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4-Isopropylbenzyl alcohol cas 536-60-7Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
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inquiry4-iso-propylbenzyl trimethylsilyl ether
cuminol
Conditions | Yield |
---|---|
With Nafion-H(R); silica gel In hexane at 20℃; for 0.333333h; | 98% |
With methanol; 1,3-disulfonic acid imidazolium hydrogen sulfate at 20℃; for 0.0666667h; Green chemistry; | 97% |
With poly (ethylene glycol)-sulfonated sodium montmorillonite nanocomposite In methanol at 20℃; for 0.0166667h; | 96% |
With methanol; vanadium hydrogen sulfate at 20℃; for 0.0166667h; | 90% |
With Nanoporous Na+-Montmorillonite Perchloric Acid In ethanol at 20℃; for 0.0333333h; | 87% |
Conditions | Yield |
---|---|
Stage #1: 4-bromobenzenemethanol With C44H35BrN2O2P2Pd In toluene at 20℃; for 0.5h; Suzuki-Miyaura Coupling; Inert atmosphere; Irradiation; Stage #2: isopropylboronic acid With potassium phosphate In water at 100℃; for 48h; Suzuki-Miyaura Coupling; Inert atmosphere; | 98% |
Conditions | Yield |
---|---|
With sodium tetrahydroborate In methanol at 0℃; Inert atmosphere; | 97% |
With methanol; sodium tetrahydroborate at 0℃; for 0.5h; | 97.3% |
With hydrogen In water at 20℃; under 760.051 Torr; for 10h; Green chemistry; chemoselective reaction; | 96% |
cuminol
Conditions | Yield |
---|---|
With N-iodo-succinimide In methanol at 20℃; for 24h; | 96% |
sulfonic acid functionalized nanoporous silica In methanol at 35℃; for 1.5h; | 95% |
With methanol at 20℃; for 2h; | 92% |
Conditions | Yield |
---|---|
With cis-Octadecenoic acid; palladium on activated charcoal In cyclohexane at 110℃; for 2h; Temperature; | 95% |
With 5 weight% palladium(0) nanoparticles supported on mesoporous natural phosphate In neat (no solvent) for 24h; Reflux; | 91% |
cuminol
Conditions | Yield |
---|---|
With silica gel In methanol for 4h; Reflux; | 91% |
4-iso-propyl-1-[(ethoxymethoxy)methyl]benzene
cuminol
Conditions | Yield |
---|---|
phosphotungstic acid In ethanol for 5h; Heating; | 83% |
4-Me2CHC6H4CH2OMOM
cuminol
Conditions | Yield |
---|---|
phosphotungstic acid In ethanol for 5.5h; Heating; | 81% |
Conditions | Yield |
---|---|
With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; oxygen In water for 4h; Reflux; | A 19% B 76% |
4-i-propylbenzyl bromide
cuminol
Conditions | Yield |
---|---|
With oxygen; eosin y In dimethyl sulfoxide at 25℃; for 12h; Irradiation; | 76% |
Conditions | Yield |
---|---|
With ferredoxin reductase; [2Fe-2S] ferredoxin; cytochrome P450 101B1 enzyme from Novosphingobium aromaticivorans DSM12444; oxygen; NADH; bovine liver catalase In aq. buffer at 30℃; pH=7.4; Catalytic behavior; Kinetics; Enzymatic reaction; | A 25% B 75% |
With lithium aluminium tetrahydride; oxygen; dibenzoyl peroxide 1.) 125 deg C; Multistep reaction. Title compound not separated from byproducts; | |
With lithium aluminium tetrahydride; 2,2'-azobis(isobutyronitrile); oxygen Product distribution; multistep reaction: 1) 90 deg C, 2) ether, 30 min, reflux; obj. of study: autoxidation, relative reaction rate; | A 84.4 % Chromat. B 15.6 % Chromat. |
With NADPH In dimethyl sulfoxide at 30℃; pH=7.4; Product distribution; Further Variations:; Reagents; | A 76 % Chromat. B 2 % Chromat. |
With ferredoxin reductase; ferredoxin; P450 monooxygenase CYP101B1 from a Novosphingobium bacterium, wild type; NADH; bovine liver catalase In aq. buffer at 30℃; pH=7.4; Kinetics; Reagent/catalyst; Enzymatic reaction; regioselective reaction; |
4-(i-propyl)benzyl acetate
A
4,4'-(oxybis(methylene))bis(isopropylbenzene)
B
cuminol
Conditions | Yield |
---|---|
