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inquiryALPHA-METHYLPHENYLACETONITRILE Basic information Product Name: ALPHA-METHYLPHENYLACETONITRILE Synonyms: alpha-methyl-benzeneacetonitril;2-PHENYLPROPIONITRILE;A-METHYLBENZYL CYANIDE;A-MET
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inquiryALPHA-METHYLPHENYLACETONITRILE CAS:1823-91-2 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality or
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquiryWith our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryfactory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
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inquiryMassive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
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inquirySuperior quality, moderate price & quick delivery. Appearance:light yellow liquid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:25kg/drum, or as per your request. Application:For medicine , pesticide interm
Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
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inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
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inquiryAppearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
alpha-Methylbenzyl cyanideAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air
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inquiryhigh qualityAppearance:white crystalline powder Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
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inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:Beijing or Guangzhou
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inquiryAnsciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
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inquiryWe are committed to providing our customers with the best products and services at the most competitive prices.Appearance:powder Storage:Room temperature with sealed well Package:according to the clients requirement Application:Use as primary and sec
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2-Phenylpropionitrile cas 1823-91-2Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
Good Quality Package:1kg/bag Application:Medical or chemical Transportation:Air/Train/Sea Port:Shenzhen
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:any port in China
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inquirybulk?production Application:Pharmaceutical intermediates
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inquiryConditions | Yield |
---|---|
Stage #1: propiononitrile With n-butyllithium In tetrahydrofuran at -78℃; for 0.25h; Stage #2: Phenyl[2-(trimethylsilyl)phenyl]iodonium trifluoromethanesulfonate With tetrabutyl ammonium fluoride In tetrahydrofuran at 0 - 20℃; for 0.916667h; | 99% |
2-phenylpropanal oxime
1-phenylethyl cyanide
Conditions | Yield |
---|---|
With copper diacetate In acetonitrile for 3h; Reflux; | 98% |
With pyridine; titanium tetrachloride at 40℃; Sealed tube; | 93% |
With acetyl chloride; zinc(II) oxide for 0.5h; Heating; | 90% |
2-Phenylpropanal
1-phenylethyl cyanide
Conditions | Yield |
---|---|
With trifluorormethanesulfonic acid; O-benzenesulfonyl-acetohydroxamic acid ethyl ester In dichloromethane at 23℃; for 24h; Inert atmosphere; | 98% |
With pyridine; hydroxylamine hydrochloride; titanium tetrachloride at 40℃; Sealed tube; | 97% |
With aluminum oxide; hydroxylamine hydrochloride; methanesulfonyl chloride at 100℃; for 0.5h; | 95% |
