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Jinan Finer Chemical Co., Ltd

Product description: Product name N,N-Diisopropylethylamine CAS number 7087-68-5 Assay ≥99% Appearance Colorless or yellowish liquid Capacity 500mt/year Application Pharmaceu

N,N-Diisopropylethylamine

Cas:7087-68-5

Min.Order:1 Kilogram

FOB Price: $12.0

Type:Lab/Research institutions

inquiry

Henan Tianfu Chemical Co., Ltd.

High purity CAS 7087-68-5 N,N-Diisopropylethylamine in stock Our main business covers the fields below: 1.Noble Metal Catalysts (Pt.Pd...) 2.Organic Phosphine Ligands (Tert-butyl-phosphine.Cyclohexyl-phosphine...) 3.OLED intermediates (

High purity CAS 7087-68-5 N,N-Diisopropylethylamine in stock

Cas:7087-68-5

Min.Order:1 Gram

FOB Price: $100.0

Type:Lab/Research institutions

inquiry
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Synthetic route

tetraethylammonium chloride
56-34-8

tetraethylammonium chloride

diisopropylamine
108-18-9

diisopropylamine

N-ethyl-N,N-diisopropylamine
7087-68-5

N-ethyl-N,N-diisopropylamine

Conditions
ConditionsYield
With potassium hydroxide In butan-1-ol at 115℃; for 7h; Solvent; Reagent/catalyst; Temperature;97.2%
chloroethane
75-00-3

chloroethane

diisopropylamine
108-18-9

diisopropylamine

N-ethyl-N,N-diisopropylamine
7087-68-5

N-ethyl-N,N-diisopropylamine

Conditions
ConditionsYield
With lithium chloride; zinc(II) chloride at 190℃; under 16501.7 Torr; for 10h; Catalytic behavior; Temperature; Pressure; Time; Reagent/catalyst; Autoclave;96.7%
ethanol
64-17-5

ethanol

diisopropylamine
108-18-9

diisopropylamine

N-ethyl-N,N-diisopropylamine
7087-68-5

N-ethyl-N,N-diisopropylamine

Conditions
ConditionsYield
With iron(III) oxide; (triphenylphosphine)ruthenium acetate at 78℃; for 24h; Reagent/catalyst; Molecular sieve;92%
With ammonium acetate In aq. phosphate buffer at 34℃; for 10h; pH=8.5; Electrochemical reaction;28%
With Ru(OAc)2(1,1′-bis(diisopropylphosphino)ferrocene)(CO); trifluoroacetic acid at 78℃; for 24h; Inert atmosphere; Schlenk technique;
acetaldehyde
75-07-0

acetaldehyde

diisopropylamine
108-18-9

diisopropylamine

N-ethyl-N,N-diisopropylamine
7087-68-5

N-ethyl-N,N-diisopropylamine

Conditions
ConditionsYield
With hydrogen; ZrO2-containing catalyst at 120 - 150℃; under 60006 Torr;80%
Stage #1: acetaldehyde; diisopropylamine With formic acid at 90 - 110℃; for 8.5h;
Stage #2: With hydrogenchloride In water
Stage #3: With sodium hydroxide In water
With hydrogen; 5% Pd(II)/C(eggshell) at 100℃; under 18751.9 Torr; for 9h; Product distribution / selectivity; Autoclave; Inert atmosphere;95.2 %Chromat.
With 5% Pd/C; hydrogen at 120℃; under 18751.9 Torr; for 3h; Autoclave;
ethyl iodide
75-03-6

ethyl iodide

diisopropylamine
108-18-9

diisopropylamine

N-ethyl-N,N-diisopropylamine
7087-68-5

N-ethyl-N,N-diisopropylamine

Conditions
ConditionsYield
With butanone
diethyl sulfate
64-67-5

diethyl sulfate

diisopropylamine
108-18-9

diisopropylamine

N-ethyl-N,N-diisopropylamine
7087-68-5

N-ethyl-N,N-diisopropylamine

Conditions
ConditionsYield
at 140℃;
at 140℃;
diisopropylamine
108-18-9

diisopropylamine

methyl iodide
74-88-4

methyl iodide

N-ethyl-N,N-diisopropylamine
7087-68-5

N-ethyl-N,N-diisopropylamine

4-Methoxyphenylacetic acid
104-01-8

4-Methoxyphenylacetic acid

1-ethyl-3-(3-dimethylaminopropyl)carbotiimide

1-ethyl-3-(3-dimethylaminopropyl)carbotiimide

N-[(R)-1-{3-(1-tert-butoxycarbonyl-4-piperidyl)propionyl}-3-piperidylcarbonyl]-2(S)-amino-β-alanine

N-[(R)-1-{3-(1-tert-butoxycarbonyl-4-piperidyl)propionyl}-3-piperidylcarbonyl]-2(S)-amino-β-alanine

