CAS No.17015-08-6,(2R,3R)-(-)-EPOXYSUCCINIC ACID Suppliers

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(2R,3R)-(-)-EPOXYSUCCINIC ACID CAS:17015-08-6 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality o

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Xi`an Eastling Biotech Co., Ltd.

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Hangzhou Fandachem Co.,Ltd

(2R,3R)-(-)-EPOXYSUCCINIC ACIDCASAppearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express

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Nanjing Raymon Biotech Co., Ltd.

2,3-Oxiranedicarboxylicacid, (2R,3R)-Appearance:Off white to slight yellow solid Storage:Store in dry and cool condition Package:25kg or according to cutomer's demand Application:Chemical research/Pharmaceutical intermediates Transportation:By Sea,by

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2,3-Oxiranedicarboxylicacid, (2R,3R)-Appearance:Off white to slight yellow solid Storage:Stored in shaded, cool and dry places Package:1L 5L 10L 25L bottle Application:pharma intermediate Transportation:Handle with cares to avoid damaging the package

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Synthetic route

: 74243-85-9
trans-2,3-bis(ethoxycarbonyl)oxirane

: 17015-08-6
(2R,3R)-oxirane-2,3-dicarboxylic acid

Conditions

Conditions	Yield
With potassium hydroxide In ethanol for 3h; Ambient temperature;	93%

: 110-17-8
(2E)-but-2-enedioic acid

: 17015-08-6
(2R,3R)-oxirane-2,3-dicarboxylic acid

Conditions

Conditions	Yield
With dihydrogen peroxide; sodium tungstate	60%

: 141-36-6, 3272-11-5, 16533-72-5, 17015-08-6, 17087-75-1, 22734-83-4
DL-trans-epoxysuccinic acid

A: 17087-75-1
(-)-trans-2,3-oxiranedicarboxylic acid

B: 17015-08-6
(2R,3R)-oxirane-2,3-dicarboxylic acid

Conditions

Conditions	Yield
Resolution of racemate;	A 46% B 41%

: 50-99-7
D-glucose

: 17015-08-6
(2R,3R)-oxirane-2,3-dicarboxylic acid

Conditions

Conditions	Yield
mit Hilfe von Aspergillus fumigatus;

: 141-36-6, 3272-11-5, 16533-72-5, 17015-08-6, 17087-75-1, 22734-83-4
DL-trans-epoxysuccinic acid

: 17015-08-6
(2R,3R)-oxirane-2,3-dicarboxylic acid

Conditions

Conditions	Yield
ueber das Morphin-Salz;
Yield given;

acetate of dimethyl ester of/the/ levorotatory β-chloro-malic acid I: acetate of dimethyl ester of/the/ levorotatory β-chloro-malic acid I

: 17015-08-6
(2R,3R)-oxirane-2,3-dicarboxylic acid

Conditions

Conditions	Yield
With hydrogenchloride; methanol; water Behandeln des Reaktionsprodukts mit Natronlauge;

diethyl ester of/the/ levorotatory β-chloro-malic acid I: diethyl ester of/the/ levorotatory β-chloro-malic acid I

: 17015-08-6
(2R,3R)-oxirane-2,3-dicarboxylic acid

Conditions

Conditions	Yield
With hydrogenchloride Behandeln mit verduennter Natronlauge;

: 74-89-5
methylamine

: 17015-08-6
(2R,3R)-oxirane-2,3-dicarboxylic acid

: L-erythro-N(α)-methyl-3-hydroxy-L-aspartic acid

Conditions

Conditions	Yield
In water Reflux;	90%

: 17015-08-6
(2R,3R)-oxirane-2,3-dicarboxylic acid

: 7298-98-8
2-(S)-amino-3-(R)-hydroxysuccinic acid

Conditions

Conditions	Yield
With ammonium hydroxide; water at 45 - 47℃; for 48h;	82%
With ammonium hydroxide at 110℃; for 30h;	42%
With ammonium hydroxide

: 77215-54-4
N-α-tert-butyloxycarbonyl-L-diaminopropanoic acid tert-butyl ester

: 17015-08-6
(2R,3R)-oxirane-2,3-dicarboxylic acid

: 1255383-49-3
Nβ-(R,R)-epoxysuccinoyl-DAP(BOC)-Otbu

Conditions

Conditions	Yield
With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; for 12h;	79%

: 17015-08-6
(2R,3R)-oxirane-2,3-dicarboxylic acid

: 5188-07-8
sodium thiomethoxide

: sodium (2S,3S)-(-)-3-methylmercaptomalate

Conditions

Conditions	Yield
Stage #1: (2R,3R)-oxirane-2,3-dicarboxylic acid With sodium hydroxide In water pH=7; Stage #2: sodium thiomethoxide In water at 0℃; Stage #3: With acetic acid In water pH=10;	57%

