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Tengzhou Runlong Fragrance Co., Ltd.

1、Our factory passed ISO 9001, ISO 14001, ISO 22000 system certification; HALAL 、KOSHER、FCC AND FDA certificate are available. We can provide customers with better prices, and the supply is stable. 2、We founded in 2004,10% of the staff have more tha

3-(Methylthio)butanal/3-(Methylthio)butyraldehyde cas 16630-52-7

Cas:16630-52-7

Min.Order:1 Kilogram

Negotiable

Type:Manufacturers

inquiry

Dayang Chem (Hangzhou) Co.,Ltd.

As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch

3-(Methylthio)butanal

Cas:16630-52-7

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

inquiry

Henan Allgreen Chemical Co.,Ltd

high quality Appearance:White or off white powder Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea Port:shanghai

3-(Methylthio)butanal

Cas:16630-52-7

Min.Order:1 Kilogram

Negotiable

Type:Manufacturers

inquiry

COLORCOM LTD.

Colorcom is a global leader in industrial chemical manufacturing and is continuously innovating and transforming to exceed client expectations and industry standards. Colorcom prides itself on superior customer and technical focus, while focusing on

3-Methylthiobutyraldehyde

Cas:16630-52-7

Min.Order:1 Metric Ton

Negotiable

Type:Manufacturers

inquiry

Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

3-(Methylthio)-butyraldehyde

Cas:16630-52-7

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

inquiry

Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Factory direct supply CAS 16630-52-7 with best quality

Cas:16630-52-7

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

inquiry

Henan Wentao Chemical Product Co., Ltd.

We are leading fine chemicals supplier in China and Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...) 2.Organic Phosphine Ligands (Tert-butyl-phosphine.Cyclohexyl-phosphine...) 3.OLED intermediat

3-(Methylthio)butanal, 99%CAS NO.: 16630-52-7

Cas:16630-52-7

Min.Order:1 Kilogram

FOB Price: $4.0 / 5.0

Type:Lab/Research institutions

inquiry

Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

Butanal,3-(methylthio)- 16630-52-7

Cas:16630-52-7

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Shanghai Minstar Chemical Co., Ltd

Product Name: 3-(Methylthio)butanal Synonyms: 3-(methylthio)-butana;3-(METHYLMERCAPTO)BUTYRALDEHYDE;3-(METHYLTHIO)BUTANAL;3-METHYLTHIO BUTYLALDEHYDE;3-(METHYLTHIO)BUTYRALDEHYDE;FEMA 3374;3-(METHYLTHIO)BUTANAL 96+%;3-(Methylyhio)Butanal CAS:

3-(Methylthio)butanal

Cas:16630-52-7

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Baoji Guokang Healthchem co.,ltd

Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At present

3-(Methylthio)butanal CAS: 16630-52-7

Cas:16630-52-7

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

inquiry

Qingdao Beluga Import and Export Co., LTD

3-(Methylthio)butanal CAS:16630-52-7 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic in

3-(Methylthio)butanal CAS:16630-52-7

Cas:16630-52-7

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Hebei Quanhe Biotechnology Co. LTD

1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures s

3-(Methylthio)butanal

Cas:16630-52-7

Min.Order:1 Kilogram

FOB Price: $30.0 / 50.0

Type:Lab/Research institutions

inquiry

Lonwin Chemical Group Limited

3-Methylthio butylaldehyde CAS: 16630-52-7 Specification Category Pharmaceutical Raw Materials, Fine Chemicals, Bulk drug Standard Medical standard Shelf life 2 years Storage should be stored i

Factory supply 3-Methylthio butylaldehyde

Cas:16630-52-7

Min.Order:1 Kilogram

Negotiable

Type:Other

inquiry

Xiamen Hisunny Chemical Co.,Ltd

Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia

3-(Methylthio)Butanal

Cas:16630-52-7

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Wuhan Han Sheng New Material Technology Co.,Ltd