1-phenylethyl cyanide
Conditions | Yield |
---|---|
With iron(III) chloride; 2,6-di-tert-butyl-4-methyl-phenol In toluene at 20℃; for 0.0833333h; Schlenk technique; | 97% |
tetra-n-butylammonium cyanide
2-(1-phenylethoxy)-tetrahydro-2H-pyran
1-phenylethyl cyanide
Conditions | Yield |
---|---|
With triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone In acetonitrile for 6h; Heating; | 94% |
2-chloro-2-phenylpropanenitrile
1-phenylethyl cyanide
Conditions | Yield |
---|---|
With sodium hydrogen telluride; acetic acid In ethanol; benzene at -20℃; for 0.333333h; | 93% |
Conditions | Yield |
---|---|
With aluminium trichloride; potassium iodide In water; acetonitrile at 80℃; for 10h; | 92% |
With phosgene In tetrahydrofuran; toluene at 25℃; for 4h; Inert atmosphere; | 82% |
With phosphorus pentoxide; benzene | |
With phosphorus pentachloride |
phenylacetonitrile
methyl iodide
A
2-methyl-2-phenylpropionitrile
B
1-phenylethyl cyanide
Conditions | Yield |
---|---|
With sodium hydroxide; tetrakis(hexylsulfinylmethyl)methane for 28h; Ambient temperature; | A 5% B 92% |
With sodium hydroxide; C(CH2S(=O)C6H13)4 for 28h; Ambient temperature; | A 5% B 92% |
With sodium hydroxide; sulfur dioxide for 24h; Product distribution; Ambient temperature; liquid-liquid two phase alkylation, other alkyl iodides, other sulfoxides containing pyridine nuklei as cat.; | A n/a B 83 % Chromat. |
2-phenyl-2-trimethylsilyloxypropanenitrile
1-phenylethyl cyanide
Conditions | Yield |
---|---|
With chloro-trimethyl-silane; water; sodium iodide In acetonitrile at 20℃; for 48h; Reduction; | 92% |
With chloro-trimethyl-silane; water; acetonitrile; sodium iodide In hexane for 24h; Ambient temperature; | 74% |
Conditions | Yield |
---|---|
Stage #1: potassium cyanide With acetic acid In ethylene glycol at 60℃; Sealed tube; Stage #2: styrene With bis(1,5-cyclooctadiene)nickel (0); 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene at 60℃; for 18h; Sealed tube; | 92% |
1-Phenylethanol
tetra-n-butylammonium cyanide
1-phenylethyl cyanide
Conditions | Yield |
---|---|
With triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone In acetonitrile at 20℃; | 91% |
Conditions | Yield |
---|---|
With potassium carbonate at 180℃; for 3.75h; | 90% |
With sodium methylate at 180℃; under 15001.5 Torr; for 5h; Reagent/catalyst; Temperature; | 88.2% |
aluminum oxide; Corundum(Al2O3) + 5wtpercent K2CO3 + 5wtpercent polyethyleneglycol (mol. weight 6000); potassium carbonate at 180℃; liquid flow rate 16 ml/h; | 88 % Chromat. |
trimethylsilyl cyanide
1-Phenylethanol
1-phenylethyl cyanide
Conditions | Yield |
---|---|
With tris(pentafluorophenyl)borate In acetonitrile at 20℃; for 1h; | 90% |
With zinc trifluoromethanesulfonate In nitromethane at 100℃; for 8h; | 43% |
Conditions | Yield |
---|---|
With fluorescein sodium salt In acetonitrile at 20℃; for 10h; Irradiation; | 90% |
Conditions | Yield |
---|---|
With bis(1,5-cyclooctadiene)nickel (0); 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene In toluene at 120℃; for 24h; Inert atmosphere; Glovebox; Sealed tube; regioselective reaction; | 90% |
Conditions | Yield |
---|---|
With 3-[bis-(4-methoxy-phenyl)-phosphanyl]-2H-isoquinolin-1-one; N-{6-[bis-(4-methoxy-phenyl)-phosphanyl]-pyridin-2-yl}-2,2-dimethyl-propionamide; bis(1,5-cyclooctadiene)nickel (0) In toluene at 35℃; for 25h; regioselective reaction; | 89% |
With bis(1,5-cyclooctadiene)nickel (0); (S)-binaphthyl chiral diphosphite In toluene at 20℃; for 24h; asymmetric hydrocyanation; |
Conditions | Yield |