: 17015-08-6
(2R,3R)-oxirane-2,3-dicarboxylic acid

: DL-erythro-β-hydroxyaspartic acid

Conditions

Conditions	Yield
Stage #1: (2R,3R)-oxirane-2,3-dicarboxylic acid With ammonium hydroxide In water at 50℃; for 24h; Stage #2: With hydrogenchloride In water at 4℃; for 72h; pH=3;	55.1%

: 68-11-1
mercaptoacetic acid

: 17015-08-6
(2R,3R)-oxirane-2,3-dicarboxylic acid

: 1377677-68-3
(2S,3S)-(-)-thiahomoisocitrate

Conditions

Conditions	Yield
With sodium hydroxide In water at 80℃; for 10h; pH=12;	42%

: 17087-75-1
(-)-trans-2,3-oxiranedicarboxylic acid

: 17015-08-6
(2R,3R)-oxirane-2,3-dicarboxylic acid

: 141-36-6, 3272-11-5, 16533-72-5, 17015-08-6, 17087-75-1, 22734-83-4
DL-trans-epoxysuccinic acid

: 17015-08-6
(2R,3R)-oxirane-2,3-dicarboxylic acid

A: 147-73-9
meso-tartaric acid

B: 87-69-4
L-Tartaric acid

Conditions

Conditions	Yield
With water
With potassium hydroxide

: 100-46-9
benzylamine

: 17015-08-6
(2R,3R)-oxirane-2,3-dicarboxylic acid

: 17126-60-2
D-(-)-Benzyl-erythro-β-hydroxy-asparaginsaeure

Conditions

Conditions	Yield
In water Heating;

: 7647-01-0
hydrogenchloride

: 60-29-7
diethyl ether

: 17015-08-6
(2R,3R)-oxirane-2,3-dicarboxylic acid

: 74841-95-5
(-)(2S:3S)-3-chloro-2-hydroxy-succinic acid

Conditions

Conditions	Yield
at 20℃;

...Expand

: 7732-18-5
water

: 17015-08-6
(2R,3R)-oxirane-2,3-dicarboxylic acid

A: 87-69-4
L-Tartaric acid

B: 75-07-0
acetaldehyde

C: 87-69-4
tartaric acid

Conditions

Conditions	Yield
Product distribution;

...Expand

: 17015-08-6
(2R,3R)-oxirane-2,3-dicarboxylic acid

: 100-51-6
benzyl alcohol

: 646532-93-6
(2R,3R)-oxirane-2,3-dicarboxylic acid monobenzyl ester

Conditions

Conditions	Yield
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In N,N-dimethyl-formamide at 20℃; for 15h;

: 7440-44-0
pyrographite

: 17015-08-6
(2R,3R)-oxirane-2,3-dicarboxylic acid

: 1186-90-9, 1860-87-3, 4294-45-5, 5174-55-0, 5753-30-0, 6532-76-9, 7298-98-8, 7298-99-9, 16417-36-0, 71653-06-0, 81601-40-3
L-threo-3-hydroxyaspartic acid

Conditions

Conditions	Yield
With hydrogenchloride; ammonium hydroxide In water	73.1 g (81.7%)

: Fmoc-Ser(tBu)-Wang resin

: 18822-58-7
(S)-O-tert-butylserine

: 102747-84-2
5-trityl-L-glutamine

: 147-85-3
L-proline

: 17015-08-6
(2R,3R)-oxirane-2,3-dicarboxylic acid

: 1631180-58-9
C25H37N7O12

Conditions

Conditions	Yield
Stage #1: Fmoc-Ser(tBu)-Wang resin With piperidine; 1,8-diazabicyclo[5.4.0]undec-7-ene In N,N-dimethyl-formamide Rink-amide MBHA resin; Stage #2: L-proline With benzotriazol-1-ol; dicyclohexyl-carbodiimide In N,N-dimethyl-formamide at 20℃; for 1h; Rink-amide MBHA resin; Stage #3: (S)-O-tert-butylserine; 5-trityl-L-glutamine; L-proline; (2R,3R)-oxirane-2,3-dicarboxylic acid Further stages;

...Expand

: Fmoc-Ser(tBu)-Wang resin

: 147-85-3
L-proline

: 17015-08-6
(2R,3R)-oxirane-2,3-dicarboxylic acid

: (S)-2-amino-5-(3-(2,2,4,6,7-pentamethyl-2,3-dihydrobenzofuran-5-ylsulfonyl)guanidino)pentanoic acid

