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Wuhan Han Sheng New Material Technology Co.,Ltd

Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We

Imidodisulfurylfluoride CAS NO.14984-73-7

Cas:14984-73-7

Min.Order:10 Kilogram

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Shanghai Upbio Tech Co.,Ltd

1.In No Less 10 years exporting experience. you can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specializ

Imidodisulfurylfluoride

Cas:14984-73-7

Min.Order:1 Gram

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Qingdao Beluga Import and Export Co., LTD

Imidodisulfurylfluoride CAS:14984-73-7 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic i

Imidodisulfurylfluoride CAS:14984-73-7

Cas:14984-73-7

Min.Order:1 Gram

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Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

Imidodisulfurylfluoride

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Min.Order:1 Kilogram

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Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

Imidodisulfurylfluoride

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Hebei Quanhe Biotechnology Co. LTD

1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures s

Imidodisulfurylfluoride

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Min.Order:1 Kilogram

FOB Price: $10.0 / 100.0

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Triumph International Development Limilted

Appearance:off-white to white solid Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application:Used for Synthesis API and Research Transportation:By Sea/Air/Courier Port:Qingdao

Imidodisulfurylfluoride 14984-73-7

Cas:14984-73-7

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Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

Imidodisulfurylfluoride

Cas:14984-73-7

Min.Order:10 Gram

FOB Price: $100.0

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SHANGHAI SYSTEAM BIOCHEM CO., LTD

We are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov

Imidodisulfurylfluoride CAS NO.14984-73-7

Cas:14984-73-7

Min.Order:100 Gram

FOB Price: $100.0 / 2000.0

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EAST CHEMSOURCES LIMITED

factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B

Imidodisulfurylfluoride CAS NO.14984-73-7

Cas:14984-73-7

Min.Order:1 Kilogram

FOB Price: $18.0 / 20.0

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Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

Imidodisulfurylfluoride CAS NO.14984-73-7

Cas:14984-73-7

Min.Order:1 Gram

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KAISA GROUP INC

1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer

Imidodisulfurylfluoride CAS NO.14984-73-7

Cas:14984-73-7

Min.Order:1 Metric Ton

FOB Price: $1.5

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Bluecrystal chem-union

We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp

Imidodisulfurylfluoride CAS NO.14984-73-7

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Hebei Mojin Biotechnology Co.,Ltd

1, High quality with competitive price:2, Fast and safe delivery3.Excellent pre-sales and after-sales service4. Well-trained and professional technologist and sales with rich experience in the field for 5-10 yearsAppearance:see detailed specification

Imidodisulfurylfluoride

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GIHI CHEMICALS CO.,LIMITED

Lower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe

Imidodisulfurylfluoride

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Hangzhou J&H Chemical Co., Ltd.

J&H CHEM is one of China's leading providers of integrated fine chemical services including offering, research and development, Custom manufacturing business, as well as other Value-added customer services, for diversified range products of chemicals

Imidodisulfurylfluoride

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Xi`an Eastling Biotech Co., Ltd.

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:Beijing or Guangzhou

Imidodisulfurylfluoride

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Henan Tianfu Chemical Co., Ltd.

1.Our services:A.Supply sampleB.The packing also can be according the customers` requirmentC.Any inquiries will be replied within 24 hoursD.we provide Commerical Invoice, Packing List, Bill of loading, COA , Health certificate and Origin certificate.

Imidodisulfurylfluoride

Cas:14984-73-7

Min.Order:0

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Xian Changyue Biological Technology Co., Ltd.

best seller Application:API

Imidodisulfurylfluoride

Cas:14984-73-7

Min.Order:0

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Hunan chemfish Pharmaceutical co.,Ltd

Hunan chemfish Pharmaceutical co.,Ltd.located in Lugu High-tech industral park ,Hunan province . with its own R&D center and more than 10000㎡manufacture plant . Chemfish owns 40 reactors from 1000L to 8000L. With complete auxiliary equipment as

Imidodisulfurylfluoride

Cas:14984-73-7

Min.Order:0 Metric Ton

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Antimex Chemical Limied

Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali

Imidodisulfurylfluoride

Cas:14984-73-7

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Hubei Langyou International Trading Co., Ltd

