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Titanium hydroxide(Ti(OH)4), (T-4)-Appearance:Off white to slight yellow solid Storage:Stored in shaded, cool and dry places Package:1L 5L 10L 25L bottle Application:pharma intermediate Transportation:Handle with cares to avoid damaging the packages.

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Synthetic route

: 7732-18-5
water

: 546-68-9
titanium(IV)isopropoxide

: 20338-08-3
titanium(IV) hydroxide

Conditions

Conditions	Yield
In ethanol washing (H2O), filtration, drying (373 K);

: dipotassium hexafluorotitanate(IV)

: titanium(IV) sulfate

: sodium thiosulfate

A: 20338-08-3
titanium(IV) hydroxide

B: 7704-34-9
sulfur

Conditions

Conditions	Yield
In water in sealed test tube above 140°C;	A >99 B n/a
In water in sealed test tube above 140°C;	A >99 B n/a

...Expand

: titanium oxide sulfate

: ammonium hydroxide

: holmium(III) nitrate

A: 20338-08-3
titanium(IV) hydroxide

B: holmium(III) hydroxide

Conditions

Conditions	Yield
In water pptn.; washing, drying at 100-110°C;

...Expand

: titanium oxide sulfate

: ammonium hydroxide

: gadolinium(III) nitrate

A: 20338-08-3
titanium(IV) hydroxide

B: gadolinium(III) hydroxide

Conditions

Conditions	Yield
In water pptn.; washing, drying at 100-110°C;

...Expand

: titanium oxide sulfate

: ammonium hydroxide

: erbium(III) nitrate

A: 20338-08-3
titanium(IV) hydroxide

B: erbium hydroxide

Conditions

Conditions	Yield
In water pptn.; washing, drying at 100-110°C;

...Expand

: 7440-32-6
titanium

: 1333-74-0
hydrogen

: 80937-33-3
oxygen

A: 20338-08-3
titanium(IV) hydroxide

B: 7704-98-5
titanium dihydride

C: 956378-98-6
[TiH(OH)3]

D: 42765-12-8
titanium dihydroxide

E: HTiO(OH)

Conditions

Conditions	Yield
In neat (no solvent) Irradiation (UV/VIS); laser ablated Zr co-deposited with H2+O2 in excess Ar onto a 10K CsI window, UV-irradiated, annealed at 22-34 K (mechanism discussed); not isolated, detected by IR;

...Expand

: 7440-32-6
titanium

: 7722-84-1
dihydrogen peroxide

A: 12137-20-1
titanium oxide

B: 20338-08-3
titanium(IV) hydroxide

C: titanium Ti(Al)

D: 42765-12-8
titanium dihydroxide

E: titanium(IV) oxide

Conditions

Conditions	Yield
In neat (no solvent) byproducts: CO2, H2O; Irradiation (UV/VIS); (further products), laser ablated Zr co-deposited with H2O2 in excess Aronto a 10K CsI window, UV-irradiated, annealed at 22-30 K; not isolated, detected by IR;

...Expand

: titanium oxide sulfate

: ammonium hydroxide

: thulium(III) nitrate

A: 20338-08-3
titanium(IV) hydroxide

B: thulium(III) hydroxide

Conditions

Conditions	Yield
In water pptn.; washing, drying at 100-110°C;

...Expand

: titanium oxide sulfate

: ammonium hydroxide

: terbium(III) nitrate

A: 20338-08-3
titanium(IV) hydroxide

B: terbium(III) hydroxide

Conditions

Conditions	Yield
In water pptn.; washing, drying at 100-110°C;

...Expand

: titanium oxide sulfate

: ammonium hydroxide

: samarium(III) nitrate

A: 20338-08-3
titanium(IV) hydroxide

B: samarium(III) hydroxide

Conditions

Conditions	Yield
In water pptn.; washing, drying at 100-110°C;

...Expand

: titanium oxide sulfate

: ammonium hydroxide

: europium(III) nitrate

A: 20338-08-3
titanium(IV) hydroxide

B: europium(III) hydroxide

Conditions

Conditions	Yield
In water pptn.; washing, drying at 100-110°C;

...Expand

: sodium hexafluorotitanate

: 7732-18-5
water

: 20338-08-3
titanium(IV) hydroxide

Conditions

Conditions	Yield
With hydrogenchloride; ammonia In water byproducts: F(1-); two-stage formation of Ti(OH)4 from a aq. solution of Na2TiF6 (0.04 N, 10 ml) with ammonia in presence of 10 ml of 0.04 N aq. HCl; mechanism discussed;; pptn.;;

: 5TiO(OH)2*13TiO2

: 7732-18-5
water

: 20338-08-3
titanium(IV) hydroxide

Conditions

Conditions	Yield
With sodium chloride In water hydrogel aged for 2 h at 80°C in 1 M NaCl; ppt. sepd. by centrifugation, triply washed by water decantation and centrifuged for 5 min at 2000 rpm; sample dried for 7 days in vac. desiccator under pressure of 50 kPa over pelletized alkali; thermal anal.;

