As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
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inquiryDIMETHYL SULFOXIDE-D6 CAS:2206-27-1 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic int
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A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc
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inquiryDIMETHYL SULFOXIDE-D6 Basic information Product Name: DIMETHYL SULFOXIDE-D6 Synonyms: Dimethyl sulfoxide-d6 99.9 atom % D, anhydrous;Dimethyl sulfoxide-d6 99.9 atom % D, contains 1 % (v/v) TMS;Dimethyl sulfoxide-d6 anhydrous, 99.9 atom % D;AMM
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inquiryhigh quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
A
dimethylsulfoxide-d6
Conditions | Yield |
---|---|
With trifluoroacetic acid In dichloromethane | A n/a B 92% |
dimethyl sulfide-d6
A
dimethylsulfoxide-d6
B
((methyl-d3)sulfonyl)methane-d3
Conditions | Yield |
---|---|
With 5,10,15,20-tetrakisphenylporphyrin; oxygen In benzene for 1.33333h; Mechanism; Product distribution; Ambient temperature; Irradiation; var. irradiation times, var. solvent, also with addition H2O; other sulfides; kinetic isotope effect; | A 5.2% B n/a C n/a |
N,N'-dimethylbenzylamine
C2H(2)H6OS(1+)
A
dimethylsulfoxide-d6
B
N,N-dimethylbenzylammonium ion
Conditions | Yield |
---|---|
at 20℃; Equilibrium constant; |
trifluoroacetate
C2H(2)H6OS(1+)
A
dimethylsulfoxide-d6
B
trifluoroacetic acid
Conditions | Yield |
---|---|
at 20℃; Equilibrium constant; Rate constant; |
dimethylsulfoxide-d6
Conditions | Yield |
---|---|
at 200℃; under 20 Torr; |
C2H(2)H6OS
A
dimethylsulfoxide-d6
B
((methyl-d3)sulfonyl)methane-d3
Conditions | Yield |
---|---|
With oxygen at -23.1℃; under 110 Torr; Rate constant; Irradiation; | |
With oxygen at -15.1℃; under 110 Torr; Rate constant; Irradiation; |
[2,2]bipyridinyl
1,3-cyclooctadiene
2-benzenesulfonyl-1,4-dibromobenzene
2,2'-bis-benzenesulfonyl-4,4'-dibromobiphenyl
dimethylsulfoxide-d6
Conditions | Yield |
---|---|
In methanol |
cis-{PtCl2(d6-Me2SO)2}
2-(2'-pyridyl)quinoxaline
A
dimethylsulfoxide-d6
(2-(2'-pyridyl)quinoxaline)platinum(II) dichloride
Conditions | Yield |
---|---|
at 24.84℃; Equilibrium constant; |
cis-{PtCl2(d6-Me2SO)2}
A
dimethylsulfoxide-d6
Conditions | Yield |
---|---|
at 24.84℃; Equilibrium constant; |
dimethylsulfoxide-d6
Conditions | Yield |
---|---|
at 20℃; for 0.0833333h; Inert atmosphere; Schlenk technique; | 100% |
Conditions | Yield |
---|---|
for 72h; | 98% |
at 50℃; for 72h; | 29% |
18% |
dimethylsulfoxide-d6
Conditions | Yield |
---|---|
Stage #1: dimethylsulfoxide-d6 With acetic anhydride at 130℃; for 1h; Sealed tube; Stage #2: With sulfuric acid for 0.0833333h; | 98% |
dimethylsulfoxide-d6
MoO2Cl2(H2O)2
Conditions | Yield |
---|---|
In diethyl ether soln. of ligand in Et2O was added with stirring to soln. of Mo complex in Et2O; mixt. was stirred for 5 min; filtered; washed (Et2O); dried (vac.); elem. anal.; | 97% |
Conditions | Yield |
---|---|
With ferrous(II) sulfate heptahydrate; trimethylsilylazide; dihydrogen peroxide at 50℃; for 3h; Inert atmosphere; Sealed tube; | 96% |
dimethylsulfoxide-d6
benzyl alcohol
d-(E)-(2-(benzyloxy)vinyl)benzene
Conditions | Yield |
