Name 4-(4-Cyclopropylnaphthalen-1-yl)-4H-1,2,4-triazole-3-thiol Molecular Formula C15H13N3S Molecular Weight 267
Cas:1533519-84-4
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Cas:1533519-84-4
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Cas:1533519-84-4
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inquiry1. made in GMP plant, commerially 2. Normal Stock: 500kgs 3. Audit accepted. Related documents are available to offer and audited by many clients, such as Lupin, MSN, Dr reddy etc 4. Chromatographic Purity (HPLC): not less than 99.0% Appearan
Cas:1533519-84-4
Min.Order:1 Gram
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inquiryAs a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis according to the contract research and development services for the fine c
Cas:1533519-84-4
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Cas:1533519-84-4
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inquiryHebei Yanxi Chemical Co., Ltd. is a professional research, development and production of lead acetate benzene acetamide enterprise backbone members by local well-known entrepreneurs and professional senior engineers in the party's "low car
Cas:1533519-84-4
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:1533519-84-4
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inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
Cas:1533519-84-4
Min.Order:10 Kilogram
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inquiryAdvantages: Hubei XinRunde Chemical Co., Ltd is a renowned pharmaceutical manufacturer. We can offer high quality products at competitive price in quick delivery with 100% custom pass guaranteed. Never stop striving to offer our best s
Cas:1533519-84-4
Min.Order:10 Gram
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Type:Other
inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:1533519-84-4
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiry4-(4-cyclopropylnaphthalen-1-yl)-1H-1,2,4-triazole-5(4H)-thione CAS: 1533519-84-4 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermedia
Cas:1533519-84-4
Min.Order:1 Gram
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:1533519-84-4
Min.Order:1 Kilogram
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inquiryAdvantage : LIDE PHARMACEUTICALS LTD. is a mid-small manufacturing-type enterprise, engaged in pharmaceutical intermediates of R&D, custom-made and production, and also involving trading chemicals for export. We have established the R&
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inquiryAppearance:white or light yellow crystalline powder Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application:Used for research and industrial manufacture. Transportation:By
Cas:1533519-84-4
Min.Order:100 Gram
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Type:Lab/Research institutions
inquiryOur company provides one-stop services of research - development - production for a variety of special prouducts. Not only do we make effective use of our strong technological strength, but also establish of cooperative relations with several well-
Cas:1533519-84-4
Min.Order:100 Gram
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Type:Lab/Research institutions
inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:1533519-84-4
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inquiryCompany Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments
Cas:1533519-84-4
Min.Order:1 Gram
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Type:Lab/Research institutions
inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Cas:1533519-84-4
Min.Order:0
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inquiryMassive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
Cas:1533519-84-4
Min.Order:1 Gram
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Type:Lab/Research institutions
inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:1533519-84-4
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquiryWe are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov
Cas:1533519-84-4
Min.Order:100 Gram
FOB Price: $100.0 / 2000.0
Type:Lab/Research institutions
inquiryOur company was built in 2009 with an ISO certificate.In the past 6 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
Cas:1533519-84-4
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Type:Lab/Research institutions
inquiryProduct name: 4-(4-Cyclopropylnaphthalen-1-yl)-1H-1,2,4-Triazole-5(4H)-Thione CAS No.:1533519-84-4 Molecule Formula:C15H13N3S Molecule Weight:267.35 Purity: 98.0% Package: 25kg/drum Description:White or off-white powder Manufacture Standards:E
Cas:1533519-84-4
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:1533519-84-4
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryWe are leading fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...)
