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inquiryAs a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis according to the contract research and development services for the fine chemicals, ph
ATORVASTATIN SODIUM CAS:134523-01-6 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic inte
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inquiryWe produce carbomer by our own factory,carbomer 940 is our best seller.It is used for cosmetic and medical.And we also become agent for lubrizol.Our carbomer 940 get high viscosity and good transparency.The price will depond on the market,surely supp
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inquiryOur company was built in 2009 with an ISO certificate.In the past 6 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so
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inquiryISO/factory/goodqualityAppearance:off white Storage:Dry,cool place Package:drum Application:active pharmaceutical ingredients Transportation:by air/sea/express Port:shenzhen/shanghai
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inquiry(3R,5R)-7-[2-(4-fluorophenyl)-5-isopropyl-3-phenyl-4-phenylcarbamoylpyrrol-1-yl]-3,5-dihydroxyheptanoic acid t-butyl ester
atorvastatin sodium
Conditions | Yield |
---|---|
With sodium hydroxide; water In 1,4-dioxane; tert-butyl methyl ether for 21h; Product distribution / selectivity; Heating / reflux; | 97.7% |
With methanol; sodium hydroxide; water In tert-butyl methyl ether for 21h; Product distribution / selectivity; Heating / reflux; | 91% |
With sodium hydroxide; water; tert-butyl alcohol In tert-butyl methyl ether for 21h; Product distribution / selectivity; Heating / reflux; | 91% |
ethyl (3R,5R)-7-(2-(4-fluorophenyl)-5-isopropyl-3-phenyl-4-(phenylcarbamoyl)-1H-pyrrol-1-yl)-3,5-dihydroxyheptanoate
atorvastatin sodium
Conditions | Yield |
---|---|
With water; sodium hydroxide at 20℃; for 15h; | 89% |
lipitor
atorvastatin sodium
Conditions | Yield |
---|---|
Stage #1: lipitor With hydrogenchloride In tetrahydrofuran; water at 20℃; Stage #2: With sodium hydroxide In methanol; water Heating / reflux; |
4-fluorobenzaldehyde
atorvastatin sodium
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 2) NEt3 / 1) ethyl thiazolium catalyst / or with methyl thiazolium catalyst; 1) EtOH 2: 75 percent / pivalic acid / toluene; heptane; tetrahydrofuran / Heating 3: aq. HCl / methanol 4: aq. NaOH / methanol View Scheme |
tert-butyl [(4R,6R)-6-aminoethyl-2,2-dimethyl-1,3-dioxan-4-yl]acetate
atorvastatin sodium
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 75 percent / pivalic acid / toluene; heptane; tetrahydrofuran / Heating 2: aq. HCl / methanol 3: aq. NaOH / methanol View Scheme | |
Multi-step reaction with 3 steps 1: Acidic conditions 2: hydrogenchloride; methanol 3: sodium hydroxide / water View Scheme | |
Multi-step reaction with 3 steps 1: Trimethylacetic acid / toluene / 1 h / 105 - 110 °C / Industrial scale 2: hydrogenchloride / methanol; water / 0 - 30 °C / Industrial scale 3: water; sodium hydroxide / methanol / 2.5 h / 0 - 30 °C / Industrial scale View Scheme | |
Multi-step reaction with 3 steps 1: Trimethylacetic acid; diisopropylamine; tetra(n-butyl)ammonium hydrogensulfate / 40 h / 78 - 85 °C 2: hydrogenchloride; water / methanol / 25 - 30 °C 3: water; sodium hydroxide View Scheme |
2-((4R, 6R)-6-cyanomethyl-2,2-dimethyl-1,3-dioxan-4-yl)acetic acid tert-butyl ester
