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inquiry2-(AMINOMETHYL)-3-CHLORO-5-(TRIFLUOROMETHYL)-PYRIDINE HYDROCHLORIDE CAS:175277-74-4 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical interme
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inquiryBUTTPARK 145\04-45; 2-(AMINOMETHYL)-3-CHLORO-5-(TRIFLUOROMETHYL)-PYRIDINE HYDROCHLORIDE;[3-Chloro-5-(trifluoromethyl)-2-pyridyl]methylamine hydrochloride;2-(Aminomethyl)- 3-chloro-5-(trifluoromethyl)pyridine hydrochloride 97%; 2-(Aminomethyl)-3-chl
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inquiryJinhua huayi chemical co., ltd. is dedicated to the development, production and marketing of chemicals. On the basis of equality and mutual benefit, and under the principle of customer first, credit first, quality first, we are ready to join hands
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inquiry★.Best quality according to requirement ★.Competitive price in China market ★.Mature Technical support ★.Professional logistic support
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inquiryAppearance:solid or liquid Storage:sealed in cool and dry place Package:As customer's requested Application:Pharma Intermediate Transportation:by courier/air/sea Port:Any port in China
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inquiry2-Pyridinemethanamine,3-chloro-5-(trifluoromethyl)- cas 175277-74-4Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
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inquiry(3-chloro-5-trifluoromethyl-pyridin-2-yl)methylamine
Conditions | Yield |
---|---|
With Ni-doped silica; hydrogen at 30℃; under 15001.5 Torr; Concentration; Pressure; Reagent/catalyst; | 98.57% |
With hydrogenchloride; tin(ll) chloride In ethanol Reflux; |
3-chloro-2-cyano-5-(trifluoromethyl)pyridine
(3-chloro-5-trifluoromethyl-pyridin-2-yl)methylamine
Conditions | Yield |
---|---|
Stage #1: 3-chloro-2-cyano-5-(trifluoromethyl)pyridine With sodium hydroxide In methanol at 70℃; Stage #2: With sodium hypochlorite In methanol at 10℃; Solvent; Reagent/catalyst; Temperature; | 98% |
With sulfuric acid; 20% palladium hydroxide-activated charcoal; tetrabutylammomium bromide; hydrogen In methanol at 20℃; under 15001.5 Torr; | 96.4% |
3-chloro-2-cyano-5-(trifluoromethyl)pyridine
A
(3-chloro-5-trifluoromethyl-pyridin-2-yl)methylamine
B
1-[5-(trifluoromethyl)pyridin-2-yl]methanamine
Conditions | Yield |
---|---|
With hydrogen; acetic acid; nickel at 40 - 45℃; under 13501.4 Torr; for 4h; | A 97% B 0.05% |
(3-chloro-5-trifluoromethyl-pyridin-2-yl)methylamine
Conditions | Yield |
---|---|
Stage #1: C10H10ClF3N2O2*ClH With hydrogenchloride In water at 90 - 100℃; for 8h; Stage #2: With sodium hydroxide In water pH=9 - 9.2; Concentration; Temperature; | 90.9% |
(3-chloro-5-trifluoromethyl-pyridin-2-yl)methylamine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: hydrogenchloride; water / toluene / 20 °C / Inert atmosphere 2: hydrogenchloride / water / 5 h / Reflux; Inert atmosphere View Scheme |
(3-chloro-5-trifluoromethyl-pyridin-2-yl)methylamine
Conditions | Yield |
---|---|
With hydrogenchloride In water for 5h; Reflux; Inert atmosphere; |
2,3-dichloro-5-trifluoromethylpyridine
(3-chloro-5-trifluoromethyl-pyridin-2-yl)methylamine
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: tetrabutylammomium bromide; potassium carbonate / toluene; propiononitrile / 22 h / Inert atmosphere; Reflux 2: hydrogenchloride; water / toluene / 20 °C / Inert atmosphere 3: hydrogenchloride / water / 5 h / Reflux; Inert atmosphere View Scheme | |