N-Trimethylsilylacetamide
13435-12-6

N-Trimethylsilylacetamide

N-ethyl-N,N-diisopropylamine
7087-68-5

N-ethyl-N,N-diisopropylamine

Conditions
ConditionsYield
In dichloromethane; N,N-dimethyl-formamide
...Expand
ethyl bromoacetate
105-36-2

ethyl bromoacetate

A

pyrrolidinylacetate ester

pyrrolidinylacetate ester

B

N-ethyl-N,N-diisopropylamine
7087-68-5

N-ethyl-N,N-diisopropylamine

Conditions
ConditionsYield
In dichloromethane; acetonitrile
vinylsulfomethylpolystyrene resin

vinylsulfomethylpolystyrene resin

n-dioctylamine
1120-48-5

n-dioctylamine

allyl bromide
106-95-6

allyl bromide

N-ethyl-N,N-diisopropylamine
7087-68-5

N-ethyl-N,N-diisopropylamine

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine In 4-(dicyanomethylene)-2-methyl-6-(p-dimethylaminostyryl)-4H-pyran; N,N-dimethyl-formamide
...Expand
acetaldehyde
75-07-0

acetaldehyde

diisopropylamine
108-18-9

diisopropylamine

A

ethanol
64-17-5

ethanol

B

N-ethyl-N,N-diisopropylamine
7087-68-5

N-ethyl-N,N-diisopropylamine

Conditions
ConditionsYield
With hydrogen; 5% Pd(II)/C(eggshell) at 100℃; under 18751.9 Torr; Product distribution / selectivity; Autoclave; Inert atmosphere; Industry scale;A 8.0 %Chromat.
B 81.8 %Chromat.
...Expand
acetaldehyde
75-07-0

acetaldehyde

diisopropylamine
108-18-9

diisopropylamine

A

N-butyldiisopropylamine
41781-44-6

N-butyldiisopropylamine

B

N-ethyl-N,N-diisopropylamine
7087-68-5

N-ethyl-N,N-diisopropylamine

Conditions
ConditionsYield
With hydrogen; 5% Pd(II)/C(eggshell) at 120℃; under 37503.8 Torr; Product distribution / selectivity; Autoclave; Inert atmosphere; Industry scale;A 6.3 %Chromat.
B 81.1 %Chromat.
...Expand
diethyl ether
60-29-7

diethyl ether

diisopropylamine
108-18-9

diisopropylamine

N-ethyl-N,N-diisopropylamine
7087-68-5

N-ethyl-N,N-diisopropylamine

Conditions
ConditionsYield
With alumina at 360℃; under 760.051 Torr; Temperature; Inert atmosphere; Gas phase; Green chemistry;
tetraethylammonium chloride
56-34-8

tetraethylammonium chloride

diisopropylamine
108-18-9

diisopropylamine

N-ethyl-N,N-diisopropylamine
7087-68-5

N-ethyl-N,N-diisopropylamine

Conditions
ConditionsYield
With potassium hydroxide In butan-1-ol at 115℃; for 7h; Solvent; Reagent/catalyst; Temperature;97.2%
chloroethane
75-00-3

chloroethane

diisopropylamine
108-18-9

diisopropylamine

N-ethyl-N,N-diisopropylamine
7087-68-5

N-ethyl-N,N-diisopropylamine

Conditions
ConditionsYield
With lithium chloride; zinc(II) chloride at 190℃; under 16501.7 Torr; for 10h; Catalytic behavior; Temperature; Pressure; Time; Reagent/catalyst; Autoclave;96.7%
ethanol
64-17-5

ethanol

diisopropylamine
108-18-9

diisopropylamine

N-ethyl-N,N-diisopropylamine
7087-68-5

N-ethyl-N,N-diisopropylamine

Conditions
ConditionsYield
With iron(III) oxide; (triphenylphosphine)ruthenium acetate at 78℃; for 24h; Reagent/catalyst; Molecular sieve;92%
With ammonium acetate In aq. phosphate buffer at 34℃; for 10h; pH=8.5; Electrochemical reaction;28%
With Ru(OAc)2(1,1′-bis(diisopropylphosphino)ferrocene)(CO); trifluoroacetic acid at 78℃; for 24h; Inert atmosphere; Schlenk technique;
acetaldehyde
75-07-0

acetaldehyde

diisopropylamine
108-18-9

diisopropylamine

N-ethyl-N,N-diisopropylamine
7087-68-5

N-ethyl-N,N-diisopropylamine

Conditions
ConditionsYield
With hydrogen; ZrO2-containing catalyst at 120 - 150℃; under 60006 Torr;80%
Stage #1: acetaldehyde; diisopropylamine With formic acid at 90 - 110℃; for 8.5h;
Stage #2: With hydrogenchloride In water
Stage #3: With sodium hydroxide In water
With hydrogen; 5% Pd(II)/C(eggshell) at 100℃; under 18751.9 Torr; for 9h; Product distribution / selectivity; Autoclave; Inert atmosphere;95.2 %Chromat.
With 5% Pd/C; hydrogen at 120℃; under 18751.9 Torr; for 3h; Autoclave;
ethyl iodide
75-03-6

