Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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inquiryShanghai Seasonsgreen Chemical is a high-tech research and development, production, sale and custom synthesis set in one high-tech chemical products enterprises. Our sales and marketing division is located in Shanghai, serving international pharmaceu
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inquiryColorcom is a global leader in industrial chemical manufacturing and is continuously innovating and transforming to exceed client expectations and industry standards. Colorcom prides itself on superior customer and technical focus, while focusing on
As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis
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122-03-2 4-Isopropylbenzaldehyde Basic information Product Name: 4-Isopropylbenzaldehyde Synonyms: 4-(1-methylethyl)-benzaldehyd;4-(1-Methylethyl)benzaldehyde;4-(1-methylethyl)-Benzald
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inquiryOur Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
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inquiryProduct name 4-Isopropylbenzaldehyde Synonyms Cuminaldehyde CAS 122-03-2 Molecular Formula C10H12O Molecular Weight
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Appearance:colorless to yellow liquid Storage:Inert atmosphere,2-8°C Package:200kg/Drum Application:Cuminaldehyde is a flavoring agent that is a liquid, colorless to yellow in appearance, with a strong pungent odor resembling cumin oil. It is inso
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inquiryAdvantage 1: The product passed the professional production process and quality inspection, the purity is 99% +. 2: Highly qualified engineers to provide technical documents and service. 3: We could provide sample for your test. 4: High qualit
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inquiryCompany Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
p-IsopropylbenzaldehydeAppearance:Colorless transparent liquid Storage:Keep away of light, cool place Package:according to customers' requirements Application:pharmaceutical intermediates Transportation:By air(EMS or EUB or FedEx or TNT ect...) or by
Product Name: Cuminaldehyde CAS: 122-03-2 MF: C10H12O MW: 148.2 EINECS: 204-516-9 Mol File: 122-03-2.mol Cuminaldehyde Structure Cuminaldehyde Chemical Properties Boiling point 235-236 °C(lit.) density 0.977 g/mL at 25
factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
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inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
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inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
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inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
R & D enterprises have their own stock in stockAppearance:To be subject to the object Package:Customized Application:pharmaceutical intermediates Transportation:Air Port:Shanghai;Guangzhou
Conditions | Yield |
---|---|
With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; oxygen In dichloromethane; water under 760.051 Torr; for 2h; Green chemistry; | 100% |
With dmap; C25H30F17N5O4S(1-)*K(1+); oxygen; copper(II) sulfate In water at 25℃; for 2h; chemoselective reaction; | 99% |
