The company has a professional R & D team, mature technology, very competitive prices and stable high quality products for customers to order high quality and low price product efforts! Appearance:White or off-white Solid Storage:Sealed, dr
Colorcom is a global leader in industrial chemical manufacturing and is continuously innovating and transforming to exceed client expectations and industry standards. Colorcom prides itself on superior customer and technical focus, while focusing on
DayangChem exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product s
Cas:1984-65-2
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:1984-65-2
Min.Order:5 Kiloliter
FOB Price: $1.2 / 5.0
Type:Manufacturers
inquiryOur advantages: 1. High quality and competitive price: 1) Standard: BP/USP/EP/ enterprise standard 2) All purity ≥99% 3) We are manufacturers and can provide high quality products at factory prices. 2. Fast and safe delivery 1) The package c
Cas:1984-65-2
Min.Order:1 Kilogram
FOB Price: $5.0 / 10.0
Type:Trading Company
inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:1984-65-2
Min.Order:1 Kilogram
FOB Price: $139.0 / 210.0
Type:Trading Company
inquiry1.In No Less 10 years exporting experience. you can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specializ
Cas:1984-65-2
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providing h
Product Name: 2,6-Dichloroanisole Synonyms: 1,3-dichloro-2-methoxy-benzen;Benzene, 2,6-dichloro-1-methoxy;1,3-Dichloro-2-methoxybenzene;2,6-DICHLOROANISOLE;2,6-DICHLOROMETHOXYBENZENE;2,6-DICHLORANISOL;2,3- Dichloro methyl phenoxide;Benzene,1,3-
Cas:1984-65-2
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryZhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed
Cas:1984-65-2
Min.Order:1 Kilogram
FOB Price: $2.0
Type:Lab/Research institutions
inquiryAppearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
High quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use
GOLDEN PHARMA CO.,LIMITED.is a professional pharmaceutical company,our team have more than 20years expereince in pharmaceutical production and sales. we are a professional technical enterprise specializing in the R & D, production,QA regulation
Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
Cas:1984-65-2
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryhigh purity,in stock Package:25kg/drum,or as per customers'demand Application:API,Pharmaceutical intermediates Transportation:air,sea,courier
Acmec is a leading manufacturer and supplier of biochemical reagents and life science products. We have over 40,000 items in stock (real-time inventory) and offer discounted prices to registered members of the online store ( www.acmec.com.cn ) Appea
Cas:1984-65-2
Min.Order:1 bottle
Negotiable
Type:Lab/Research institutions
inquiryTAIHO Unique Advantages:1.We're factory2.Free samples available3.Commodity inspection can be done4.ISO9001,Kosher certifications5.10 years experiences Storage:Store in cool &dry place Package:aluminium foil bag/fiber can/plastic drum Application:comp
Cangzhou Enke Pharma Tech Co.,ltd. is located in Cangzhou City, Hebei province ,where is a famous petroleum chemical industry city?in China. Enke Pharma a high-tech enterprise ,and we are dedicated to developing and manufacturing new api,?intermediat
Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
We are committed to providing our customers with the best products and services at the most competitive prices.Appearance:off-white powder Storage:Room temperature with sealed well Package:according to the clients requirement Application:Use as prima
2,6-Dichloroanisole cas 1984-65-2Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
