Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:13547-70-1
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inquiryhigh quality Appearance:White or off-white Solid Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Cangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new api, intermedi
Colorcom is a global leader in industrial chemical manufacturing and is continuously innovating and transforming to exceed client expectations and industry standards. Colorcom prides itself on superior customer and technical focus, while focusing on
As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis
Cas:13547-70-1
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inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:13547-70-1
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inquiryOur company was built in 2009 with an ISO certificate.In the past 6 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so
Cas:13547-70-1
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inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufactu
Cas:13547-70-1
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:13547-70-1
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inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
Cas:13547-70-1
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inquiryName: 1-Chloro-3,3-dimethyl-2-butanone Synonyms: Chloropinacoline CAS:13547-70-1 MF: C6H11ClO Appearance:White or yellowy transparent liquid Storage: Preserve in well-closed, light-resistant and airtight containers. Package: 25kgs/drum Applic
Cas:13547-70-1
Min.Order:1 Kilogram
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inquiryAppearance:Clear colorless liquid Storage:Room temperature Package:200kg/Barrel Application:Used as an intermediate for medicine, pesticides Transportation:Express/Sea/Air Port:Any port in china
Cas:13547-70-1
Min.Order:200 Kilogram
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inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:13547-70-1
Min.Order:1 Kilogram
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inquiry1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highly qualifie
Cas:13547-70-1
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:13547-70-1
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
Cas:13547-70-1
Min.Order:4 Kilogram
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Type:Lab/Research institutions
inquiryWe are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov
Cas:13547-70-1
Min.Order:100 Gram
FOB Price: $100.0 / 2000.0
Type:Lab/Research institutions
inquirySuperior quality Appearance:clear slightly yellow liquid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:According to customer demand Application:Used as Pharmaceutical Intermediates Transportation:as per your req
factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
Cas:13547-70-1
Min.Order:1 Kilogram
FOB Price: $18.0 / 20.0
Type:Trading Company
inquiryProduct name: 1-Chloropinacolone CAS No.:13547-70-1 Molecule Formula:C6H11ClO Molecule Weight:134.60 Purity: 95.0% Package: 200kg/drum Description:White or light yellow transparent liquid Manufacture Standards:Enterprise Standard
Cas:13547-70-1
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
Cas:13547-70-1
Min.Order:1 Gram
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Type:Lab/Research institutions
inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
Cas:13547-70-1
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inquiryAppearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp
Cas:13547-70-1
Min.Order:1 Metric Ton
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Type:Trading Company
inquiryThe process is mature and can be mass produced to 100 kg, with good quality and purity up to 99%.The product has a large stock and can be supplied stably. Package:bottle Application:Drug R&D Transportation:Sealed drying(25℃) Port:ShangHai
Cas:13547-70-1
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryISO/factory/goodqualityAppearance:off white Storage:Dry,cool place Package:drum Application:active pharmaceutical ingredients Transportation:by air/sea/express Port:shenzhen/shanghai
Lower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
3,3-dimethyl-butan-2-one
1-chloro-3,3-dimethyl-butan-2-one
Conditions | Yield |
---|---|
With chlorine In methanol; (2S)-N-methyl-1-phenylpropan-2-amine hydrate | 92% |
With p-toluenesulfonyl chloride; lithium diisopropyl amide In tetrahydrofuran -78 deg C to room t., 1 h; | 65% |
With hydrogenchloride; sodium chlorate at 0℃; for 1h; | 48.8% |
pinacoyl (4-methoxyphenyl)tellurium dichloride
A
1-chloro-3,3-dimethyl-butan-2-one
B
bis(4-methoxyphenyl)ditelluride
Conditions | Yield |
---|---|
at 210℃; under 30 Torr; for 0.0833333h; | A 85% B n/a C n/a |
3,3-dimethyl-2-(trimethylsilyl)oxy-1-butene
1-chloro-3,3-dimethyl-butan-2-one
Conditions | Yield |
---|---|
With copper dichloride In N,N-dimethyl-formamide 1) r.t., 3 h, 2) 50 deg C, 30 min; further reagent: FeCl3 in MeCN; | 65% |
Multi-step reaction with 2 steps 1: 94 percent / benzene / 10 h / Heating 2: 85 percent / 0.08 h / 210 °C / 30 Torr View Scheme |
(E)-1-chloro-3,3-dimethyl-2-methylthiobut-1-ene
1-chloro-3,3-dimethyl-butan-2-one
Conditions | Yield |
---|---|
With trifluoroacetic acid at 0℃; for 1h; | 60% |
1-chloro-3,3-dimethyl-butan-2-one
Conditions | Yield |
---|---|
With trifluoroacetic acid at 0℃; for 1h; | 60% |
1-chloro-3,3-dimethyl-butan-2-one
Conditions | Yield |
---|---|
With trifluoroacetic acid at 0℃; for 1h; | 60% |
(Z)-1-chloro-3,3-dimethyl-2-p-tolylthiobut-1-ene
1-chloro-3,3-dimethyl-butan-2-one
Conditions | Yield |
---|---|
With trifluoroacetic acid at 0℃; for 1h; | 60% |
3,3-dimethyl-butan-2-one
A
1-chloro-3,3-dimethyl-butan-2-one
B
1,1-dichloro-3,3-dimethylbutan-2-one
C
1,4-dichloro-3,3-dimethyl-butan-2-one
Conditions | Yield |
---|---|
beim Chlorieren in der Dampfphase; |
diazomethane
pivaloyl chloride
1-chloro-3,3-dimethyl-butan-2-one
Conditions | Yield |
---|---|
(i), (ii) HCl; Multistep reaction; |
(1-dichloromethyl-2,2-dimethyl-propoxy)-trimethyl-silane
1-chloro-3,3-dimethyl-butan-2-one
Conditions | Yield |
---|---|
With n-butyllithium In tetrahydrofuran; diethyl ether at -110 - -50℃; |
1,1-dichloro-3,3-dimethyl-2-butanol
1-chloro-3,3-dimethyl-butan-2-one
Conditions | Yield |
---|---|
With piperidine; n-butyllithium | |
at 130 - 140℃; | |
Multi-step reaction with 2 steps 1: Py / benzene / 18 h / Ambient temperature 2: nBuLi / diethyl ether; tetrahydrofuran / -110 - -50 °C View Scheme |
4-chloro-3-methoxy-2,3-dimethyl-butan-2-ol
1-chloro-3,3-dimethyl-butan-2-one
Conditions | Yield |
---|---|
With sulfuric acid |
1-chloro-3,3-dimethyl-butan-2-one
Conditions | Yield |
---|---|
With hydrogenchloride |
2-tert-Butyl-2-chlorooxirane
A
1-chloro-3,3-dimethyl-butan-2-one
B
1-fluoro-3,3-dimethyl-2-butanone
Conditions | Yield |
---|---|
With F In diethyl ether at -75℃; | |
With silver tetrafluoroborate In diethyl ether for 1h; Ambient temperature; Yield given. Yields of byproduct given; |
1-chloro-3,3-dimethyl-butan-2-one
Conditions | Yield |