Multi-step reaction with 2 steps 1: potassium hydroxide / dimethyl sulfoxide / 20 °C 2: tin(ll) chloride; hydrogenchloride / ethanol / Reflux View Scheme | |
Multi-step reaction with 3 steps 1.1: potassium carbonate; tetraethylammonium bromide / toluene / 18 h / 90 °C / Inert atmosphere 2.1: sodium tetraborate; hydrogenchloride / water / 12 h / 25 °C / Inert atmosphere 3.1: hydrogenchloride / water / 8 h / 90 - 100 °C 3.2: pH 9 - 9.2 View Scheme |
Conditions | Yield |
---|---|
With acetic anhydride at 20℃; for 16h; Concentration; | 91% |
With acetic anhydride at 20℃; for 16h; |
(3-chloro-5-trifluoromethyl-pyridin-2-yl)methylamine
3,4,6-tribromopyridazine
Conditions | Yield |
---|---|
With triethylamine In methanol at 20℃; | 85% |
(3-chloro-5-trifluoromethyl-pyridin-2-yl)methylamine
3,4,6-trichloropyridazine
Conditions | Yield |
---|---|
With triethylamine In methanol at 20℃; | 82.2% |
(3-chloro-5-trifluoromethyl-pyridin-2-yl)methylamine
thiophosgene
8-chloro-6-(trifluoromethyl)imidazo[1,5-a]pyridine-3-thiol
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In dichloromethane; water at 0 - 20℃; Inert atmosphere; | 80% |
(3-chloro-5-trifluoromethyl-pyridin-2-yl)methylamine
Conditions | Yield |
---|---|
Stage #1: 2-methyl-4-(5-(trifluoromethyl)-5-(3,4,5-trifluorophenyl)-4,5-dihydroisoxazol-3-yl)benzoic acid With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In dichloromethane at 0℃; for 2h; Stage #2: (3-chloro-5-trifluoromethyl-pyridin-2-yl)methylamine In dichloromethane at 20℃; for 15h; | 76% |
(3-chloro-5-trifluoromethyl-pyridin-2-yl)methylamine
bis(trichloromethyl) carbonate
8-chloro-6-(trifluoromethyl)imidazo[1,5-a]pyridin-3-ol
Conditions | Yield |
---|---|
With sodium hydrogencarbonate In dichloromethane; water at 0 - 20℃; Inert atmosphere; | 72% |
(3-chloro-5-trifluoromethyl-pyridin-2-yl)methylamine
4-[5-(3,5-dichloro-4-fluorophenyl)-5-(trifluoromethyl)-4,5-dihydro-1,2-oxazol-3-yl]-2-methylbenzoic acid
Conditions | Yield |
---|---|
Stage #1: 4-[5-(3,5-dichloro-4-fluorophenyl)-5-(trifluoromethyl)-4,5-dihydro-1,2-oxazol-3-yl]-2-methylbenzoic acid With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In dichloromethane at 0℃; for 2h; Stage #2: (3-chloro-5-trifluoromethyl-pyridin-2-yl)methylamine In dichloromethane at 20℃; for 15h; | 72% |
(3-chloro-5-trifluoromethyl-pyridin-2-yl)methylamine
p-(chloromethyl)benzoyl chloride
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; | 68% |
(3-chloro-5-trifluoromethyl-pyridin-2-yl)methylamine
4-(4'-trifluoromethyl-biphenyl-2-carbonylamino)-1-methyl-pyrrole-2-carboxylic acid
N-ethyl-N,N-diisopropylamine
N-(3-chloro-5-trifluoromethylpyridin-2-yl-methyl)-4-(4'-trifluoromethylbiphenyl-2-carbonylamino)-1-methyl-pyrrole-2-carboxylic acid amide
Conditions | Yield |
---|---|
With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate In N-methyl-acetamide |
(3-chloro-5-trifluoromethyl-pyridin-2-yl)methylamine
4-(4'-trifluoromethyl-biphenyl-2-carbonylamino)-1-methyl-pyrrole-2-carboxylic acid
N-(3-chloro-5-trifluoromethylpyridin-2-yl-methyl)-4-(4'-trifluoromethylbiphenyl-2-carbonylamino)-1-methyl-pyrrole-2-carboxylic acid amide
Conditions | Yield |
---|---|
With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine In N-methyl-acetamide |
(3-chloro-5-trifluoromethyl-pyridin-2-yl)methylamine
2-amino-4-methanesulfinyl-6-(4-methyl-furan-2-yl)-pyrimidine-5-carbonitrile
2-Amino-4-[(3-chloro-5-trifluoromethyl-pyridin-2-yl-methyl)-amino]-6-(4-methyl-furan-2-yl)-pyrimidine-5-carbonitrile
Conditions | Yield |
---|---|
In 1,2-dimethoxyethane |
(3-chloro-5-trifluoromethyl-pyridin-2-yl)methylamine
2-trifluoromethylbenzoyl chloride
