DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe
Cas:10297-73-1
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inquiry4'-Methylsulphonylacetophenone CAS No.:10297-73-1 Name: 4'-Methylsulphonylacetophenone Synonyms: 1-[4-(Methylsulfonyl)phenyl]ethan-1-one Molecular Structure Molecular Formula: C9H10O3S M
Cas:10297-73-1
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Cas:10297-73-1
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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inquiryAppearance:White to slightly yellow powder Storage:room temperature Package:25kg/drum Application:Determination of nitrogenous matter in water. Transportation:Express/Sea/Air Port:any port in china
Cas:10297-73-1
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inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:10297-73-1
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Cas:10297-73-1
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:10297-73-1
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providing h
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Cas:10297-73-1
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inquiryProduct name: 4’-Methylsulphonyl Acetophenone CAS No.:10297-73-1 Molecule Formula:C9H10O3S2 Molecule Weight:198.23 Purity: 99% Package: 25kg/drum Description:White crystalline powder Manufacture Standards:Enterprise Standard
Cas:10297-73-1
Min.Order:1 Kilogram
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inquiryOur Advantages A. International Top level TechnologyOur company owned biomedicine experts are famous at home and abroad with rich experience in research and development in the field of efficient chiral functional molecules research and development an
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Cas:10297-73-1
Min.Order:1 Milligram
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inquiry4-Methylsulphonylacetophenone Basic information Product Name: 4-Methylsulphonylacetophenone Synonyms: P-METHYLSULFONYLACETOPHENONE;1-[4-(METHYLSULFONYL)PHENYL]-1-ETHANONE;1-[4-(METHYLSULFONYL)PHENYL]ETHAN-1-ONE;1-(4-(METHYLSULFONYL)PHENYL)ETHANONE;1
Cas:10297-73-1
Min.Order:1 Gram
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Type:Lab/Research institutions
inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
Cas:10297-73-1
Min.Order:1 Kilogram
FOB Price: $18.0 / 20.0
Type:Trading Company
inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:10297-73-1
Min.Order:1 Kilogram
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inquiryZhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed
Cas:10297-73-1
Min.Order:1 Kilogram
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inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
Cas:10297-73-1
Min.Order:1 Gram
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Type:Lab/Research institutions
inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
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Min.Order:1 Metric Ton
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inquiryAppearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
GOLDEN PHARMA CO.,LIMITED.is a professional pharmaceutical company,our team have more than 20years expereince in pharmaceutical production and sales. we are a professional technical enterprise specializing in the R & D, production,QA regulation
We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp
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inquiryStock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
Cas:10297-73-1
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inquiryLower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
Cas:10297-73-1
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inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
R & D enterprises have their own stock in stockAppearance:To be subject to the object Package:Customized Application:pharmaceutical intermediates Transportation:Air Port:Shanghai;Guangzhou
4-(Methylthio)acetophenone
4-(methanesulfonyl)acetophenone
Conditions | Yield |
---|---|
With MMPP In methanol; dichloromethane at 20℃; for 3h; | 100% |
With sulfuric acid; dihydrogen peroxide; acetic acid at 0 - 70℃; for 2h; | 99% |
With dihydrogen peroxide; Cu2H4O40Te2W8(12-)*(x)H2O*12Na(1+) In acetonitrile at 20℃; for 10h; Sealed tube; | 98% |
4-Iodoacetophenone
sodium methansulfinate
4-(methanesulfonyl)acetophenone
Conditions | Yield |
---|---|
With copper(l) iodide; N,N-dimethyl-N-benzyl-N-(2-methacryloyloxyethyl)ammonium bromide; caesium carbonate In chlorobenzene at 110℃; for 24h; Reagent/catalyst; Solvent; Temperature; Inert atmosphere; | 94.9% |
With potassium phosphate; copper(l) iodide; (2S,4R)-N-(2,6-dimethylphenyl)-4-hydroxypyrrolidine-2-carboxamide In dimethyl sulfoxide at 20℃; for 24h; Inert atmosphere; | 83% |
With copper(l) iodide; sodium L-prolinate In dimethyl sulfoxide at 80℃; for 24h; | 80% |
With copper(I) trifluoromethanesulfonate benzene; N,N`-dimethylethylenediamine In dimethyl sulfoxide at 110℃; for 20h; |
4-(Methylthio)acetophenone
A
1-(4-methansulfinylphenyl)ethanone
B
4-(methanesulfonyl)acetophenone
Conditions | Yield |
---|---|
With boron trifluoride diethyl etherate In acetonitrile for 0.0833333h; cooling; | A 94% B 2% |
With oxygen at 80℃; for 20h; chemoselective reaction; | A 67% B 9% |
With oxygen; 4C24H20P(1+)*2H(1+)*V10O28(6-) In water; butanone at 30℃; under 760.051 Torr; for 2h; Irradiation; Schlenk technique; | A 65% B 11 %Chromat. |
1-(4-(methylsulfonyl)phenyl)ethan-1-one oxime
4-(methanesulfonyl)acetophenone
Conditions | Yield |
---|---|
With sodium nitrite In water; acetonitrile at 40℃; for 4.33333h; | 89% |
sodium methansulfinate
para-bromoacetophenone
4-(methanesulfonyl)acetophenone
Conditions | Yield |
---|---|
With potassium phosphate; copper(l) iodide; (2S,4R)-N-(2,6-dimethylphenyl)-4-hydroxypyrrolidine-2-carboxamide In dimethyl sulfoxide at 90℃; for 24h; Inert atmosphere; | 80% |
With copper(l) iodide; sodium L-prolinate In dimethyl sulfoxide at 95℃; for 48h; | 62% |
4-(methanesulfonyl)acetophenone
Conditions | Yield |
---|---|
With 2,6-bis[1-(2,6-dimethylphenylimino)ethyl]pyridine cobalt(II)dichloride; bis(pinacol)diborane; sodium t-butanolate In tetrahydrofuran; methanol at 65℃; for 3h; Schlenk technique; Inert atmosphere; | 80% |
di-tert-butyl peroxide
4-(methanesulfonyl)acetophenone
Conditions | Yield |
---|---|
With water at 110℃; for 12h; Sealed tube; Green chemistry; | 75% |
sodium methansulfinate
4-acetylphenylboronic acid
4-(methanesulfonyl)acetophenone
Conditions | Yield |
---|---|
With copper diacetate; 4 Angstroem MS; potassium carbonate In dimethyl sulfoxide at 20 - 60℃; for 16h; | 71% |
1-(4-(methylsulfonyl)phenyl)ethan-1-ol
A
4-(methanesulfonyl)acetophenone
B
4-methylsulfonylbenzoic acid
Conditions | Yield |
---|---|
Stage #1: 1-(4-(methylsulfonyl)phenyl)ethan-1-ol With oxygen; sodium hydride In tetrahydrofuran at 0 - 20℃; for 16h; Stage #2: With hydrogenchloride In water | A 30% B 68% |