---|---|
With sulfuric acid for 0.25h; |
2,2-dimethyl-3-butyne
1-chloro-3,3-dimethyl-butan-2-one
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: CCl4 / Ambient temperature 2: 60 percent / CF3COOH / 1 h / 0 °C View Scheme | |
Multi-step reaction with 2 steps 1: CHCl3 / Ambient temperature 2: 60 percent / CF3COOH / 1 h / 0 °C View Scheme | |
Multi-step reaction with 2 steps 1: CCl4 / Ambient temperature 2: 60 percent / CF3COOH / 1 h / 0 °C View Scheme | |
Multi-step reaction with 2 steps 1: CHCl3 / Ambient temperature 2: 60 percent / CF3COOH / 1 h / 0 °C View Scheme |
3,3-dimethyl-butan-2-one
1-chloro-3,3-dimethyl-butan-2-one
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 78 percent / benzene / 72 h / Heating 2: 85 percent / 0.08 h / 210 °C / 30 Torr View Scheme |
2-chloro-3,3-dimethyl-1-butene
1-chloro-3,3-dimethyl-butan-2-one
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 60.5 percent / m-chloroperbenzoic acid / CH2Cl2 / 18 h / Ambient temperature 2: AgBF4 / diethyl ether / 1 h / Ambient temperature View Scheme | |
Multi-step reaction with 2 steps 1: 31 percent / acide m-chloroperoxybenzoique / CH2Cl2 / 15 h / Ambient temperature 2: n-Bu3MePF / diethyl ether / -75 °C View Scheme |
pivalaldehyde
1-chloro-3,3-dimethyl-butan-2-one
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: (i) nBuLi, (ii) /BRN= 506060/ 2: nBuLi, piperidine View Scheme |
1,1-dichloro-3,3-dimethylbutan-2-one
1-chloro-3,3-dimethyl-butan-2-one
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: LiAlH4, Et2O 2: 130 - 140 °C View Scheme |
tert-butyl-2-chloro-acetylene
1-chloro-3,3-dimethyl-butan-2-one
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: dimethylformamide; methanol 2: aq. HCl View Scheme |
3,3-dimethyl-butan-2-one
A
1-chloro-3,3-dimethyl-butan-2-one
B
1,1-dichloro-3,3-dimethylbutan-2-one
Conditions | Yield |
---|---|
With chlorine; hydrogenchloride at 150℃; Heating / reflux; | |
With chlorine; hydrogenchloride Heating / reflux; | |
With chlorine | |
With 1,3-dichloro-5,5-dimethylhydantoin; silica gel In methanol for 1h; Reflux; |
1-chloro-3,3-dimethyl-butan-2-one
Conditions | Yield |
---|---|
With hydrogenchloride; formic acid |
1-hydroxy-3,3-dimethylbutan-2-one
A
1-chloro-3,3-dimethyl-butan-2-one
B
4-tert-butyl-5H-[1,2,3]oxathiazole 2,2-dioxide
Conditions | Yield |
---|---|
With pyridine; formic acid; isocyanate de chlorosulfonyle In acetonitrile at 0 - 10℃; Inert atmosphere; |
3,3-dimethyl-butan-2-one
A
1-chloro-3,3-dimethyl-butan-2-one
B
1,1-dichloro-3,3-dimethylbutan-2-one
C
1,4-dichloro-3,3-dimethyl-butan-2-one
D
2,2,5,6,6-pentamethyl-hept-4-en-3-one
E
1,1,1-trichloro-3,3-dimethyl-2-butanone
F
1,1,4-trichloro-3,3-dimethyl-butan-2-one
G
4-chloro-3,3-dimethylbutane-2-one
H
1,4-dichloro-3-chloromethyl-3-methyl-butan-2-one
I
1,1,4,4-tetrachloro-3,3-dimethyl-butan-2-one
J
1,1,4-trichloro-3-chloromethyl-3-methyl-butan-2-one
Conditions | Yield |
---|---|
With chlorine In tetrachloromethane for 1h; Irradiation; |
3,3-dimethyl-butan-2-one
A
1-chloro-3,3-dimethyl-butan-2-one
B
4-chloro-3,3-dimethylbutane-2-one
Conditions | Yield |
---|---|
With sulfuryl dichloride In tetrachloromethane at 20℃; |
3'-[4-(hydroxy)-3-methylphenyl]-3'-[4-methylthiophen-2-yl]pentane
1-chloro-3,3-dimethyl-butan-2-one
1-{4-[1-ethyl-1-(4-methyl-thiophen-2-yl)-propyl]-2-methyl-phenoxy}-3,3-dimethyl-butan-2-one
Conditions | Yield |
---|---|
With potassium carbonate In acetone Heating / reflux; | 100% |
With potassium carbonate In acetone Heating / reflux; | 100% |