Imidodisulfurylfluoride CAS NO.14984-73-7 Application:Imidodisulfurylfluoride CAS NO.14984-73-7

Imidodisulfurylfluoride CAS NO.14984-73-7

Cas:14984-73-7

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DB BIOTECH CO., LTD

best seller Application:API

Imidodisulfurylfluoride

Cas:14984-73-7

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NANJING SUNNY PHARMATECH CO., LTD

We are professional supplier in China for this product, we are dedicated to providing customers with the best quality, price, and service. Please feel free to send us inquiries.Appearance:Please contact us for product details Package:As per shipment

Imidodisulfurylfluoride

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Henan Kanbei Chemical Co.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

Imidodisulfurylfluoride

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Hangzhou ZeErRui Chemical Co., Ltd.

Hangzhou ZeErRui Chemical Co., Ltd. is focused on customization, research and development and production of APIs and advanced intermediates, which can effectively compensate for the deficiencies of traditional CRO and CMO. Priority of high-tech barri

Imidodisulfurylfluoride

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Koning Pharmchem Co., Ltd.

Imidodisulfurylfluoride CAS NO.14984-73-7Appearance:off-white fine crystalline powder Storage:Dry and ventilated Package:Standard or as customer's require Application:intermediates Transportation:Delivery by EMS, DHL, FEDEX, UPS, TNT

Imidodisulfurylfluoride CAS NO.14984-73-7

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Hunan Longxianng Runhui Trading Co.,Ltd

Imidodisulfurylfluoride CAS NO.14984-73-7Appearance:off-white fine crystalline powder Storage:Dry and ventilated Package:Standard or as customer's require Application:intermediates Transportation:By express (Door to door) such as FEDEX, DHL, EMS for

Imidodisulfurylfluoride CAS NO.14984-73-7

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Shanghai Chinqesen Biotechnology Co., Ltd.

Good Quality Package:1kg/bag Application:Medical or chemical Transportation:Air/Train/Sea Port:Shenzhen

14984-73-7

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Saiwante (shanghai) New Material Technology Co., Ltd.

Stable supply of goods and provision of high-quality services Application:As raw materials in the field of medicine and biology

Imidodisulfurylfluoride CAS NO.14984-73-7

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Synthetic route

1,1,1,3,3,3-hexamethyl-disilazane
999-97-3

1,1,1,3,3,3-hexamethyl-disilazane

A

trimethylsilyl fluoride
420-56-4

trimethylsilyl fluoride

B

bis(fluorosulfonyl)amide
14984-73-7

bis(fluorosulfonyl)amide

Conditions
ConditionsYield
With fluorosulfonyl fluoride In acetonitrile at 20 - 90℃; for 3h; Autoclave;A n/a
B 98%
bis(chlorosulfonyl)amine
15873-42-4

bis(chlorosulfonyl)amine

bis(fluorosulfonyl)amide
14984-73-7

bis(fluorosulfonyl)amide

Conditions
ConditionsYield
With perfluorooctylsulfonyl fluoride; hydrogen fluoride at 65 - 70℃; for 15h; Time;95.3%
With hydrogen fluoride; dimethyl sulfate at 90℃; for 16h; Reagent/catalyst; Inert atmosphere;90%
With zinc(II) fluoride In acetic acid butyl ester at 25℃; for 6h; Product distribution / selectivity; Inert atmosphere;79%
1,1,1,3,3,3-hexamethyl-disilazane
999-97-3

1,1,1,3,3,3-hexamethyl-disilazane

bis(fluorosulfonyl)amide
14984-73-7

bis(fluorosulfonyl)amide

Conditions
ConditionsYield
With fluorosulfonyl fluoride In ethyl acetate at 100℃; for 3h; Solvent; Temperature; Autoclave;95%
bis(chlorosulfonyl)amine
15873-42-4

bis(chlorosulfonyl)amine

bismuth trifluoride

bismuth trifluoride

bis(fluorosulfonyl)amide
14984-73-7

bis(fluorosulfonyl)amide

Conditions
ConditionsYield
at 20℃; for 12h; Concentration; Inert atmosphere;90%
at 20 - 50℃;Ca. 93 g
bis(chlorosulfonyl)amine
15873-42-4

