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Wuhan PharmChem Co.,Ltd

Appearance:White powder Storage:Store in a cool, dry and well-ventilated area Package:1kg/foil bag; 25kg/drum Application:Veterinary drug intermediate Transportation:Prompt delivery Port:Shanghai port

99% N-Ethyl-D-glucamine C8H19NO5

Cas:14216-22-9

Min.Order:1 Kilogram

FOB Price: $85.0

Type:Trading Company

inquiry

Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality n-ethylglucamine supplier in China

Cas:14216-22-9

Min.Order:1 Kilogram

Negotiable

Type:Manufacturers

inquiry

Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply N-Ethylglucamine

Cas:14216-22-9

Min.Order:1

Negotiable

Type:Other

inquiry

Dayang Chem (Hangzhou) Co.,Ltd.

DayangChem exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product s

N-Ethyl-D-glucamine

Cas:14216-22-9

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

inquiry

Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

N-Ethylglucamine

Cas:14216-22-9

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

inquiry

Henan Tianfu Chemical Co., Ltd.

Our company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O

high quality N-Ethyl-D-glucamine

Cas:14216-22-9

Min.Order:1 Gram

FOB Price: $1.0

Type:Lab/Research institutions

inquiry

Hebei Nengqian Chemical Import and Export Co., LTD

With our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin

N-Ethyl-D-Glucamine :14216-22-9

Cas:14216-22-9

Min.Order:1 Kilogram

FOB Price: $32.0 / 65.0

Type:Trading Company

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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Factory direct supply CAS 14216-22-9 with best quality

Cas:14216-22-9

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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LIDE PHARMACEUTICALS LIMITED

Advantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&amp

N-Ethyl-D-glucamine/ LIDE PHARMA- Factory supply / Best price

Cas:14216-22-9

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hebei Sankai Chemical Technology Co., Ltd

1. Product advantages ♦ High purity, all above 98.5%, no impurities after dissolution ♦ We will test each batch to ensure quality ♦ OEM and private brand services designed for free ♦ Various cap colors available ♦ W

N-Ethyl-D-glucamine CAS14216-22-9

Cas:14216-22-9

Min.Order:1 Kilogram

FOB Price: $289.0 / 499.0

Type:Trading Company

inquiry

Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

D-Glucitol,1-deoxy-1-(ethylamino)- 14216-22-9

Cas:14216-22-9

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Qingdao Beluga Import and Export Co., LTD

N-Ethyl-D-glucamine CAS:14216-22-9 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic inter

N-Ethyl-D-glucamine CAS:14216-22-9

Cas:14216-22-9

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

D-Glucitol,1-deoxy-1-(ethylamino)-

Cas:14216-22-9

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Hebei Mojin Biotechnology Co.,Ltd

Hebei Mojin Biotechnology Co., Ltd, Our company is a professional chemical raw materials and chemical reagents research and development production enterprises. We have several production line,So we can control the lowest price. We also have sever

High quality N-Ethyl-D-glucamine cas:14216-22-9

Cas:14216-22-9

Min.Order:25 Kilogram

FOB Price: $30.0 / 40.0

Type:Trading Company

inquiry

Leader Biochemical Group

PRODUCT DETAILS

China Largest Manufacturer factory sales N-Ethyl-D-glucamine CAS 14216-22-9

Cas:14216-22-9

Min.Order:500 Kilogram

FOB Price: $1.0 / 2.0

Type:Lab/Research institutions

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

D-Glucitol,1-deoxy-1-(ethylamino)-

Cas:14216-22-9

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Shanxi Ankesi Biotechnology Co., Ltd

Our Advantage 1. Rich experience We specialize in this filed for many years, our APIs exported to all over the world and and we established long friendly relations of cooperation with our clients. 2. Great quality,purity and favorable Good qual

Factory direct supply N-Ethyl-D-glucamine CAS 14216-22-9 with best quality AKS

Cas:14216-22-9

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

inquiry

Xiamen Hisunny Chemical Co.,Ltd

Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia

N-Ethylglucamine

Cas:14216-22-9

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Zhengzhou Yuanli Biological Technology Co., Ltd.