---|---|
With (1,2-dimethoxyethane)dichloronickel(II); (1S,2R)-(+)-norphedrine; lithium hexamethyldisilazane; water; cesium fluoride In N,N-dimethyl acetamide at 60℃; for 16h; Hiyama cross-coupling; | 88% |
benzyl methoxymethyl ether
(1-methoxymethoxy)ethylbenzene
tetra-n-butylammonium cyanide
A
phenylacetonitrile
B
1-phenylethyl cyanide
Conditions | Yield |
---|---|
With 1-(n-butyl)-3-methylimidazolium tetrachloroindate at 135 - 140℃; for 0.075h; Microwave irradiation; Neat (no solvent); chemoselective reaction; | A 88% B 19% |
hydratropic acid
1-phenylethyl cyanide
Conditions | Yield |
---|---|
With sodium azide; triethylamine; triphenylphosphine; (bis-(2-methoxyethyl)amino)sulfur trufluoride In dichloromethane; dimethyl sulfoxide at 0 - 20℃; for 0.833333h; | 87% |
With sodium azide; TEA; triethylphosphine; (bis-(2-methoxyethyl)amino)sulfur trufluoride In dichloromethane; dimethyl sulfoxide at 0℃; for 30h; | 85% |
Multi-step reaction with 3 steps 1: thionyl chloride / 0.5 h / 25 °C / Inert atmosphere 2: ammonia / water / 0.5 h / 25 °C 3: phosgene / toluene; tetrahydrofuran / 4 h / 25 °C / Inert atmosphere View Scheme |
Conditions | Yield |
---|---|
With carbon monoxide; hydrogen; dodecacarbonyl-triangulo-triruthenium In N,N-dimethyl-formamide at 230℃; under 76000.1 Torr; for 16h; other active methylene compounds, other aldehydes; | 86% |
With carbon monoxide; hydrogen; dodecacarbonyl-triangulo-triruthenium In N,N-dimethyl-formamide at 230℃; under 76000.1 Torr; for 16h; | 86% |
Conditions | Yield |
---|---|
With bis(η3-allyl-μ-chloropalladium(II)); 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene In 1,3,5-trimethyl-benzene at 20 - 140℃; for 10.1667h; Inert atmosphere; Sealed tube; chemoselective reaction; | 86% |
Conditions | Yield |
---|---|
With cobalt(II) tetrafluoroborate hexahydrate; tris(2-diphenylphosphinoethyl)phosphine; potassium carbonate at 100℃; for 24h; Autoclave; Glovebox; Inert atmosphere; | 85% |
With [carbonylchlorohydrido{bis[2-(diphenylphosphinomethyl)ethyl]amino}ethylamino] ruthenium(II); potassium tert-butylate In toluene at 135℃; for 4h; Inert atmosphere; | 83% |
With bis(1,5-cyclooctadiene)diiridium(I) dichloride; potassium tert-butylate; 1,2-bis-(diphenylphosphino)ethane at 150℃; for 48h; Inert atmosphere; | 80% |
Conditions | Yield |
---|---|
With sodium cyanide; N-benzyl-N,N,N-triethylammonium chloride In acetonitrile at 35℃; for 45h; | 83% |
Conditions | Yield |
---|---|
With trimethylamine-borane; 1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine; potassium tert-butylate In 1,2-dimethoxyethane at 120℃; for 16h; Sealed tube; | 83% |
Conditions | Yield |
---|---|
With (3S,4S)-1-benzyl-3,4-pyrrolidin-diol-onium iodide; potassium carbonate In N,N-dimethyl-formamide for 12h; Ambient temperature; | 82% |
1-phenylethyl cyanide
Conditions | Yield |
---|---|
IrH5(P-(i-Pr)3)2 In toluene at 150℃; for 12h; | 82% |
styrene
benzonitrile
A
stilbene
B
dihydrocinnamonitrile
C
1-phenylethyl cyanide
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); dimethylaluminum chloride; CyJohnPhos In hexane; toluene at 100℃; for 16h; Inert atmosphere; Glovebox; regioselective reaction; | A 82% B 57 %Chromat. C 13 %Chromat. |
Conditions | Yield |
---|---|
With bis(1,5-cyclooctadiene)nickel (0); 4,5-bis(diphenylphos4,5-bis(diphenylphosphino)-9,9-dimethylxanthenephino)-9,9-dimethylxanthene In benzene at 90℃; for 18h; Catalytic behavior; Reagent/catalyst; Solvent; Temperature; Schlenk technique; Inert atmosphere; Glovebox; regioselective reaction; | 82% |