---|---|
With potassium hydroxide at 20℃; | 95% |
With potassium hydroxide; phenol at 60℃; for 12h; Green chemistry; | 65% |
Conditions | Yield |
---|---|
With ammonium iodide; water at 130℃; for 24h; Sealed tube; Glovebox; stereoselective reaction; | 95% |
Conditions | Yield |
---|---|
With ferrous(II) sulfate heptahydrate; trimethylsilylazide; dihydrogen peroxide at 50℃; for 3h; Inert atmosphere; Sealed tube; | 95% |
dimethylsulfoxide-d6
para-iodoanisole
(4-methoxyphenyl)(methyl)sulfane-d3
Conditions | Yield |
---|---|
With copper(l) iodide; zinc diacetate at 135℃; for 24h; Reagent/catalyst; regioselective reaction; | 94% |
Conditions | Yield |
---|---|
With ammonium peroxydisulfate In 1,4-dioxane at 100℃; for 6h; Green chemistry; | 94% |
Conditions | Yield |
---|---|
With acetic acid at 120℃; for 3h; | 93% |
dimethylsulfoxide-d6
Conditions | Yield |
---|---|
With thionyl chloride at 25℃; regioselective reaction; | 93% |
dimethylsulfoxide-d6
methyl 2-(phenylethynyl)benzoate
Conditions | Yield |
---|---|
With thionyl chloride at 25℃; | 92% |
dimethylsulfoxide-d6
Conditions | Yield |
---|---|
With thionyl chloride at 25℃; regioselective reaction; | 92% |
dimethylsulfoxide-d6
2-((2-phenyl)ethynyl)-5-methylbenzoic acid methyl ester
Conditions | Yield |
---|---|
With thionyl chloride at 25℃; | 91% |
dimethylsulfoxide-d6
Conditions | Yield |
---|---|
With thionyl chloride at 25℃; regioselective reaction; | 91% |
dimethylsulfoxide-d6
Conditions | Yield |
---|---|
With thionyl chloride at 25℃; regioselective reaction; | 91% |
dimethylsulfoxide-d6
N,N'-(2,2'-(ethyne-1,2-diyl)bis(2,1-phenylene))bis(4-methylbenzenesulfonamide)
Conditions | Yield |
---|---|
With thionyl chloride at 0 - 70℃; | 91% |
With thionyl chloride at 0 - 70℃; for 0.0833333h; | 91% |
dimethylsulfoxide-d6
Conditions | Yield |
---|---|
In dimethylsulfoxide-d6 Kinetics; 308.2 K; detected by NMR; | A <1 B 90% |
dimethylsulfoxide-d6
Conditions | Yield |
---|---|
With thionyl chloride at 25℃; | 90% |
dimethylsulfoxide-d6
Conditions | Yield |
---|---|
With thionyl chloride at 25℃; regioselective reaction; | 90% |
Conditions | Yield |
---|---|
With iodine at 80℃; for 12h; Inert atmosphere; | 90% |
Conditions | Yield |
---|---|
With copper(ll) sulfate pentahydrate at 130℃; | 90% |
Conditions | Yield |
---|---|
With dipotassium peroxodisulfate; silver(I) acetate; cobalt acetylacetonate at 130℃; for 12h; Mechanism; regioselective reaction; | 89% |
Conditions | Yield |
---|---|
With potassium tert-butylate at 120℃; for 10h; Inert atmosphere; | 89% |
Conditions | Yield |
---|---|
With sodium t-butanolate In water-d2 at 75℃; for 24h; Inert atmosphere; | 88.6% |
Conditions | Yield |
---|---|
With copper(II) nitrate trihydrate; iodine at 100℃; for 8h; | 88% |
1,1-Diphenylethylene
dimethylsulfoxide-d6
deuterated 2-(methylsulfonyl)-1-phenylethanone
Conditions | Yield |
---|---|
With D-Fructose; carbon monoxide; oxygen; copper(II) dipivaloate; palladium dichloride at 80℃; under 760.051 Torr; for 15h; | 88% |
dimethylsulfoxide-d6
2-Nitroanisole
A
C8H7(2)H2NO3
B
C8H6(2)H3NO3
Conditions | Yield |
---|---|
With trimethylsulphonium iodide; sodium hydride | A 11.5% B 87.8% |
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