Cas:1533519-84-4
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
Cas:1533519-84-4
Min.Order:1 Kilogram
FOB Price: $18.0 / 20.0
Type:Trading Company
inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
Cas:1533519-84-4
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
Cas:1533519-84-4
Min.Order:1 Metric Ton
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Type:Trading Company
inquiryLocated in Hangzhou National Hi-Tech Industrial Development Zone, zhongqichem is a technical company mainly focus on the Custom synthesis, manufacturing, sales of chemicals to various industries. Benefiting from the outstanding customer service an
Cas:1533519-84-4
Min.Order:1 Gram
Negotiable
Type:Other
inquiryN-(4-cyclopropylnaphthalen-1-yl)-2-formylhydrazine-1-thiocarboxamide
4-(4-cyclopropylnaphthalen-1-yl)-4Η-1,2,4-triazole-3-thiol
Conditions | Yield |
---|---|
With water; sodium hydroxide In N,N-dimethyl-formamide at 30℃; for 16h; Solvent; Temperature; Reagent/catalyst; | 90% |
With potassium hydrogencarbonate In water; N,N-dimethyl-formamide at 90 - 140℃; |
cyclopropylmagnesium bromide
4-(4-cyclopropylnaphthalen-1-yl)-4Η-1,2,4-triazole-3-thiol
Conditions | Yield |
---|---|
In tetrahydrofuran for 2h; | 89.89% |
1-amino-4-cyclopropylnaphthalene
4-(4-cyclopropylnaphthalen-1-yl)-4Η-1,2,4-triazole-3-thiol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: water; 5,5-dimethyl-1,3-cyclohexadiene / 90 - 140 °C 2: N,N-dimethyl-formamide / 50 - 55 °C 3: potassium hydrogencarbonate / N,N-dimethyl-formamide; water / 90 - 140 °C View Scheme | |
Multi-step reaction with 4 steps 1: toluene; water 2: potassium hydroxide 3: N,N-dimethyl-formamide / 50 - 55 °C 4: potassium hydrogencarbonate / N,N-dimethyl-formamide; water / 90 - 140 °C View Scheme | |
Multi-step reaction with 3 steps 1.1: potassium carbonate / water; N,N-dimethyl-formamide / 3.5 h / 15 °C 1.2: 1 h / 0 °C 1.3: 2 h 2.1: ethyl acetate / 2 h / 60 °C 3.1: sodium hydroxide; water / N,N-dimethyl-formamide / 16 h / 30 °C View Scheme |
1-Bromonaphthalene
4-(4-cyclopropylnaphthalen-1-yl)-4Η-1,2,4-triazole-3-thiol
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1: 1,3-bis[(diphenylphosphino)propane]dichloronickel(II) / tetrahydrofuran / 0 - 5 °C 2: nitric acid / 0 - 20 °C 3: palladium on activated charcoal; hydrogen 4: water; 5,5-dimethyl-1,3-cyclohexadiene / 90 - 140 °C 5: N,N-dimethyl-formamide / 50 - 55 °C 6: potassium hydrogencarbonate / N,N-dimethyl-formamide; water / 90 - 140 °C View Scheme | |
Multi-step reaction with 6 steps 1: 1,3-bis[(diphenylphosphino)propane]dichloronickel(II) / tetrahydrofuran / 0 - 5 °C 2: nitric acid / 0 - 20 °C 3: hydrazine hydrate / methanol / Reflux 4: potassium hydroxide / dichloromethane 5: N,N-dimethyl-formamide / 50 - 55 °C 6: potassium hydrogencarbonate / N,N-dimethyl-formamide; water / 90 - 140 °C View Scheme | |
Multi-step reaction with 7 steps 1: 1,3-bis[(diphenylphosphino)propane]dichloronickel(II) / tetrahydrofuran / 0 - 5 °C 2: nitric acid / 0 - 20 °C 3: palladium on activated charcoal; hydrogen 4: toluene; water 5: potassium hydroxide 6: N,N-dimethyl-formamide / 50 - 55 °C 7: potassium hydrogencarbonate / N,N-dimethyl-formamide; water / 90 - 140 °C View Scheme |
1-cyclopropyl-naphthalene
4-(4-cyclopropylnaphthalen-1-yl)-4Η-1,2,4-triazole-3-thiol
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: nitric acid / 0 - 20 °C 2: palladium on activated charcoal; hydrogen 3: water; 5,5-dimethyl-1,3-cyclohexadiene / 90 - 140 °C 4: N,N-dimethyl-formamide / 50 - 55 °C 5: potassium hydrogencarbonate / N,N-dimethyl-formamide; water / 90 - 140 °C View Scheme | |
