CAS No.2501-94-2,T-BUTYLPHOSPHINE Suppliers

Ality Chemical Corporation

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Shanghai Upbio Tech Co.,Ltd

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Phosphine,(1,1-dimethylethyl)-

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TAIZHOU ZHENYU BIOTECHNOLOGY CO., LTD

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Antimex Chemical Limied

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t-Butylphosphine, Min. 95% TBP (10 wt% in hexane)

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Zibo Hangyu Biotechnology Development Co., Ltd

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ZHEJIANG JIUZHOU CHEM CO.,LTD

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Changzhou Extraordinary Pharmatech co.,LTD

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Shanghai united Scientific Co.,Ltd.

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Strem Chemicals, Inc.

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FMC Lithium

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Synthetic route

: 7360-64-7
(dimethylamino)dibromoborane

: 67877-34-3, 112215-24-4
lithium tert-butylphosphide

A: 122501-55-7, 112438-33-2
1,3-di-tert-butyl-2,4-bis(dimethylamino)-1,2,3,4-diphosphadiboretane

B: 2501-94-2
tert-butylphosphine

Conditions

Conditions	Yield
In pentane under N2 or Ar or in vac., cooled to -45°C, addn. of LiPHtBu in pentane, warmed to ambient temp.; filtration of insolubles, from filtrate evapn. of volatiles; elem. anal.;	A 95% B n/a

...Expand

: 1113-31-1
dichlorodimethylaminoborane

: 67877-34-3, 112215-24-4
lithium tert-butylphosphide

A: 122501-55-7, 112438-33-2
1,3-di-tert-butyl-2,4-bis(dimethylamino)-1,2,3,4-diphosphadiboretane

B: 2501-94-2
tert-butylphosphine

Conditions

Conditions	Yield
In pentane byproducts: LiCl; under N2 or Ar or in vac., cooled to -45°C, addn. of LiPHtBu in pentane, warmed to ambient temp.; filtration of insolubles, from filtrate evapn. of volatiles; elem. anal.;	A 95% B n/a

...Expand

: C4H11AlCl3P

: 2501-94-2
tert-butylphosphine

Conditions

Conditions	Yield
With triethylamine In toluene	88%

: 25979-07-1
tert-butyldichlorophosphine

: 2501-94-2
tert-butylphosphine

Conditions

Conditions	Yield
With lithium aluminium tetrahydride In butyl diglyme at 20 - 100℃;	82%
With lithium aluminium tetrahydride at 20℃; for 3h; Schlenk technique; Inert atmosphere;	82%
With lithium aluminium tetrahydride In diethylene glycol dimethyl ether at -78℃;	80%
With lithium aluminium tetrahydride In dibutyl ether
With lithium aluminium tetrahydride

: 29149-32-4
tert-butyldifluorophosphine

: 2501-94-2
tert-butylphosphine

Conditions

Conditions	Yield
With ethyl trimethylsilyl ether at 20℃; for 1h;	65%

: 105414-84-4
S-ethyl tert-butylthiophosphinite

: 75-36-5
acetyl chloride

: 811-51-8
sodium thioethylate

A: 625-60-5
ethyl thioacetate

B: 2501-94-2
tert-butylphosphine

C: 78187-17-4
S,S-diethyl tert-butyldithiophosphonite

D: 25979-07-1
tert-butyldichlorophosphine

Conditions

Conditions	Yield
for 20h; Ambient temperature; sealed;	A 51% B 24% C n/a D n/a

...Expand

: 115-11-7
isobutene

: 2501-94-2
tert-butylphosphine

Conditions

Conditions	Yield
With phosphan; toluene-4-sulfonic acid at 110℃; for 14h;	37%

: 7621-12-7
1,4-dipotassium-1,2,3,4-tetra-t-butyl-tetraphosphane

: 2501-94-2
tert-butylphosphine

Conditions

Conditions	Yield
With water In 1,4-dioxane

: t-Butylfluorphosphan

A: 2501-94-2
tert-butylphosphine

B: 29149-32-4
tert-butyldifluorophosphine

C: C8H19FP2

Conditions

Conditions	Yield
Ambient temperature;