With sodium hydroxide In methanol; water for 3h; Heating; | A 24% B 72% |
Conditions | Yield |
---|---|
With bis(tri-t-butylphosphine)palladium(0) In toluene at 20℃; for 1h; | 61% |
4-methylisopropylbenzene
A
2-(4-isopropylbenzyl)-1,4-benzoquinone
B
4-(2-hydroxy-2-propyl)benzene-1-carbaldehyde
C
(4-isopropylbenzaldehyde)
D
cuminol
Conditions | Yield |
---|---|
With sodium persulfate; sulfuric acid; silver nitrate; p-benzoquinone In water at 60℃; for 0.5h; Further byproducts given; | A 45% B 10% C 20% D 5% |
4-methylisopropylbenzene
p-benzoquinone
A
2-(4-isopropylbenzyl)-1,4-benzoquinone
B
4-(2-hydroxy-2-propyl)benzene-1-carbaldehyde
C
(4-isopropylbenzaldehyde)
D
cuminol
Conditions | Yield |
---|---|
With sodium persulfate; sulfuric acid; silver nitrate In water at 60℃; for 0.5h; Further byproducts given; | A 45% B 10% C 20% D 5% |
(1R,2S,4S,6R)-7,7-dimethyl-3-oxabicyclo[4.1.1.02.4]octane-2-methanol
B
cuminol
Conditions | Yield |
---|---|
With askanite-bentonite clay In dichloromethane at 20℃; for 0.666667h; | A 27% B 16% |
(1R)-Myrtenol
A
6,6-dimethyl-2-methylene-bicyclo[3.1.1]heptan-3-ol
B
(-)-perillyl alcohol
C
cuminol
Conditions | Yield |
---|---|
With askanite-bentonite clay In dichloromethane at 20℃; for 1h; | A 9% B 12% C 6% |
p-isopropylbenzoic acid methyl ester
A
4-Isopropylbenzoic acid
B
cuminol
Conditions | Yield |
---|---|
With methanol; copper oxide-chromium oxide barium oxide; hydrogen at 155 - 160℃; under 220652 - 294203 Torr; |
(4-isopropylbenzyl)magnesium chloride
cuminol
Conditions | Yield |
---|---|
With diethyl ether; oxygen |
Conditions | Yield |
---|---|
With potassium carbonate |
Conditions | Yield |
---|---|
With ammonia; nickel at 60℃; under 66195.7 Torr; Hydrogenation; |
Conditions | Yield |
---|---|
With potassium carbonate; acetone | |
Multi-step reaction with 2 steps 1: 55.7 percent / triethylamine / ethyl acetate / Heating 2: 72 percent / sodium hydroxide / methanol; H2O / 3 h / Heating View Scheme |
p-isopropylbenzoic acid methyl ester
cuminol
Conditions | Yield |
---|---|
With bis(cyclopentadienyl)titanium dichloride; sodium In benzene |
4-methylisopropylbenzene
A
p-cymene-8-ol
B
8-hydroperoxy-p-cymene
C
4-isopropylbenzyl nitrate
D
para-methylacetophenone
E
(4-isopropylbenzaldehyde)
F
cuminol
Conditions | Yield |
---|---|
With oxygen In acetonitrile for 5h; photochemical autooxidation; | A n/a B n/a C 9 % Spectr. D n/a E 31 % Spectr. F 9 % Spectr. |
4-methylisopropylbenzene
A
4-isopropyl-benzyl hydroperoxide
B
4-isopropylbenzyl nitrate
C
(4-isopropylbenzaldehyde)
D
cuminol
Conditions | Yield |
---|---|
With oxygen; ammonium cerium(IV) nitrate In acetonitrile for 5h; Ambient temperature; Irradiation; Further byproducts given. Title compound not separated from byproducts; | A 6 % Spectr. B 9 % Spectr. C 31 % Spectr. D 9 % Spectr. |
Conditions | Yield |
---|---|
Yield given. Multistep reaction; | |
Multi-step reaction with 3 steps 1: N-methyl-N,N,N-tributylammonium methyl sulfate / 57 °C / Electrochemical reaction 2: water / 2 h / Industry scale; Reflux 3: hydrogen / 24 h / 180 °C / 150015 Torr View Scheme | |
With p-cymene methyl hydroxylase; NADH at 25℃; for 2h; pH=7; aq. phosphate buffer; Enzymatic reaction; |
4-methylisopropylbenzene
A
CH3C6H4CH(CH3)OH
B
p-cymene-8-ol
C
cuminol
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride; oxygen; cobalt(II) stearate Product distribution; multistep reaction; other p-dialkylbenzenes; var. catalysts, solvents and temperatures; | A n/a B 61 % Chromat. C 17 % Chromat. |
4-methylisopropylbenzene
A
p-cymene-8-ol
B
para-cymen-9-ol
C
cuminol