3'-[4-(hydroxy)-3-methylphenyl]-3'-[5-methoxycarbonyl-4-methylthiophen-2-yl]pentane
1-chloro-3,3-dimethyl-butan-2-one
3'-[4-(2-oxo-3,3-dimethylbutoxy)-3-methylphenyl]-3'-[5-methoxycarbonyl-4-methylthiophen-2-yl]pentane
Conditions | Yield |
---|---|
With potassium carbonate In acetone Heating / reflux; | 100% |
With potassium carbonate In acetone at 20℃; Product distribution / selectivity; Heating / reflux; | 100% |
1-chloro-3,3-dimethyl-butan-2-one
1-azido-3,3-dimethyl-2-butanone
Conditions | Yield |
---|---|
With sodium azide In acetone at 25℃; | 100% |
With sodium azide In acetone for 36h; Inert atmosphere; | 79% |
With sodium azide In acetone at 25℃; |
1-chloro-3,3-dimethyl-butan-2-one
methyl 3-(3-(3-(4-hydroxy-3-methylphenyl)pentan-3-yl)-1H-indol-6-yl)propanoate
methyl 3-(3-(3-(4-(3,3-dimethyl-2-oxobutoxy)-3-methylphenyl)pentan-3-yl)-1H-indol-6-yl)propanoate
Conditions | Yield |
---|---|
With potassium carbonate Inert atmosphere; | 100% |
1-chloro-3,3-dimethyl-butan-2-one
pivalaldehyde
5-hydroxy-2,2,6,6-tetramethyl-3-heptanone
Conditions | Yield |
---|---|
With samarium diiodide In tetrahydrofuran at -78℃; for 1.41667h; Reformatsky type reaction; Inert atmosphere; | 99% |
1-chloro-3,3-dimethyl-butan-2-one
cyclohexanecarbaldehyde
1-cyclohexyl-1-hydroxy-4,4-dimethylpentan-3-one
Conditions | Yield |
---|---|
With samarium diiodide In tetrahydrofuran at -78℃; for 1.41667h; Reformatsky type reaction; Inert atmosphere; | 99% |
1-chloro-3,3-dimethyl-butan-2-one
p-toluidine
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In N,N-dimethyl-formamide at 75℃; for 48h; | 99% |
7-hydroxy-3-methoxycarbonylmethyl-4-methyl-2H-chromen-2-one
1-chloro-3,3-dimethyl-butan-2-one
methyl [4-methyl-7-(3',3'-dimethyl-2'-oxobutoxy)-2-oxo-2H-benzopyran-3-yl]-acetate
Conditions | Yield |
---|---|
With triethylamine In water at 130℃; for 0.333333h; Microwave irradiation; | 98% |
With potassium carbonate In acetone at 50 - 56℃; Williamson reaction; | 78% |
4-[3-(4-amino-3-methylphenyl)pentan-3-yl]-2-methylphenol
1-chloro-3,3-dimethyl-butan-2-one
1-{4-[3-(4-amino-3-methylphenyl)pentan-3-yl]-2-methylphenoxy}-3,3-dimethylbutan-2-one
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide for 1h; | 97% |
With sodium hydride In N,N-dimethyl-formamide for 21h; | 97% |
1-chloro-3,3-dimethyl-butan-2-one
Conditions | Yield |
---|---|
With potassium carbonate In butanone Heating / reflux; | 97% |
1-chloro-3,3-dimethyl-butan-2-one
Conditions | Yield |
---|---|
With potassium carbonate In butanone Heating / reflux; | 97% |
1-chloro-3,3-dimethyl-butan-2-one
5-(4-chlorophenyl)-2,4-dihydro-3H-pyrazol-3-one
3-(4-chlorophenyl)-l-(3, 3-dimethyl-2-oxobutyl)-4, 5-dihydropyrazol-5-one
Conditions | Yield |
---|---|
With potassium carbonate In acetonitrile | 97% |
(R)-(-)-1-(2-oxo-5-phenyl-1,3,4,5-tetrahydro-2H-1,5-benzodiazepin-3-yl)-3-[3-(1-methyl-1-tert-butoxycarbonyl)ethylphenyl]urea
1-chloro-3,3-dimethyl-butan-2-one
Conditions | Yield |
---|---|
Stage #1: (R)-(-)-1-(2-oxo-5-phenyl-1,3,4,5-tetrahydro-2H-1,5-benzodiazepin-3-yl)-3-[3-(1-methyl-1-tert-butoxycarbonyl)ethylphenyl]urea With sodium hydride In N,N-dimethyl-formamide for 1h; Stage #2: 1-chloro-3,3-dimethyl-butan-2-one In N,N-dimethyl-formamide at 20℃; for 1.5h; | 97% |
1-chloro-3,3-dimethyl-butan-2-one
1-hydroxy-3,3-dimethylbutan-2-one
Conditions | Yield |
---|---|
With potassium hydroxide In tetrahydrofuran; water at 40 - 60℃; Reagent/catalyst; | 97% |
With sodium hydroxide In water at 110℃; for 2h; Reagent/catalyst; Solvent; | 89% |
3,5-dimethoxyphenol
1-chloro-3,3-dimethyl-butan-2-one