Our advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We have s

3-Methylthio butylaldehyde

Cas:16630-52-7

Min.Order:10 Kilogram

Negotiable

Type:Trading Company

inquiry

Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

3-Methylthio butylaldehyde

Cas:16630-52-7

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

JINING XINHE CHEMICAL CO., LTD

Advantage 1: The product passed the professional production process and quality inspection, the purity is 99% +. 2: Highly qualified engineers to provide technical documents and service. 3: We could provide sample for your test. 4: High

3-Methylthio butylaldehyde16630-52-7 3-(Methylthio)Butyraldehyde

Cas:16630-52-7

Min.Order:1 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

3-(Methylthio)butanal

Cas:16630-52-7

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply 3-(Methylthio)butyraldehyde

Cas:16630-52-7

Min.Order:0 Metric Ton

Negotiable

Type:Other

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

cas:16630-52-7

Cas:16630-52-7

Min.Order:10 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Henan Tianfu Chemical Co., Ltd.

Butanal,3-(methylthio)- 3-(methylthio)-butana;3-(METHYLMERCAPTO)BUTYRALDEHYDE;3-(METHYLTHIO)BUTANAL;3-METHYLTHIO BUTYLALDEHYDE;3-(METHYLTHIO)BUTYRALDEHYDE;FEMA 3374;3-(METHYLTHIO)BUTANAL 96+%;3-(Methylyhio)Butanal 3-methylthiobutyraldehyde Bo

16630-52-7

Cas:16630-52-7

Min.Order:100 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Henan Sinotech Import&Export Corporation

Product Name: 3-(Methylthio)butanal Synonyms: 3-(METHYLMERCAPTO)BUTYRALDEHYDE;3-(METHYLTHIO)BUTANAL;3-METHYLTHIO BUTYLALDEHYDE;3-(METHYLTHIO)BUTYRALDEHYDE;FEMA 3374;3-(METHYLTHIO)BUTANAL 96+%;3-(Methylyhio)Butanal;Butanal, 3-(

3-(Methylthio)butanal CAS:16630-52-7

Cas:16630-52-7

Min.Order:1 Kilogram

FOB Price: $1.0

Type:Other

inquiry

EAST CHEMSOURCES LIMITED

factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B

3-Methylthio butylaldehyde

Cas:16630-52-7

Min.Order:1 Kilogram

FOB Price: $18.0 / 20.0

Type:Trading Company

inquiry

Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

3-(Methylthio)butanal

Cas:16630-52-7

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

KAISA GROUP INC

1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer

3-Methylthio butylaldehyde

Cas:16630-52-7

Min.Order:1 Metric Ton

FOB Price: $1.5

Type:Trading Company

inquiry

NIGNXIA XINDACHANG TECHNOLOGY CO.,LTD

Donglian as a factory and supplier of aroma chemicals in China, We can provide different quantities of custom synthesis chemicals in food flavor scale more than fourteen years.in addition, our company has researched and developed four series

3-(Methylthio)butanal

Cas:16630-52-7

Min.Order:1 Kilogram

Negotiable

Type:Manufacturers

inquiry

Bluecrystal chem-union

We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp

3-(Methylthio) butanal

Cas:16630-52-7

Min.Order:1 Metric Ton

FOB Price: $1.0

Type:Trading Company

inquiry

Kono Chem Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou

3-(Methylthio)butyraldehyde

Cas:16630-52-7

Min.Order:0

Negotiable

Type:Other

inquiry

GIHI CHEMICALS CO.,LIMITED

high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,Pharmaceutical intermediates Transportation:air,sea,courier

3-Methylthiobutanal

Cas:16630-52-7

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

JINHUA HUAYI CHEMICAL CO., LTD.