Product Name:N-Ethyl-D-glucamine CAS No.:14216-22-9 MF:C8H19NO5 MW:209.24 Assay : 99% EINECS No.:238-073-8 Packaging: 25kg/kg Shipping: Timely delivery after your payment Superiority : ISO certificate Powerful R & D team The abili

99% N-Ethyl-D-glucamine factory supply

Cas:14216-22-9

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Triumph International Development Limilted

Triumph has the complete production of G- KG - MT service chain,we can make the new technology into productivity quickly in the research and development of new products. Main Service 1.Own made fine chemical products 2.Out sourcin

N-Ethyl Glucamine

Cas:14216-22-9

Min.Order:100 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Afine Chemicals Limited

Our Services 1. New Molecules R&D 2. Own test center HPLC NMR GC LC-MS 3. API and Intermediates from China reputed manufacturers 4. Documents support COA MOA MSDS DMF open part Our advantages 1. Government awarded company. Top 100 enter

N-Ethyl-D-glucamine

Cas:14216-22-9

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

N-Ethyl-D-glucamine

Cas:14216-22-9

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

N-Ethyl-D-glucamine

Cas:14216-22-9

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

N-Ethyl-D-glucamine

Cas:14216-22-9

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

inquiry

Hebei Kunsui Technology Co., Ltd.

1. A strong scientific research team . 2. Stable quality (with a complete scientific research center and testing center to ensure the quality stability of each batch of products). 3. Rich export experience (with practical experience in exporting to m

Organic Chemical N-ethylglucamine Powder CAS 14216-22-9

Cas:14216-22-9

Min.Order:1 Kilogram

FOB Price: $8.2 / 8.8

Type:Trading Company

inquiry

Zibo Dorne chemical technology co. LTD

Product Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,

N-ethylglucamine CAS:14216-22-9 Safe delivery Free of customs clearance

Cas:14216-22-9

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Jiangsu Qianyu Molecular Technology Co., LTD.

Our Advantages A. International Top level TechnologyOur company owned biomedicine experts are famous at home and abroad with rich experience in research and development in the field of efficient chiral functional molecules research and development an

Reliable Quality N-Ethyl-D-glucamine

Cas:14216-22-9

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Hangzhou Think Chemical Co. Ltd

HANGZHOU THINK CHEMICAL CO., LTD. (THINKCHEM) is an integrative corporation of trade, research and contract manufacture. With about ten years of business experiences on the marketing & distribution, thinkchem specializes in exp

N-Ethylglucamine CAS:14216-22-9

Cas:14216-22-9

Min.Order:0 Metric Ton

Negotiable

Type:Other

inquiry

EAST CHEMSOURCES LIMITED

factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B

high quality N-Ethyl-D-glucamine

Cas:14216-22-9

Min.Order:1 Kilogram

FOB Price: $18.0 / 20.0

Type:Trading Company

inquiry

Siwei Development Group Ltd.

Product name: N-Ethyl Glucamine CAS No.:14216-22-9 Molecule Formula:C8H19NO5 Molecule Weight:209.24 Purity: 99% Package: 25kg/drum Description:White crystalline powder Manufacture Standards:Enterprise Standard TEST

Best Quality N-Ethyl Glucamine

Cas:14216-22-9

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

inquiry

Synthetic route

D-glucose
50-99-7

D-glucose

ethylamine
75-04-7

ethylamine

N-ethyl-D-glucamine
14216-22-9

N-ethyl-D-glucamine

Conditions
ConditionsYield
Stage #1: D-glucose; ethylamine With hydrogen In methanol at 25 - 35℃; for 0.5h;
Stage #2: In methanol at 60 - 80℃; for 12h; Reagent/catalyst; Solvent; Sealed tube; Inert atmosphere;
95.69%
With nickel kieselguhr; water at 90 - 100℃; under 73550.8 Torr; Hydrogenation;
With nickel kieselguhr; water at 90 - 100℃; under 73550.8 Torr; Hydrogenation;
N-ethyl-D-glucosylamine