With titanium(IV) oxide; oxygen at 29.84℃; under 760.051 Torr; for 6h; Sealed tube; Irradiation; | 99% |
Conditions | Yield |
---|---|
Stage #1: 4-bromo-benzaldehyde With bis(tri-tert-butylphosphine)palladium(0); sodium chloride In water at 20℃; for 0.166667h; Negishi Coupling; Schlenk technique; Stage #2: isopropyllithium With zinc(II) chloride In 2-methyltetrahydrofuran; water at 10℃; for 0.00555556h; Schlenk technique; chemoselective reaction; | 98% |
4-isopropylbenzaldehyde oxime
(4-isopropylbenzaldehyde)
Conditions | Yield |
---|---|
With iron(III) chloride; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; oxygen In water; toluene at 60℃; under 760.051 Torr; for 4h; | 95% |
With tungsten(VI) chloride; zinc In acetonitrile at 20℃; for 0.333333h; | 92% |
(4-isopropylbenzaldehyde)
Conditions | Yield |
---|---|
With 1,3,5-trichloro-2,4,6-triazine; dimethyl sulfoxide In dichloromethane at 20℃; for 1h; | 94% |
2-(4-isopropylphenyl)-1,3-dithiolane
(4-isopropylbenzaldehyde)
Conditions | Yield |
---|---|
With 1,3,5-trichloro-2,4,6-triazine; dimethyl sulfoxide In dichloromethane at 20℃; for 2.45h; | 93% |
With Oxone; potassium bromide In water; acetonitrile at 20℃; for 0.333333h; | 92% |
With iodosylbenzene In dichloromethane at 20℃; for 0.25h; | 91% |
Conditions | Yield |
---|---|
With dihydrogen peroxide In acetonitrile at 65℃; for 6h; | 93% |
With sodium periodate In water; ethyl acetate; acetonitrile at 0℃; for 3.5h; | 63% |
Stage #1: 4-isopropylstyrene With BO40W12(5-)*2C12H12N6*Co(2+)*3H(1+)*10H2O In acetonitrile for 0.0833333h; Stage #2: With dihydrogen peroxide In acetonitrile at 70℃; for 7h; |
Conditions | Yield |
---|---|
With potassium hydroxide; cetyltrimethylammonim bromide; potassium nitrate In water for 4h; pH=10 - 11; Reflux; | 92% |
With 4Na(1+)*6H(1+)*NiMo6O24(10-)=Na4H6NiMo6O24; oxygen In water; acetonitrile at 20℃; under 760.051 Torr; for 12h; Irradiation; | 92% |
With potassium nitrite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; oxygen; potassium bromide In water for 5h; Reflux; | 89% |
4-i-propylbenzyl bromide
(4-isopropylbenzaldehyde)
Conditions | Yield |
---|---|
With potassium nitrite; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; oxygen In water for 4h; Reflux; | 92% |
Multi-step reaction with 2 steps 1: eosin y; oxygen / dimethyl sulfoxide / 12 h / 25 °C / Irradiation 2: eosin y / dimethyl sulfoxide / 24 h / 80 °C / Irradiation View Scheme |
Conditions | Yield |
---|---|
Stage #1: 4-bromo-benzaldehyde With C40H55Cl5N3Pd In toluene at 0℃; for 0.0833333h; Negishi Coupling; Inert atmosphere; Cooling with ice; Stage #2: isopropyl zinc bromide In tetrahydrofuran; toluene at 23℃; for 0.5h; Inert atmosphere; | 92% |
With dichloro(1,3-bis(2,6-bis(3-pentyl)phenyl)imidazolin-2-ylidene)(3-chloropyridyl)palladium(II) In tetrahydrofuran; toluene at 0 - 20℃; for 3h; Negishi coupling reaction; Inert atmosphere; | 78% |
(4-isopropylbenzaldehyde)
Conditions | Yield |
---|---|
With N-hydroxyphthalimide; oxygen; cobalt(II) benzoate In acetonitrile at 20℃; for 0.666667h; | 90% |
Conditions | Yield |
---|---|
With saccharin sulfonic acid at 90℃; for 0.0333333h; Neat (no solvent); | 90% |
With water at 20℃; for 0.166667h; Green chemistry; | 96 %Chromat. |
2-(4-isopropyl-phenyl)-[1,3]oxathiolane
(4-isopropylbenzaldehyde)
Conditions | Yield |
---|---|