ethyl iodide

diisopropylamine
108-18-9

diisopropylamine

N-ethyl-N,N-diisopropylamine
7087-68-5

N-ethyl-N,N-diisopropylamine

Conditions
ConditionsYield
With butanone
diethyl sulfate
64-67-5

diethyl sulfate

diisopropylamine
108-18-9

diisopropylamine

N-ethyl-N,N-diisopropylamine
7087-68-5

N-ethyl-N,N-diisopropylamine

Conditions
ConditionsYield
at 140℃;
at 140℃;
diisopropylamine
108-18-9

diisopropylamine

methyl iodide
74-88-4

methyl iodide

N-ethyl-N,N-diisopropylamine
7087-68-5

N-ethyl-N,N-diisopropylamine

4-Methoxyphenylacetic acid
104-01-8

4-Methoxyphenylacetic acid

1-ethyl-3-(3-dimethylaminopropyl)carbotiimide

1-ethyl-3-(3-dimethylaminopropyl)carbotiimide

N-[(R)-1-{3-(1-tert-butoxycarbonyl-4-piperidyl)propionyl}-3-piperidylcarbonyl]-2(S)-amino-β-alanine

N-[(R)-1-{3-(1-tert-butoxycarbonyl-4-piperidyl)propionyl}-3-piperidylcarbonyl]-2(S)-amino-β-alanine

N-Trimethylsilylacetamide
13435-12-6

N-Trimethylsilylacetamide

N-ethyl-N,N-diisopropylamine
7087-68-5

N-ethyl-N,N-diisopropylamine

Conditions
ConditionsYield
In dichloromethane; N,N-dimethyl-formamide
...Expand
ethyl bromoacetate
105-36-2

ethyl bromoacetate

A

pyrrolidinylacetate ester

pyrrolidinylacetate ester

B

N-ethyl-N,N-diisopropylamine
7087-68-5

N-ethyl-N,N-diisopropylamine

Conditions
ConditionsYield
In dichloromethane; acetonitrile
vinylsulfomethylpolystyrene resin

vinylsulfomethylpolystyrene resin

n-dioctylamine
1120-48-5

n-dioctylamine

allyl bromide
106-95-6

allyl bromide

N-ethyl-N,N-diisopropylamine
7087-68-5

N-ethyl-N,N-diisopropylamine

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine In 4-(dicyanomethylene)-2-methyl-6-(p-dimethylaminostyryl)-4H-pyran; N,N-dimethyl-formamide
...Expand
acetaldehyde
75-07-0

acetaldehyde

diisopropylamine
108-18-9

diisopropylamine

A

ethanol
64-17-5

ethanol

B

N-ethyl-N,N-diisopropylamine
7087-68-5

N-ethyl-N,N-diisopropylamine

Conditions
ConditionsYield
With hydrogen; 5% Pd(II)/C(eggshell) at 100℃; under 18751.9 Torr; Product distribution / selectivity; Autoclave; Inert atmosphere; Industry scale;A 8.0 %Chromat.
B 81.8 %Chromat.
...Expand
acetaldehyde
75-07-0

acetaldehyde

diisopropylamine
108-18-9

diisopropylamine

A

N-butyldiisopropylamine
41781-44-6

N-butyldiisopropylamine

B

N-ethyl-N,N-diisopropylamine
7087-68-5

N-ethyl-N,N-diisopropylamine

Conditions
ConditionsYield
With hydrogen; 5% Pd(II)/C(eggshell) at 120℃; under 37503.8 Torr; Product distribution / selectivity; Autoclave; Inert atmosphere; Industry scale;A 6.3 %Chromat.
B 81.1 %Chromat.
...Expand
diethyl ether
60-29-7

diethyl ether

diisopropylamine
108-18-9

diisopropylamine

N-ethyl-N,N-diisopropylamine
7087-68-5

N-ethyl-N,N-diisopropylamine

Conditions
ConditionsYield
With alumina at 360℃; under 760.051 Torr; Temperature; Inert atmosphere; Gas phase; Green chemistry;
2-(5,8-Dimethoxy-quinolin-4-yl)-phenylamine
114552-24-8

2-(5,8-Dimethoxy-quinolin-4-yl)-phenylamine

N-ethyl-N,N-diisopropylamine
7087-68-5

N-ethyl-N,N-diisopropylamine

trifluoroacetic anhydride
407-25-0

trifluoroacetic anhydride

N-[2-(5,8-Dimethoxy-quinolin-4-yl)-phenyl]-2,2,2-trifluoro-acetamide
114552-23-7

N-[2-(5,8-Dimethoxy-quinolin-4-yl)-phenyl]-2,2,2-trifluoro-acetamide

Conditions
ConditionsYield
at 0℃; for 0.5h;100%
...Expand
N-ethyl-N,N-diisopropylamine
7087-68-5

N-ethyl-N,N-diisopropylamine

phenylacetylene
536-74-3

phenylacetylene

4-(1-methyl-2,4-dioxo-6-(2-phenylethynyl)-1,4-dihydro-2H-quinazolin-3-ylmethyl)-benzoic acid
451473-18-0

4-(1-methyl-2,4-dioxo-6-(2-phenylethynyl)-1,4-dihydro-2H-quinazolin-3-ylmethyl)-benzoic acid

