nickel In methanol85%
formaldehyd
50-00-0

formaldehyd

dimethyl 5-nitroisophthalate
13290-96-5

dimethyl 5-nitroisophthalate

dimethyl 5-(N,N-dimethylamino)isophthalate
2718-64-1

dimethyl 5-(N,N-dimethylamino)isophthalate

Conditions
ConditionsYield
With formic acid; triethylamine In water; tert-butyl alcohol at 100℃; for 44h;82%
dimethyl 5-nitroisophthalate
13290-96-5

dimethyl 5-nitroisophthalate

serinol
534-03-2

serinol

C12H14N2O7

C12H14N2O7

Conditions
ConditionsYield
In methanol at 20 - 65℃; for 24h; Time;75.3%
dimethyl 5-nitroisophthalate
13290-96-5

dimethyl 5-nitroisophthalate

5-nitro-1,3-benzenedicarboxylic acid, monomethyl ester
1955-46-0

5-nitro-1,3-benzenedicarboxylic acid, monomethyl ester

Conditions
ConditionsYield
With water; sodium hydroxide In methanol for 2h; Reflux;75%
3-Amino-1,2-propanediol
616-30-8, 13552-31-3

3-Amino-1,2-propanediol

dimethyl 5-nitroisophthalate
13290-96-5

dimethyl 5-nitroisophthalate

methyl 3-((2,3-dihydroxypropyl)carbamoyl)-5-nitrobenzoate

methyl 3-((2,3-dihydroxypropyl)carbamoyl)-5-nitrobenzoate

Conditions
ConditionsYield
In methanol at 20 - 65℃; for 24.5h;56%
dimethyl 5-nitroisophthalate
13290-96-5

dimethyl 5-nitroisophthalate

3-hydroxymethyl-5-nitrobenzoic acid methyl ester
53732-08-4

3-hydroxymethyl-5-nitrobenzoic acid methyl ester

Conditions
ConditionsYield
With diisobutylaluminium hydride In tetrahydrofuran; toluene at -78 - 20℃;50%
dimethyl 5-nitroisophthalate
13290-96-5

dimethyl 5-nitroisophthalate

5-nitrobenzene-1,3-dicarbaldehyde
36308-36-8

5-nitrobenzene-1,3-dicarbaldehyde

Conditions
ConditionsYield
With diisobutylaluminium hydride In toluene at -78℃; for 1h; Inert atmosphere;48%
dimethyl 5-nitroisophthalate
13290-96-5

dimethyl 5-nitroisophthalate

tetra-methyl 3,3’,5,5’-azobenzenetetracarboxylate

tetra-methyl 3,3’,5,5’-azobenzenetetracarboxylate

Conditions
ConditionsYield
With lead; ammonium acetate In methanol at 20℃; for 24.25h; Inert atmosphere;34%
dimethyl 5-nitroisophthalate
13290-96-5

dimethyl 5-nitroisophthalate

A

dimethyl 5-aminoisophthalate
99-27-4

dimethyl 5-aminoisophthalate

B

5-hydroxyamino-isophthalic acid dimethyl ester

5-hydroxyamino-isophthalic acid dimethyl ester

Conditions
ConditionsYield
With ethanol; hydrogen sulfide; ammonia
dimethyl 5-nitroisophthalate
13290-96-5

dimethyl 5-nitroisophthalate

5-nitro-isophthalic acid dihydrazide
98488-89-2

5-nitro-isophthalic acid dihydrazide

Conditions
ConditionsYield
With hydrazine hydrate
dimethyl 5-nitroisophthalate
13290-96-5

dimethyl 5-nitroisophthalate

5-hydroxyamino-isophthalic acid dimethyl ester

5-hydroxyamino-isophthalic acid dimethyl ester

Conditions
ConditionsYield
With hydrazine; Rh on carbon In tetrahydrofuran Catalytic hydrogenation;
dimethyl 5-nitroisophthalate
13290-96-5

dimethyl 5-nitroisophthalate

1-amino-naphthalene
134-32-7

1-amino-naphthalene

petroleum ether

petroleum ether

compound C10H9N+C10H9O6N

compound C10H9N+C10H9O6N

dimethyl 5-nitroisophthalate
13290-96-5

dimethyl 5-nitroisophthalate

acetone
67-64-1

acetone

potassium 1-acetonyl-2,4-di(methoxycarbonyl)-6-nitrocyclohexa-2,5-dienide

potassium 1-acetonyl-2,4-di(methoxycarbonyl)-6-nitrocyclohexa-2,5-dienide

Conditions
ConditionsYield
With potassium hydroxide In dimethylsulfoxide-d6 at 25℃; for 4h; Yanovsky reaction;
dimethyl 5-nitroisophthalate
13290-96-5