N-ethyl-D-glucosylamine

N-ethyl-D-glucamine
14216-22-9

N-ethyl-D-glucamine

Conditions
ConditionsYield
With methanol; palladium on activated charcoal at 15 - 40℃; under 18387.7 Torr; Hydrogenation;
methanol
67-56-1

methanol

D-glucose-ethylimine

D-glucose-ethylimine

palladium

palladium

coal

coal

N-ethyl-D-glucamine
14216-22-9

N-ethyl-D-glucamine

Conditions
ConditionsYield
at 15 - 40℃; under 18387.7 Torr; Hydrogenation;
N-ethyl-D-glucamine
14216-22-9

N-ethyl-D-glucamine

m-tolyl aldehyde
620-23-5

m-tolyl aldehyde

(2R,5S)-3-ethyl-2-(3-methylphenyl)-5-(D-arabino-1,2,3,4-tetrahydroxybutyl)oxazolidine

(2R,5S)-3-ethyl-2-(3-methylphenyl)-5-(D-arabino-1,2,3,4-tetrahydroxybutyl)oxazolidine

Conditions
ConditionsYield
In benzene Dean-Stark; Reflux;74%
N-ethyl-D-glucamine
14216-22-9

N-ethyl-D-glucamine

3-methoxy-benzaldehyde
591-31-1

3-methoxy-benzaldehyde

(2R,5S)-3-ethyl-2-(3-methoxyphenyl)-5-(D-arabino-1,2,3,4-tetrahydroxybutyl)oxazolidine

(2R,5S)-3-ethyl-2-(3-methoxyphenyl)-5-(D-arabino-1,2,3,4-tetrahydroxybutyl)oxazolidine

Conditions
ConditionsYield
In benzene Dean-Stark; Reflux;74%
N-ethyl-D-glucamine
14216-22-9

N-ethyl-D-glucamine

4-methyl-benzaldehyde
104-87-0

4-methyl-benzaldehyde

(2R,5S)-3-ethyl-2-(4-methylphenyl)-5-(D-arabino-1,2,3,4-tetrahydroxybutyl)oxazolidine

(2R,5S)-3-ethyl-2-(4-methylphenyl)-5-(D-arabino-1,2,3,4-tetrahydroxybutyl)oxazolidine

Conditions
ConditionsYield
In benzene Dean-Stark; Reflux;71%
N-ethyl-D-glucamine
14216-22-9

N-ethyl-D-glucamine

C23H20ClNO4S

C23H20ClNO4S

C31H38N2O9S

C31H38N2O9S

Conditions
ConditionsYield
In water; isopropyl alcohol at 80℃; for 13h;59%
N-ethyl-D-glucamine
14216-22-9

N-ethyl-D-glucamine

4-nitrobenzaldehdye
555-16-8

4-nitrobenzaldehdye

(5S)-3-ethyl-2-(4-nitrophenyl)-5-(D-arabino-1,2,3,4-tetrahydroxybutyl)oxazolidine

(5S)-3-ethyl-2-(4-nitrophenyl)-5-(D-arabino-1,2,3,4-tetrahydroxybutyl)oxazolidine

Conditions
ConditionsYield
In methanol; water Heating; Green chemistry;52%
N-ethyl-D-glucamine
14216-22-9

N-ethyl-D-glucamine

(4-isopropylbenzaldehyde)
122-03-2

(4-isopropylbenzaldehyde)

(2R,5S)-3-ethyl-2-(4-isopropylphenyl)-5-(D-arabino-1,2,3,4-tetrahydroxybutyl)oxazolidine

(2R,5S)-3-ethyl-2-(4-isopropylphenyl)-5-(D-arabino-1,2,3,4-tetrahydroxybutyl)oxazolidine

Conditions
ConditionsYield
In benzene Dean-Stark; Reflux;49%
N-ethyl-D-glucamine
14216-22-9

N-ethyl-D-glucamine

chromium(III) trifluoride tetrahydrate

chromium(III) trifluoride tetrahydrate

Ni(2+)*CO3(2-)*(x)H2O*2HO(1-)*Ni(2+)

Ni(2+)*CO3(2-)*(x)H2O*2HO(1-)*Ni(2+)

Trimethylacetic acid
75-98-9

Trimethylacetic acid

[Cr7NiF3(N-ethyl-D-glucamine)(O2CtBu)15(H2O)]

[Cr7NiF3(N-ethyl-D-glucamine)(O2CtBu)15(H2O)]