Conditions
ConditionsYield
CuI; dichlorobis(triphenylphosphine)palladium[II]100%
di-tert-butyl dicarbonate
24424-99-5

di-tert-butyl dicarbonate

N-ethyl-N,N-diisopropylamine
7087-68-5

N-ethyl-N,N-diisopropylamine

4-iodophenylalanine tert-butyl ester

4-iodophenylalanine tert-butyl ester

N-[(1,1-dimethylethoxy)carbonyl]-4-iodo-L-phenylalanine 1,1-dimethylethyl ester
217326-89-1

N-[(1,1-dimethylethoxy)carbonyl]-4-iodo-L-phenylalanine 1,1-dimethylethyl ester

Conditions
ConditionsYield
In dichloromethane100%
...Expand
concentrated H2 SO4

concentrated H2 SO4

di-tert-butyl dicarbonate
24424-99-5

di-tert-butyl dicarbonate

4-iodo-L-phenylalanine
1991-81-7, 14173-41-2, 24250-85-9, 62561-75-5

4-iodo-L-phenylalanine

N-ethyl-N,N-diisopropylamine
7087-68-5

N-ethyl-N,N-diisopropylamine

4-iodophenylalanine tert-butyl ester

4-iodophenylalanine tert-butyl ester

A

(S)-2'-methoxybiphenylalanine t-butyl Ester Hydrochloride

(S)-2'-methoxybiphenylalanine t-butyl Ester Hydrochloride

B

N-[(1,1-dimethylethoxy)carbonyl]-4-iodo-L-phenylalanine 1,1-dimethylethyl ester
217326-89-1

N-[(1,1-dimethylethoxy)carbonyl]-4-iodo-L-phenylalanine 1,1-dimethylethyl ester

Conditions
ConditionsYield
With hydrogenchloride; sodium hydroxide In dichloromethane; diethylene glycol dimethyl ether; ethyl acetateA 100%
B n/a
...Expand
1-(4-benzyloxy-benzenesulfonyl)-5-methoxy-piperidine-2-carboxylic acid

1-(4-benzyloxy-benzenesulfonyl)-5-methoxy-piperidine-2-carboxylic acid

O-allylhydroxylamine hydrochloride
38945-21-0

O-allylhydroxylamine hydrochloride

N-ethyl-N,N-diisopropylamine
7087-68-5

N-ethyl-N,N-diisopropylamine

1-(4-benzyloxy-benzenesulfonyl)-5-methoxy-piperidine-2-carboxylic acid allyloxy-amide

1-(4-benzyloxy-benzenesulfonyl)-5-methoxy-piperidine-2-carboxylic acid allyloxy-amide

Conditions
ConditionsYield
With benzotriazol-1-ol In dichloromethane100%
...Expand
ditertbutyldicarbonate

ditertbutyldicarbonate

N-ethyl-N,N-diisopropylamine
7087-68-5

N-ethyl-N,N-diisopropylamine

4-iodophenylalanine tert-butyl ester

4-iodophenylalanine tert-butyl ester

N-[(1,1-dimethylethoxy)carbonyl]-4-iodo-L-phenylalanine 1,1-dimethylethyl ester
217326-89-1

N-[(1,1-dimethylethoxy)carbonyl]-4-iodo-L-phenylalanine 1,1-dimethylethyl ester

Conditions
ConditionsYield
With hydrogenchloride In dichloromethane100%
...Expand
3-bromo-7-chloro-5-(2-chlorophenyl)pyrazolo[1,5-a]pyrimidine
672323-76-1

3-bromo-7-chloro-5-(2-chlorophenyl)pyrazolo[1,5-a]pyrimidine

N-ethyl-N,N-diisopropylamine
7087-68-5

N-ethyl-N,N-diisopropylamine

tert-butyl 4-(aminomethyl)piperidine-1-carboxylate
144222-22-0

tert-butyl 4-(aminomethyl)piperidine-1-carboxylate

4-{[3-BROMO-5-(2-CHLOROPHENYL)PYRAZOLO[1,5-a]PYRIMIDIN-7-YLAMINO]METHYL}PIPERIDINE-1-CARBOXYLIC ACID tert-BUTYL ESTER
672316-65-3

4-{[3-BROMO-5-(2-CHLOROPHENYL)PYRAZOLO[1,5-a]PYRIMIDIN-7-YLAMINO]METHYL}PIPERIDINE-1-CARBOXYLIC ACID tert-BUTYL ESTER

Conditions
ConditionsYield
In 1,4-dioxane100%
...Expand
2-ethyl-4,5-dihydrooxazole
10431-98-8