: titanium(IV) oxide

: ammonium hydroxide

: 7732-18-5
water

: 20338-08-3
titanium(IV) hydroxide

Conditions

Conditions	Yield
In hydrogen fluoride aq. HF; TiO2 dissolved, pptd. (aq. NH4OH); washed (aq. NH4OH); elem. anal.;

...Expand

: 7732-18-5
water

: 7550-45-0
titanium tetrachloride

A: 20338-08-3
titanium(IV) hydroxide

B: 19977-99-2, 13780-39-7
titanium oxydichloride

Conditions

Conditions	Yield
In water byproducts: HCl; a large amounts of water was added to TiCl4;	A n/a B 0%

...Expand

: 7732-18-5
water

: 7550-45-0
titanium tetrachloride

: 20338-08-3
titanium(IV) hydroxide

Conditions

Conditions	Yield
In butan-1-ol TiCl4 dissolved in H2O and n-butanol, cooled in ice bath with stirring for 20 min;
hydrolysis;
In ethylene glycol hydrolysis in diethylene glycol medium;

: 546-68-9
titanium(IV) isopropylate

: 7732-18-5
water

: 20338-08-3
titanium(IV) hydroxide

Conditions

Conditions	Yield
With sodium carbonate In water hydrolysis of metal salt with 5% aq. Na2CO3; filtrated; washed with deionized water to pH=7;
With ammonium hydroxide In ethanol Ti compd. added into water and EtOH at pH 9 (by dropwise addn. of aq. NH3; dried overnight at 22°C and at 110°C;
In water hydrolysis;

: 7550-45-0
titanium tetrachloride

: 1310-73-2
sodium hydroxide

: 20338-08-3
titanium(IV) hydroxide

Conditions

Conditions	Yield
In water liq. TiCl4 added to twice distd. water and neutralized with 2 M NaOH until pH 3 was stable for 5 min; ppt. sepd. by centrifugation, triply washed by water decantation and centrifuged for 5 min at 2000 rpm; sample dried for 7 days in vac. desiccator under pressure of 50 kPa over pelletized alkali; thermal anal.;
In sulfuric acid TiCl4 dissolved in 5% soln. of H2SO4; 40% soln. of NaOH added in small portions; ppt. washed repeatedly (water);

: dipotassium hexafluorotitanate(IV)

: potassium hydroxide

A: potassium fluoride

B: 20338-08-3
titanium(IV) hydroxide

...Expand

: titanium(IV) sulfate

: 20338-08-3
titanium(IV) hydroxide

Conditions

Conditions	Yield
With water In water hydrolysis at 363 K; washed, filtered, dried at 383 K for 20 h;
With polyethylene glycol In water mixed, pptd.; washed (ethanol), dried at 353 K under Ar;
In water at 60℃; for 20h; pH=8.0;

: titanium(IV) sulfate

: 7664-41-7
ammonia

: 20338-08-3
titanium(IV) hydroxide

Conditions

Conditions	Yield
With acetylene black In water NH3 addn. with stirring (pptn.); decantation, washing, drying at 200°C; detd. by thermogravimetry,X-ray diffraction, sedimentation analysis and electron microscopy;

: titanium(IV) oxohydroxide

: 7664-93-9
sulfuric acid

: 7664-41-7
ammonia

: 20338-08-3
titanium(IV) hydroxide

Conditions

Conditions	Yield
In sulfuric acid H2TiO3 dissolved in concd.H2SO4, pptd.(ammonia);

...Expand

: oxotitanium(IV)sulfate hydrate

: ammonium hydroxide

: 20338-08-3
titanium(IV) hydroxide

Conditions

Conditions	Yield
In water titanyl sulfate (17.3 g) added slowly to distd. H2O (room temp.); 3 M NH4OH added; ppt. filtered; washed with H2O;

: ammonium oxosulfatotitanate monohydrate

: 20338-08-3
titanium(IV) hydroxide

Conditions

Conditions	Yield
With ammonia Ti-salt soln. pptn. with ammonia soln., according to: V. V. Sakharov, L.M. Zitsev, V. N. Zabelin, I. A. Apraksin, Zhur. Neorg. Khim. 17 (1972) 2392; Russ. J. Inorg. Chem. 17 (1972) No. 9; ppt. sepn. from mother liquor;

: 7550-45-0
titanium tetrachloride

: 20338-08-3
titanium(IV) hydroxide

Conditions

Conditions	Yield
With H2O

: lead(II) nitrate

: zirconyl nitrate

: 7550-45-0
titanium tetrachloride

A: 20338-08-3
titanium(IV) hydroxide

B: 756456-88-9, 14475-63-9
zirconium tetrahydroxide

C: lead (II) hydroxide

Conditions

Conditions	Yield
With ammonia In ammonia; water; nitric acid aq. HNO3; aq. ammonia=NH3; copptd. by adding the mixed nitrate soln. to aq. NH3 of pH 9, filtered,washed, dried at 100°C for 4 h, then heated at 400°C for 5 h;