With Iron(III) nitrate nonahydrate at 90℃; for 0.05h; | 90% |
4-iso-propylbenzyl trimethylsilyl ether
(4-isopropylbenzaldehyde)
Conditions | Yield |
---|---|
With N-hydroxyphthalimide; oxygen; cobalt(II) benzoate In acetonitrile at 20℃; for 0.333333h; | 89% |
With silica chromate; silica gel In dichloromethane at 20℃; for 0.666667h; | 82% |
2-(4-Isopropylbenzyloxy)-tetrahydropyran
(4-isopropylbenzaldehyde)
Conditions | Yield |
---|---|
With 1,4-dichloro-1,4-diazoniabicyclo[2,2,2]octane bis-chloride In water at 50℃; for 0.25h; pH=7; | 88% |
1-(4-isopropylphenyl)ethanol
A
4-Isopropylbenzoic acid
B
(4-isopropylbenzaldehyde)
Conditions | Yield |
---|---|
With sodium nitrate; water; oxygen In dimethyl sulfoxide at 130℃; for 24h; | A 88% B 8% |
Conditions | Yield |
---|---|
With immobilised amine transaminase from the moderate halophilic bacterium Halomonas elongata; sodium pyruvate In aq. phosphate buffer; dimethyl sulfoxide at 37℃; under 760.051 Torr; for 5h; pH=8; | 84% |
Conditions | Yield |
---|---|
With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; oxygen In water for 4h; Reflux; | A 19% B 76% |
4-isopropylbenzyl chloride
A
4-Isopropylbenzoic acid
B
(4-isopropylbenzaldehyde)
Conditions | Yield |
---|---|
With potassium hydroxide; cetyltrimethylammonim bromide; potassium nitrate In water for 4h; pH=10 - 11; Reflux; | A 2 g B 71% |
Conditions | Yield |
---|---|
Stage #1: carbon dioxide With zinc(II) cyanide; ruthenium trichloride; rhodium (III) acetate; cobalt(II) acetate; zirconium(IV) acetate for 1h; Autoclave; Stage #2: Isopropylbenzene at 50℃; under 15001.5 Torr; for 5h; | 70.2% |
4-isopropylbenzaldehyde oxime
A
p-Cyanocumen
B
(4-isopropylbenzaldehyde)
Conditions | Yield |
---|---|
With pyridine; N-chloro-succinimide In acetonitrile at 20℃; | A 70% B n/a |
(4-isopropylphenyl)acetic acid
A
1-(fluoromethyl)-4-isopropylbenzene
B
(4-isopropylbenzaldehyde)
Conditions | Yield |
---|---|
With xenon fluoride In dichloromethane at 20℃; for 14 - 18h; Inert atmosphere; | A 67% B 10% |
isopropylboronic acid
4-(trifluormethanesulfonyloxy)benzaldehyde
(4-isopropylbenzaldehyde)
Conditions | Yield |
---|---|
With potassium phosphate; C20H34O3P2; [Pd(cinnamyl)Cl]2 In toluene at 110℃; for 12h; Suzuki-Miyaura Coupling; Inert atmosphere; | 67% |
4-methylisopropylbenzene
A
(4-Isopropyl-phenyl)-nitromethan
B
4-isopropylbenzyl nitrate
C
para-methylacetophenone
D
(4-isopropylbenzaldehyde)
Conditions | Yield |
---|---|
With ammonium cerium(IV) nitrate In acetonitrile at 17℃; for 0.666667h; Irradiation; | A 3% B 62% C 6% D 6% |
With ammonium cerium(IV) nitrate In acetonitrile at 17℃; for 0.666667h; Irradiation; Further byproducts given; | A 3% B 62% C 6% D 6% |
2-hydroxy-2-(4-isopropylphenyl)acetonitrile
A
4-Isopropylbenzoic acid
B
(4-isopropylbenzaldehyde)
Conditions | Yield |
---|---|
Stage #1: 2-hydroxy-2-(4-isopropylphenyl)acetonitrile With (η(6)-benzene)chloro[1,2-bis(diphenylphosphino)ethane]ruthenium(II) chloride In benzene at 120℃; for 24h; Inert atmosphere; Schlenk technique; Stage #2: With water In dichloromethane; ethyl acetate; benzene for 24h; | A 58% B 36% |
4-isopropyl-1-cyclopropylbenzene
A
(E)-3-(4-isopropylphenyl)acrylaldehyde
B
5-(4-isopropylphenyl)isoxazoline
C
(4-isopropylbenzaldehyde)
Conditions | Yield |
---|---|
With dinitrogen tetraoxide; triethylamine In dichloromethane at -30℃; for 1h; | A 28% B 50% C 7% |