Conditions
ConditionsYield
Stage #1: N-ethyl-D-glucamine; chromium(III) trifluoride tetrahydrate; Trimethylacetic acid at 160℃; for 2h;
Stage #2: Ni(2+)*CO3(2-)*(x)H2O*2HO(1-)*Ni(2+) at 160℃; for 50h;
43%
manganese(II)carbonate

manganese(II)carbonate

N-ethyl-D-glucamine
14216-22-9

N-ethyl-D-glucamine

chromium(III) trifluoride tetrahydrate

chromium(III) trifluoride tetrahydrate

Trimethylacetic acid
75-98-9

Trimethylacetic acid

[Cr7MnF3(N-ethyl-D-glucamine)(O2CtBu)15(H2O)]

[Cr7MnF3(N-ethyl-D-glucamine)(O2CtBu)15(H2O)]

Conditions
ConditionsYield
Stage #1: N-ethyl-D-glucamine; chromium(III) trifluoride tetrahydrate; Trimethylacetic acid at 160℃; for 2h;
Stage #2: manganese(II)carbonate at 160℃; for 50h;
42%
N-ethyl-D-glucamine
14216-22-9

N-ethyl-D-glucamine

chromium(III) trifluoride tetrahydrate

chromium(III) trifluoride tetrahydrate

zinc(II) carbonate
743369-26-8

zinc(II) carbonate

Trimethylacetic acid
75-98-9

Trimethylacetic acid

[Cr7ZnF3(N-ethyl-D-glucamine)(O2CtBu)15(H2O)]

[Cr7ZnF3(N-ethyl-D-glucamine)(O2CtBu)15(H2O)]

Conditions
ConditionsYield
Stage #1: N-ethyl-D-glucamine; chromium(III) trifluoride tetrahydrate; Trimethylacetic acid at 160℃; for 2h;
Stage #2: zinc(II) carbonate at 160℃; for 50h;
38%
N-ethyl-D-glucamine
14216-22-9

N-ethyl-D-glucamine

2,4-dimethylbenzaldehyde
15764-16-6

2,4-dimethylbenzaldehyde

(2S,5S)-2-(2,4-dimethylphenyl)-3-ethyl-5-(D-arabino-1,2,3,4-tetrahydroxybutyl)oxazolidine

(2S,5S)-2-(2,4-dimethylphenyl)-3-ethyl-5-(D-arabino-1,2,3,4-tetrahydroxybutyl)oxazolidine

Conditions
ConditionsYield
In benzene Dean-Stark; Reflux;35%
N-ethyl-D-glucamine
14216-22-9

N-ethyl-D-glucamine

4-ethylbenzylaldehyde
4748-78-1

4-ethylbenzylaldehyde

(2R,5S)-3-ethyl-2-(4-ethylphenyl)-5-(D-arabino-1,2,3,4-tetrahydroxybutyl)oxazolidine

(2R,5S)-3-ethyl-2-(4-ethylphenyl)-5-(D-arabino-1,2,3,4-tetrahydroxybutyl)oxazolidine

Conditions
ConditionsYield
In benzene Dean-Stark; Reflux;30%
carbon disulfide
75-15-0

carbon disulfide

N-ethyl-D-glucamine
14216-22-9

N-ethyl-D-glucamine

ethyl-D-fructos-1-yl-dithiocarbamic acid
10225-80-6

ethyl-D-fructos-1-yl-dithiocarbamic acid

N-ethyl-D-glucamine
14216-22-9

N-ethyl-D-glucamine

cridanimod
38609-97-1

cridanimod

1-desoxy-1-(ethylamino)-D-glucitole salt of 10-(carboxymethyl)-9(10H)acridone
937021-67-5

1-desoxy-1-(ethylamino)-D-glucitole salt of 10-(carboxymethyl)-9(10H)acridone

Conditions
ConditionsYield
In water for 0.416667 - 0.583333h; Heating / reflux;
Elinogrel

Elinogrel

N-ethyl-D-glucamine
14216-22-9

N-ethyl-D-glucamine

[4-(6-chloro-7-methylamino-2,4-dioxo-1,4-dihydro-2H-quinazolin-3-yl)-phenyl]-5-chloro-thiophen-2-yl-sulfonylurea N-ethylglucamine salt
1079989-99-3