Conditions | Yield |
---|---|
With bis(acetylacetonate)nickel(II); 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; zinc at 150℃; for 24h; Reagent/catalyst; Sealed tube; | 81% |
With bis(acetylacetonate)nickel(II); 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; zinc for 24h; Mechanism; Reagent/catalyst; Inert atmosphere; Sealed tube; Heating; Green chemistry; regioselective reaction; | 78% |
Allyl acetate
1-phenylethyl cyanide
2-methyl-2-phenyl-4-pentenenitrile
Conditions | Yield |
---|---|
With potassium hydroxide; Pd(PhCH=CH)2CO>2CO; 1,2-bis-(diphenylphosphino)ethane In dichloromethane Ambient temperature; | 100% |
Diphenyliodonium triflate
1-phenylethyl cyanide
N-phenyl-2-phenylpropanamide
Conditions | Yield |
---|---|
With copper (I) trifluoromethane sulfonate toluene complex; caesium carbonate In toluene at 80℃; for 0.333333h; Catalytic behavior; Mechanism; Solvent; Reagent/catalyst; Temperature; | 100% |
allyl bromide
1-phenylethyl cyanide
2-methyl-2-phenyl-4-pentenenitrile
Conditions | Yield |
---|---|
With sodium hexamethyldisilazane In tetrahydrofuran; dimethyl sulfoxide for 0.666667h; | 99.5% |
Stage #1: 1-phenylethyl cyanide With lithium hexamethyldisilazane In tetrahydrofuran at -78℃; Stage #2: allyl bromide In tetrahydrofuran at -78 - 20℃; | |
Stage #1: 1-phenylethyl cyanide With n-butyllithium; diisopropylamine In tetrahydrofuran; hexane at 0℃; for 0.5h; Stage #2: allyl bromide In tetrahydrofuran; hexane at 0 - 20℃; |
1-phenylethyl cyanide
hydratropic acid
Conditions | Yield |
---|---|
With recombinant nitrilase from Pseudomonas fluorescens EBC 191 In methanol; phosphate buffer at 25℃; pH=6; | 99% |
With water; sodium hydroxide at 120℃; for 6h; Temperature; | 97% |
Stage #1: 1-phenylethyl cyanide With sodium hydroxide at 105℃; for 12.5h; Reflux; Stage #2: With sulfuric acid for 0.583333h; pH=3; Temperature; pH-value; | 93% |
Conditions | Yield |
---|---|
With dichloro( 1,5-cyclooctadiene)platinum(ll); 4,5-dihydro-3H-dinaphtho[2,1-c:1',2'-e]phosphepine-4-oxide; water; silver nitrate In tert-Amyl alcohol at 80℃; for 1h; Catalytic behavior; Reagent/catalyst; Time; chemoselective reaction; | 99% |
With [RuH(tBu-PNP(-))(CO)]; water In tert-butyl alcohol at 20℃; for 24h; | 99% |
With sodium hydroxide; dihydrogen peroxide In methanol; water for 2h; pH=8.0; | 95% |
ethanol
1-phenylethyl cyanide
ethyl 2-methyl-2-phenylacetoimidate hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride at 0 - 5℃; Addition; | 99% |
With hydrogenchloride In diethyl ether at 20℃; | 84% |
Conditions | Yield |
---|---|
Stage #1: 1-phenylethyl cyanide With lithium diisopropyl amide In tetrahydrofuran at -78℃; for 0.333333h; Stage #2: 1-azido-3-chlorobenzene With N,N,N,N,N,N-hexamethylphosphoric triamide In tetrahydrofuran at -78 - 20℃; for 1h; Stage #3: dimethyl sulfate at 20℃; for 1h; | 99% |
Conditions | Yield |
---|---|
Stage #1: 1-phenylethyl cyanide With lithium diisopropyl amide In tetrahydrofuran at -78℃; for 0.333333h; Stage #2: 3-methoxyphenyl azide With N,N,N,N,N,N-hexamethylphosphoric triamide In tetrahydrofuran at -78 - 20℃; for 1h; Stage #3: dimethyl sulfate at -78℃; for 1h; | 99% |
Conditions | Yield |
---|---|
With samarium diiodide; water; triethylamine In tetrahydrofuran at 20℃; for 0.0833333h; Inert atmosphere; | 98% |
With hydrogenchloride; ethanol; palladium Hydrogenation; | |
With ethanol; ammonia; nickel Hydrogenation; | |
With lithium aluminium tetrahydride In diethyl ether | |