2-ethyl-4,5-dihydrooxazole

N-ethyl-N,N-diisopropylamine
7087-68-5

N-ethyl-N,N-diisopropylamine

methyl trifluoromethanesulfonate
333-27-7

methyl trifluoromethanesulfonate

M-PEOZ-OH 2000

M-PEOZ-OH 2000

Conditions
ConditionsYield
Stage #1: 2-ethyl-4,5-dihydrooxazole; methyl trifluoromethanesulfonate In chlorobenzene at 20 - 110℃; for 0.666667h;
Stage #2: N-ethyl-N,N-diisopropylamine In chlorobenzene at 0 - 50℃; for 18h;		100%
...Expand
sodium hydroxide
1310-73-2

sodium hydroxide

(+/-)-1-[9-benzyl-3,9-diazabicyclo[4.2.1]non-9-yl]-propane-1-one

(+/-)-1-[9-benzyl-3,9-diazabicyclo[4.2.1]non-9-yl]-propane-1-one

N-ethyl-N,N-diisopropylamine
7087-68-5

N-ethyl-N,N-diisopropylamine

9-benzyl-3,9-diazabicyclo[4.2.1]nonane

9-benzyl-3,9-diazabicyclo[4.2.1]nonane

Conditions
ConditionsYield
Stage #1: (+/-)-1-[9-benzyl-3,9-diazabicyclo[4.2.1]non-9-yl]-propane-1-one; N-ethyl-N,N-diisopropylamine With propionic acid In tetrahydrofuran for 1h;
Stage #2: sodium hydroxide In diethyl ether		100%
...Expand
disodium (11-(3-carboxypropyl)-2,2,10,10-tetramethyl-1-(3-sulfonatopropyl)-2,3,4,8,9,10-hexahydro-1H-dipyrido[3,2-b:2',3'-i]phenoxazine-11-ium-4,8-diyl)dimethanesulfonate

disodium (11-(3-carboxypropyl)-2,2,10,10-tetramethyl-1-(3-sulfonatopropyl)-2,3,4,8,9,10-hexahydro-1H-dipyrido[3,2-b:2',3'-i]phenoxazine-11-ium-4,8-diyl)dimethanesulfonate

O-(N-succinimidyl)-N,N,N',N'-tetramethyluronium tetrafluoroborate
105832-38-0

O-(N-succinimidyl)-N,N,N',N'-tetramethyluronium tetrafluoroborate

N-ethyl-N,N-diisopropylamine
7087-68-5

N-ethyl-N,N-diisopropylamine

2C8H19N*C35H44N4O14S3

2C8H19N*C35H44N4O14S3

Conditions
ConditionsYield
In N,N-dimethyl-formamide at 20℃; for 2h; Inert atmosphere;100%
...Expand
C11H13ClN4
1228231-19-3

C11H13ClN4

3-azetidinecarboxylic acid
36476-78-5

3-azetidinecarboxylic acid

N-ethyl-N,N-diisopropylamine
7087-68-5

N-ethyl-N,N-diisopropylamine

1-(7-methyl-6,7,8,9-tetrahydro-5H-1,4,7,10a-tetraaza-cyclohepta[f]inden-10-yl)-azetidine-3-carboxylic acid diisopropylethylamine salt
1228231-28-4

1-(7-methyl-6,7,8,9-tetrahydro-5H-1,4,7,10a-tetraaza-cyclohepta[f]inden-10-yl)-azetidine-3-carboxylic acid diisopropylethylamine salt

Conditions
ConditionsYield
In ethanol at 75℃; for 4h;100%
...Expand
(6S,7S)-6-((4-phenylpiperazin-1-yl)carbonyl)-5-azaspiro(2,5)octane-7-carboxylic acid
791834-68-9

(6S,7S)-6-((4-phenylpiperazin-1-yl)carbonyl)-5-azaspiro(2,5)octane-7-carboxylic acid

O-benzylhydroxylamine hydrochloride

O-benzylhydroxylamine hydrochloride

N-ethyl-N,N-diisopropylamine
7087-68-5

N-ethyl-N,N-diisopropylamine

(6S,7S)-N-(benzyloxy)-6-((4-phenylpiperazin-1-yl)carbonyl)-5-azaspiro(2,5)octane-7-carboxamide

(6S,7S)-N-(benzyloxy)-6-((4-phenylpiperazin-1-yl)carbonyl)-5-azaspiro(2,5)octane-7-carboxamide

Conditions
ConditionsYield
Stage #1: (6S,7S)-6-((4-phenylpiperazin-1-yl)carbonyl)-5-azaspiro(2,5)octane-7-carboxylic acid; O-benzylhydroxylamine hydrochloride With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate In N,N-dimethyl-formamide at 0℃; for 0.0833333h;
Stage #2: N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; for 3h;		100%
...Expand
C66H52N6O8

C66H52N6O8

zinc diacetate
557-34-6

zinc diacetate

N-ethyl-N,N-diisopropylamine
7087-68-5

N-ethyl-N,N-diisopropylamine

C66H49N6O8Zn(1-)*H(1+)*C8H19N

C66H49N6O8Zn(1-)*H(1+)*C8H19N

Conditions
ConditionsYield
In chloroform-d1; d(4)-methanol at 20℃;100%
...Expand
α-methyl-ω-aminopoly(ethylene glycol)

α-methyl-ω-aminopoly(ethylene glycol)

N-ethyl-N,N-diisopropylamine
7087-68-5

N-ethyl-N,N-diisopropylamine

2-Bromoacetyl bromide
598-21-0

2-Bromoacetyl bromide

A

N-ethyldiisopropylamine hydrobromide

N-ethyldiisopropylamine hydrobromide

B

α-methyl-ω-(2-bromoacetamido)poly(ethylene glycol)