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride; Perbenzoic acid Mechanism; Product distribution; 2.) ether, 30 min, reflux; study of the regioselectivity of autoxidation by reduction of the corresponding oxidation-mixture; |
Conditions | Yield |
---|---|
With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; oxygen In dichloromethane; water under 760.051 Torr; for 2h; Green chemistry; | 100% |
With dmap; C25H30F17N5O4S(1-)*K(1+); oxygen; copper(II) sulfate In water at 25℃; for 2h; chemoselective reaction; | 99% |
With titanium(IV) oxide; oxygen at 29.84℃; under 760.051 Torr; for 6h; Sealed tube; Irradiation; | 99% |
Conditions | Yield |
---|---|
With copper(II) bis(trifluoromethanesulfonate) at 100℃; for 0.0833333h; Microwave irradiation; | 100% |
Conditions | Yield |
---|---|
With di-tert-butyl-diazodicarboxylate In dichloromethane at 20℃; for 18h; | 100% |
With di-tert-butyl-diazodicarboxylate In dichloromethane at 20℃; for 18h; | 100% |
Conditions | Yield |
---|---|
Stage #1: cuminol With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; for 1h; Stage #2: 5-bromo-2-fluoropyridine In N,N-dimethyl-formamide; mineral oil at 20℃; for 72h; | 100% |
Stage #1: cuminol With sodium hydride In N,N-dimethyl-formamide; mineral oil at 0 - 20℃; for 1h; Stage #2: 5-bromo-2-fluoropyridine In N,N-dimethyl-formamide; mineral oil at 20℃; for 72h; | 100% |
Conditions | Yield |
---|---|
With C23H26IrN2(1+)*C32H12BF24(1-) In 1,2-dichloro-ethane for 0.0166667h; Catalytic behavior; Schlenk technique; Inert atmosphere; | 100% |
1,1,1,3,3,3-hexamethyl-disilazane
cuminol
4-iso-propylbenzyl trimethylsilyl ether
Conditions | Yield |
---|---|
With polyvinylpolypyrrolidonium tribromide In acetonitrile at 20℃; for 0.0833333h; | 99% |
iodine In dichloromethane at 20℃; for 0.0333333h; Substitution; | 98% |
With L-Aspartic acid In acetonitrile at 20℃; for 0.1h; | 98% |
Conditions | Yield |
---|---|
With Co2Rh2 nanoparticles immobilized on charcoal at 100℃; for 24h; Inert atmosphere; Schlenk technique; Green chemistry; chemoselective reaction; | 99% |
With 1,10-Phenanthroline; potassium tert-butylate; nickel dibromide In toluene at 130℃; for 48h; chemoselective reaction; | 84% |
With potassium carbonate at 160℃; for 12h; | 82% |
1-Phenylethanol
cuminol
3-(4-isopropylphenyl)-1-phenylprop-2-en-1-one
Conditions | Yield |
---|---|
With oxygen; lithium hydroxide In water; tert-butyl alcohol at 70℃; | 99% |
cuminol
Conditions | Yield |
---|---|
With bis(1,5-cyclooctadiene)rhodium(I) trifluoromethanesulfonate; hydrogen; iodine; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl In 1,2-dichloro-ethane at 20℃; under 22502.3 Torr; Autoclave; Schlenk technique; | 99% |
cuminol
4-i-propylbenzyl bromide
Conditions | Yield |
---|---|
With 1,1,1,2,2,2-hexamethyldisilane In chloroform for 1.5h; Reflux; | 98% |
Stage #1: cuminol With copper(l) chloride; diisopropyl-carbodiimide at 20℃; for 0.5h; Stage #2: With N-Bromosuccinimide In 1,2-dichloro-ethane at 80℃; for 2h; | 85% |
With phosphorus tribromide In diethyl ether at 0℃; for 0.0833333h; | 84% |
Conditions | Yield |
---|---|
With diethylene glycol dimethyl ether at 70℃; for 0.5h; Sonication; | 98% |
With methyl 3,5-bis((1H-1,2,4-triazol-1-yl)methyl)benzoate; oxygen; sodium acetate; nickel dibromide at 120℃; under 760.051 Torr; for 72h; | 94% |
With C14H14N6O2; oxygen; sodium acetate; palladium diacetate at 120℃; under 760.051 Torr; for 72h; | 94% |
Conditions | Yield |
---|---|
With tri-tert-butyl phosphine; potassium tert-butylate; nickel diacetate In 1,4-dioxane; toluene at 80℃; for 12h; Inert atmosphere; Glovebox; Schlenk technique; | 98% |
Conditions | Yield |
---|---|