[4-(6-chloro-7-methylamino-2,4-dioxo-1,4-dihydro-2H-quinazolin-3-yl)-phenyl]-5-chloro-thiophen-2-yl-sulfonylurea N-ethylglucamine salt

Conditions
ConditionsYield
In water for 2h;
PD 126055

PD 126055

N-ethyl-D-glucamine
14216-22-9

N-ethyl-D-glucamine

(S)-2-(diphenylacetyl)-1,2,3,4-tetrahydro-6-methoxy-5-(phenylmethoxy)-3-isoquinoline carboxylic acid, N-ethylglucamine salt

(S)-2-(diphenylacetyl)-1,2,3,4-tetrahydro-6-methoxy-5-(phenylmethoxy)-3-isoquinoline carboxylic acid, N-ethylglucamine salt

Conditions
ConditionsYield
In isopropyl alcohol at 5 - 50℃; for 5.5h; Product distribution / selectivity;
N-ethyl-D-glucamine
14216-22-9

N-ethyl-D-glucamine

5,7-Dihydroxy-3-(4-hydroxy-phenyl)-chromen-4-on
446-72-0

5,7-Dihydroxy-3-(4-hydroxy-phenyl)-chromen-4-on

4',5,7-trihydroxyisoflavone-5,7-dihydroxy-3-(4-hydroxyphenyl)-4H-1-benzopyran-4-one N-ethylglucamine salt

4',5,7-trihydroxyisoflavone-5,7-dihydroxy-3-(4-hydroxyphenyl)-4H-1-benzopyran-4-one N-ethylglucamine salt

Conditions
ConditionsYield
at 20 - 25℃; for 24h;
N-ethyl-D-glucamine
14216-22-9

N-ethyl-D-glucamine

methyl n-dodecanoate
111-82-0

methyl n-dodecanoate

n-dodecanoyl-N-ethyl-glucamide

n-dodecanoyl-N-ethyl-glucamide

Conditions
ConditionsYield
With sodium hydroxide In propylene glycol at 95 - 120℃; under 750.075 - 9750.98 Torr; for 1.2h;
N-ethyl-D-glucamine
14216-22-9

N-ethyl-D-glucamine

2-[bis-(2-pyridylmethyl)aminomethyl]pyridine-5-carboxylic acid
440367-79-3

2-[bis-(2-pyridylmethyl)aminomethyl]pyridine-5-carboxylic acid

6-((bis(pyridin-2-ylmethyl)amino)methyl)-N-ethyl-N-((2S,3R,4R,5R)-2,3,4,5,6-pentahydroxyhexyl)nicotinamide

6-((bis(pyridin-2-ylmethyl)amino)methyl)-N-ethyl-N-((2S,3R,4R,5R)-2,3,4,5,6-pentahydroxyhexyl)nicotinamide

Conditions
ConditionsYield
With 4-methyl-morpholine; 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In N,N-dimethyl-formamide at 50℃; for 18h;0.135 g
N-ethyl-D-glucamine
14216-22-9

N-ethyl-D-glucamine

tranilast

tranilast

tranilast N-ethylglucamine salt

tranilast N-ethylglucamine salt

Conditions
ConditionsYield
In acetone at 20℃; for 24h;
N-ethyl-D-glucamine
14216-22-9

N-ethyl-D-glucamine

4-methoxy-benzaldehyde
123-11-5

4-methoxy-benzaldehyde

(2R,5S)-3-ethyl-2-(4-methoxyphenyl)-5-(D-arabino-1,2,3,4-tetrahydroxybutyl)oxazolidine

(2R,5S)-3-ethyl-2-(4-methoxyphenyl)-5-(D-arabino-1,2,3,4-tetrahydroxybutyl)oxazolidine

Conditions
ConditionsYield
In benzene Dean-Stark; Reflux;
N-ethyl-D-glucamine
14216-22-9

N-ethyl-D-glucamine

4-nitrobenzaldehdye
555-16-8

4-nitrobenzaldehdye

A

(2R,5S)-3-ethyl-2-(4-nitrophenyl)-5-(D-arabino-1,2,3,4-tetrahydroxybutyl)oxazolidine