Conditions | Yield |
---|---|
With copper(I) oxide; potassium tert-butylate; oxygen; acetylacetone at 100℃; for 20h; | 52% |
carbonic acid dimethyl ester
4-acetylphenylboronic acid
4-(methanesulfonyl)acetophenone
Conditions | Yield |
---|---|
With sodium metabisulfite; tetrabutylammomium bromide; palladium dichloride; tert-butyl XPhos In N,N-dimethyl-formamide at 120℃; for 12h; Inert atmosphere; | 50% |
methyl magnesium iodide
4-(methylsulfonyl)benzonitrile
4-(methanesulfonyl)acetophenone
Conditions | Yield |
---|---|
With diethyl ether; benzene Erwaermen des Reaktionsgemisches mit wss. H2SO4; |
4-methylsulfonylbenzoyl chloride
4-(methanesulfonyl)acetophenone
Conditions | Yield |
---|---|
With benzene Erhitzen einer Loesung des Reaktionsprodukts in Benzol mit wss. HCl und Essigsaeure; |
1-(4-methansulfinylphenyl)ethanone
4-(methanesulfonyl)acetophenone
Conditions | Yield |
---|---|
With potassium chromite; sodium perchlorate; oxalic acid In acetic acid at 40℃; Rate constant; | |
With potassium bromate; sulfuric acid; mercury(II) diacetate In acetic acid at 35℃; Kinetics; Mechanism; Thermodynamic data; other temperatures, ΔH(excit.), ΔS(excit.); | |
With peroxomonophosphoric acid; sodium perchlorate In water; acetic acid at 35℃; Kinetics; Further Variations:; Temperatures; | |
With oxo(salen)chromium(V) perchlorate In acetonitrile at 24.85℃; Kinetics; Further Variations:; Reagents; |
diazomethane
para-methanesulfonylbenzaldehyde
4-(methanesulfonyl)acetophenone
Conditions | Yield |
---|---|
In diethyl ether |
(4-Acetyl-phenylsulfon)-essigsaeure
4-(methanesulfonyl)acetophenone
Conditions | Yield |
---|---|
at 160 - 180℃; |
4-(methanesulfonyl)acetophenone
Conditions | Yield |
---|---|
With dihydrogen peroxide; acetic acid at 100℃; |
tetrachloromethane
3-hydroxy-3-(4-methanesulfonyl-phenyl)-2-phenyl-butyric acid
A
phenylacetic acid
B
4-(methanesulfonyl)acetophenone
Conditions | Yield |
---|---|
at 65℃; Rate constant; sowie bei 75grad; |
methyl-phenyl-thioether
4-(methanesulfonyl)acetophenone
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 79 percent / potassium peroxymonosulfate / H2O; tetrahydrofuran; methanol / 15 h / 25 °C View Scheme |
methyl-phenyl-thioether
4-(methanesulfonyl)acetophenone
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 82 percent / AlCl3 / CHCl3 / 1.5 h / 5 °C 2: 100 percent / MMPP / methanol; CH2Cl2 / 3 h / 20 °C View Scheme | |
Multi-step reaction with 2 steps 1: 90 percent / AlCl3 / CHCl3 / 0 - 5 °C 2: KMnO4, AcOH / H2O / 60 - 70 °C View Scheme | |
Multi-step reaction with 2 steps 1: aluminum (III) chloride / chloroform / 2 h / Cooling 2: dihydrogen peroxide; ammonium molybdate / water; methanol / 20 °C View Scheme |
p-cyanophenyl methyl sulfide
4-(methanesulfonyl)acetophenone
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 98.5 percent / tetrahydrofuran; diethyl ether / 1.) -78 deg C - RT, 2.) RT, 2.5 h 2: 91 percent / mCPBA / CH2Cl2 / Ambient temperature View Scheme |
(phenylthio)acetic acid
4-(methanesulfonyl)acetophenone
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: AlCl3 / nitrobenzene; CS2 2: aq. H2O2, HCl 3: 160 - 180 °C View Scheme |
(4-acetyl-phenylsulfanyl)-acetic acid
4-(methanesulfonyl)acetophenone
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: aq. H2O2, HCl 2: 160 - 180 °C View Scheme |
1-diacetoxymethyl-4-methanesulfonyl-benzene
4-(methanesulfonyl)acetophenone