...Expand

: t-Butyl-t-butylaminophosphan

A: 2501-94-2
tert-butylphosphine

B: 228703-72-8
(CH3)3CP[HNC(CH3)3]2

C: C12H29NP2

Conditions

Conditions	Yield
Ambient temperature;

...Expand

: 42491-33-8
tert-butylbis(trimethylsilyl)phosphine

A: 2501-94-2
tert-butylphosphine

B: 67033-70-9
tert-butyl(trimethylsilyl)phosphine

Conditions

Conditions	Yield
With trans-Crotonaldehyde other reagent: mesityl oxide;

: 75-75-2
methanesulfonic acid

: 142-82-5
n-heptane

: 115-11-7
isobutene

phosphine: phosphine

A: 2501-94-2
tert-butylphosphine

B di-tert-butylphosphine: di-tert-butylphosphine

Conditions

Conditions	Yield
at 60℃; under 24271.8 - 25742.8 Torr;
at 60℃; under 24271.8 - 25742.8 Torr;

...Expand

: 90600-97-8
1,2-Di-tert-butyldiphosphane

A: 2501-94-2
tert-butylphosphine

B: 82240-49-1
tert-Butyldiphosphan

C: 1,2-Di-tert-butyltriphosphan

D PH3, P3H5: PH3, P3H5

Conditions

Conditions	Yield
With diphosphane In 1,2-dimethoxyethane at 60℃; for 1h; THF; Title compound not separated from byproducts;
With diphosphane In 1,2-dimethoxyethane at 60℃; for 1h; THF; Yield given. Title compound not separated from byproducts;

...Expand

: tris(tert-butylphosphino)phosphane

A: 2501-94-2
tert-butylphosphine

B: 90600-97-8
1,2-Di-tert-butyldiphosphane

C higher tert-butylphosphanes: higher tert-butylphosphanes

Conditions

Conditions	Yield
at -30℃; Mechanism; disproportination and decomposition studies;

...Expand

: 115713-55-8
(Et2P(CH2)2PEt2)Ni(η-Me3SiPPCMe3)

A: 54910-60-0
bis{1,2-bis(diethylphosphino)ethane}nickel(0)

B: 96555-93-0
(((C2H5)2PCH2CH2P(C2H5)2)Ni)2P2

C: 1825-61-2
Methoxytrimethylsilane

D: 2501-94-2
tert-butylphosphine

E: 90600-97-8
1,2-Di-tert-butyldiphosphane

Conditions

Conditions	Yield
With methanol In toluene excess CH3OH, reaction proceeds slowly at 0°C and rapidly at 20°C; observed by NMR-spectroscopy;

...Expand

: 115713-56-9
((C6H11)2PCH2CH2P(C6H11)2)Ni(HPPC(CH3)3)

A: 96555-95-2
((C6H11)2PCH2CH2P(C6H11)2Ni)2P2

B: 2501-94-2
tert-butylphosphine

Conditions

Conditions	Yield
In toluene 5 d at 80°C;

: tert-butylphosphine trimethylaluminum complex

A: 2501-94-2
tert-butylphosphine

B: 75-24-1
trimethylaluminum

Conditions

Conditions	Yield
In gas above 298 K;

: 25979-07-1
tert-butyldichlorophosphine

A: 79082-91-0, 5995-07-3
1,2,3,4-Tetra-tert-butyl-tetraphosphetane

B: 2501-94-2
tert-butylphosphine

C: 90600-97-8
1,2-Di-tert-butyldiphosphane

Conditions

Conditions	Yield
With triethylsilane; gallium(III) trichloride In chlorobenzene at 100℃; for 168h;

...Expand

: 25979-07-1
tert-butyldichlorophosphine

A: 79082-91-0, 5995-07-3
1,2,3,4-Tetra-tert-butyl-tetraphosphetane

B: 2501-94-2
tert-butylphosphine

Conditions

Conditions	Yield
With triethylsilane; gallium(III) trichloride In chlorobenzene at 100℃; for 168h;

