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Cas:19261-06-4
Min.Order:1 Gram
FOB Price: $0.1
Type:Manufacturers
inquiryAs a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis according to the contract research and development services for the fine chemicals, ph
With our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin
Cas:19261-06-4
Min.Order:1 Kilogram
FOB Price: $1.0 / 10.0
Type:Trading Company
inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:19261-06-4
Min.Order:10 Gram
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inquiryZhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed
Cas:19261-06-4
Min.Order:1 Kilogram
FOB Price: $2.0
Type:Lab/Research institutions
inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:Beijing or Guangzhou
factory?direct?sale Application:Fine chemical intermediates, used as the main raw material for the synthesis of various pesticides, medicines, surfactants, polymer monomers, and antifungal agents
We product this chemical more than 10 years . We are very experience to export it to many countries, Our superior & stable quality , competitive price gain warm reception from our customers. Application:Chemical intermediate
4-DIBENZOFURANOLCASAppearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
factory?direct?sale Application:Fine chemical intermediates, used as the main raw material for the synthesis of various pesticides, medicines, surfactants, polymer monomers, and antifungal agents
factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
Compound sourcing ServicesAgency of testing serviceFactory audit serviceFounded in Dec. 1999, Nanjing Chemlin Chemical Industrial Co.,Ltd(CHEMLIN) has been covering the business scope from trading of chemicals to custom-synthesis & Manufacturing. Co
4-methoxydibenzo[b,d]furan
4-hydroxydibenzofuran
Conditions | Yield |
---|---|
With boron tribromide In dichloromethane at -78 - 20℃; | 100% |
4-hydroxydibenzofuran
Conditions | Yield |
---|---|
With Oxone; water In acetone at 20℃; for 0.0833333h; | 97% |
4-dibenzofurylboronic acid
dihydrogen peroxide
4-hydroxydibenzofuran
Conditions | Yield |
---|---|
With ammonium bicarbonate In water at 20℃; for 2h; Schlenk technique; | 96% |
4-dibenzofurylboronic acid
4-hydroxydibenzofuran
Conditions | Yield |
---|---|
With dihydrogen peroxide In water at 20℃; for 0.0833333h; | 95% |
With sodium hydroxide; dihydrogen peroxide In tetrahydrofuran at 20℃; for 24h; | 94% |
With copper(II) ferrite; water; sodium hydroxide at 40℃; for 24h; Green chemistry; | 93% |
dibenzofuran
4-hydroxydibenzofuran
Conditions | Yield |
---|---|
Stage #1: dibenzofuran With n-butyllithium; N,N,N,N,-tetramethylethylenediamine In hexanes; diethyl ether for 1h; Heating / reflux; Stage #2: With boric acid tributyl ester In hexanes; diethyl ether at 0 - 20℃; Stage #3: With dihydrogen peroxide In hexanes; diethyl ether; water at 0℃; for 1.5h; Heating / reflux; | 81% |
Stage #1: dibenzofuran With n-butyllithium; N,N,N,N,-tetramethylethylenediamine In diethyl ether; hexane for 1h; Heating; Stage #2: With boric acid tributyl ester In diethyl ether; hexane at 20℃; for 1h; Stage #3: With dihydrogen peroxide In diethyl ether; hexane; water for 1.5h; Heating; | 71% |
Stage #1: dibenzofuran With n-butyllithium In tetrahydrofuran at -78 - 40℃; for 18h; Stage #2: With methylmagnesium bromide In tetrahydrofuran at -5 - 20℃; for 1h; Stage #3: With hydrogenchloride; water; oxygen more than 3 stages; | 47% |