bis(chlorosulfonyl)amine

hydrogen fluoride
7664-39-3

hydrogen fluoride

bis(fluorosulfonyl)amide
14984-73-7

bis(fluorosulfonyl)amide

Conditions
ConditionsYield
With chlorosulfonic acid; isocyanate de chlorosulfonyle at 160℃; under 60006 Torr; for 0.25h; Reagent/catalyst; Temperature; Pressure; Time;89%
at 130℃; for 2h; Product distribution / selectivity; Autoclave;55%
fluorosulphonic acid
7789-21-1

fluorosulphonic acid

urea
57-13-6

urea

A

sodium fluorosulfonate
14483-63-7

sodium fluorosulfonate

B

bis(fluorosulfonyl)amide
14984-73-7

bis(fluorosulfonyl)amide

Conditions
ConditionsYield
With sodium chloride In dichloromethane distn. of a react.-mixt. of urea and HSO3F under vac.; distillate dissolved in CH2Cl2; NaCl added; stirred for 6 h under reflux;; NaSO3F filtered off; filtrate cooled to -80°C; filtn., recrystn. (CFCl3, -80°C).;A n/a
B 87.8%
bis(chlorosulfonyl)amine
15873-42-4

bis(chlorosulfonyl)amine

zinc(II) fluoride

zinc(II) fluoride

ammonia
7664-41-7

ammonia

A

{Zn(NH3)4}(2+)*2Cl(1-)={Zn(NH3)4}Cl2

{Zn(NH3)4}(2+)*2Cl(1-)={Zn(NH3)4}Cl2

B

bis(fluorosulfonyl)amide
14984-73-7

bis(fluorosulfonyl)amide

Conditions
ConditionsYield
Stage #1: bis(chlorosulfonyl)amine; zinc(II) fluoride In acetic acid butyl ester at 25℃; for 6h; Inert atmosphere;
Stage #2: ammonia In acetic acid butyl ester; water Product distribution / selectivity;
A n/a
B 81%
chlorosulfonic acid
7790-94-5

chlorosulfonic acid

aminosulfonic acid
5329-14-6

aminosulfonic acid

thionyl fluoride
7783-42-8

thionyl fluoride

bis(fluorosulfonyl)amide
14984-73-7

bis(fluorosulfonyl)amide

Conditions
ConditionsYield
In 1,2-dichloro-ethane at 80℃; under 16501.7 Torr; for 17h; Solvent; Autoclave;77%
bis(chlorosulfonyl)amine
15873-42-4

bis(chlorosulfonyl)amine

antimony(III) fluoride
7783-56-4

antimony(III) fluoride

bis(fluorosulfonyl)amide
14984-73-7

bis(fluorosulfonyl)amide

Conditions
ConditionsYield
In neat (no solvent) absence of air and moisture; slight excess amine, stirring for 4 h; fractional distn. (25°C, 0.01 Torr), decantation from residual SbCl3;70%
potassium bis(fluorosulfuryl)amide

potassium bis(fluorosulfuryl)amide

fluorosulphonic acid
7789-21-1

fluorosulphonic acid

bis(fluorosulfonyl)amide
14984-73-7

bis(fluorosulfonyl)amide

Conditions
ConditionsYield
In neat (no solvent) under dry N2; KN(SO2F)2 placed in dry Schlenk vessel and HSO3F added under stream of dry nitrogen; mixture stirred with a glass stick and allowed to stay for one hour; HN(SO2F)2 distilled off under vacuum; contains small amounts of HSO3F according to (19)F-NMR;62%
fluorosulfonyl fluoride
640723-20-2, 2699-79-8, 12769-73-2

fluorosulfonyl fluoride

aminosulfonic acid
5329-14-6

aminosulfonic acid

fluorosulphonic acid
7789-21-1

fluorosulphonic acid

bis(fluorosulfonyl)amide
14984-73-7

bis(fluorosulfonyl)amide

Conditions
ConditionsYield
In 1,2-dichloro-ethane at 92℃; under 27752.8 Torr; for 10h; Solvent; Autoclave;53%
thionyl chloride
7719-09-7