Best quality with low priceAppearance:Clear colourless liquid Storage:ln stock Package:25kg/Barrel Application:Chemicals Transportation:Express/Sea/Air Port:Shanghai
factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
The factory supplies Application:manufacturing supplies
Good Quality Package:1kg/bag Application:Medical or chemical Transportation:Air/Train/Sea Port:Shenzhen
Conditions | Yield |
---|---|
With N,N'-dimethylimidazolium-2-carboxylate In acetonitrile at 160℃; for 2h; Microwave irradiation; Green chemistry; | 97% |
Conditions | Yield |
---|---|
With sodium hydroxide In water at 90℃; for 0.5h; | 77% |
With alkali |
sodium methylate
1,2,3-trichlorobenzene
A
2,3-dichloroanisole
B
2,6-dichloroanisole
Conditions | Yield |
---|---|
In N,N,N,N,N,N-hexamethylphosphoric triamide at 120℃; for 1h; | A 46% B 25% |
In methanol; dimethyl sulfoxide at 50.1℃; Rate constant; |
1,2,3-trichlorobenzene
A
2,6-Dichlorophenol
B
2,3-dichloroanisole
C
2,6-dichloroanisole
Conditions | Yield |
---|---|
With potassium hydroxide; Tris(3,6-dioxaheptyl)amine at 135℃; for 2h; | A 23% B 756 g C 496 g |
2,4,6-trichloroanisole
A
4-chloromethoxybenzene
B
1,3-dichloro-4-methoxybenzene
C
2-Chloroanisole
D
2,6-dichloroanisole
Conditions | Yield |
---|---|
With (C2H5)3NH2CO2; palladium on activated charcoal In acetonitrile at 80℃; Yield given. Further byproducts given. Yields of byproduct given; |
methoxybenzene
A
4-chloromethoxybenzene
B
1,3-dichloro-4-methoxybenzene
C
2-Chloroanisole
D
2,6-dichloroanisole
Conditions | Yield |
---|---|
With chlorine at 25℃; for 2h; Product distribution; var. time; other substituted aromatic ethers; | A 61.4 % Chromat. B 0.8 % Chromat. C 15.4 % Chromat. D 0.2 % Chromat. |
methanol
1,2,3-trichlorobenzene
A
2,3-dichloroanisole
B
2,6-dichloroanisole
Conditions | Yield |
---|---|
With potassium hydroxide; Tris(3,6-dioxaheptyl)amine at 135℃; for 2h; | A 756 g B 496 g |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: chlorine / Reaktion ueber mehrere Stufen 2: alkali View Scheme |
chloro-trimethyl-silane
2,6-dichloroanisole
(4,6-dichloro-5-methoxy-1,3-phenylene)bis(trimethylsilane)
Conditions | Yield |
---|---|
Stage #1: 2,6-dichloroanisole With lithium diisopropyl amide In tetrahydrofuran at -78 - -65℃; for 3h; Inert atmosphere; Stage #2: chloro-trimethyl-silane In tetrahydrofuran at -78 - -40℃; for 22.5h; Inert atmosphere; | 100% |
Stage #1: 2,6-dichloroanisole With lithium diisopropyl amide In tetrahydrofuran at -78 - -65℃; for 3.5h; Inert atmosphere; Schlenk technique; Stage #2: chloro-trimethyl-silane In tetrahydrofuran at -75 - -65℃; for 1h; Inert atmosphere; Schlenk technique; Stage #3: chloro-trimethyl-silane Further stages; | 74% |
carbon dioxide
2,6-dichloroanisole
A
3,5-dichloro-4-methoxybenzoic acid
B
2,4-dichloro-3-methoxybenzoic acid
Conditions | Yield |
---|---|
Stage #1: 2,6-dichloroanisole With sec.-butyllithium In tetrahydrofuran; cyclohexane at -75℃; for 0.75h; Stage #2: carbon dioxide In tetrahydrofuran; cyclohexane at 25℃; | A n/a B 85% |
Conditions | Yield |
---|---|
Stage #1: benzyl bromide With magnesium In diethyl ether Metallation; Stage #2: 2,6-dichloroanisole; 1,3-bis[(diphenylphosphino)propane]dichloronickel(II) In diethyl ether for 12h; Alkylation; Heating; | 78% |
2,6-dichloroanisole
N,N-diisopropyl benzamide
3',5'-dichloro-N,N-diisopropyl-4'-methoxy-[1,1'-biphenyl]-2-carboxamide
Conditions | Yield |
---|---|
With silver hexafluoroantimonate; dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; hexabromobenzene; 2-chloro-1,4-dimethyl-benzene; copper diacetate; cesium pivalate; Trimethylacetic acid at 150℃; for 21h; Inert atmosphere; | 71% |