Multi-step reaction with 5 steps 1: nitric acid / 0 - 20 °C 2: hydrazine hydrate / methanol / Reflux 3: potassium hydroxide / dichloromethane 4: N,N-dimethyl-formamide / 50 - 55 °C 5: potassium hydrogencarbonate / N,N-dimethyl-formamide; water / 90 - 140 °C View Scheme | |
Multi-step reaction with 6 steps 1: nitric acid / 0 - 20 °C 2: palladium on activated charcoal; hydrogen 3: toluene; water 4: potassium hydroxide 5: N,N-dimethyl-formamide / 50 - 55 °C 6: potassium hydrogencarbonate / N,N-dimethyl-formamide; water / 90 - 140 °C View Scheme |
1-cyclopropyl-4-nitronaphthalene
4-(4-cyclopropylnaphthalen-1-yl)-4Η-1,2,4-triazole-3-thiol
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: palladium on activated charcoal; hydrogen 2: water; 5,5-dimethyl-1,3-cyclohexadiene / 90 - 140 °C 3: N,N-dimethyl-formamide / 50 - 55 °C 4: potassium hydrogencarbonate / N,N-dimethyl-formamide; water / 90 - 140 °C View Scheme | |
Multi-step reaction with 4 steps 1: hydrazine hydrate / methanol / Reflux 2: potassium hydroxide / dichloromethane 3: N,N-dimethyl-formamide / 50 - 55 °C 4: potassium hydrogencarbonate / N,N-dimethyl-formamide; water / 90 - 140 °C View Scheme | |
Multi-step reaction with 5 steps 1: palladium on activated charcoal; hydrogen 2: toluene; water 3: potassium hydroxide 4: N,N-dimethyl-formamide / 50 - 55 °C 5: potassium hydrogencarbonate / N,N-dimethyl-formamide; water / 90 - 140 °C View Scheme |
1-amino-4-cyclopropylnaphthalene oxalate
4-(4-cyclopropylnaphthalen-1-yl)-4Η-1,2,4-triazole-3-thiol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: potassium hydroxide 2: N,N-dimethyl-formamide / 50 - 55 °C 3: potassium hydrogencarbonate / N,N-dimethyl-formamide; water / 90 - 140 °C View Scheme |
(1-cyclopropylnaphthalen-4-yl)isothiocyanate
4-(4-cyclopropylnaphthalen-1-yl)-4Η-1,2,4-triazole-3-thiol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: N,N-dimethyl-formamide / 50 - 55 °C 2: potassium hydrogencarbonate / N,N-dimethyl-formamide; water / 90 - 140 °C View Scheme | |
Multi-step reaction with 2 steps 1: ethyl acetate / 2 h / 60 °C 2: sodium hydroxide; water / N,N-dimethyl-formamide / 16 h / 30 °C View Scheme |
1-amino-4-cyclopropylnaphthalene hydrochloride
4-(4-cyclopropylnaphthalen-1-yl)-4Η-1,2,4-triazole-3-thiol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: potassium hydroxide / dichloromethane 2: N,N-dimethyl-formamide / 50 - 55 °C 3: potassium hydrogencarbonate / N,N-dimethyl-formamide; water / 90 - 140 °C View Scheme |
tert-butyl 4-cyclopropylnaphthalen-1-ylcarbamate
4-(4-cyclopropylnaphthalen-1-yl)-4Η-1,2,4-triazole-3-thiol
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: hydrogenchloride / ethanol 2: potassium hydroxide / dichloromethane 3: N,N-dimethyl-formamide / 50 - 55 °C 4: potassium hydrogencarbonate / N,N-dimethyl-formamide; water / 90 - 140 °C View Scheme |
4-Bromo-1-naphthylamine
4-(4-cyclopropylnaphthalen-1-yl)-4Η-1,2,4-triazole-3-thiol
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1.1: potassium phosphate; palladium diacetate / toluene; water / 3 h / 110 °C / Inert atmosphere 2.1: potassium carbonate / water; N,N-dimethyl-formamide / 3.5 h / 15 °C 2.2: 1 h / 0 °C 2.3: 2 h 3.1: ethyl acetate / 2 h / 60 °C 4.1: sodium hydroxide; water / N,N-dimethyl-formamide / 16 h / 30 °C View Scheme |
4-(4-cyclopropylnaphthalen-1-yl)-4Η-1,2,4-triazole-3-thiol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: N,N-dimethyl-formamide / dichloromethane / 4 h / Reflux 2: tetrahydrofuran / 2 h View Scheme |
4-bromo-1-naphthol