thionyl chloride

fluorosulphonic acid
7789-21-1

fluorosulphonic acid

urea
57-13-6

urea

A

imido-bis(sulfuric acid) fluoride chloride
237763-01-8

imido-bis(sulfuric acid) fluoride chloride

B

bis(fluorosulfonyl)amide
14984-73-7

bis(fluorosulfonyl)amide

Conditions
ConditionsYield
In thionyl chloride under dry N2; urea placed into a flask and flask immersed to a cold water bath; thionyl chloride added; HSO3F added dropwise, then the flask fitted with a reflux condenser, connected to a CaCl2 drying tube; heated at110°C for 42 h; reaction mixture fractionally distilled under vacuum; main fraction collected in the range 45-65°C/650 Pa; mixture of HN(SO2F)2, HN(SO2Cl)(SO2F), HSO3F in a ratio of 2.9:2.3:1 according to (19)F-NMR;
thionyl chloride
7719-09-7

thionyl chloride

aminosulfonic acid
5329-14-6

aminosulfonic acid

fluorosulphonic acid
7789-21-1

fluorosulphonic acid

A

imido-bis(sulfuric acid) fluoride chloride
237763-01-8

imido-bis(sulfuric acid) fluoride chloride

B

bis(fluorosulfonyl)amide
14984-73-7

bis(fluorosulfonyl)amide

Conditions
ConditionsYield
In thionyl chloride amidosulfuric acid placed into a flask and thionyl dichloride added under dry argon; HSO3F added dropwise, then the flask fitted with a reflux condenser, connected to a CaCl2 drying tube; heated at 120°C for 38 h; reaction mixture fractionally distilled under vacuum; main fraction collected in the range 47-80°C/650 Pa; mixture of HN(SO2F)2, HN(SO2Cl)(SO2F), HSO3F in a ratio of 4.8:10.5:1 according to (19)F-NMR;
fluorosulfonyl isocyanate
1495-51-8

fluorosulfonyl isocyanate

fluorosulphonic acid
7789-21-1

fluorosulphonic acid

bis(fluorosulfonyl)amide
14984-73-7

bis(fluorosulfonyl)amide

Conditions
ConditionsYield
In not given byproducts: CO2; distilled;
potassium fluoride

potassium fluoride

bis(chlorosulfonyl)amine
15873-42-4

bis(chlorosulfonyl)amine

bis(fluorosulfonyl)amide
14984-73-7

bis(fluorosulfonyl)amide

Conditions
ConditionsYield
In acetonitrile at 25℃; for 24h;
potassium bis(fluorosulfuryl)amide

potassium bis(fluorosulfuryl)amide

perchloric acid
7601-90-3

perchloric acid

bis(fluorosulfonyl)amide
14984-73-7

bis(fluorosulfonyl)amide

fluorosulfonyl fluoride
640723-20-2, 2699-79-8, 12769-73-2

fluorosulfonyl fluoride

ammonia
7664-41-7

ammonia

bis(fluorosulfonyl)amide
14984-73-7

bis(fluorosulfonyl)amide

Conditions
ConditionsYield
With N,N,N'N'-tetramethyl-1,3-propanediamine In acetonitrile at 11 - 25℃; under 123 - 760 Torr; for 13h; Product distribution / selectivity; Industry scale;
fluorosulphonic acid
7789-21-1

fluorosulphonic acid

urea
57-13-6

urea

bis(fluorosulfonyl)amide
14984-73-7

bis(fluorosulfonyl)amide

Conditions
ConditionsYield
at 120℃; Large scale;
dimethylmercury
593-74-8

dimethylmercury

bis(fluorosulfonyl)amide
14984-73-7

bis(fluorosulfonyl)amide

MeHg(N(SO2F)2)

MeHg(N(SO2F)2)

Conditions
ConditionsYield
In dichloromethane at 0 - 20℃; Schlenk technique; Inert atmosphere;100%
tetramethylstannane
594-27-4

tetramethylstannane

bis(fluorosulfonyl)amide
14984-73-7

bis(fluorosulfonyl)amide

trimethyltin(IV) di(fluorosulfonyl)amide
7240-46-2

trimethyltin(IV) di(fluorosulfonyl)amide

Conditions
ConditionsYield
In dichloromethane N2 atm.; equimolar ratio, refluxing (4 h); evapn.; elem. anal.;97%
bis(fluorosulfonyl)amide
14984-73-7