atorvastatin sodium
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 95 percent / H2, ammonia / Molybdenum doped Raney nickel / methanol / 2585.7 Torr 2: 75 percent / pivalic acid / toluene; heptane; tetrahydrofuran / Heating 3: aq. HCl / methanol 4: aq. NaOH / methanol View Scheme | |
Multi-step reaction with 4 steps 1: hydrogen; nickel; ammonia / methanol 2: Acidic conditions 3: hydrogenchloride; methanol 4: sodium hydroxide / water View Scheme | |
Multi-step reaction with 4 steps 1: hydrogen; ammonia / cyclohexane; water / 30 - 40 °C / 3750.38 Torr / Autoclave 2: Trimethylacetic acid; diisopropylamine; tetra(n-butyl)ammonium hydrogensulfate / 40 h / 78 - 85 °C 3: hydrogenchloride; water / methanol / 25 - 30 °C 4: water; sodium hydroxide View Scheme |
2-[2-(4-fluorophenyl)-2-oxo-1-phenylethyl]-4-methyl-3-oxopentanoic acid phenylamide
atorvastatin sodium
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 75 percent / pivalic acid / toluene; heptane; tetrahydrofuran / Heating 2: aq. HCl / methanol 3: aq. NaOH / methanol View Scheme | |
Multi-step reaction with 2 steps 1.1: Trimethylacetic acid / n-heptane / 100 °C 2.1: hydrogenchloride; water / methanol / 25 - 30 °C 2.2: -10 °C View Scheme | |
Multi-step reaction with 3 steps 1: Trimethylacetic acid / toluene / 1 h / 105 - 110 °C / Industrial scale 2: hydrogenchloride / methanol; water / 0 - 30 °C / Industrial scale 3: water; sodium hydroxide / methanol / 2.5 h / 0 - 30 °C / Industrial scale View Scheme |
tert-butyl (4R,6R)-6-{2-[2-(4-fluorophenyl)-5-isopropyl-3-phenyl-4-(phenylcarbamoyl)pyrrol-1-yl]ethyl}-2,2-dimethyl-1,3-dioxane-4-acetate
atorvastatin sodium
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: aq. HCl / methanol 2: aq. NaOH / methanol View Scheme | |
Stage #1: tert-butyl (4R,6R)-6-{2-[2-(4-fluorophenyl)-5-isopropyl-3-phenyl-4-(phenylcarbamoyl)pyrrol-1-yl]ethyl}-2,2-dimethyl-1,3-dioxane-4-acetate With hydroxylamine hydrochloride In methanol; water; acetone at 55 - 65℃; Industry scale; Stage #2: With sodium hydroxide In methanol; water at 35 - 45℃; Product distribution / selectivity; | |
Stage #1: tert-butyl (4R,6R)-6-{2-[2-(4-fluorophenyl)-5-isopropyl-3-phenyl-4-(phenylcarbamoyl)pyrrol-1-yl]ethyl}-2,2-dimethyl-1,3-dioxane-4-acetate With hydrogenchloride; water In tetrahydrofuran at 25℃; for 6.25h; Industry scale; Stage #2: With sodium hydroxide In tetrahydrofuran at 31℃; for 14h; Product distribution / selectivity; Cooling; |
[R(R*,R*)]-2-(4-fluorophenyl)-β,δ-di(tert-butyldimethylsiloxy)-5-(1-methylethyl)-3-phenyl-4-[(pheny)carbonyl]-1H-pyrrole-1-heptanoic acid test-butyl ester
atorvastatin sodium
Conditions | Yield |
---|---|
With sodium hydroxide In methanol; water for 6h; Heating / reflux; |
atorvastatin
atorvastatin sodium
Conditions | Yield |
---|---|
With sodium hydroxide In water; acetonitrile at 20℃; for 144h; | |
With sodium hydroxide In water | |
With sodium hydroxide In water |
atorvastatin sodium
Conditions | Yield |
---|---|
Stage #1: (6-{2-[2-(4-fluoro-phenyl)-5-isopropyl-3-phenyl-4-phenylcarbamoylpyrrolidin-1-yl]-ethyl}-2-phenyl-[1,3,2] dioxaborinan-4-yl)-acetic acid tert-butyl ester In tetrahydrofuran for 0.5h; Stage #2: With sodium hydroxide; water In tetrahydrofuran for 2 - 4h; Product distribution / selectivity; Heating / reflux; |
atorvastatin sodium
Conditions | Yield |
---|---|