α-methyl-ω-(2-bromoacetamido)poly(ethylene glycol)

Conditions
ConditionsYield
In dichloromethane at 0 - 20℃; for 18h;A n/a
B 100%
...Expand
N-ethyl-N,N-diisopropylamine
7087-68-5

N-ethyl-N,N-diisopropylamine

2,2,2,2-Tetrafluor-1,3-dihydro-4,6-bis(trifluormethyl)-1,3,5,2λ5-triazaphosphinin

2,2,2,2-Tetrafluor-1,3-dihydro-4,6-bis(trifluormethyl)-1,3,5,2λ5-triazaphosphinin

2,2,2,2-Tetrafluor-1,3-dihydro-4,6-bis(trifluormethyl)-1,3,5,2λ5-triazaphosphininethyl-diisopropylaminaddukt

2,2,2,2-Tetrafluor-1,3-dihydro-4,6-bis(trifluormethyl)-1,3,5,2λ5-triazaphosphininethyl-diisopropylaminaddukt

Conditions
ConditionsYield
In tetrahydrofuran at -20℃;99%
N-ethyl-N,N-diisopropylamine
7087-68-5

N-ethyl-N,N-diisopropylamine

N2-Z-N5-acetyl-N5-O-acetyl-L-ornithyl-N5-acetyl-N5-O-acetyl-L-ornithyl-N5-acetyl-N5-O-acetyl-L-ornithine
250215-21-5

N2-Z-N5-acetyl-N5-O-acetyl-L-ornithyl-N5-acetyl-N5-O-acetyl-L-ornithyl-N5-acetyl-N5-O-acetyl-L-ornithine

N2-Z-N5-acetyl-N5-hydroxyl-L-ornithyl-N5-acetyl-N5-hydroxyl-L-ornithyl-N5-acetyl-N5-hydroxyl-L-ornithine, DIPEA salt

N2-Z-N5-acetyl-N5-hydroxyl-L-ornithyl-N5-acetyl-N5-hydroxyl-L-ornithyl-N5-acetyl-N5-hydroxyl-L-ornithine, DIPEA salt

Conditions
ConditionsYield
In methanol at 20℃; for 12h; Deacetylation;99%
4-(4'-trifluoromethyl-biphenyl-2-carbonylamino)-1-methyl-pyrrole-2-carboxylic acid
486436-98-0

4-(4'-trifluoromethyl-biphenyl-2-carbonylamino)-1-methyl-pyrrole-2-carboxylic acid

4-(pyrimidin-4-yl-carbonylamino)-benzylamine
486437-37-0

4-(pyrimidin-4-yl-carbonylamino)-benzylamine

N-ethyl-N,N-diisopropylamine
7087-68-5

N-ethyl-N,N-diisopropylamine

N-[4-(pyrimidin-4-yl-carbonylamino)-phenylmethyl]-4-(4'-trifluoromethylbiphenyl-2-carbonylamino)-1-methyl-pyrrole-2-carboxylic acid amide
486435-54-5

N-[4-(pyrimidin-4-yl-carbonylamino)-phenylmethyl]-4-(4'-trifluoromethylbiphenyl-2-carbonylamino)-1-methyl-pyrrole-2-carboxylic acid amide

Conditions
ConditionsYield
With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate In N-methyl-acetamide99%
...Expand
(RS)-2-amino-2-methyl-1-[N-(2-methoxybenzyl)amino]-3-(1H-indol-3-yl)propane

(RS)-2-amino-2-methyl-1-[N-(2-methoxybenzyl)amino]-3-(1H-indol-3-yl)propane

4-nitrophenol acetate
830-03-5

4-nitrophenol acetate

N-ethyl-N,N-diisopropylamine
7087-68-5

N-ethyl-N,N-diisopropylamine

1-(2-methoxybenzyl)-2,4-dimethyl-4-(1H-indol-3-ylmethyl)-2-imidazoline
176249-60-8

1-(2-methoxybenzyl)-2,4-dimethyl-4-(1H-indol-3-ylmethyl)-2-imidazoline

Conditions
ConditionsYield
In tetrahydrofuran; ethyl acetate99%
...Expand
pyridin-2-yl (1,1,1-trifluoro-2-methylpropan-2-yl) carbonate
630424-75-8

pyridin-2-yl (1,1,1-trifluoro-2-methylpropan-2-yl) carbonate

methyl tert-leucinate
3850-31-5

methyl tert-leucinate

N-ethyl-N,N-diisopropylamine
7087-68-5

N-ethyl-N,N-diisopropylamine

(S)-3,3-Dimethyl-2-(2,2,2-trifluoro-1,1-dimethyl-ethoxycarbonylamino)-butyric acid methyl ester
1028801-63-9

(S)-3,3-Dimethyl-2-(2,2,2-trifluoro-1,1-dimethyl-ethoxycarbonylamino)-butyric acid methyl ester