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: aq. H2SO4 / ethanol 2: diethyl ether View Scheme |
Methyl p-tolyl sulfone
4-(methanesulfonyl)acetophenone
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: CrO3, H2SO4 / acetic acid 2: aq. H2SO4 / ethanol 3: diethyl ether View Scheme |
ethylenediaminetetraacetic acid
4-(Methylthio)acetophenone
4-(methanesulfonyl)acetophenone
Conditions | Yield |
---|---|
With oxone In water; acetone |
dichloromethane
4-(Methylthio)acetophenone
4-(methanesulfonyl)acetophenone
Conditions | Yield |
---|---|
With sodium hydrogencarbonate; magnesium bis(monoperoxyphthalate) hexahydrate In methanol | |
With sodium hydrogencarbonate; magnesium bis(monoperoxyphthalate) hexahydrate In methanol | |
With sodium hydrogencarbonate; magnesium bis(monoperoxyphthalate) hexahydrate In methanol |
4-(Methylthio)acetophenone
B
4-(methanesulfonyl)acetophenone
Conditions | Yield |
---|---|
With m-chloroperoxybenzoic acid In dichloromethane | A n/a B 11.91 g (91%) |
acetophenone
4-(methanesulfonyl)acetophenone
Conditions | Yield |
---|---|
With m-chloroperoxybenzoic acid In dichloromethane; 4-(Methylthio)acetophenone | 11.91 g (91%) |
4-(methanesulfonyl)acetophenone
5,5-dimethyl-2-phenyl-1,3,2-dioxaborinane
Conditions | Yield |
---|---|
With hydrogenchloride; bis(1,5-cyclooctadiene)nickel (0); sodium methylate; C67H68N2 In cyclohexane; water at 50℃; for 1h; Inert atmosphere; enantioselective reaction; | 99% |
4-(methanesulfonyl)acetophenone
phenylhydrazine
4-(methylsulfonyl)acetophenone phenylhydrazone
Conditions | Yield |
---|---|
With acetic acid In ethanol at 70℃; | 97% |
In ethanol; acetic acid |
4-(methanesulfonyl)acetophenone
2-bromo-1-(4-methanesulfonylphenyl)ethanone
Conditions | Yield |
---|---|
With bromine In chloroform at 34 - 36℃; for 0.25h; Solvent; | 94.4% |
With bromine; acetic acid at 20℃; | 93% |
With N-Bromosuccinimide; toluene-4-sulfonic acid In acetonitrile at 80℃; | 89% |
Conditions | Yield |
---|---|
With tetrabutylammonium tetrafluoroborate; hydrogen iodide In ethanol at 50℃; for 24h; Electrochemical reaction; Schlenk technique; Green chemistry; | 94% |
With indium(III) triflate; copper(l) iodide; oxygen In 1-methyl-pyrrolidin-2-one at 100℃; under 760.051 Torr; for 30h; Schlenk technique; | 90% |
With iodine In ethanol at 20℃; for 3h; Green chemistry; | 74% |
4-(methanesulfonyl)acetophenone
1-(4-(methylsulfonyl)phenyl)ethan-1-ol
Conditions | Yield |
---|---|
With tris(pentafluorophenyl)borate; hydrogen In toluene at 60℃; under 45603.1 Torr; for 12h; Reagent/catalyst; Molecular sieve; | 94% |
With methanol; sodium tetrahydroborate In tetrahydrofuran at 0℃; for 2h; | 87% |
With water; 1,8-diazabicyclo[5.4.0]undec-7-ene; bis(pinacol)diborane at 60℃; for 10h; Sealed tube; chemoselective reaction; | 80% |
With sodium tetrahydroborate In methanol at 0 - 25℃; | 68% |
With methanol; sodium tetrahydroborate at 0 - 20℃; Inert atmosphere; Schlenk technique; |
4-(methanesulfonyl)acetophenone
(R)-1-(4-(methylsulfonyl)phenyl)ethan-1-ol
Conditions | Yield |
---|---|
With C37H40MnN2O2P2(1+)*Br(1-); sodium t-butanolate In isopropyl alcohol at 50℃; for 3h; Inert atmosphere; Schlenk technique; enantioselective reaction; | 93% |
Stage #1: 4-(methanesulfonyl)acetophenone With (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole Stage #2: With dimethylsulfide borane complex |
4-(methanesulfonyl)acetophenone
α,α-dibromo-4-methanesulfonylacetophenone
Conditions | Yield |
---|---|