Jinhua huayi chemical co., ltd. is dedicated to the development, production and marketing of chemicals. On the basis of equality and mutual benefit, and under the principle of customer first, credit first, quality first, we are ready to join hands

3-(Methylthio)Butyraldehyde

Cas:16630-52-7

Min.Order:100 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Synthetic route

crotonaldehyde
123-73-9

crotonaldehyde

sodium thiomethoxide
5188-07-8

sodium thiomethoxide

3-(methylthio)butyraldehyde
16630-52-7

3-(methylthio)butyraldehyde

Conditions
ConditionsYield
With propionic acid In water; toluene at 2 - 70℃; Product distribution / selectivity; Inert atmosphere;95%
With acetic acid In water; toluene at 2 - 22℃; under 39.754 Torr; Product distribution / selectivity; Inert atmosphere;
trans-Crotonaldehyde
123-73-9

trans-Crotonaldehyde

methylthiol
74-93-1

methylthiol

A

3-(methylthio)butyraldehyde
16630-52-7

3-(methylthio)butyraldehyde

B

1,3-bis-methylsulfanyl-but-1-ene
99116-25-3

1,3-bis-methylsulfanyl-but-1-ene

Conditions
ConditionsYield
With hydrogenchloride; tetrachloromethane
methylthiol
74-93-1

methylthiol

crotonaldehyde
123-73-9

crotonaldehyde

3-(methylthio)butyraldehyde
16630-52-7

3-(methylthio)butyraldehyde

Conditions
ConditionsYield
With ascaridole
With piperidine
With hydrogenchloride In tetrachloromethane
pyrrolidine
123-75-1

pyrrolidine

3-(methylthio)butyraldehyde
16630-52-7

3-(methylthio)butyraldehyde

3-(methylthio)-1-(pyrrolidin-1-yl)-1-butene
1045854-57-6

3-(methylthio)-1-(pyrrolidin-1-yl)-1-butene

Conditions
ConditionsYield
With potassium carbonate at -5℃; for 0.166667h;96%
With potassium carbonate at 4 - 20℃; Inert atmosphere;
In toluene at 3 - 26℃; under 18.0018 Torr; Product distribution / selectivity;
methyl 4-{1-[(tert-butoxycarbonyl)amino]prop-2-yn-1-yl}benzoate

methyl 4-{1-[(tert-butoxycarbonyl)amino]prop-2-yn-1-yl}benzoate

3-(methylthio)butyraldehyde
16630-52-7

3-(methylthio)butyraldehyde

tert-butyl 2-[4-(methoxycarbonyl)phenyl]-5-[2-(methylthio)propyl]-1H-pyrrole-1-carboxylate

tert-butyl 2-[4-(methoxycarbonyl)phenyl]-5-[2-(methylthio)propyl]-1H-pyrrole-1-carboxylate

Conditions
ConditionsYield
Stage #1: methyl 4-{1-[(tert-butoxycarbonyl)amino]prop-2-yn-1-yl}benzoate; 3-(methylthio)butyraldehyde With bis(norbornadiene)rhodium(l)tetrafluoroborate; 1,1-dicyclohexyl-N-(dicyclohexylphosphino)-N-methylphosphinamine In acetone at 20℃; for 4h; Inert atmosphere;
Stage #2: With toluene-4-sulfonic acid In acetone; acetonitrile at 20℃; for 4h; Inert atmosphere;
75%
3-(methylthio)butyraldehyde
16630-52-7

3-(methylthio)butyraldehyde

(4,4-dibromobutan-2-yl)(methyl)sulfane

(4,4-dibromobutan-2-yl)(methyl)sulfane

Conditions
ConditionsYield
With triphenyl phosphite; bromine; triethylamine In dichloromethane at -78 - 20℃; Schlenk technique; Inert atmosphere;41%
methyl (2E)-3-methoxy-2-propenoate
5788-17-0

methyl (2E)-3-methoxy-2-propenoate

3-(methylthio)butyraldehyde
16630-52-7

3-(methylthio)butyraldehyde

4-methoxy-5-(2-methyl-sulfanyl-propyl)-5H-furan-2-one
852530-60-0

4-methoxy-5-(2-methyl-sulfanyl-propyl)-5H-furan-2-one

Conditions
ConditionsYield
Stage #1: methyl (2E)-3-methoxy-2-propenoate With lithium diisopropyl amide In tetrahydrofuran at -100 - -95℃; for 0.1h;
Stage #2: 3-(methylthio)butyraldehyde In tetrahydrofuran at -100 - -78℃; for 1.53333h;
30%
formaldehyd
50-00-0