With dinitrogen tetraoxide In pentane at -30℃; for 6h; | A 41% B 40% C 10% |
With dinitrogen tetraoxide In pentane at -30℃; for 6h; | A 40% B 40% C 10% |
With dinitrogen tetraoxide In dichloromethane at -30℃; for 1h; | A 39% B 40% C 8% |
4-methylisopropylbenzene
A
1-methyl-4-isopropenylbenzene
B
2-(4-isopropylbenzyl)-1,4-benzoquinone
C
4-(2-hydroxy-2-propyl)benzene-1-carbaldehyde
D
(4-isopropylbenzaldehyde)
Conditions | Yield |
---|---|
With sodium persulfate; sulfuric acid; silver nitrate; p-benzoquinone In water at 60℃; for 0.5h; | A 5% B 45% C 10% D 20% |
4-methylisopropylbenzene
A
2-(4-isopropylbenzyl)-1,4-benzoquinone
B
4-(2-hydroxy-2-propyl)benzene-1-carbaldehyde
C
(4-isopropylbenzaldehyde)
D
cuminol
Conditions | Yield |
---|---|
With sodium persulfate; sulfuric acid; silver nitrate; p-benzoquinone In water at 60℃; for 0.5h; Further byproducts given; | A 45% B 10% C 20% D 5% |
4-methylisopropylbenzene
p-benzoquinone
A
2-(4-isopropylbenzyl)-1,4-benzoquinone
B
4-(2-hydroxy-2-propyl)benzene-1-carbaldehyde
C
(4-isopropylbenzaldehyde)
D
cuminol
Conditions | Yield |
---|---|
With sodium persulfate; sulfuric acid; silver nitrate In water at 60℃; for 0.5h; Further byproducts given; | A 45% B 10% C 20% D 5% |
Conditions | Yield |
---|---|
Stage #1: Isopropylbenzene; tris(diformylamino)methane With aluminium trichloride In 1,2-dichloro-ethane at -13 - -1℃; for 14h; Stage #2: With water | 38% |
With aluminium trichloride In 1,2-dichloro-ethane at -13 - -1℃; for 14h; | 38% |
(4-isopropylbenzaldehyde)
4-isopropylbenzaldehyde oxime
Conditions | Yield |
---|---|
With hydroxylamine hydrochloride; sodium acetate In ethanol; water Reflux; | 100% |
With hydroxylamine hydrochloride; sodium carbonate In methanol; water at 20℃; for 19.5h; | 99% |
With bismuth(lll) trifluoromethanesulfonate; acetylhydroxamic acid In methanol for 24h; Reflux; | 97% |
cis, trans-1,3-dimethylaminocyclohexane
(4-isopropylbenzaldehyde)
C28H38N2
Conditions | Yield |
---|---|
In methanol at 20℃; Molecular sieve; | 100% |
In methanol at 20℃; Molecular sieve; |
Conditions | Yield |
---|---|
at 20℃; for 12h; | 100% |
Conditions | Yield |
---|---|
With 1-methyl-3-octylimidazolium hydrogen sulfate ionic liquid [OMIm]HSO4 inside the mesochannels of SBA-15-Pr-SO3H In neat (no solvent) at 20℃; for 2h; chemoselective reaction; | 100% |
With oxygen In acetonitrile at 20℃; for 24h; Irradiation; Green chemistry; chemoselective reaction; | 95% |
With cobalt(II) chloride In acetonitrile at 20℃; | 93% |
With boron trifluoride diethyl etherate In dichloromethane Inert atmosphere; |
Conditions | Yield |
---|---|
With ammonium acetate In ethanol at 20℃; for 17h; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
With ammonium acetate In ethanol at 60℃; Inert atmosphere; Sealed tube; | 100% |
Conditions | Yield |
---|---|
With ammonium acetate In ethanol at 20℃; for 16h; Inert atmosphere; Sealed tube; | 100% |
Conditions | Yield |
---|---|
In ethanol at 20℃; for 6h; | 99% |
In methanol for 6h; | 92% |
In ethanol at 40℃; for 10h; | 80% |
at 120℃; | |
In methanol Inert atmosphere; |
Conditions | Yield |
---|---|
With C4H11FeMo6NO24(3-)*3C16H36N(1+); water; oxygen; sodium carbonate at 50℃; under 760.051 Torr; for 8h; Green chemistry; | 99% |