With sodium hydroxide In methanol; water; acetone at 60℃; for 0.666667h; pH=12; Product distribution / selectivity; | |
With sodium hydroxide In water; isopropyl alcohol; acetone at 65℃; for 0.75h; pH=11.9; Product distribution / selectivity; |
atorvastatin lactone
(3R,5R)-7-[2-(4-fluorophenyl)-5-isopropyl-3-phenyl-4-phenylcarbamoylpyrrol-1-yl]-3,5-dihydroxyheptanoic acid t-butyl ester
atorvastatin sodium
Conditions | Yield |
---|---|
With sodium hydroxide; water In methanol at 35 - 45℃; for 0.5 - 0.666667h; Product distribution / selectivity; | |
With sodium hydroxide; water In ethanol at 35 - 45℃; for 0.5 - 0.666667h; Product distribution / selectivity; |
tert-butyl 2-((4R,6R)-6-(2-(2-(4-fluorophenyl)-5-isopropyl-3-phenyl-4-(phenylcarbamoyl)-1H-pyrrol-1-yl)ethyl)-2-phenyl-1,3,2-dioxaborinan-4-yl)acetate
atorvastatin sodium
Conditions | Yield |
---|---|
With water; sodium hydroxide In tetrahydrofuran at 20℃; for 3h; | |
With water; sodium hydroxide In tetrahydrofuran at 20℃; for 3h; |
tert-butyl (4S,6S)-6-{2-[2-(4-fluorophenyl)-5-isopropyl-3-phenyl-4-(phenylcarbamoyl)pyrrol-1-yl]ethyl}-2,2-dimethyl-1,3-dioxane-4-acetate
atorvastatin sodium
Conditions | Yield |
---|---|
Stage #1: tert-butyl (4S,6S)-6-{2-[2-(4-fluorophenyl)-5-isopropyl-3-phenyl-4-(phenylcarbamoyl)pyrrol-1-yl]ethyl}-2,2-dimethyl-1,3-dioxane-4-acetate With hydrogenchloride In acetonitrile at 20℃; Stage #2: With sodium hydroxide In water; acetonitrile at 20℃; Stage #3: With hydrogenchloride In water; acetonitrile pH=9.0 - 9.5; Product distribution / selectivity; |
atorvastatin sodium
Conditions | Yield |
---|---|
With sodium hydroxide In methanol; water at 100℃; for 4h; |
cis-t-butyl-7-nitro-3,5-dihydroxy-heptanoate
atorvastatin sodium
Conditions | Yield |
---|---|
Multi-step reaction with 7 steps 1: methanesulfonic acid / tetrahydrofuran / 0 °C 2: hydrogen; ammonia / palladium 10% on activated carbon / water; tetrahydrofuran; methanol / 6 h / 20 °C 3: triethylamine / acetonitrile / 0 - 20 °C / Inert atmosphere 4: triethylamine / dichloromethane / 0 °C / Inert atmosphere 5: acetic anhydride / 5 h / 75 - 80 °C / Inert atmosphere 6: hydrogenchloride; water / methanol / 1.5 h / 20 °C 7: sodium hydroxide; water / methanol / 0 - 20 °C / pH 12 View Scheme |
atorvastatin sodium
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: triethylamine / dichloromethane / 0 °C / Inert atmosphere 2: acetic anhydride / 5 h / 75 - 80 °C / Inert atmosphere 3: hydrogenchloride; water / methanol / 1.5 h / 20 °C 4: sodium hydroxide; water / methanol / 0 - 20 °C / pH 12 View Scheme |
atorvastatin sodium
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: acetic anhydride / 5 h / 75 - 80 °C / Inert atmosphere 2: hydrogenchloride; water / methanol / 1.5 h / 20 °C 3: sodium hydroxide; water / methanol / 0 - 20 °C / pH 12 View Scheme |
atorvastatin sodium
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1: hydrogen; ammonia / palladium 10% on activated carbon / water; tetrahydrofuran; methanol / 6 h / 20 °C 2: triethylamine / acetonitrile / 0 - 20 °C / Inert atmosphere 3: triethylamine / dichloromethane / 0 °C / Inert atmosphere 4: acetic anhydride / 5 h / 75 - 80 °C / Inert atmosphere 5: hydrogenchloride; water / methanol / 1.5 h / 20 °C 6: sodium hydroxide; water / methanol / 0 - 20 °C / pH 12 View Scheme |
atorvastatin sodium