: 2501-94-2
tert-butylphosphine

: t-butylphosphine-borane

Conditions

Conditions	Yield
With borane-THF In tetrahydrofuran; hexane at 0℃; for 1h;	99%

: 2501-94-2
tert-butylphosphine

: borane tetrahydrofuran

: 162053-46-5
tert-butylphosphine-borane

Conditions

Conditions	Yield
In tetrahydrofuran; hexane (Ar); transferring of soln. of t-BuPH2 in hexane to flask via syringe, slowly addn. of BH3-THF complex in THF at 0°C , stirring for 1 h at this temp.; removal of solvents under vac., distn. in vac.;	99%

: 148892-97-1
tris(3,4,5-trifluorophenyl)borane

: 2501-94-2
tert-butylphosphine

: 184044-79-9
tris(3,4,5-trifluorophenyl)boron-tert-butylphosphine adduct

Conditions

Conditions	Yield
In light petroleum (inert atmosphere); stirring (48 h); decantation, drying (vac.), further material from the supernatant; no reliable elemental analysis;	99%

: 2501-94-2
tert-butylphosphine

: 1109-15-5
tris(pentafluorophenyl)borate

: 184044-76-6
tris(pentafluorophenyl)boron-tert-butylphosphine adduct

Conditions

Conditions	Yield
In light petroleum (inert atmosphere); stirring (48 h); decantation, drying (vac.), further material from the supernatant; no reliable elemental analysis;	99%

: 2501-94-2
tert-butylphosphine

: 146355-09-1
tris(2,6-difluorophenyl)borane triethylphosphine oxide

: 184044-78-8
tris(2,6-difluorophenyl)boron-tert-butylphosphine adduct

Conditions

Conditions	Yield
In light petroleum (inert atmosphere); stirring (48 h); decantation, drying (vac.), further material from the supernatant; no reliable elemental analysis;	99%

: 2501-94-2
tert-butylphosphine

: 19287-45-7
diborane

: 162053-46-5
tert-butylphosphine-borane

Conditions

Conditions	Yield
In tetrahydrofuran at 0 - 20℃;	99%

: 12128-23-3
tricarbonylcyclopentadienylmolybdenum(II) chloride

: 2501-94-2
tert-butylphosphine

: cis-dicarbonyl(chloro)(η5-cyclopentadienyl)(tert-butylphosphine)molybdenum(II)

Conditions

Conditions	Yield
In methyl cyclohexane under N2; equimolar mixt. of Mo complex and ligand in methylcyclohexaneheated at 70°C for 1 h; cooled to room temp.; concd. in vac.; crystd. at 0°C; filtered; washed with pentane; dried in vac.; elem. anal.;	98%

: pentamethylcyclopentadienyl tantalum(V) tetrachloride

: 2501-94-2
tert-butylphosphine

: 406943-02-0
C5(CH3)5TaCl4(PH2C(CH3)3)

Conditions

Conditions	Yield
In toluene in dry Ar atmosphere C5(CH3)5TaCl4 suspended in toluene, equimolar amt. of PH2C(CH3)3 added, stirred at room temp. until clear soln. obtained; solvent removed to dryness, residue extd. with-pentane, cooled to 5 °C, crystn.; elem. anal.;	96%

: 2501-94-2
tert-butylphosphine

: 630-19-3
pivalaldehyde

: 1246895-41-9
C9H21OP

Conditions

Conditions	Yield
With trifluoroacetic acid at 80℃;	96%

: 2501-94-2
tert-butylphosphine

: 100-52-7
benzaldehyde

: t-butylbenzylphosphine oxide

Conditions

Conditions	Yield
With trifluoroacetic acid at 80℃;	95%

: 2501-94-2
tert-butylphosphine

: 187879-67-0
1,5-dihydro-benzo[e][1,3,2]dioxathiepine 3,3-dioxide

: 104229-83-6
2-tert-butyl-1,3-dihydro-isophosphindole 2-oxide

Conditions

Conditions	Yield
Multistep reaction;	94%
With n-butyllithium; dihydrogen peroxide; sodium sulfate In tetrahydrofuran	94%