With decamolybdodivanadogermanic acid nanoparticles at 24.84℃; for 0.0583333h; Neat (no solvent); | 97% |
With polyvinylpolypyrrolidone-bound boron trifluoride In acetonitrile at 20℃; for 1.5h; | 97% |
With lithium trifluoromethanesulfonate at 20℃; for 13h; | 96% |
Conditions | Yield |
---|---|
With Co2Rh2 nanoparticles immobilized on charcoal at 140℃; for 24h; Inert atmosphere; Schlenk technique; Green chemistry; chemoselective reaction; | 97% |
Conditions | Yield |
---|---|
With Co2Rh2 nanoparticles immobilized on charcoal at 80℃; for 24h; Schlenk technique; Inert atmosphere; Green chemistry; chemoselective reaction; | 96% |
Conditions | Yield |
---|---|
With thionyl chloride In dichloromethane at 0℃; for 0.833333h; Temperature; | 95% |
With 1-methyl-pyrrolidin-2-one; benzenesulfonyl chloride In 1,2-dichloro-ethane at 80℃; for 1.5h; | 92% |
With thionyl chloride for 1h; Chlorination; Heating; | 87% |
Conditions | Yield |
---|---|
With air; copper diacetate; potassium carbonate at 150℃; for 12h; | 95% |
With copper diacetate; potassium carbonate at 150℃; for 12h; | 95% |
With potassium carbonate at 160℃; for 12h; | 93% |
cuminol
4-(i-propyl)benzyl acetate
Conditions | Yield |
---|---|
With phenyl-trimethyl-ammonium perbromide In acetone at 20℃; for 0.833333h; | 95% |
Conditions | Yield |
---|---|
With C27H24Cl3F6IrN2; sodium hydroxide In toluene at 135℃; for 8h; | 95% |
With C21H18MnN5O4; potassium tert-butylate In toluene at 110℃; under 750.075 Torr; for 24h; Inert atmosphere; | 78% |
With N,N,N,N,-tetramethylethylenediamine; potassium hydroxide; nickel dibromide In octane at 130℃; for 18h; Schlenk technique; Inert atmosphere; | 78% |
With C30H43ClCoN2P3(1+)*Cl(1-); potassium tert-butylate In toluene at 110℃; for 24h; Inert atmosphere; Glovebox; Sealed tube; | 79 %Spectr. |
Conditions | Yield |
---|---|
With nanolayered cobalt-molybdenum sulphide with Co/(Mo+Co) mole ratio 0.83 In Hexadecane; toluene at 180℃; under 2625.26 Torr; for 18h; Inert atmosphere; Autoclave; chemoselective reaction; | 95% |
cuminol
p-Cyanocumen
Conditions | Yield |
---|---|
With copper(II) choride dihydrate; ammonium formate; potassium carbonate In neat (no solvent) at 135℃; under 760.051 Torr; for 24h; Sealed tube; Schlenk technique; Green chemistry; | 94% |
With ammonia at 250℃; Inert atmosphere; | 83% |
With ammonium hydroxide; sodium periodate; potassium iodide at 60℃; for 3h; | 77% |
Conditions | Yield |
---|---|
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 0 - 20℃; for 1h; Inert atmosphere; | 94% |
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 0 - 20℃; Mitsunobu Displacement; | |
With di-isopropyl azodicarboxylate; triphenylphosphine In tetrahydrofuran at 0 - 20℃; for 3h; Mitsunobu Displacement; Inert atmosphere; | |
With triphenylphosphine In tetrahydrofuran at 0 - 20℃; |
acetic anhydride
cuminol
A
4-(i-propyl)benzyl acetate
B
acetic acid
Conditions | Yield |
---|---|
With 3-((3-(trisilyloxy)propyl)propionamide)-1-methylimidazolium chloride ionic liquid supported on magnetic nanoparticle Fe2O3 at 20℃; for 0.416667h; | A 93% B n/a |
Conditions | Yield |
---|---|
With CeO2 nanorods anchored on mesoporous carbon; air In toluene at 80℃; under 760.051 Torr; for 2h; | 93% |
With air; iron catalyst supported on mesoporous carbon In toluene at 80℃; under 750.075 Torr; for 8h; Green chemistry; | 84.2% |
With air; Mg-Al acid-base bifunctional oxide catalyst In toluene under 750.075 Torr; for 12h; | 76.1% |
Conditions | Yield |
---|---|
With Co2Rh2 nanoparticles immobilized on charcoal at 140℃; for 24h; Schlenk technique; Inert atmosphere; Green chemistry; chemoselective reaction; | 93% |
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