Conditions | Yield |
---|---|
With n-butyllithium; diethyl ether anschl. mit Butylmagnesiumbromid in Aether und mit Sauerstoff; |
2-chloro-dibenzofuran-4-ol
4-hydroxydibenzofuran
Conditions | Yield |
---|---|
With palladium on activated charcoal; Lindlar's catalyst; ethanol |
4-acetoxydibenzofuran
S-benzylcysteine methyl ester
A
4-hydroxydibenzofuran
B
(+)-2-acetamido-3-benzylthiopropanoic acid methyl ester
Conditions | Yield |
---|---|
In dimethyl sulfoxide at 25℃; Rate constant; |
4-acetoxydibenzofuran
S-benzyl-L-cysteine ethyl ester
A
4-hydroxydibenzofuran
B
(R)-2-Acetylamino-3-benzylsulfanyl-propionic acid ethyl ester
Conditions | Yield |
---|---|
In dimethyl sulfoxide at 25℃; Rate constant; |
phenol
A
2-hydroxydibenzofuran
B
4-hydroxydibenzofuran
C
2-Phenoxyphenol
D
2,2'-dihydroxybiphenyl
Conditions | Yield |
---|---|
With oxygen In benzene at 499.84℃; for 0.0125h; Product distribution; Further Variations:; Reagents; Temperatures; slow combustion; |
2-bromoanisole
4-hydroxydibenzofuran
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 78 percent / K2CO3; Cu2O / 2.5 h / Heating 2: 15 percent / Pd(OAc)3 / acetic acid / 7 h / Heating 3: 100 percent / BBr3 / CH2Cl2 / -78 - 20 °C View Scheme |
2-methoxyphenyl phenyl ether
4-hydroxydibenzofuran
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 15 percent / Pd(OAc)3 / acetic acid / 7 h / Heating 2: 100 percent / BBr3 / CH2Cl2 / -78 - 20 °C View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 78 percent / K2CO3; Cu2O / 2.5 h / Heating 2: 15 percent / Pd(OAc)3 / acetic acid / 7 h / Heating 3: 100 percent / BBr3 / CH2Cl2 / -78 - 20 °C View Scheme |
2-chlorodibenzofuran
4-hydroxydibenzofuran
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: butyl lithium; diethyl ether; etheric butyl magnesium bromide solution / anschliessend mit Sauerstoff behandeln 2: palladium/calcium carbonate; ethanol View Scheme |
2-bromodibenzo[b,d]furan
4-hydroxydibenzofuran
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: benzene; butyl lithium; diethyl ether / erneutes Versetzen mit 2-Brom-dibenzofuran- und Behandeln des Reaktionsgemisches mit festem Kohlendioxid und Aether. 2: butyl lithium; diethyl ether / anschliessend mit aether. Butylmagnesiumbromid-Loesung und mit Sauerstoff View Scheme | |
Multi-step reaction with 2 steps 1: benzene; butyl lithium; diethyl ether / erneutes Versetzen mit 2-Brom-dibenzofuran- und Behandeln des Reaktionsgemisches mit festem Kohlendioxid und Aether. 2: butyl lithium; diethyl ether / anschl. mit Butylmagnesiumbromid in Aether und mit Sauerstoff View Scheme |
Conditions | Yield |
---|---|
With hydrogenchloride; n-butyllithium In diethyl ether |
Conditions | Yield |
---|---|
With sulfuric acid for 4h; | 100% |
With sulfuric acid |
Conditions | Yield |
---|---|
With potassium carbonate In acetone for 18h; Heating / reflux; | 100% |
With potassium carbonate In acetone Reflux; | 99% |
With potassium carbonate In acetone for 11h; Heating; | 93% |
4-hydroxydibenzofuran
N,N-diethylcarbamyl chloride
Conditions | Yield |
---|---|
With pyridine at 85℃; for 15h; | 98% |
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 2h; | 93% |
Conditions | Yield |
---|---|