Conditions | Yield |
---|---|
Stage #1: 2,6-dichloroanisole With N,N,N',N'',N'''-pentamethyldiethylenetriamine; C8H18Mg*2Li(1+)*2C8H17O(1-) In toluene at 25℃; for 1h; Inert atmosphere; Schlenk technique; Stage #2: 2-formylbenzo[b]furan In toluene at 25℃; for 1h; Inert atmosphere; Schlenk technique; | 70% |
Conditions | Yield |
---|---|
With dipotassium peroxodisulfate; palladium diacetate at 80℃; for 24h; | 65% |
With dipotassium peroxodisulfate; palladium diacetate; acetic acid at 80℃; Inert atmosphere; | 65% |
2,6-dichloroanisole
3-Chloro-2-methoxyphenol
Conditions | Yield |
---|---|
Stage #1: 2,6-dichloroanisole With potassium hydroxide; tris-(dibenzylideneacetone)dipalladium(0); tert-butyl XPhos In 1,4-dioxane; water at 100℃; for 2h; Stage #2: With hydrogenchloride In 1,4-dioxane; water | 62% |
2,6-dichloroanisole
o-tolyl magnesium chloride
Conditions | Yield |
---|---|
With triphenylphosphine; nickel dibromide In o-xylene Inert atmosphere; | 39% |
piperazine
2,6-dichloroanisole
1-(3-chloro-2-methoxyphenyl)piperazine
Conditions | Yield |
---|---|
With sodium t-butanolate; palladium diacetate; tri(tert-butyl)phosphite In toluene at 70℃; for 21h; | 37% |
With sodium t-butanolate; tri(tert-butyl)phosphite; palladium diacetate In toluene at 70℃; for 21h; | 37% |
With palladium diacetate; johnphos; sodium t-butanolate In toluene at 80℃; for 21h; Buchwald-Hartwig cross-coupling; | |
With palladium diacetate; johnphos; sodium t-butanolate In toluene at 80℃; for 21h; |
Conditions | Yield |
---|---|
With sodium methylate In N,N,N,N,N,N-hexamethylphosphoric triamide at 120℃; | 33% |
2,6-dichloroanisole
B
1,3-Dichloro-2-trichloromethoxy-benzene
C
1,2,3-trichlorobenzene
Conditions | Yield |
---|---|
With chlorine; phosphorus pentachloride at 195℃; for 11.5h; | A n/a B 24.5% C n/a |
carbon dioxide
2,6-dichloroanisole
2,4-dichloro-3-methoxybenzoic acid
Conditions | Yield |
---|---|
Stage #1: 2,6-dichloroanisole With isopropyllithium In tetrahydrofuran; cyclohexane at -78℃; for 0.75h; Stage #2: carbon dioxide In tetrahydrofuran; cyclohexane | 24% |
With sec.-butyllithium In tetrahydrofuran; dichloromethane |
2,6-dichloroanisole
m,p-dichloroaniline
2,3',4,4'-tetrachloro-3-methoxybiphenyl
Conditions | Yield |
---|---|
With n-Amyl nitrite at 60℃; | 16% |
2,6-dichloroanisole
1-t-Butoxycarbonylpiperazine
4-(3-chloro-2-methoxy-phenyl)-piperazine-1-carboxylic acid tert-butyl ester
Conditions | Yield |
---|---|
With caesium carbonate; tris-(dibenzylideneacetone)dipalladium(0); DavePhos In toluene at 100℃; for 16h; | 8% |
2,6-dichloroanisole
propionyl chloride
1-(3',5'-dichloro-4'-methoxyphenyl)-1-propanone
Conditions | Yield |
---|---|
With carbon disulfide; aluminium trichloride |
Conditions | Yield |
---|---|
With carbon disulfide; aluminium trichloride |
2,6-dichloroanisole
A
3,5-dichloro-4-hydroxybenzene sulfonic acid
B
2,6-dichloroanisole-4-sulfonic acid
Conditions | Yield |
---|---|
With sulfuric acid at 20℃; for 91.6667h; |
Conditions | Yield |
---|---|
With tetrabutylammonium perchlorate In N,N-dimethyl-formamide at 25 - 30℃; Title compound not separated from byproducts; | A 7 % Chromat. B 39 % Chromat. |
2,6-dichloroanisole
2,6-dichloroanisole-4-sulfonic acid
Conditions | Yield |
---|---|
With sulfuric acid at 20℃; Rate constant; |
Conditions | Yield |
---|---|
With isopentyl nitrite at 120℃; for 1.5h; Cadogan diaryl coupling reaction; |
Conditions | Yield |
---|---|
Stage #1: 2,3,4-trichloroaniline; 2,6-dichloroanisole With isopentyl nitrite at 140℃; Cadogan coupling; Stage #2: With boron tribromide In dichloromethane demethylation; |
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