: 80432-35-5
pentamethylcyclopentadienyl niobium(V) tetrachloride

: 2501-94-2
tert-butylphosphine

: 499219-54-4
C5(CH3)5NbCl4(PH2C(CH3)3)

Conditions

Conditions	Yield
In toluene; pentane in dry Ar atmosphere C5(CH3)5NbCl4 suspended in toluene, equimolar amt. of PH2C(CH3)3 added, stirred at room temp. until clear soln. obtained; solvent removed to dryness, residue extd. with-pentane, cooled to 5 °C, crystn.; elem. anal.;	94%

: 2501-94-2
tert-butylphosphine

: 78463-57-7, 74399-62-5, 74399-57-8
di-tert-butyldichloromethylenediphosphine

: 25979-07-1
tert-butyldichlorophosphine

: 1,2,3,4-Tetra-tert-butyl-[1,2,3,4]tetraphospholane

Conditions

Conditions	Yield
In toluene at 60℃; for 12h;	93%

...Expand

: 487-68-3
mesytaldehyde

: 2501-94-2
tert-butylphosphine

: 1246895-43-1
C14H23OP

Conditions

Conditions	Yield
With trifluoroacetic acid at 80℃;	93%

: [(η(5)-cyclopentadienyl)Fe(CO)3] tetrafluoroborate

: 2501-94-2
tert-butylphosphine

: 215736-16-6
[(tert-butyl)phosphane]dicarbonyl(η(5)-cyclopentadienyl)iron(II) tetrafluoroborate

Conditions

Conditions	Yield
In acetonitrile byproducts: CO; N2-atmosphere; stirring Fe-complex with slight excess of phosphine (70°C, 20 h); concn. (vac.), pptn. on ether addn., filtration, drying (vac.); elem. anal.;	91%
In acetonitrile byproducts: CO; N2 atmosphere, mixing of cooled soln. of Fe complex (0°C) with phosphane, stirring (60°C, 10 h); reduction of volume (vacuum), pptn. (ether), filtration, washing (ether), drying (vacuum); elem. anal.;	85%

: 3150-16-1
methyl 4,6-O-benzylidene-2,3-anhydro-α-D-mannopyranoside

: 2501-94-2
tert-butylphosphine

: (methyl 3-deoxy-4,6-oxo-benzylidene-α-D-pyranopyranoside)-3-tert-butylphosphine

Conditions

Conditions	Yield
Stage #1: tert-butylphosphine In tetrahydrofuran; hexane at -78 - 20℃; for 2h; Schlenk technique; Inert atmosphere; Stage #2: methyl 4,6-O-benzylidene-2,3-anhydro-α-D-mannopyranoside In tetrahydrofuran for 6h; Schlenk technique;	90%

: 685-83-6
bis(diethylamino)chlorophosphine

: 2501-94-2
tert-butylphosphine

: 1,1,3,3-Tetrakis(diethylamino)-2-tert-butyl-triphosphan

Conditions

Conditions	Yield
With n-butyllithium 1.) Et2O, n-hexane, reflux, 0.5 h, 2.) n-pentane, -78 deg C, 1 h;	89%

: 92695-35-7
(η5-cyclopentadienyl)Re(NO)(P(C6H5)3)(CF3SO3)

: 2501-94-2
tert-butylphosphine

: Re(C5H5)(P(C6H5)3)(PH2C(CH3)3)(NO)(1+)*OSO2CF3(1-)={Re(C5H5)(P(C6H5)3)(PH2C(CH3)3)(NO)}OSO2CF3

Conditions

Conditions	Yield
In benzene addn. of P(t-Bu)H2 to complex in a Schlenk tube with stirring, react. time 3 h; addn. of hexane, ppt. filtered, washed with hexane, dissolved in THF, slowly addn. of ether, ppt. filtered, dried under oil pump vac.; elem. anal.;	89%

: Re(C5H5)(P(C6H5)3)(OSO2CF3)(NO)