formaldehyd

3-(methylthio)butyraldehyde
16630-52-7

3-(methylthio)butyraldehyde

2-(hydroxymethyl)-2-(1-(methylthio)ethyl)propane-1,3-diol

2-(hydroxymethyl)-2-(1-(methylthio)ethyl)propane-1,3-diol

Conditions
ConditionsYield
Stage #1: formaldehyd With sodium hydroxide In acetonitrile at 60℃; for 0.333333h; Cannizzaro Reaction;
Stage #2: 3-(methylthio)butyraldehyde In acetonitrile for 1h; Reflux;
28%
3-(methylthio)butyraldehyde
16630-52-7

3-(methylthio)butyraldehyde

sodium cyanide
143-33-9

sodium cyanide

5-(2-methylsulfanyl-propyl)-imidazolidine-2,4-dione
858206-51-6

5-(2-methylsulfanyl-propyl)-imidazolidine-2,4-dione

Conditions
ConditionsYield
With ammonium carbonate
pyrrolidine
123-75-1

pyrrolidine

3-(methylthio)butyraldehyde
16630-52-7

3-(methylthio)butyraldehyde

1-((E)-3-methylthiobut-1-enyl)pyrrolidine

1-((E)-3-methylthiobut-1-enyl)pyrrolidine

Conditions
ConditionsYield
With potassium carbonate at 10 - 20℃;
With potassium carbonate at 4 - 20℃;
With potassium carbonate at 4 - 20℃;
3-(methylthio)butyraldehyde
16630-52-7

3-(methylthio)butyraldehyde

dimethyl amine
124-40-3

dimethyl amine

N,N-dimethyl-(3-methylthiobut-1-enyl)amine

N,N-dimethyl-(3-methylthiobut-1-enyl)amine

Conditions
ConditionsYield
With potassium carbonate In acetonitrile at 20℃; for 1.5h;
3-(methylthio)butyraldehyde
16630-52-7

3-(methylthio)butyraldehyde

4-methyl-D,L-methionine
16820-66-9

4-methyl-D,L-methionine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 4>2CO3
2: Hydrolysis
View Scheme
3-(methylthio)butyraldehyde
16630-52-7

3-(methylthio)butyraldehyde

2-amino-4-methanesulfinyl-valeric acid

2-amino-4-methanesulfinyl-valeric acid

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 4>2CO3
2: Hydrolysis
3: H2O2
View Scheme
3-(methylthio)butyraldehyde
16630-52-7

3-(methylthio)butyraldehyde

2-amino-4-(imino-methyl-oxo-λ6-sulfanyl)-valeric acid
70056-02-9

2-amino-4-(imino-methyl-oxo-λ6-sulfanyl)-valeric acid

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: 4>2CO3
2: Hydrolysis
3: H2O2
4: HN3
View Scheme
3-(methylthio)butyraldehyde
16630-52-7

3-(methylthio)butyraldehyde

2-amino-4-methanesulfonyl-valeric acid

2-amino-4-methanesulfonyl-valeric acid

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: 4>2CO3
2: Hydrolysis
3: H2O2
4: H2O2
View Scheme
3-(methylthio)butyraldehyde
16630-52-7

3-(methylthio)butyraldehyde

1-Phenyl-2-propyn-1-ol
4187-87-5

1-Phenyl-2-propyn-1-ol

C14H16OS
1360610-97-4

C14H16OS

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: bis(norbornadiene)rhodium(l)tetrafluoroborate; 1,2-bis-(diphenylphosphino)ethane / 1,2-dichloro-ethane / 1 h / 65 °C / Inert atmosphere
2: toluene-4-sulfonic acid / 1,2-dichloro-ethane / 2 h / 20 °C / Inert atmosphere
View Scheme
3-(methylthio)butyraldehyde
16630-52-7