Multi-step reaction with 2 steps 1: woollins’ reagent / toluene / 6 h / Inert atmosphere; Reflux 2: water; samarium diiodide / tetrahydrofuran / 20 °C / Inert atmosphere View Scheme |
Conditions | Yield |
---|---|
With ammonia; sodium amide at -70℃; for 0.0333333h; | 98% |
benzyl bromide
1-phenylethyl cyanide
α-benzyl-α-methylphenylacetonitrile
Conditions | Yield |
---|---|
Stage #1: 1-phenylethyl cyanide With n-butyllithium; diisopropylamine In tetrahydrofuran; hexane at 0℃; for 0.5h; Stage #2: benzyl bromide In tetrahydrofuran; hexane at 0 - 20℃; | 98% |
Stage #1: 1-phenylethyl cyanide With lithium diisopropyl amide In tetrahydrofuran at -78℃; for 0.666667h; Stage #2: benzyl bromide In tetrahydrofuran at -78 - 20℃; for 6h; |
1-phenylethyl cyanide
2-deuterio-2-phenyl-propionitrile
Conditions | Yield |
---|---|
With water-d2; triethylamine at 20℃; for 72h; Inert atmosphere; | 98% |
Conditions | Yield |
---|---|
Stage #1: 1-phenylethyl cyanide With lithium diisopropyl amide In tetrahydrofuran at -78℃; for 0.333333h; Stage #2: 3-methoxyphenyl azide With N,N,N,N,N,N-hexamethylphosphoric triamide In tetrahydrofuran at -78 - 20℃; for 1h; Stage #3: diethyl sulfate at 20℃; for 1h; | 97% |
1-phenylethyl cyanide
Conditions | Yield |
---|---|
With trimethylaluminum; ammonium chloride In toluene at 20 - 80℃; for 17h; | 95% |
With trimethylaluminum; ammonium chloride In toluene at 80℃; for 48h; | 92% |
triisopropylsilyl chloride
1-phenylethyl cyanide
Conditions | Yield |
---|---|
Stage #1: 1-phenylethyl cyanide With n-butyllithium; diisopropylamine In tetrahydrofuran; hexane at -78℃; for 0.0833333h; Inert atmosphere; Stage #2: triisopropylsilyl chloride In tetrahydrofuran; hexane at -78 - 20℃; for 12h; Inert atmosphere; | 95% |
acrylonitrile
1-phenylethyl cyanide
(+/-)-3-Methyl-3-phenyl-2,6-piperidinedione
Conditions | Yield |
---|---|
With IrH5(P-(i-Pr)3)2; water In tetrahydrofuran at 150℃; for 20h; | 94% |
Conditions | Yield |
---|---|
Stage #1: 1-phenylethyl cyanide With lithium diisopropyl amide In tetrahydrofuran at -78℃; for 0.333333h; Stage #2: 1-azido-4-chlorobenzene With N,N,N,N,N,N-hexamethylphosphoric triamide In tetrahydrofuran at -78 - 20℃; for 1h; Stage #3: dimethyl sulfate at 20℃; for 1h; | 94% |
Conditions | Yield |
---|---|
Stage #1: 1-phenylethyl cyanide With lithium diisopropyl amide In tetrahydrofuran at -78℃; for 0.333333h; Stage #2: 1-azido-4-bromobenzene With N,N,N,N,N,N-hexamethylphosphoric triamide In tetrahydrofuran at -78 - 20℃; for 1h; Stage #3: dimethyl sulfate at 20℃; for 1h; | 94% |
C-phenyl-N-methylnitrone
Triethylsilyl trifluoromethanesulfonate
1-phenylethyl cyanide
Conditions | Yield |
---|---|
With triethylamine In 1,2-dichloro-ethane at -30℃; for 0.5h; Inert atmosphere; | 94% |
1-phenylethyl cyanide
3-hydroxy-2-methyl-1-propene
2,4-dimethyl-2-phenyl-4-pentenenitrile
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); carbon dioxide In dimethyl sulfoxide at 90℃; under 760.051 Torr; for 14h; Sealed tube; | 94% |
1-phenylethyl cyanide
2-methyl-3-(naphthalen-2-yl)-2-phenylpropanenitrile
Conditions | Yield |
---|---|
With bis(1,5-cyclooctadiene)nickel(0); 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; lithium tert-butoxide In toluene at 100℃; for 12h; | 94% |
4-Methoxybenzophenone
1-phenylethyl cyanide
2-(4-benzoylphenyl)-2-phenylpropanenitrile
Conditions | Yield |
---|---|
With phosphazene base-P4-tert-butyl In tetrahydrofuran; hexane at 60℃; for 18h; Catalytic behavior; Reagent/catalyst; Solvent; Temperature; Inert atmosphere; Molecular sieve; Sealed tube; | 93% |
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