With 4H3N*4H(1+)*CuMo6O18(OH)6(4-); water; oxygen; sodium carbonate at 50℃; under 760.051 Torr; for 12h; | 99% |
With tris[2-(4,6-difluorophenyl)pyridinato-C2,N]-iridium(III); oxygen In acetonitrile at 20℃; Irradiation; Sealed tube; Green chemistry; chemoselective reaction; | 95% |
acetone
(4-isopropylbenzaldehyde)
(E)-4-(4-isopropylphenyl)but-3-en-2-one
Conditions | Yield |
---|---|
With sodium hydroxide In water at 20℃; for 6h; Claisen-Schmidt Condensation; | 99% |
With sodium hydroxide In water at 25℃; for 18h; | 41% |
With sodium hydroxide In water Ambient temperature; | 16% |
With sodium hydroxide In water at 25℃; for 12h; | |
With sodium hydroxide at 20℃; for 24h; Claisen-Schmidt Condensation; |
cycl-isopropylidene malonate
(4-isopropylbenzaldehyde)
3-(p-isopropylphenyl)propionic acid
Conditions | Yield |
---|---|
Stage #1: cycl-isopropylidene malonate; (4-isopropylbenzaldehyde) With formic acid; triethylamine In N,N-dimethyl-formamide at 0 - 80℃; for 14h; Stage #2: With hydrogenchloride; water In N,N-dimethyl-formamide pH=1 - 2; | 99% |
ethyl acetoacetate
(4-isopropylbenzaldehyde)
malononitrile
6-amino-2,4-dihydro-4-(4-isopropylphenyl)-3-methylpyrano[2,3-c]pyrazole-5-carbonitrile
Conditions | Yield |
---|---|
With hydrazine hydrate; heptakis(6-amino-6-deoxy)-β-cyclodextrin at 20℃; for 0.0166667h; Neat (no solvent); | 99% |
With hydrazine hydrate; 2-amino-2-hydroxymethyl-1,3-propanediol In ethanol; water at 20℃; for 2.5h; Green chemistry; | 84% |
Conditions | Yield |
---|---|
With Zn(N4,N4'-di(pyridin-4-yl)biphenyl-4,4'-dicarboxamide)(5-aminoisophthalate) In neat (no solvent) for 4h; Knoevenagel Condensation; | 99% |
With 1-butyl-1,2,4-triazolium tetrafluoroborate In ethanol; water at 70℃; for 0.25h; Reagent/catalyst; Knoevenagel Condensation; | 92% |
With tin dioxide In neat (no solvent) at 20℃; Knoevenagel Condensation; Green chemistry; | 90% |
2-Hydroxy-1,4-naphthoquinone
1,3-cylohexanedione
(4-isopropylbenzaldehyde)
Conditions | Yield |
---|---|
With silica-supported tungstic acid In neat (no solvent) at 60℃; for 0.0666667h; Sonication; Green chemistry; | 99% |
(4-isopropylbenzaldehyde)
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane
Conditions | Yield |
---|---|
With C34H28N6Zn In neat (no solvent) at 20℃; for 1h; Glovebox; Schlenk technique; | 99% |
With C24H34N5PSeTi In neat (no solvent) at 30℃; for 2h; Glovebox; Schlenk technique; chemoselective reaction; | 96% |
With [{2-(AdN=CH)–C4H3NK(THF)}n] at 30℃; for 1h; Inert atmosphere; Glovebox; Schlenk technique; | 92 %Spectr. |
triethylsilane
(4-isopropylbenzaldehyde)
triethyl((4-isopropylbenzyl)oxy)silane
Conditions | Yield |
---|---|
With C42H43BN3P2(1+)*C18HBF15(1-) In chloroform at 40℃; for 1h; Reagent/catalyst; Temperature; Schlenk technique; Glovebox; | 99% |
ethane-1,2-dithiol
(4-isopropylbenzaldehyde)
2-(4-isopropylphenyl)-1,3-dithiolane
Conditions | Yield |
---|---|
at 20℃; | 99% |
Conditions | Yield |
---|---|
With ruthenium trichloride In methanol at 20℃; for 0.05h; | 98% |
2-hydroxy-2-phenylacetophenone
(4-isopropylbenzaldehyde)
2‐(4‐isopropylphenyl)‐4,5‐diphenyl‐1H‐imidazole
Conditions | Yield |
---|---|
With 4,4'-diiodobiphenyl; ammonium acetate In ethanol for 0.5h; Heating; | 98% |
With oxaline; ammonium acetate at 110℃; for 1h; | 80% |
3-amino-2-methyl-6,7-methylenedioxyquinazolin-4(3H)-one
(4-isopropylbenzaldehyde)