4-(4-cyclopropylnaphthalen-1-yl)-4Η-1,2,4-triazole-3-thiol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: sodium hydroxide / ethanol / 3 h / 30 °C 2: N,N-dimethyl-formamide / dichloromethane / 4 h / Reflux 3: tetrahydrofuran / 2 h View Scheme |
1,2-bis(chloroacetoxy)ethane
4-(4-cyclopropylnaphthalen-1-yl)-4Η-1,2,4-triazole-3-thiol
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In N,N-dimethyl-formamide at 20℃; for 72h; Time; | 100% |
With potassium hydrogencarbonate In ethanol at 50 - 55℃; Inert atmosphere; | 92% |
4-(4-cyclopropylnaphthalen-1-yl)-4Η-1,2,4-triazole-3-thiol
bromoacetic acid methyl ester
2-((4-(4-cyclopropylnaphthalen-1-yl)-4H-1,2,4-triazole-3-yl)thio)acetic acid methyl ester
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 25℃; for 3h; | 99.5% |
With potassium carbonate In N,N-dimethyl-formamide at 50℃; for 4h; | 85% |
With sodium carbonate In N,N-dimethyl-formamide at 27 - 35℃; Concentration; Time; Temperature; Large scale; | |
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 1.5h; | 4 g |
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 1.5h; | 4 g |
ethane-1,2-diyl bis(2-bromoacetate)
4-(4-cyclopropylnaphthalen-1-yl)-4Η-1,2,4-triazole-3-thiol
Conditions | Yield |
---|---|
With potassium hydrogencarbonate In ethanol at 50 - 55℃; Inert atmosphere; | 94% |
phenyl 2-bromoacetate
4-(4-cyclopropylnaphthalen-1-yl)-4Η-1,2,4-triazole-3-thiol
Conditions | Yield |
---|---|
Stage #1: 4-(4-cyclopropylnaphthalen-1-yl)-4Η-1,2,4-triazole-3-thiol With triethylamine In isopropyl alcohol at 20℃; for 0.333333h; Stage #2: phenyl 2-bromoacetate In isopropyl alcohol at 0 - 20℃; for 2h; | 92% |
4-(4-cyclopropylnaphthalen-1-yl)-4Η-1,2,4-triazole-3-thiol
bromoacetic acid
Conditions | Yield |
---|---|
Stage #1: 4-(4-cyclopropylnaphthalen-1-yl)-4Η-1,2,4-triazole-3-thiol With sodium hydrogencarbonate In ethanol; water at 25 - 45℃; Stage #2: bromoacetic acid In ethanol; water at 25 - 55℃; for 1h; Stage #3: With acetic acid In ethanol; water at 25 - 50℃; | 91.9% |
phenyl chloroacetate
4-(4-cyclopropylnaphthalen-1-yl)-4Η-1,2,4-triazole-3-thiol
Conditions | Yield |
---|---|
Stage #1: 4-(4-cyclopropylnaphthalen-1-yl)-4Η-1,2,4-triazole-3-thiol With triethylamine In acetone at 20℃; for 0.333333h; Stage #2: phenyl chloroacetate In isopropyl alcohol; acetone at 0 - 20℃; for 2h; | 90% |
4-(4-cyclopropylnaphthalen-1-yl)-4Η-1,2,4-triazole-3-thiol
2-((4-(4-cyclopropylnaphthalen-1-yl)-4H-1,2,4-triazole-3-yl)thio)acetic acid methyl ester
Conditions | Yield |
---|---|
With potassium phosphate In water; acetone at 40℃; for 6h; | 90% |
(R)-1-phenylethyl 2-bromoacetate
4-(4-cyclopropylnaphthalen-1-yl)-4Η-1,2,4-triazole-3-thiol
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 15℃; for 3h; | 87% |
With potassium carbonate In N,N-dimethyl-formamide at 15℃; for 2.5h; |
4-(4-cyclopropylnaphthalen-1-yl)-4Η-1,2,4-triazole-3-thiol
chloroacetic acid 2-[2-(2-chloro-acetoxy)-ethoxy]-ethyl ester
Conditions | Yield |
---|---|
In ethanol at 50 - 55℃; Inert atmosphere; | 86% |
chloroacetic acid 4-(2-chloroacetoxy)phenyl ester
4-(4-cyclopropylnaphthalen-1-yl)-4Η-1,2,4-triazole-3-thiol
Conditions | Yield |
---|---|
In acetonitrile at 50 - 55℃; Inert atmosphere; | 83% |
Methyl 3-bromopropionate
4-(4-cyclopropylnaphthalen-1-yl)-4Η-1,2,4-triazole-3-thiol
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 60℃; for 96h; Autoclave; | 67% |
4-(4-cyclopropylnaphthalen-1-yl)-4Η-1,2,4-triazole-3-thiol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: N,N-dimethyl-formamide 2: N-Bromosuccinimide / tetrahydrofuran View Scheme |