With bromine In chloroform; water at 50 - 55℃; for 0.25h; | 91.7% |
With bromine; acetic acid | |
With bromine In acetic acid at 40℃; |
4-(methanesulfonyl)acetophenone
2-amino-1-benzylamine
Conditions | Yield |
---|---|
With copper(II) bis(trifluoromethanesulfonate); toluene-4-sulfonic acid In toluene at 100℃; for 36h; Schlenk technique; Sealed tube; | 91% |
4-(methanesulfonyl)acetophenone
Conditions | Yield |
---|---|
With acetic acid In ethanol at 70℃; | 91% |
4-(methanesulfonyl)acetophenone
phenylhydrazine
(1E)-1-{1-[4-(methylsulfonyl)phenyl]ethylidene}-2-phenylhyldrazine
Conditions | Yield |
---|---|
With acetic acid In ethanol for 1h; | 89% |
N-methyl-3-formylindole
4-(methanesulfonyl)acetophenone
Conditions | Yield |
---|---|
With sodium hydroxide In ethanol; water at 20℃; for 10h; Claisen-Schmidt Condensation; | 89% |
morpholine
4-(methanesulfonyl)acetophenone
Conditions | Yield |
---|---|
With sulfur at 75℃; for 3h; Temperature; | 88% |
With toluene-4-sulfonic acid; sulfur for 3h; Willgerodt-Kindler reaction; Reflux; | 60% |
5-bromo-1H-indole-3-carboxaldehyde
4-(methanesulfonyl)acetophenone
Conditions | Yield |
---|---|
With sodium hydroxide In ethanol; water at 20℃; for 10h; Claisen-Schmidt Condensation; | 88% |
Conditions | Yield |
---|---|
With copper(II) nitrate trihydrate; iodine at 100℃; for 8h; | 88% |
4-(methanesulfonyl)acetophenone
Conditions | Yield |
---|---|
With nickel(II) tetrafluoroborate hexahydrate; ammonia; hydrogen; bis(2-diphenylphosphinoethyl)phenylphosphine In 2,2,2-trifluoroethanol at 120℃; for 24h; chemoselective reaction; | 88% |
With ammonia; hydrogen In tetrahydrofuran at 120℃; for 20h; | 82% |
With ammonium hydroxide; hydrogen at 140℃; under 48754.9 Torr; for 20h; |
2-aminopyridine
4-(methanesulfonyl)acetophenone
toluene-4-sulfonic acid hydrazide
Conditions | Yield |
---|---|
With iodine; dimethyl sulfoxide; triphenylphosphine at 100℃; for 12h; | 88% |
Conditions | Yield |
---|---|
With acetic acid In ethanol at 70℃; | 88% |
4-(methanesulfonyl)acetophenone
Conditions | Yield |
---|---|
With acetic acid In ethanol at 70℃; | 88% |
4-(methanesulfonyl)acetophenone
2-Fluorobenzaldehyde
Conditions | Yield |
---|---|
With sodium hydroxide In methanol; water at 20℃; for 12h; Claisen-Schmidt Condensation; | 86% |
Conditions | Yield |
---|---|
With copper(II) nitrate trihydrate; iodine at 100℃; for 8h; | 85% |
Trimethyl orthoacetate
4-(methanesulfonyl)acetophenone
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In methanol at 60℃; for 4h; | 85% |
piperonal
4-(methanesulfonyl)acetophenone
Conditions | Yield |
---|---|
With sodium hydroxide In methanol; water at 20℃; for 12h; Claisen-Schmidt Condensation; | 85% |
4-(methanesulfonyl)acetophenone
N-methoxylamine hydrochloride
1-(4-(methylsulfonyl)phenyl)ethanone-O-methyl oxime
Conditions | Yield |
---|---|
With sodium acetate In ethanol; water for 2h; Reflux; | 84% |
4-(4-morpholinyl)benzaldehyde
4-(methanesulfonyl)acetophenone
Conditions | Yield |
---|---|
With sodium hydroxide In methanol; water at 20℃; Claisen-Schmidt Condensation; | 84% |
4-(methanesulfonyl)acetophenone
4-(bis(2-chloroethyl)amino)benzaldehyde
Conditions | Yield |
---|---|
With sodium hydroxide In methanol; water at 20℃; Claisen-Schmidt Condensation; | 84% |
4-(methanesulfonyl)acetophenone
3-Fluorobenzaldehyde
Conditions | Yield |
---|---|
With sodium hydroxide In methanol; water at 20℃; for 12h; Claisen-Schmidt Condensation; | 84% |
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