3-[(4-isopropylbenzylidene)amino]-2-methyl-6,7-methylenedioxy-quinazolin-4(3H)-one
Conditions | Yield |
---|---|
With hydrogenchloride In ethanol; water at 20℃; for 1h; diastereoselective reaction; | 98% |
anthranilic acid amide
(4-isopropylbenzaldehyde)
2,3-dihydro-2-(4-isopropylphenyl)quinazolin-4(1H)-one
Conditions | Yield |
---|---|
With phosphatidylcholine In water at 80℃; for 1h; Green chemistry; | 98% |
With 1,3,5-trichloro-2,4,6-triazine In acetonitrile at 20℃; for 0.166667h; chemoselective reaction; | 90% |
With silica supported ceric ammonium nitrate (CAN*SiO2) In acetonitrile at 20℃; for 0.166667h; | 90% |
Conditions | Yield |
---|---|
With cyclohexane-1,2-dione hydrolase In aq. buffer at 30℃; for 48h; pH=6.5; Enzymatic reaction; | 98% |
1H-benzimidazol-2-amine
(4-isopropylbenzaldehyde)
malononitrile
2-amino-4-(4-isopropylphenyl)-1,4-dihydrobenzo[4,5]imidazolo[1,2-a]pyrimidine-3-carbonitrile
Conditions | Yield |
---|---|
With poly(vinylpyrrolidonium) perchlorate ([PVPH]ClO4) at 100℃; for 0.0666667h; | 98% |
With toluene-4-sulfonic acid In neat (no solvent) at 80℃; for 0.55h; Green chemistry; | 92% |
With 1-methyl-3-(trimethoxysilylpropyl)imidazolium hydrogen sulfate supported on rice husk ash In neat (no solvent) at 100℃; for 0.0833333h; Green chemistry; | 88% |
cyclohexanecarbohydrazide
(4-isopropylbenzaldehyde)
Conditions | Yield |
---|---|
In ethanol at 20℃; for 2h; | 98% |
Conditions | Yield |
---|---|
With dibutylamine In neat (no solvent) at 20℃; Green chemistry; | 98% |
1-(7-hydroxy-2,2-dimethylchroman-6-yl)ethanone
(4-isopropylbenzaldehyde)
Conditions | Yield |
---|---|
With potassium hydroxide In ethanol at 90℃; Claisen-Schmidt Condensation; Microwave irradiation; | 98% |
Conditions | Yield |
---|---|
With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; oxygen In dichloromethane; water under 760.051 Torr; for 2h; Green chemistry; | 100% |
With dmap; C25H30F17N5O4S(1-)*K(1+); oxygen; copper(II) sulfate In water at 25℃; for 2h; chemoselective reaction; | 99% |
With titanium(IV) oxide; oxygen at 29.84℃; under 760.051 Torr; for 6h; Sealed tube; Irradiation; | 99% |
Conditions | Yield |
---|---|
Stage #1: 4-bromo-benzaldehyde With bis(tri-tert-butylphosphine)palladium(0); sodium chloride In water at 20℃; for 0.166667h; Negishi Coupling; Schlenk technique; Stage #2: isopropyllithium With zinc(II) chloride In 2-methyltetrahydrofuran; water at 10℃; for 0.00555556h; Schlenk technique; chemoselective reaction; | 98% |
4-isopropylbenzaldehyde oxime
(4-isopropylbenzaldehyde)
Conditions | Yield |
---|---|
With iron(III) chloride; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; oxygen In water; toluene at 60℃; under 760.051 Torr; for 4h; | 95% |
With tungsten(VI) chloride; zinc In acetonitrile at 20℃; for 0.333333h; | 92% |
(4-isopropylbenzaldehyde)
Conditions | Yield |
---|---|
With 1,3,5-trichloro-2,4,6-triazine; dimethyl sulfoxide In dichloromethane at 20℃; for 1h; | 94% |
2-(4-isopropylphenyl)-1,3-dithiolane
(4-isopropylbenzaldehyde)
Conditions | Yield |
---|---|
With 1,3,5-trichloro-2,4,6-triazine; dimethyl sulfoxide In dichloromethane at 20℃; for 2.45h; | 93% |
With Oxone; potassium bromide In water; acetonitrile at 20℃; for 0.333333h; | 92% |
With iodosylbenzene In dichloromethane at 20℃; for 0.25h; | 91% |
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