...Expand

: ammonium hydroxide

: 7550-45-0
titanium tetrachloride

: 20338-08-3
titanium(IV) hydroxide

Conditions

Conditions	Yield
In water TiCl4 dissolved in deionized water, NH4OH added until pH 8.0; filtration, washing (distd. water), drying (80 °C, 6 h);
In water addn. of excess of soln. NH4OH (25 %) to soln. of TiCl4 (0.2 M)(stirring); filtration, washing (H2O), drying (120°C), washing (aq. 0.25 M H2SO4), drying;
In water hydrothermal decompn. of Ti(IV) chloride; NH4OH soln. introduced into react. mixt., pH adjusted to 6.5-6.8; ppt. washing (distd. water);

: 20338-08-3
titanium(IV) hydroxide

: cesium hydroxide

: 144-62-7
oxalic acid

: cesium-bis(oxalato)oxo-titanate(IV) hydrate

Conditions

Conditions	Yield
With HCl In water addition of oxalic acid to a soln. of Ti(OH)4, cooling (ice), CsOH added slowly with stirring, ethanol is added to get two layers; elem. anal.;	85%

...Expand

: 20338-08-3
titanium(IV) hydroxide

: titanium(IV) oxide

Conditions

Conditions	Yield
With dihydrogen peroxide In water Ti(OH)4 peptized with 30% H2O2 (stirring); refluxed (100°C, 2, 6,or 10 h); soln. applied on glass substrates (dip-coating, room temp., w ithdrawing speed 5-6 cm/min); dried under IR light (100°C);
With sodium hydroxide In sodium hydroxide High Pressure; titanium hydroxide and 15 M NaOH mixed; transfered into autoclave; heated (110°C, 48 h); solid centrifuged; washed with H2O, 0.1 M HCl, H2O to pH 7; dispersed in H2O; centrifuged; dried (110°C, 1 d); calcined (400°C, 3 h) in air; XRD; TEM;
In neat (no solvent) calcined for 1 h;

: 20338-08-3
titanium(IV) hydroxide

: 7440-32-6
titanium

Conditions

Conditions	Yield
In sodium hydroxide Electrolysis; 90-95 °C, current density 0.625 A/dm^2, Cu cathode;
With 4-aminobenzene sulfonic acid In water Electrolysis; 15-20 ° C, current density 0.1-0.15 A/dm^2, Cu cathode, Pt or Zn-Ti anode;
With sulfanilic acid In water Electrolysis; 15-20 ° C, current density 0.1-0.15 A/dm^2, Cu cathode, Pt or Zn-Ti anode;
In sodium hydroxide aq. NaOH; Electrolysis; 90-95 °C, current density 0.625 A/dm^2, Cu cathode;

: 20338-08-3
titanium(IV) hydroxide

: rutile

Conditions

Conditions	Yield
With nitric acid dissoln. in HNO3 then hydrolysis;
With sodium chloride In neat (no solvent) annealed;
With hydrogenchloride; sodium hydroxide heating the intermediate solid prod. with aq.HCl;

: 20338-08-3
titanium(IV) hydroxide

: titanium(IV) oxide

Conditions

Conditions	Yield
thermal decompn. of the hydroxide at 600°C in air for 6 h;
dehydration (373 K), calcination (773 K);
With dihydrogen peroxide

: 20338-08-3
titanium(IV) hydroxide

: 7722-84-1
dihydrogen peroxide

: titanium(IV) oxide

Conditions

Conditions	Yield
In water sol of amorphous Ti peroxide (obtained by adding soln. of hydrogen peroxide to Ti hydroxide soln.) heated at 100°C (TiO2 sol) and at 400-430°C;

: potassium dihydrogenphosphate

: 20338-08-3
titanium(IV) hydroxide

: 584-08-7
potassium carbonate

: 239809-02-0
potassium titanyl phosphate

Conditions

Conditions	Yield
With HCl; tetra potassium pyrophosphate In neat (no solvent) freshly pptd. Ti(OH)4 dissolved in HCl, mixed with tetra potassium pyrophosphate, aq. soln. of KH2PO4 and K2CO3 added drop-wise under stirring (pH=5), ppt. filtered, washed with water, dried at 100 °C, heated at 500 - 650 °C for 2 h in air; powder XRD;
With HCl; triethanolamine In neat (no solvent) freshly pptd. Ti(OH)4 dissolved in HCl, mixed with triethanolamine, aq. soln. of KH2PO4 and K2CO3 added drop-wise under stirring (pH=5), ppt. filtered, washed with water, dried at 100 °C, heated at 500 - 650 °C for 2 h in air; powder XRD;
With HCl In neat (no solvent) freshly pptd. Ti(OH)4 dissolved in HCl, aq. soln. of KH2PO4 added drop-wise under stirring, aq. soln. of K2CO3 added (pH=5), ppt. filtered, washed with water, dried at 100 °C, heated at 500 - 650 °C for2 h in air; powder XRD, TG-DTA;

...Expand

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