dimethyl 5-nitroisophthalate

acetone
67-64-1

acetone

A

potassium 1-acetonyl-2,4-di(methoxycarbonyl)-6-nitrocyclohexa-2,5-dienide

potassium 1-acetonyl-2,4-di(methoxycarbonyl)-6-nitrocyclohexa-2,5-dienide

B

potassium 1-acetonyl-2,6-di(methoxycarbonyl)-4-nitrocyclohexa-2,5-dienide

potassium 1-acetonyl-2,6-di(methoxycarbonyl)-4-nitrocyclohexa-2,5-dienide

Conditions
ConditionsYield
With potassium methanolate In methanol at 25℃; Yanovsky reaction; Title compound not separated from byproducts;
dimethyl 5-nitroisophthalate
13290-96-5

dimethyl 5-nitroisophthalate

C14H19N3O8
1056157-89-1

C14H19N3O8

dimethyl 5-nitroisophthalate
13290-96-5

dimethyl 5-nitroisophthalate

[(2-{3-[2-(bis-carboxymethyl-amino)-ethylcarbamoyl]-5-nitro-benzoylamino}-ethyl)-carboxymethyl-amino]-acetic acid
925416-16-6

[(2-{3-[2-(bis-carboxymethyl-amino)-ethylcarbamoyl]-5-nitro-benzoylamino}-ethyl)-carboxymethyl-amino]-acetic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 96.8 percent / 24 h / 0 °C
2: 89 percent / NaOH / H2O / 20 - 70 °C / pH 5 - 10
View Scheme
dimethyl 5-nitroisophthalate
13290-96-5

dimethyl 5-nitroisophthalate

3-azidomethyl-5-nitrobenzoic acid methyl ester
167215-64-7

3-azidomethyl-5-nitrobenzoic acid methyl ester

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 50 percent / diisobutylaluminum hydride / tetrahydrofuran; toluene / -78 - 20 °C
2: 95 percent / triethylamine / CH2Cl2 / 0.5 h / 0 °C
3: 100 percent / sodium azide / dimethylformamide / 2 h / 50 °C
View Scheme
dimethyl 5-nitroisophthalate
13290-96-5

dimethyl 5-nitroisophthalate

3-[(tert-butyloxycarbonyl)aminomethyl]-5-nitrobenzoic acid methyl ester
913077-69-7

3-[(tert-butyloxycarbonyl)aminomethyl]-5-nitrobenzoic acid methyl ester

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: 50 percent / diisobutylaluminum hydride / tetrahydrofuran; toluene / -78 - 20 °C
2: 95 percent / triethylamine / CH2Cl2 / 0.5 h / 0 °C
3: 100 percent / sodium azide / dimethylformamide / 2 h / 50 °C
4: 85 percent / triethylamine; 1,3-propanedithiol / methanol / 12 h / 20 °C
5: 100 percent / triethylamine / tetrahydrofuran / 12 h / 0 °C
View Scheme
dimethyl 5-nitroisophthalate
13290-96-5

dimethyl 5-nitroisophthalate

3-[(tert-butyloxycarbonyl)aminomethyl]-5-nitrobenzoic acid
209604-83-1

3-[(tert-butyloxycarbonyl)aminomethyl]-5-nitrobenzoic acid

Conditions
ConditionsYield
Multi-step reaction with 6 steps
1: 50 percent / diisobutylaluminum hydride / tetrahydrofuran; toluene / -78 - 20 °C
2: 95 percent / triethylamine / CH2Cl2 / 0.5 h / 0 °C
3: 100 percent / sodium azide / dimethylformamide / 2 h / 50 °C
4: 85 percent / triethylamine; 1,3-propanedithiol / methanol / 12 h / 20 °C
5: 100 percent / triethylamine / tetrahydrofuran / 12 h / 0 °C
6: 100 percent / NaOH / H2O; dioxane
View Scheme
dimethyl 5-nitroisophthalate
13290-96-5

dimethyl 5-nitroisophthalate

{3-amino-5-[(5-dimethylamino-naphthalene-1-sulfonylamino)-methyl]-benzoylamino}-thioacetic acid S-ethyl ester

{3-amino-5-[(5-dimethylamino-naphthalene-1-sulfonylamino)-methyl]-benzoylamino}-thioacetic acid S-ethyl ester

Conditions
ConditionsYield
Multi-step reaction with 7 steps
1: 50 percent / diisobutylaluminum hydride / tetrahydrofuran; toluene / -78 - 20 °C
2: 95 percent / triethylamine / CH2Cl2 / 0.5 h / 0 °C
3: 100 percent / sodium azide / dimethylformamide / 2 h / 50 °C
4: 85 percent / triethylamine; 1,3-propanedithiol / methanol / 12 h / 20 °C
5: 100 percent / triethylamine / tetrahydrofuran / 12 h / 0 °C
6: 100 percent / NaOH / H2O; dioxane
View Scheme
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