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: triethylamine / acetonitrile / 0 - 20 °C / Inert atmosphere 2: triethylamine / dichloromethane / 0 °C / Inert atmosphere 3: acetic anhydride / 5 h / 75 - 80 °C / Inert atmosphere 4: hydrogenchloride; water / methanol / 1.5 h / 20 °C 5: sodium hydroxide; water / methanol / 0 - 20 °C / pH 12 View Scheme |
atorvastatin sodium
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 24 h / 20 °C 2: benzaldehyde; potassium tert-butylate / tetrahydrofuran / 1.75 h / -5 °C 3: hydrogenchloride / water; methanol; tetrahydrofuran / 3 h / 50 °C 4: sodium hydroxide; water / 15 h / 20 °C View Scheme |
atorvastatin sodium
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: hexane; isopropyl alcohol / 50 - 60 °C 2: hydrogenchloride / water; methanol; tetrahydrofuran / 3 h / 50 °C 3: sodium hydroxide; water / 15 h / 20 °C View Scheme |
atorvastatin sodium
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: benzaldehyde; potassium tert-butylate / tetrahydrofuran / 1.75 h / -5 °C 2: hydrogenchloride / water; methanol; tetrahydrofuran / 3 h / 50 °C 3: sodium hydroxide; water / 15 h / 20 °C View Scheme |
atorvastatin sodium
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: hydrogenchloride / water; methanol; tetrahydrofuran / 3 h / 50 °C 2: sodium hydroxide; water / 15 h / 20 °C View Scheme |
atorvastatin sodium
atorvastatin
Conditions | Yield |
---|---|
With sodium hydroxide at 60 - 70℃; pH=12-13; | 95% |
With hydrogenchloride In dichloromethane; water for 0.5h; Cooling with ice; | 94% |
atorvastatin sodium
lipitor
Conditions | Yield |
---|---|
With calcium acetate In water at 20℃; for 2h; | 93% |
With calcium acetate In methanol; water at 60 - 65℃; for 2h; Industrial scale; | 85.4% |
With calcium acetate In water at 13 - 63℃; |
methanol
atorvastatin sodium
(3R,5R)-methyl 7-(2-(4-fluorophenyl)-5-isopropyl-3-phenyl-4-(phenylcarbamoyl)-1H-pyrrol-1-yl)-3,5-dihydroxyheptanoate
Conditions | Yield |
---|---|
With sulfuric acid at 0 - 20℃; for 2.58333h; | 88% |
atorvastatin sodium
hexan-1-ol
Conditions | Yield |
---|---|
With sulfuric acid In dichloromethane at 0 - 20℃; for 2.58333h; | 70% |
ethanol
atorvastatin sodium
ethyl (3R,5R)-7-(2-(4-fluorophenyl)-5-isopropyl-3-phenyl-4-(phenylcarbamoyl)-1H-pyrrol-1-yl)-3,5-dihydroxyheptanoate
Conditions | Yield |
---|---|
With sulfuric acid at 0 - 20℃; for 2.58333h; | 68% |
atorvastatin sodium
butan-1-ol
Conditions | Yield |
---|---|
With sulfuric acid In dichloromethane at 0 - 20℃; for 2.58333h; | 59% |
atorvastatin sodium
Conditions | Yield |
---|---|
With magnesium chloride In tert-butyl methyl ether; water for 1.41667h; | |
With hydrogenchloride; magnesium acetate In water; acetone at 25 - 45℃; for 73.5h; pH=8 - 8.5; Product distribution / selectivity; |
atorvastatin sodium
Conditions | Yield |
---|---|
With iron(II) sulfate In water at 40 - 45℃; for 1h; Product distribution / selectivity; | |
With iron(II) chloride In water at 40 - 45℃; for 2h; Product distribution / selectivity; |
Conditions | Yield |
---|---|
In methanol; water at 13 - 63℃; Product distribution / selectivity; |
atorvastatin sodium
Conditions | Yield |
---|---|
With calcium chloride In water at 35 - 45℃; for 0.166667 - 0.5h; Product distribution / selectivity; | |
With calcium acetate In methanol; water at 50℃; | |
With calcium chloride In methanol; tert-butyl methyl ether; water at 25 - 30℃; pH=7.5 - 8.5; Product distribution / selectivity; |
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