(2R,5S)-3-ethyl-2-(4-nitrophenyl)-5-(D-arabino-1,2,3,4-tetrahydroxybutyl)oxazolidine

B

(2S,5S)-3-ethyl-2-(4-nitrophenyl)-5-(D-arabino-1,2,3,4-tetrahydroxybutyl)oxazolidine

(2S,5S)-3-ethyl-2-(4-nitrophenyl)-5-(D-arabino-1,2,3,4-tetrahydroxybutyl)oxazolidine

Conditions
ConditionsYield
In benzene Dean-Stark; Reflux; Overall yield = 82 percent;A n/a
B n/a
N-ethyl-D-glucamine
14216-22-9

N-ethyl-D-glucamine

2-chloro-benzaldehyde
89-98-5

2-chloro-benzaldehyde

A

(2R,5S)-2-(2-chlorophenyl)-3-ethyl-5-(D-arabino-1,2,3,4-tetrahydroxybutyl)oxazolidine

(2R,5S)-2-(2-chlorophenyl)-3-ethyl-5-(D-arabino-1,2,3,4-tetrahydroxybutyl)oxazolidine

B

(2S,5S)-2-(2-chlorophenyl)-3-ethyl-5-(D-arabino-1,2,3,4-tetrahydroxybutyl)oxazolidine

(2S,5S)-2-(2-chlorophenyl)-3-ethyl-5-(D-arabino-1,2,3,4-tetrahydroxybutyl)oxazolidine

Conditions
ConditionsYield
In benzene Dean-Stark; Reflux;A n/a
B n/a
N-ethyl-D-glucamine
14216-22-9

N-ethyl-D-glucamine

2-methylphenyl aldehyde
529-20-4

2-methylphenyl aldehyde

A

(2R,5S)-3-ethyl-2-(2-methylphenyl)-5-(D-arabino-1,2,3,4-tetrahydroxybutil)oxazolidine

(2R,5S)-3-ethyl-2-(2-methylphenyl)-5-(D-arabino-1,2,3,4-tetrahydroxybutil)oxazolidine

B

(2S,5S)-3-ethyl-2-(2-methylphenyl)-5-(D-arabino-1,2,3,4-tetrahydroxybutil)oxazolidine

(2S,5S)-3-ethyl-2-(2-methylphenyl)-5-(D-arabino-1,2,3,4-tetrahydroxybutil)oxazolidine

Conditions
ConditionsYield
In benzene Dean-Stark; Reflux; Overall yield = 63 percent;A n/a
B n/a
N-ethyl-D-glucamine
14216-22-9

N-ethyl-D-glucamine

3-Fluorobenzaldehyde
456-48-4

3-Fluorobenzaldehyde

A

(2R,5S)-3-ethyl-2-(3-fluorophenyl)-5-(D-arabino-1,2,3,4-tetrahydroxybutyl)oxazolidine

(2R,5S)-3-ethyl-2-(3-fluorophenyl)-5-(D-arabino-1,2,3,4-tetrahydroxybutyl)oxazolidine

B

(2S,5S)-3-ethyl-2-(3-fluorophenyl)-5-(D-arabino-1,2,3,4-tetrahydroxybutyl)oxazolidine

(2S,5S)-3-ethyl-2-(3-fluorophenyl)-5-(D-arabino-1,2,3,4-tetrahydroxybutyl)oxazolidine

Conditions
ConditionsYield
In benzene Dean-Stark; Reflux; Overall yield = 31 percent;A n/a
B n/a
N-ethyl-D-glucamine
14216-22-9

N-ethyl-D-glucamine

4-methyl-benzaldehyde
104-87-0

4-methyl-benzaldehyde

(5S)-3-ethyl-2-(4-methylphenyl)-5-(D-arabino-1,2,3,4-tetrahydroxybutyl)oxazolidine

(5S)-3-ethyl-2-(4-methylphenyl)-5-(D-arabino-1,2,3,4-tetrahydroxybutyl)oxazolidine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: benzene / Dean-Stark; Reflux
2: dimethylsulfoxide-d6 / 336 h
View Scheme

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