Conditions
ConditionsYield
With sodium hydroxide In 4-(dicyanomethylene)-2-methyl-6-(p-dimethylaminostyryl)-4H-pyran99%
...Expand
ammonium chloride

ammonium chloride

N-ethyl-N,N-diisopropylamine
7087-68-5

N-ethyl-N,N-diisopropylamine

2,4-Dihydroxybenzaldehyde
95-01-2

2,4-Dihydroxybenzaldehyde

ethyl chloromethyl ether
3188-13-4

ethyl chloromethyl ether

2,4-bis(ethoxymethoxy)benzaldehyde
128837-29-6

2,4-bis(ethoxymethoxy)benzaldehyde

Conditions
ConditionsYield
In N,N-dimethyl-formamide99%
...Expand
1,5-dioxaspiro[5.5]undecane-2,4-dione
1658-27-1

1,5-dioxaspiro[5.5]undecane-2,4-dione

pentafluoronitrobenzen
880-78-4

pentafluoronitrobenzen

N-ethyl-N,N-diisopropylamine
7087-68-5

N-ethyl-N,N-diisopropylamine

C15H11F4NO6*C8H19N

C15H11F4NO6*C8H19N

Conditions
ConditionsYield
In acetonitrile at 30℃; for 0.333333h;99%
...Expand
N-ethyl-N,N-diisopropylamine
7087-68-5

N-ethyl-N,N-diisopropylamine

N-ethyl-N-isopropylpropan-2-amine oxide

N-ethyl-N-isopropylpropan-2-amine oxide

Conditions
ConditionsYield
With 2,2,2-Trifluoroacetophenone; dihydrogen peroxide; acetonitrile In tert-butyl alcohol at 20℃; for 18h; Green chemistry; chemoselective reaction;98%
With 2,2,6,6-tetramethylpiperidin-1-oxoammonium chloride Ambient temperature;
With sodium hydroxide; dihydrogen peroxide; N-tosylimidazole In methanol for 1.5h;
With C19H16FeN4O5(1-); dihydrogen peroxide at 20℃; for 2h; pH=10; aq. buffer;40.2 %Chromat.
With dihydrogen peroxide In water at 0 - 30℃;
pyrrolidine
123-75-1

pyrrolidine

4-bromo-2-methylbenzoic acid
68837-59-2

4-bromo-2-methylbenzoic acid

O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate
125700-67-6

O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate

N-ethyl-N,N-diisopropylamine
7087-68-5

N-ethyl-N,N-diisopropylamine

(4-bromo-2-methylphenyl)(pyrrolidin-1-yl)methanone
276678-35-4

(4-bromo-2-methylphenyl)(pyrrolidin-1-yl)methanone

Conditions
ConditionsYield
In tetrahydrofuran; water98%
...Expand
2-[4-(N-benzyl-methylamino)-3-nitro-phenyl]-2-methyl-3-amino-1-pyrrolidino-propan-1-one

2-[4-(N-benzyl-methylamino)-3-nitro-phenyl]-2-methyl-3-amino-1-pyrrolidino-propan-1-one

di-tert-butyl dicarbonate
24424-99-5

di-tert-butyl dicarbonate

N-ethyl-N,N-diisopropylamine
7087-68-5

N-ethyl-N,N-diisopropylamine

2-[4-(N-benzyl-methylamino)-3-nitro-phenyl]-2-methyl-3-tert.butyloxycarbonylamino-1-pyrrolidino-propan-1-one
345957-94-0

2-[4-(N-benzyl-methylamino)-3-nitro-phenyl]-2-methyl-3-tert.butyloxycarbonylamino-1-pyrrolidino-propan-1-one

Conditions
ConditionsYield
In 1,4-dioxane98%
...Expand
5-Iodo-thiophene-2-carboxylic acid
60166-85-0

5-Iodo-thiophene-2-carboxylic acid

hydrochloric acid salt of (S)-3-amino-2-(2,4,6,-trimethyl-benzyloxycarbonylamino)-propionic acid tert-butyl ester

hydrochloric acid salt of (S)-3-amino-2-(2,4,6,-trimethyl-benzyloxycarbonylamino)-propionic acid tert-butyl ester

N-ethyl-N,N-diisopropylamine
7087-68-5

N-ethyl-N,N-diisopropylamine

HATU
200731-31-3, 148893-10-1

HATU

(S)-3-[(5-Iodo-thiophene-2-carbonyl)-amino]-2-(2,4,6-trimethyl-benzenesulfonylamino)-propionic acid tert-butyl ester

(S)-3-[(5-Iodo-thiophene-2-carbonyl)-amino]-2-(2,4,6-trimethyl-benzenesulfonylamino)-propionic acid tert-butyl ester

Conditions
ConditionsYield
With sodium hydrogencarbonate; citric acid In N,N-dimethyl-formamide98%
...Expand
(-)-2,3,7,8-tetrahydro-2,2,3,3,7,7,8,8-octamethyl-N(1),N(9)-(2,2,2',2'-tetramethyl-1,1'-({(1S,2S)-cyclohexan-1,2-diyl}dinitrilo)bis{propyl})-11H-dipyrrin-1,9-diimine