4-(4-cyclopropylnaphthalen-1-yl)-4Η-1,2,4-triazole-3-thiol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: sodium carbonate / N,N-dimethyl-formamide / 27 - 35 °C / Large scale 2: N-Bromosuccinimide / tetrahydrofuran / 27 - 32 °C / Large scale View Scheme | |
Multi-step reaction with 2 steps 1: potassium phosphate / water; acetone / 6 h / 40 °C 2: 1,3-dibromo-5,5-dimethylimidazolidine-2,4-dione / ethyl acetate / Reflux View Scheme | |
Multi-step reaction with 2 steps 1: potassium carbonate / N,N-dimethyl-formamide / 1.5 h / 20 °C 2: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; N-Bromosuccinimide / tetrahydrofuran / 3 h / 30 - 32 °C View Scheme |
4-(4-cyclopropylnaphthalen-1-yl)-4Η-1,2,4-triazole-3-thiol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: sodium carbonate / N,N-dimethyl-formamide / 27 - 35 °C / Large scale 2: N-Bromosuccinimide / tetrahydrofuran / 27 - 32 °C / Large scale 3: sodium hydroxide; water / toluene / 18 - 25 °C View Scheme | |
Multi-step reaction with 4 steps 1: sodium carbonate / N,N-dimethyl-formamide / 27 - 35 °C / Large scale 2: N-Bromosuccinimide / tetrahydrofuran / 27 - 32 °C / Large scale 3: sodium hydroxide / toluene; water / 18 - 25 °C / Large scale 4: hydrogen bromide / water; ethyl acetate / 30 - 35 °C / pH 2 - 4 / Large scale View Scheme | |
Multi-step reaction with 3 steps 1.1: triethylamine / acetone / 0.33 h / 20 °C 1.2: 2 h / 0 - 20 °C 2.1: 1,1'-Thiocarbonyldiimidazole / dichloromethane / 0.25 h / 20 °C 3.1: sodium hydrogencarbonate / acetone / 12 h / 65 °C View Scheme |
4-(4-cyclopropylnaphthalen-1-yl)-4Η-1,2,4-triazole-3-thiol
2-((5-bromo-4-(4-cyclopropylnaphthalen-1-yl)-4H-1,2,4-triazol-3-yl)thio)acetic acid sodium salt
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: sodium carbonate / N,N-dimethyl-formamide / 27 - 35 °C / Large scale 2: N-Bromosuccinimide / tetrahydrofuran / 27 - 32 °C / Large scale 3: sodium hydroxide / toluene; water / 18 - 25 °C / Large scale View Scheme | |
Multi-step reaction with 3 steps 1: potassium carbonate / N,N-dimethyl-formamide / 1.5 h / 20 °C 2: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; N-Bromosuccinimide / tetrahydrofuran / 3 h / 30 - 32 °C 3: sodium hydroxide; water / tetrahydrofuran / 2 h View Scheme | |
Multi-step reaction with 3 steps 1: potassium carbonate / N,N-dimethyl-formamide / 3 h / 25 °C 2: sodium hydroxide; N-Bromosuccinimide / N,N-dimethyl-formamide / 3 h / 25 °C 3: sodium hydroxide / ethanol; water / 2 h / 50 °C View Scheme | |
Multi-step reaction with 3 steps 1: potassium carbonate / N,N-dimethyl-formamide / 1.5 h / 20 °C 2: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; N-Bromosuccinimide / tetrahydrofuran / 3 h / 30 - 32 °C 3: sodium hydroxide / tetrahydrofuran; water / 2 h View Scheme | |
Multi-step reaction with 3 steps 1: potassium carbonate / N,N-dimethyl-formamide / 4 h / 50 °C 2: N-Bromosuccinimide / tetrahydrofuran / 2 - 32 °C 3: sodium hydroxide / toluene; water / 10 - 15 °C View Scheme |
4-(4-cyclopropylnaphthalen-1-yl)-4Η-1,2,4-triazole-3-thiol
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide |
4-(4-cyclopropylnaphthalen-1-yl)-4Η-1,2,4-triazole-3-thiol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: triethylamine / isopropyl alcohol / 0.33 h / 20 °C 1.2: 2 h / 0 - 20 °C 2.1: 1,1'-Thiocarbonyldiimidazole / dichloromethane / 0.25 h / 20 °C View Scheme | |
Multi-step reaction with 2 steps 1.1: triethylamine / acetone / 0.33 h / 20 °C 1.2: 2 h / 0 - 20 °C 2.1: 1,1'-Thiocarbonyldiimidazole / dichloromethane / 0.25 h / 20 °C View Scheme |
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