: 2501-94-2
tert-butylphosphine

: Re(C5H5)(P(C6H5)3)(PH2C(CH3)3)(NO)(1+)*OSO2CF3(1-)={Re(C5H5)(P(C6H5)3)(PH2C(CH3)3)(NO)}OSO2CF3

Conditions

Conditions	Yield
In benzene addn. of P(t-Bu)H2 to complex in a Schlenk tube with stirring, react. time 3 h; addn. of hexane, ppt. filtered, washed with hexane, dissolved in THF, slow addn. of ether by vapor diffusion, ppt. filtered, dried under oil pump vac., pure by 1H- and 31P-NMR;	88%

: 2501-94-2
tert-butylphosphine

: 28240-64-4
bis(diphenylphosphino)methane

: 25979-07-1
tert-butyldichlorophosphine

: 2,3-Di-tert-butyl-1,4-diphenyl-[1,2,3,4]tetraphospholane

Conditions

Conditions	Yield
In toluene at 60 - 80℃; for 12h;	86%

...Expand

: 75-77-4
chloro-trimethyl-silane

: 2501-94-2
tert-butylphosphine

: 42491-33-8
tert-butylbis(trimethylsilyl)phosphine

Conditions

Conditions	Yield
Stage #1: tert-butylphosphine With n-butyllithium In diethyl ether at -78 - 20℃; for 2.25h; Inert atmosphere; Schlenk technique; Glovebox; Stage #2: chloro-trimethyl-silane In diethyl ether at -78 - 20℃;	86%

: 19519-59-6
2-chloroacetylenephosphonic acid dimethyl ester

: 2501-94-2
tert-butylphosphine

: dimethyl <(tert-butylphosphino)ethynyl>phosphonate

Conditions

Conditions	Yield
	85%

: 15321-51-4
diiron nonacarbonyl

: 2501-94-2
tert-butylphosphine

: 85737-35-5
Fe(CO)4{PH2(C(CH3)3)}

Conditions

Conditions	Yield
In diethyl ether byproducts: Fe(CO)5; strirring at room temp. for 24 h in dark; filtration, removing Fe(CO)5, distn.; elem. anal.;	84%

: 2501-94-2
tert-butylphosphine

: 1252080-10-6
(5aS,9aS)-octahydrobenzo[e][1,3,2]dioxathiepine 3,3-dioxide

: 1252080-12-8
(3aS,7aS)-2-(tert-butyl)octahydro-1H-isophosphindole 2-sulfide

Conditions

Conditions	Yield
Stage #1: tert-butylphosphine With n-butyllithium In tetrahydrofuran; octane; hexane at -78 - 20℃; for 1h; Inert atmosphere; Stage #2: (5aS,9aS)-octahydrobenzo[e][1,3,2]dioxathiepine 3,3-dioxide In tetrahydrofuran; octane; hexane at -78 - 20℃; for 4h; Inert atmosphere; Further stages;	81%
Stage #1: tert-butylphosphine With n-butyllithium In tetrahydrofuran; octane; hexane at -78 - 20℃; Stage #2: (5aS,9aS)-octahydrobenzo[e][1,3,2]dioxathiepine 3,3-dioxide With n-butyllithium In tetrahydrofuran; octane; hexane at -78 - 20℃; Stage #3: With sulfur In tetrahydrofuran; octane; hexane; water at 20℃; for 2h; optical yield given as %ee;	81%

: 2501-94-2
tert-butylphosphine

: 4718-00-7
di-tert-butylantimony chloride

: C12H28PSb

Conditions

Conditions	Yield
Stage #1: tert-butylphosphine With n-butyllithium In hexane; pentane at 0℃; Schlenk technique; Inert atmosphere; Stage #2: di-tert-butylantimony chloride In hexane; pentane at -20 - 20℃; Schlenk technique; Inert atmosphere;	81%

: 2501-94-2
tert-butylphosphine

: 436-59-9
dimesitylfluoroborane

: 118496-13-2
(Mes)2BP(H)(C(CH3)3)

Conditions

Conditions	Yield
In diethyl ether 0°C, stirring for 1 h at room temp.;	80%

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Antimex Chemical Limied

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FMC Lithium

FMC Lithium

Synthetic route

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