3-(methylthio)butyraldehyde

1-Phenyl-2-propyn-1-ol
4187-87-5

1-Phenyl-2-propyn-1-ol

C14H18O2S

C14H18O2S

Conditions
ConditionsYield
With bis(norbornadiene)rhodium(l)tetrafluoroborate; 1,2-bis-(diphenylphosphino)ethane In 1,2-dichloro-ethane at 65℃; for 1h; Inert atmosphere;
3-(methylthio)butyraldehyde
16630-52-7

3-(methylthio)butyraldehyde

1-triphenylphosphoranylidene-2-propanone
1439-36-7

1-triphenylphosphoranylidene-2-propanone

(E)-6-methylsulfanylhept-3-en-2-one
1615212-09-3

(E)-6-methylsulfanylhept-3-en-2-one

Conditions
ConditionsYield
In dichloromethane for 7h; Reflux;5.409 g
In dichloromethane for 7h; Reflux;5.409 g
3-(methylthio)butyraldehyde
16630-52-7

3-(methylthio)butyraldehyde

ethyl 2-(2-methylsulfanylpropyl)-4,6-dioxocyclohexanecarboxylate
1615212-10-6

ethyl 2-(2-methylsulfanylpropyl)-4,6-dioxocyclohexanecarboxylate

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: dichloromethane / 7 h / Reflux
2.1: sodium / ethanol / 1.33 h / 20 °C / Inert atmosphere; Cooling with ice
2.2: 20 °C / Inert atmosphere; Cooling with ice
View Scheme
Multi-step reaction with 2 steps
1.1: dichloromethane / 7 h / Reflux
2.1: sodium; ethanol / 1.33 h / 20 °C / Cooling with ice; Inert atmosphere
2.2: 4 h / 20 °C / Cooling with ice
View Scheme
3-(methylthio)butyraldehyde
16630-52-7

3-(methylthio)butyraldehyde

5-(2-methylsulfanylpropyl)cyclohexane-1,3-dione
108463-70-3

5-(2-methylsulfanylpropyl)cyclohexane-1,3-dione

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: dichloromethane / 7 h / Reflux
2.1: sodium / ethanol / 1.33 h / 20 °C / Inert atmosphere; Cooling with ice
2.2: 20 °C / Inert atmosphere; Cooling with ice
3.1: hydrogenchloride / water / 6 h / Heating
View Scheme
Multi-step reaction with 3 steps
1.1: dichloromethane / 7 h / Reflux
2.1: sodium; ethanol / 1.33 h / 20 °C / Cooling with ice; Inert atmosphere
2.2: 4 h / 20 °C / Cooling with ice
3.1: hydrogenchloride / water / 6 h / Heating
View Scheme
3-(methylthio)butyraldehyde
16630-52-7

3-(methylthio)butyraldehyde

sulfoxaflor
946578-00-3

sulfoxaflor

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: potassium carbonate / toluene / 5 h / 10 - 20 °C / Inert atmosphere
2: acetonitrile / 15 - 20 °C / Inert atmosphere
3: ammonium acetate / acetonitrile / 0.5 h / 80 °C / Inert atmosphere
4: [bis(acetoxy)iodo]benzene / acetonitrile / 2.17 h / 10 - 30 °C
5: sodium permanganate / water; dichloromethane / 1.92 h / 13 - 20 °C
View Scheme
3-(methylthio)butyraldehyde
16630-52-7

3-(methylthio)butyraldehyde

1,1,1-trifluoro-6-(methylthio)-5-(pyrrolidine-1-ylmethylene)hept-3-en-2-one
1380070-36-9

1,1,1-trifluoro-6-(methylthio)-5-(pyrrolidine-1-ylmethylene)hept-3-en-2-one

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: potassium carbonate / toluene / 5 h / 10 - 20 °C / Inert atmosphere
2: acetonitrile / 15 - 20 °C / Inert atmosphere
View Scheme
3-(methylthio)butyraldehyde
16630-52-7

