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trifluoromethyl hypochlorite
trifluoromethanol
Conditions | Yield |
---|---|
With hydrogenchloride; chlorotrifluoromethane | |
With hydrogenchloride In various solvent(s) |
methane
trifluoroketone
A
methyl radical
B
trifluoromethanol
Conditions | Yield |
---|---|
at 86.9℃; Kinetics; Thermodynamic data; Irradiation; in buffer gas (He); | |
In various solvent(s) at -38.1℃; under 45.004 Torr; Kinetics; Thermodynamic data; Irradiation; further temperatures; Arrhenius expression, ΔH; |
Conditions | Yield |
---|---|
at 86.9℃; Kinetics; Thermodynamic data; Irradiation; in buffer gas (He); | |
at 22.9℃; Rate constant; |
propane
trifluoroketone
A
n-Propyl-Radikal
B
trifluoromethanol
Conditions | Yield |
---|---|
at 97.9℃; Kinetics; Thermodynamic data; Irradiation; in buffer gas (He); |
Isobutane
trifluoroketone
A
t-Butyl radical
B
trifluoromethanol
Conditions | Yield |
---|---|
at 93.9℃; Kinetics; Thermodynamic data; Irradiation; in buffer gas (He); |
Conditions | Yield |
---|---|
at 23.9℃; Mechanism; Rate constant; other alkenes; also eith NO, O2; |
Bromotrifluoromethane
A
hypofluorous acid trifluoromethyl ester
B
Carbonyl fluoride
C
carbonyl bromide fluoride
D
trifluoromethan
E
trifluoromethanol
Conditions | Yield |
---|---|
With hydrogen; oxygen at 469℃; under 500 Torr; Thermodynamic data; Product distribution; E(act); further reaction times,; |
1,1,1,2-tetrafluoroethane
A
Carbonyl fluoride
B
formyl fluoride
C
trifluoroacetyl fluoride
D
trifluoromethanol
E
Bis-trifluormethyl-trioxid
Conditions | Yield |
---|---|
With air; water; chlorine at 22.9℃; under 700 Torr; Product distribution; Irradiation; other partial pressures of the components; reaction without water; |
bis(trifluoromethyl)peroxide
methyl 3,3,3-trifluoropyruvate
A
trifluoromethanol
B
2-(trifluoroacetyloxy)-2-methyl-1-propyl radical
Conditions | Yield |
---|---|
In 1,1,2-Trichloro-1,2,2-trifluoroethane at -11℃; Product distribution; Irradiation; in EPR cavity; variation of temperature;; |
Conditions | Yield |
---|---|
With Isobutane at 23.9℃; Rate constant; |
trifluoroketone
trifluoromethanol
Conditions | Yield |
---|---|
With methane at -41.8℃; Mechanism; Rate constant; further temperatures; |
1,1,1,2-tetrafluoroethane
trifluoroketone
A
trifluoromethanol
B
1,2,2,2-tetrafluoro-ethyl
Conditions | Yield |
---|---|
at 21.9℃; Rate constant; |
2,2,2-Trifluoroacetaldehyde
trifluoroketone
A
trifluoromethanol
B
trifluoroacetyl radical
Conditions | Yield |
---|---|
Rate constant; |
Conditions | Yield |
---|---|
With nitric acid at 21.9℃; under 0.4 Torr; Rate constant; other reagents; |
Conditions | Yield |
---|---|
In gas at 24.9℃; Thermodynamic data; ΔH; |
1,1,1,2,2-pentafluoroethane
A
Carbonyl fluoride
B
trifluoromethanol
C
Bis-trifluormethyl-trioxid
D
Perfluormethyl-perfluorethyl-trioxid
Conditions | Yield |
---|---|
With air; chlorine at 21.85℃; under 700 Torr; Kinetics; Further Variations:; Reagents; radical reaction; UV-irradiation; |
Conditions | Yield |
---|---|
at 22.9℃; Rate constant; |
Conditions | Yield |
---|---|
With ozone; dinitrogen monoxide at 21.9℃; under 37.5 Torr; for 0.000833333h; Rate constant; Mechanism; Irradiation; further at 14 K, with <18O>O3, var. conc.; |
Conditions | Yield |
---|---|
With water at 22.9℃; under 700 Torr; Rate constant; |
Conditions | Yield |
---|---|
With water at 81.9℃; Rate constant; Mechanism; |
Conditions | Yield |
---|---|
With nitrogen(II) oxide at 23.9℃; Rate constant; Product distribution; Mechanism; variation of p and NO concentration; |
2,2,3,3,3-Pentafluoro-propionaldehyde
A
Carbonyl fluoride
B
pentafluoropropionic acid
C
trifluoromethanol
Conditions | Yield |
---|---|
With hydrogen; oxygen; chlorine at 22.85℃; Product distribution; Further Variations:; Pressures; var. concentration ratio H2:C2F5CHO; UV-irradiation; |
Conditions | Yield |
---|---|
With hydrogen fluoride at -196 - 0℃; | |
With hydrogen fluoride at -196 - 20℃; Autoclave; Sealed tube; |
4,6-dibromobenzo[c][1,2,5]oxadiazole
3-Formylphenylboronic acid
trifluoromethanol
Conditions | Yield |
---|---|
With dmap; sodium tetrahydroborate; tetrabutyl ammonium fluoride; sodium carbonate; triethylamine; aniline |
3-ethyl-3-(hydroxymethyl)oxetane
trifluoromethanol
1,3-dimethylperfluorobenzene
Conditions | Yield |
---|---|
Stage #1: 3-ethyl-3-(hydroxymethyl)oxetane; 2,4,5,6-tetrafluoro-m-xylene With potassium hydride In tetrahydrofuran at 20℃; for 22h; Inert atmosphere; Cooling with ice; Stage #2: trifluoromethanol With potassium hydride In tetrahydrofuran at 20℃; for 20h; | 86% |
Cyclopentanecarboxylic acid chloride
trifluoromethanol
4-chloro-7-fluoro-6-nitroquinazoline
Conditions | Yield |
---|---|
Stage #1: trifluoromethanol; 2-methyl-5,6,7-trihydropyrido[2,3-d]pyrimidine; 4-chloro-7-fluoro-6-nitroquinazoline Stage #2: With iron(III) chloride; hydrazine hydrate; pyrographite Stage #3: Cyclopentanecarboxylic acid chloride | 48.7% |
Conditions | Yield |
---|---|
With 2,6-dimethylpyridine; water at 70℃; Kinetics; | A 14 % Chromat. B 86 % Chromat. |
trifluoromethanol
Conditions | Yield |
---|---|
With 2,6-dimethylpyridine; water at 80℃; Rate constant; | A 15 % Chromat. B 85 % Chromat. |
trifluoromethanol
Trifluoro-methanesulfonic acid 4-trimethylsilanyl-bicyclo[2.2.1]hept-1-yl ester
A
4-Trimethylsilanyl-bicyclo[2.2.1]heptan-1-ol
Conditions | Yield |
---|---|
With 2,6-dimethylpyridine; water at 55℃; Kinetics; | A 18 % Chromat. B 82 % Chromat. |
Conditions | Yield |
---|---|
at 22.9℃; Rate constant; | |
In various solvent(s) at 298℃; for 0.833333h; Rate constant; |
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