Conditions | Yield |
---|---|
With potassium hydrogencarbonate; sodium iodide In butanone Heating; | 96% |
1-chloro-3,3-dimethyl-butan-2-one
methyl (E)-3-(5-(3-(4-hydroxy-3-methylphenyl)pentan-3-yl)-3-methylthiophen-2-yl)acrylate
methyl (E)-3-(5-(3-(4-(3,3-dimethyl-2-oxobutoxy)-3-methylphenyl)pentan-3-yl)-3-methylthiophen-2-yl)acrylate
Conditions | Yield |
---|---|
With potassium carbonate Inert atmosphere; | 95% |
sodium cyanide
1-chloro-3,3-dimethyl-butan-2-one
trimethylacetylacetonitrile
Conditions | Yield |
---|---|
With sodium carbonate; sodium iodide In methanol at 60℃; for 3h; | 95% |
1,2,4-Triazole
1-chloro-3,3-dimethyl-butan-2-one
Conditions | Yield |
---|---|
With potassium carbonate In ethyl acetate at 50℃; for 5h; | 95% |
methyl 2-(7-hydroxy-4,8-dimethyl-2-oxo-2H-chromen-3-yl)acetate
1-chloro-3,3-dimethyl-butan-2-one
methyl [4,8-dimethyl-7-(3',3'-dimethyl-2'-oxobutoxy)-2-oxo-2H-benzopyran-3-yl]-acetate
Conditions | Yield |
---|---|
With triethylamine In water at 130℃; for 0.333333h; Microwave irradiation; | 94% |
With potassium carbonate In acetone at 50 - 56℃; Williamson reaction; | 81% |
2-methyl-1,3,4-oxadiazol-5(4H)-one
1-chloro-3,3-dimethyl-butan-2-one
Conditions | Yield |
---|---|
Stage #1: 2-methyl-1,3,4-oxadiazol-5(4H)-one With sodium methylate In methanol at 20℃; for 0.25h; Stage #2: 1-chloro-3,3-dimethyl-butan-2-one; tetrabutylammomium bromide In chloroform at 20℃; Heating / reflux; | 94% |
Conditions | Yield |
---|---|
In methanol at 55℃; for 2.5h; Product distribution / selectivity; | 94% |
1-chloro-3,3-dimethyl-butan-2-one
sodium thiocyanide
3,3-dimethyl-2-oxobutyl thiocyanate
Conditions | Yield |
---|---|
In methanol at 55℃; for 2.5h; | 94% |
1-chloro-3,3-dimethyl-butan-2-one
methyl 3-(3-(3-(4-hydroxy-3-methylphenyl)pentan-3-yl)-1-methyl-1H-indol-6-yl)propanoate
methyl 3-(3-(3-(4-(3,3-dimethyl-2-oxobutoxy)-3-methylphenyl)pentan-3-yl)-1-methyl-1H-indol-6-yl)propanoate
Conditions | Yield |
---|---|
With potassium carbonate Inert atmosphere; | 94% |
3,3-dimethyl-butan-2-one
1-chloro-3,3-dimethyl-butan-2-one
5-hydroxy-2,2,5,6,6-pentamethylheptan-3-one
Conditions | Yield |
---|---|
With samarium diiodide In tetrahydrofuran at -78℃; for 2.41667h; Reformatsky type reaction; Inert atmosphere; | 93% |
1-chloro-3,3-dimethyl-butan-2-one
1-tert-butylimidazole
1-(tert-butyl)-3-(3,3-dimethyl-2-oxobutyl)imidazolium chloride
Conditions | Yield |
---|---|
In toluene for 5h; Inert atmosphere; Schlenk technique; Reflux; | 93% |
In toluene for 24h; Reflux; | 57% |
1-chloro-3,3-dimethyl-butan-2-one
4-(3-(4-(benzyloxy)phenyl)pentan-3-yl)-2-methylphenol
1-(4-(3-(4-(benzyloxy)phenyl)pentan-3-yl)-2-methylphenoxy)-3,3-dimethylbutan-2-one
Conditions | Yield |
---|---|
With potassium carbonate Inert atmosphere; | 93% |
With potassium carbonate In acetonitrile for 12h; Reflux; | 93% |
1-chloro-3,3-dimethyl-butan-2-one
methyl 2-(benzyloxy)-5-(3-(4-hydroxy-3-methylphenyl)-pentan-3-yl)benzoate
methyl 2-(benzyloxy)-5-(3-(4-(3,3-dimethyl-2-oxobutoxy)-3-methylphenyl)pentan-3-yl)benzoate
Conditions | Yield |
---|---|
With potassium carbonate Inert atmosphere; | 93% |
With potassium carbonate In acetonitrile for 12h; Reflux; | 93% |
1-chloro-3,3-dimethyl-butan-2-one
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide; acetone Williamson Ether Synthesis; Heating; | 93% |
1-chloro-3,3-dimethyl-butan-2-one
benzyl-methyl-amine
2-(N-benzyl-N-methylamino)-3,3-dimethyl-2-butanone
Conditions | Yield |
---|---|
In 1,2-dimethoxyethane Heating; | 92% |
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