N-[(3-Chloro-5-trifluoromethyl-pyridin-2-yl)methyl]-α,α,α-trifluoro-o-toluamide
Conditions | Yield |
---|---|
With triethylamine In water; ethyl acetate |
(3-chloro-5-trifluoromethyl-pyridin-2-yl)methylamine
2-furancarbonyl chloride
B
N-[(3-Chloro-5-trifluoromethyl-pyridin-2-yl)methyl]-2-furamide
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran |
(3-chloro-5-trifluoromethyl-pyridin-2-yl)methylamine
ethyl 2-(2-amino-4,6-dichloropyrimidin-5-yl)acetate
ethyl 2-(2-amino-4-chloro-6-((3-chloro-5-(trifluoromethyl)pyridin-2-yl)methylamino)pyrimidin-5-yl)acetate
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In butan-1-ol at 80 - 90℃; |
(3-chloro-5-trifluoromethyl-pyridin-2-yl)methylamine
3-(8-chloro-6-(trifluoromethyl)imidazo[1,5-a]pyridin-3-yl)phenyl acetate
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 20 °C 2: trichlorophosphate / benzene / 6 h / 20 °C / Reflux View Scheme |
(3-chloro-5-trifluoromethyl-pyridin-2-yl)methylamine
3-(8-chloro-6-(trifluoromethyl)imidazo[1,5-a]pyridin-3-yl)phenyl cyclohexane carboxylate
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 20 °C 2: trichlorophosphate / benzene / 6 h / 20 °C / Reflux 3: sodium hydroxide / tetrahydrofuran; water / 3 h / 20 °C 4: triethylamine View Scheme |
(3-chloro-5-trifluoromethyl-pyridin-2-yl)methylamine
1-(3-(8-chloro-6-(trifluoromethyl)imidazo[1,5-a]pyridin-3-yl)phenoxy)propan-2-one
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 20 °C 2: trichlorophosphate / benzene / 6 h / 20 °C / Reflux 3: sodium hydroxide / tetrahydrofuran; water / 3 h / 20 °C 4: potassium carbonate View Scheme |
(3-chloro-5-trifluoromethyl-pyridin-2-yl)methylamine
N-(3-(8-chloro-6-(trifluoromethyl)imidazo[1,5-a]pyridin-3-yl)phenyl)acetamide
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 20 °C 2: trifluoroacetic acid / dichloromethane / 20 °C 3: dmap / dichloromethane / 20 °C 4: pyridine; trichlorophosphate / 1,2-dichloro-ethane / 7 h / 20 °C / Reflux View Scheme |
(3-chloro-5-trifluoromethyl-pyridin-2-yl)methylamine
N-(3-(8-chloro-6-(trifluoromethyl)imidazo[1,5-a]pyridin-3-yl)phenyl)cyclohexane carboxamide
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 20 °C 2: trifluoroacetic acid / dichloromethane / 20 °C 3: triethylamine; dmap / dichloromethane / 20 °C 4: pyridine; trichlorophosphate / 1,2-dichloro-ethane / 7 h / 20 °C / Reflux View Scheme |
(3-chloro-5-trifluoromethyl-pyridin-2-yl)methylamine
1-(3-(8-chloro-6-(trifluoromethyl)imidazo[1,5-a]pyridin-3-yl)phenyl)pyrrolidine-2,5-dione
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 20 °C 2: trifluoroacetic acid / dichloromethane / 20 °C 3: potassium carbonate / acetonitrile / Reflux 4: pyridine; trichlorophosphate / 1,2-dichloro-ethane / 7 h / 20 °C / Reflux View Scheme |
(3-chloro-5-trifluoromethyl-pyridin-2-yl)methylamine
tert-butyl (3-(8-chloro-6-(trifluoromethyl)imidazo[1,5-a]pyridin-3-yl)phenyl)carbamate
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 20 °C 2: pyridine; trichlorophosphate / 1,2-dichloro-ethane / 7 h / 20 °C / Reflux View Scheme |
(3-chloro-5-trifluoromethyl-pyridin-2-yl)methylamine
C14H8ClF3N2O
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 20 °C 2: trichlorophosphate / benzene / 6 h / 20 °C / Reflux 3: sodium hydroxide / tetrahydrofuran; water / 3 h / 20 °C View Scheme |
(3-chloro-5-trifluoromethyl-pyridin-2-yl)methylamine
C16H13ClF3N3O2
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 20 °C 2: trifluoroacetic acid / dichloromethane / 20 °C 3: dmap / dichloromethane / 20 °C View Scheme |
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