: 1631179-75-3
C28H43N9O10

Conditions

Conditions	Yield
Stage #1: Fmoc-Ser(tBu)-Wang resin With piperidine; 1,8-diazabicyclo[5.4.0]undec-7-ene In N,N-dimethyl-formamide Rink-amide MBHA resin; Stage #2: L-proline With benzotriazol-1-ol; dicyclohexyl-carbodiimide In N,N-dimethyl-formamide at 20℃; for 1h; Rink-amide MBHA resin; Stage #3: L-proline; (2R,3R)-oxirane-2,3-dicarboxylic acid; (S)-2-amino-5-(3-(2,2,4,6,7-pentamethyl-2,3-dihydrobenzofuran-5-ylsulfonyl)guanidino)pentanoic acid Further stages;

Yield

Stage #1: Fmoc-Ser(tBu)-Wang resin With piperidine; 1,8-diazabicyclo[5.4.0]undec-7-ene In N,N-dimethyl-formamide Rink-amide MBHA resin;
Stage #2: L-proline With benzotriazol-1-ol; dicyclohexyl-carbodiimide In N,N-dimethyl-formamide at 20℃; for 1h; Rink-amide MBHA resin;
Stage #3: L-proline; (2R,3R)-oxirane-2,3-dicarboxylic acid; (S)-2-amino-5-(3-(2,2,4,6,7-pentamethyl-2,3-dihydrobenzofuran-5-ylsulfonyl)guanidino)pentanoic acid Further stages;

...Expand

: Fmoc-Ser(tBu)-Wang resin

: 4378-13-6
(O-tert-butyl)-L-threonine

: 147-85-3
L-proline

: 17015-08-6
(2R,3R)-oxirane-2,3-dicarboxylic acid

: 1631180-28-3
C26H38N6O11

Conditions

Conditions	Yield
Stage #1: Fmoc-Ser(tBu)-Wang resin With piperidine; 1,8-diazabicyclo[5.4.0]undec-7-ene In N,N-dimethyl-formamide Rink-amide MBHA resin; Stage #2: L-proline With benzotriazol-1-ol; dicyclohexyl-carbodiimide In N,N-dimethyl-formamide at 20℃; for 1h; Rink-amide MBHA resin; Stage #3: (O-tert-butyl)-L-threonine; L-proline; (2R,3R)-oxirane-2,3-dicarboxylic acid Further stages;

...Expand

: Fmoc-Ser(tBu)-Wang resin

: 18822-58-7
(S)-O-tert-butylserine

: 147-85-3
L-proline

: 17015-08-6
(2R,3R)-oxirane-2,3-dicarboxylic acid

: 1631179-65-1
C25H36N6O11

Conditions

Conditions	Yield
Stage #1: Fmoc-Ser(tBu)-Wang resin With piperidine; 1,8-diazabicyclo[5.4.0]undec-7-ene In N,N-dimethyl-formamide Rink-amide MBHA resin; Stage #2: L-proline With benzotriazol-1-ol; dicyclohexyl-carbodiimide In N,N-dimethyl-formamide at 20℃; for 1h; Rink-amide MBHA resin; Stage #3: (S)-O-tert-butylserine; L-proline; (2R,3R)-oxirane-2,3-dicarboxylic acid Further stages;

...Expand

: Fmoc-Ser(tBu)-Wang resin

: 18822-58-7
(S)-O-tert-butylserine

: 147-85-3
L-proline

: 17015-08-6
(2R,3R)-oxirane-2,3-dicarboxylic acid

: 1631180-31-8
C23H34N6O12

Conditions

Conditions	Yield
Stage #1: Fmoc-Ser(tBu)-Wang resin With piperidine; 1,8-diazabicyclo[5.4.0]undec-7-ene In N,N-dimethyl-formamide Rink-amide MBHA resin; Stage #2: L-proline With benzotriazol-1-ol; dicyclohexyl-carbodiimide In N,N-dimethyl-formamide at 20℃; for 1h; Rink-amide MBHA resin; Stage #3: (S)-O-tert-butylserine; L-proline; (2R,3R)-oxirane-2,3-dicarboxylic acid Further stages;

...Expand

: 17015-08-6
(2R,3R)-oxirane-2,3-dicarboxylic acid

A: 5753-30-0
erythro-β-hydroxy-D-aspartic acid

B: 7298-98-8
2-(S)-amino-3-(R)-hydroxysuccinic acid

Conditions

Conditions	Yield
With ammonium hydroxide at 0 - 48℃; for 48h;

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Antimex Chemical Limied

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