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inquirymiconasole nitrate
benzene
1-[β-(2,4-dichlorophenyl)-phenethyl]imidazole
Conditions | Yield |
---|---|
Stage #1: miconasole nitrate With sodium hydroxide In chloroform Stage #2: benzene With trifluorormethanesulfonic acid In chloroform at 25℃; for 4h; Friedel Crafts alkylation; | 65% |
miconasole nitrate
A
(2,4-dichlorophenyl)methanol
B
2,4 dichlorobenzoic acid
C
2,4-dichlorobenzaldeyhde
D
1-(2,4-Dichloro-phenyl)-2-imidazol-1-yl-ethanol; compound with nitric acid
E
1-[2,4-dichloro-β-(2,4-dichlorophenylcarbonyloxy)phenethyl]-imidazole nitrate
Conditions | Yield |
---|---|
With 2,2'-azobis(isobutyronitrile); oxygen In ethanol at 77.5℃; under 5171.5 Torr; for 3.4h; Product distribution; Mechanism; other times; | A 0.2 % Chromat. B 0.7 % Chromat. C 1.3 % Chromat. D 0.9 % Chromat. E 2.3 % Chromat. F 0.3 % Chromat. |
miconasole nitrate
A
2,4 dichlorobenzoic acid
B
2,4-dichlorobenzaldeyhde
C
1-(2,4-Dichloro-phenyl)-2-imidazol-1-yl-ethanol; compound with nitric acid
D
1-[2,4-dichloro-β-(2,4-dichlorophenylcarbonyloxy)phenethyl]-imidazole nitrate
Conditions | Yield |
---|---|
With 2,2'-azobis(isobutyronitrile); oxygen In ethanol at 77.5℃; under 5171.5 Torr; for 3.4h; Further byproducts given; | A 0.7 % Chromat. B 1.3 % Chromat. C 0.9 % Chromat. D 2.3 % Chromat. |
miconasole nitrate
D
1-(2,4-dichloro-benzoyloxy)-1-(2,4-dichloro-phenyl)-2-imidazol-1-yl-ethane
Conditions | Yield |
---|---|
With sodium hydroxide; 2,2'-azobis(isobutyronitrile); oxygen In ethanol at 111℃; under 10343 Torr; for 3.3h; Further byproducts given; |
miconasole nitrate
D
1-(2,4-dichloro-benzoyloxy)-1-(2,4-dichloro-phenyl)-2-imidazol-1-yl-ethane
Conditions | Yield |
---|---|
With sodium hydroxide; 2,2'-azobis(isobutyronitrile); oxygen In ethanol at 111℃; under 10343 Torr; for 3.3h; Further byproducts given; |
miconasole nitrate
D
1-(2,4-dichloro-benzoyloxy)-1-(2,4-dichloro-phenyl)-2-imidazol-1-yl-ethane
Conditions | Yield |
---|---|
With sodium hydroxide; 2,2'-azobis(isobutyronitrile); oxygen In ethanol at 111℃; under 10343 Torr; for 3.3h; Further byproducts given; |
2,6-di-tert-butyl-4-methyl-phenol
miconasole nitrate
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