(-)-2,3,7,8-tetrahydro-2,2,3,3,7,7,8,8-octamethyl-N(1),N(9)-(2,2,2',2'-tetramethyl-1,1'-({(1S,2S)-cyclohexan-1,2-diyl}dinitrilo)bis{propyl})-11H-dipyrrin-1,9-diimine

N-ethyl-N,N-diisopropylamine
7087-68-5

N-ethyl-N,N-diisopropylamine

cobalt(II) chloride
7646-79-9

cobalt(II) chloride

(+)-dibromo(2,3,7,8-tetrahydro-2,2,3,3,7,7,8,8-octamethyl-N(1),N(9)-(2,2,2',2'-tetramethyl-1,1'-({(1S,2S)-cyclohexan-1,2-diyl}dinitrilo)bis{propyl})-11H-dipyrrin-1,9-diiminato(1-))cobalt(III)

(+)-dibromo(2,3,7,8-tetrahydro-2,2,3,3,7,7,8,8-octamethyl-N(1),N(9)-(2,2,2',2'-tetramethyl-1,1'-({(1S,2S)-cyclohexan-1,2-diyl}dinitrilo)bis{propyl})-11H-dipyrrin-1,9-diiminato(1-))cobalt(III)

Conditions
ConditionsYield
With iodine; potassium bromide In dichloromethane; acetonitrile addn. of CoCl2 in MeCN to soln. of org. ligand and EtN(i-Pr)2 in CH2Cl2, stirring at room temp. overnight, evapn., dissolving residue in CH2Cl2 and aq. satd. soln. of KBr with stirring, addn. of I2 in CH2Cl2; extn. of aq. phase (CH2Cl2), washing (satd. KBr soln., H2O), filtration (silica gel, CH2Cl2/MeOH 100:3), drying in vac. at room temp.;98%
...Expand
Bis(p-nitrophenyl) phosphate
645-15-8

Bis(p-nitrophenyl) phosphate

N-ethyl-N,N-diisopropylamine
7087-68-5

N-ethyl-N,N-diisopropylamine

N-ethyl-N-isopropylpropan-2-aminium bis(4-nitrophenyl) phosphate

N-ethyl-N-isopropylpropan-2-aminium bis(4-nitrophenyl) phosphate

Conditions
ConditionsYield
In toluene at 20℃; for 2h;98%
tert-butyl (23-((bis(benzyloxy)phosphoryl)oxy)-11-oxo-3,6,9,15,18,21-hexaoxa-12-azatricosyl)carbamate

tert-butyl (23-((bis(benzyloxy)phosphoryl)oxy)-11-oxo-3,6,9,15,18,21-hexaoxa-12-azatricosyl)carbamate

N-ethyl-N,N-diisopropylamine
7087-68-5

N-ethyl-N,N-diisopropylamine

2,2-dimethyl-4,16-dioxo-3,8,11,14,20,23,26-heptaoxa-5,17-diazaoctacosan-28-yl phosphate di diisopropylaethylamonium salt

2,2-dimethyl-4,16-dioxo-3,8,11,14,20,23,26-heptaoxa-5,17-diazaoctacosan-28-yl phosphate di diisopropylaethylamonium salt

Conditions
ConditionsYield
Stage #1: tert-butyl (23-((bis(benzyloxy)phosphoryl)oxy)-11-oxo-3,6,9,15,18,21-hexaoxa-12-azatricosyl)carbamate With palladium 10% on activated carbon; hydrogen In methanol for 1.5h; Inert atmosphere;
Stage #2: N-ethyl-N,N-diisopropylamine Inert atmosphere;		98%
4-((5-azidopentyl)oxy)benzonitrile

4-((5-azidopentyl)oxy)benzonitrile

N-ethyl-N,N-diisopropylamine
7087-68-5

N-ethyl-N,N-diisopropylamine

2-(4-iodophenyl)-1,8a-dihydroazulene-1,1-dicarbonitrile
298212-99-4

2-(4-iodophenyl)-1,8a-dihydroazulene-1,1-dicarbonitrile

1,1-dicyano-2-(4-(1-(5-(4-cyanophenoxy)pentyl)-1H-1,2,3-triazol-4-yl)phenyl)-1,8a-dihydroazulene

1,1-dicyano-2-(4-(1-(5-(4-cyanophenoxy)pentyl)-1H-1,2,3-triazol-4-yl)phenyl)-1,8a-dihydroazulene

Conditions
ConditionsYield
With copper(l) iodide In toluene at 20℃; for 48h;98%
...Expand
1,5-dioxaspiro[5.5]undecane-2,4-dione
1658-27-1

1,5-dioxaspiro[5.5]undecane-2,4-dione

2,3,4-trifluoronitrobenzene
771-69-7

2,3,4-trifluoronitrobenzene

N-ethyl-N,N-diisopropylamine
7087-68-5

N-ethyl-N,N-diisopropylamine

C15H13F2NO6*C8H19N

C15H13F2NO6*C8H19N

Conditions
ConditionsYield
In acetonitrile at 45℃; for 20h;98%
...Expand

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