3-(methylthio)butyraldehyde

(1-{6-[trifluoromethyl]pyridin-3-yl}ethyl)-(methyl)-λ4-sulfanylidenecyanamide
1049684-75-4, 1049684-74-3, 1046119-63-4

(1-{6-[trifluoromethyl]pyridin-3-yl}ethyl)-(methyl)-λ4-sulfanylidenecyanamide

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: potassium carbonate / toluene / 5 h / 10 - 20 °C / Inert atmosphere
2: acetonitrile / 15 - 20 °C / Inert atmosphere
3: ammonium acetate / acetonitrile / 0.5 h / 80 °C / Inert atmosphere
4: [bis(acetoxy)iodo]benzene / acetonitrile / 2.17 h / 10 - 30 °C
View Scheme
3-(methylthio)butyraldehyde
16630-52-7

3-(methylthio)butyraldehyde

(±)5-(1-(methylthio)ethyl)-2-trifluoromethyl pyridine

(±)5-(1-(methylthio)ethyl)-2-trifluoromethyl pyridine

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: potassium carbonate / toluene / 5 h / 10 - 20 °C / Inert atmosphere
2: acetonitrile / 15 - 20 °C / Inert atmosphere
3: ammonium acetate / acetonitrile / 0.5 h / 80 °C / Inert atmosphere
View Scheme
3-(methylthio)butyraldehyde
16630-52-7

3-(methylthio)butyraldehyde

C20H29NO5S

C20H29NO5S

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: formic acid / water; methanol / 20 h / 20 °C / Inert atmosphere
2: C46H34I4O6; potassium fluoride / o-xylene / 24 h / 25 °C / Inert atmosphere
View Scheme
3-(methylthio)butyraldehyde
16630-52-7

3-(methylthio)butyraldehyde

C20H29NO5S

C20H29NO5S

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: formic acid / water; methanol / 20 h / 20 °C / Inert atmosphere
2: Tetraethylene glycol; potassium fluoride / o-xylene / 24 h / 25 °C / Inert atmosphere
View Scheme
3-(methylthio)butyraldehyde
16630-52-7

3-(methylthio)butyraldehyde

tert-Butyl N-hydroxycarbamate
36016-38-3

tert-Butyl N-hydroxycarbamate

sodium benzenesulfonate
873-55-2

sodium benzenesulfonate

C16H25NO5S2

C16H25NO5S2

Conditions
ConditionsYield
With formic acid In methanol; water at 20℃; for 20h; Inert atmosphere;
3-(methylthio)butyraldehyde
16630-52-7

3-(methylthio)butyraldehyde

C20H21F4N3O

C20H21F4N3O

1-benzyl-3-(3-fluoro-5-(trifluoromethyl)phenyl)-1-(1-(3-(methylthio)butyl)piperidin-4-yl)urea

1-benzyl-3-(3-fluoro-5-(trifluoromethyl)phenyl)-1-(1-(3-(methylthio)butyl)piperidin-4-yl)urea

Conditions
ConditionsYield
With phenylsilane; dibutyltin chloride In tetrahydrofuran at 20℃; for 16h;
3-(methylthio)butyraldehyde
16630-52-7

3-(methylthio)butyraldehyde

(3-(methylthio)butane-1,1-diyl)bis(dimethyl(phenyl)silane)

(3-(methylthio)butane-1,1-diyl)bis(dimethyl(phenyl)silane)

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: triphenyl phosphite; bromine; triethylamine / dichloromethane / -78 - 20 °C / Schlenk technique; Inert atmosphere
2: copper(I) bromide dimethylsulfide complex; 4,4'-di-tert-butyl-2,2'-bipyridine; lithium tert-butoxide / tetrahydrofuran; dimethyl sulfoxide / 0 - 20 °C / Schlenk technique; Inert atmosphere
View Scheme

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