bis(fluorosulfonyl)amide

cyhexatin
13121-70-5

cyhexatin

tricyclohexyltin(IV)-di(fluorosulfonyl)amide
187884-60-2

tricyclohexyltin(IV)-di(fluorosulfonyl)amide

Conditions
ConditionsYield
With Na2SO4 In dichloromethane N2 atm.; equimolar ratio, stirring (1 h); filtn., evapn. (vac.); elem. anal.;97%
ammonia
7664-41-7

ammonia

bis(fluorosulfonyl)amide
14984-73-7

bis(fluorosulfonyl)amide

ammonium imido-bis(sulfuric acid fluoride)

ammonium imido-bis(sulfuric acid fluoride)

Conditions
ConditionsYield
In trichlorofluoromethane dropwise addn. of CFCl3 to HN(SO2F)2 (exclusion of moisture), NH3 flow is passed into this soln. at room temp. until ppt. dissolves; evapn. under reduced pressure, washing with CFCl3, elem. anal.;96.5%
bis(fluorosulfonyl)amide
14984-73-7

bis(fluorosulfonyl)amide

bis(fluorosulfonyl)imide lithium salt

bis(fluorosulfonyl)imide lithium salt

Conditions
ConditionsYield
With lithium acetate; acetic acid at 0 - 5℃; for 4h; Reagent/catalyst;94.9%
With lithium hydroxide In water Product distribution / selectivity;90%
With lithium fluoride; carbonic acid dimethyl ester at 0 - 5℃; for 3h; Reagent/catalyst;
zinc(II) trifluoroacetate
21907-47-1

zinc(II) trifluoroacetate

bis(fluorosulfonyl)amide
14984-73-7

bis(fluorosulfonyl)amide

zinc salt of bis[di(fluorosulfonyl)]amine

zinc salt of bis[di(fluorosulfonyl)]amine

Conditions
ConditionsYield
In trifluoroacetic acid byproducts: CF3COOH; Excess of HN(SO2F)2 is added to Zn(OOCCF3)2, the mixture is refluxed for 16 h.; compd. is filtered, washed with CF3COOH, CH2Cl2, dried in vacuo at 80°C, elem. anal.;92%
lithium carbonate
554-13-2

lithium carbonate

bis(fluorosulfonyl)amide
14984-73-7

bis(fluorosulfonyl)amide

bis(fluorosulfonyl)imide lithium salt

bis(fluorosulfonyl)imide lithium salt

Conditions
ConditionsYield
In water at -78 - 20℃; pH=7;92%
In water pH=7;
cobalt trifluoroacetate
6185-58-6, 24517-83-7, 50517-80-1

cobalt trifluoroacetate

bis(fluorosulfonyl)amide
14984-73-7

bis(fluorosulfonyl)amide

cobalt(II) bis(fluorosulphuryl)imide

cobalt(II) bis(fluorosulphuryl)imide

Conditions
ConditionsYield
In trifluoroacetic acid Addn. of excess HN(SO2F)2 to Co(O2CCF3) soln. under N2, refluxing (14 h), pink solid forms.; Filtn. under positive N2 pressure, washing (trifluoroacetic acid, CH2Cl2), drying in vac., elem. anal.;91%
Tetramethylblei-(IV)
75-74-1

Tetramethylblei-(IV)

bis(fluorosulfonyl)amide
14984-73-7

bis(fluorosulfonyl)amide

trimethyllead(IV)-di(fluorosulfonyl)amide
187884-58-8

trimethyllead(IV)-di(fluorosulfonyl)amide

Conditions
ConditionsYield
In dichloromethane N2 atm.; refluxing (3 h); evapn., recrystn. (CH2Cl2/petroleum ether 3/1); elem. anal.;87%
xenon difluoride
13709-36-9

xenon difluoride

bis(fluorosulfonyl)amide
14984-73-7

bis(fluorosulfonyl)amide

fluoro[imidobis(sulfuryl fluoride)]xenon(II)
53719-78-1

fluoro[imidobis(sulfuryl fluoride)]xenon(II)