With potassium carbonate In 1-methyl-pyrrolidin-2-one for 6h; Inert atmosphere; Reflux; | 93% |
Cyclopentyl bromide
4-hydroxydibenzofuran
4-cyclopentyloxydibenzo[b,d]furan
Conditions | Yield |
---|---|
With sodium hydride | 92% |
With potassium carbonate In N,N-dimethyl-formamide at 50 - 100℃; for 4 - 5h; | 90% |
Stage #1: 4-hydroxydibenzofuran With potassium carbonate In N,N-dimethyl-formamide at 80℃; for 0.5h; Stage #2: Cyclopentyl bromide In N,N-dimethyl-formamide at 80℃; for 3h; |
4-hydroxydibenzofuran
cyclopropylcarbinyl bromide
Conditions | Yield |
---|---|
Stage #1: 4-hydroxydibenzofuran With sodium hydride In DMF (N,N-dimethyl-formamide) at 0℃; for 0.0833333h; Stage #2: cyclopropylcarbinyl bromide In DMF (N,N-dimethyl-formamide) at 0 - 20℃; for 1.16667h; | 90% |
Conditions | Yield |
---|---|
Stage #1: 4-hydroxydibenzofuran With sodium hydride In DMF (N,N-dimethyl-formamide) at 0℃; for 0.0833333h; Stage #2: ethyl iodide In DMF (N,N-dimethyl-formamide) at 0 - 20℃; for 1.16667h; | 82% |
4-hydroxydibenzofuran
methanesulfonyl chloride
dibenzo[b,d]furan-4-yl methanesulfonate
Conditions | Yield |
---|---|
With pyridine In dichloromethane at 0 - 20℃; Inert atmosphere; | 77% |
4-hydroxydibenzofuran
trifluoromethylsulfonic anhydride
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 0 - 20℃; for 2h; Inert atmosphere; | 73% |
Conditions | Yield |
---|---|
Stage #1: 2-methyl-8-quinolinol; aluminum isopropoxide In ethanol for 2h; Reflux; Inert atmosphere; Stage #2: 4-hydroxydibenzofuran In ethanol Reflux; | 62% |
4-hydroxydibenzofuran
Conditions | Yield |
---|---|
With N-Bromosuccinimide In dichloromethane at -12 - 20℃; Inert atmosphere; regioselective reaction; | 62% |
With N-Bromosuccinimide In N,N-dimethyl-formamide at 20℃; | |
With bromine; acetic acid at 0 - 20℃; for 5h; |
4-hydroxydibenzofuran
chloroform
4-hydroxydibenzofuran-3-carboxaldehyde
Conditions | Yield |
---|---|
Stage #1: 4-hydroxydibenzofuran; chloroform With sodium hydroxide In water at 60 - 65℃; Reimer-Tiemann formylation; Stage #2: In water at 90℃; for 0.25h; | 13% |
Conditions | Yield |
---|---|
With sodium hydroxide |
Conditions | Yield |
---|---|
With potassium hydroxide |
Conditions | Yield |
---|---|
With bromine |
n-butyllithium
4-hydroxydibenzofuran
diethyl ether
methylammonium carbonate
benzene
6-hydroxy-dibenzofuran-4-carboxylic acid
4-hydroxydibenzofuran
4-aminodibenzofuran
Conditions | Yield |
---|---|
With ammonium hydroxide; sodium disulfite at 195℃; | |
With ammonium chloride; zinc(II) chloride at 280℃; |
4-hydroxydibenzofuran
dibenzofuran-1,4-dione
Conditions | Yield |
---|---|
With sodium periodate; acetic acid unter Lichtausschluss; |
4-hydroxydibenzofuran
1-chloro-4-hydroxydibenzofuran
Conditions | Yield |
---|---|
With sulfuryl dichloride; chloroform; iodine |
4-hydroxydibenzofuran
1-bromodibenzofuran-4-ol
Conditions | Yield |
---|---|
With bromine; acetic acid | |
Multi-step reaction with 3 steps 1: 1H-imidazole / dichloromethane / 18 h / 20 °C / Inert atmosphere 2: N-Bromosuccinimide / tetrahydrofuran / 17 h / 20 °C / Inert atmosphere 3: cesium fluoride / tetrahydrofuran / 19 h / 20 °C / Inert atmosphere View Scheme |
4-hydroxydibenzofuran
3-chloro-4-hydroxydibenzofuran
Conditions | Yield |
---|---|
With tetrachloromethane; chlorine; iron | |
With chlorine In tetrachloromethane Heating; | 50 mg |
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