Conditions
ConditionsYield
In Dichlorodifluoromethane byproducts: HF; HN(SO2F)2 syringed onto vessel with XeF2 cooled to -196°C, dry CF2Cl2 condensed onto sample at -196°C, warmed to 0°C with vigorously agitation, when formed HF extd. into upper CF2Cl2 layer, mixt. stood for 1 d at 0°C; volatiles removed in vac. at 0°C, tube and contents allowed to warm to room temp., pumped;86%
xenon fluoride

xenon fluoride

bis(fluorosulfonyl)amide
14984-73-7

bis(fluorosulfonyl)amide

fluoro[imidobis(sulfuryl fluoride)]xenon(II)
53719-78-1

fluoro[imidobis(sulfuryl fluoride)]xenon(II)

Conditions
ConditionsYield
With CF2Cl2 liquid HN(SO2F)2 was syringed onto XeF2 at -196°C, then CF2Cl2 was condenced on to the sample and warmed to 0°C with vogorous agitation for 1 day, when HF was exctrated into upper CF2Cl2 layer; CF2Cl2 and HF were removed in vac. at 0°C, a residue was warmed to room temp. and XeF2 was removed in vac.;86%
xenon difluoride
13709-36-9

xenon difluoride

bis(fluorosulfonyl)amide
14984-73-7

bis(fluorosulfonyl)amide

A

fluoro[imidobis(sulfuryl fluoride)]xenon(II)
53719-78-1

fluoro[imidobis(sulfuryl fluoride)]xenon(II)

B

hydrogen fluoride
7664-39-3

hydrogen fluoride

Conditions
ConditionsYield
In Dichlorodifluoromethane 3 d at 0°C, 1:1 molar ratio; The reactor was pumped for 3 h at 0°C to remove the byproducts, elem. anal.;A 80%
B n/a
bis(fluorosulfonyl)amide
14984-73-7

bis(fluorosulfonyl)amide

lithium hydroxide
1310-65-2

lithium hydroxide

bis(fluorosulfonyl)imide lithium salt

bis(fluorosulfonyl)imide lithium salt

Conditions
ConditionsYield
In isopropyl alcohol at 20℃; for 7h;73%
tetramethylgermane
865-52-1

tetramethylgermane

bis(fluorosulfonyl)amide
14984-73-7

bis(fluorosulfonyl)amide

trimethylgermyl-di(fluorosulfonyl)amine
187884-57-7

trimethylgermyl-di(fluorosulfonyl)amine

Conditions
ConditionsYield
In dichloromethane N2 atm.; 18 h, 20°C; evapn., distn. (vac.); elem. anal.;63%
Tetraphenyllead
595-89-1

Tetraphenyllead

bis(fluorosulfonyl)amide
14984-73-7

bis(fluorosulfonyl)amide

triphenyllead(IV)-di(fluorosulfonyl)amide
187884-62-4

triphenyllead(IV)-di(fluorosulfonyl)amide

Conditions
ConditionsYield
In dichloromethane N2 atm.; equimolar ratio, refluxing (2 d); filtn., evapn., washing (CCl4), drying (vac.); elem. anal.;43%
xenon difluoride
13709-36-9

xenon difluoride

bis(fluorosulfonyl)amide
14984-73-7

bis(fluorosulfonyl)amide

A

Xe[N(SO2F)2]2
85883-06-3

Xe[N(SO2F)2]2

B

hydrogen fluoride
7664-39-3

hydrogen fluoride

Conditions
ConditionsYield
In Dichlorodifluoromethane byproducts: [N(SO2F)2]2, SO2F2, HF; 2 weeks from -22°C to -12°C, 2:1 molar ratio; The reactor was pumped at -4°C to remove the byproducts, elem. anal.;A 20%
B n/a
cadmium(II) trifluoroacetate
37054-04-9

cadmium(II) trifluoroacetate

bis(fluorosulfonyl)amide
14984-73-7

bis(fluorosulfonyl)amide

cadmium(II) bis(bis(fluorosulphuryl)imide)

cadmium(II) bis(bis(fluorosulphuryl)imide)

Conditions
ConditionsYield
In trifluoroacetic acid byproducts: CF3COOH; Excess of HN(SO2F)2 is added to Cd(OOCCF3)2, the mixture is refluxed for 16 h.; compd. is filtered, washed with CF3COOH, CH2Cl2, dried in vacuo at 80°C, elem. anal.;>90

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