Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
Cas:487-68-3
Min.Order:1 Kilogram
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Type:Lab/Research institutions
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Cas:487-68-3
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
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Cas:487-68-3
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inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:487-68-3
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inquiry1. Product advantages High purity, all above 98.5%, no impurities after dissolution We will test each batch to ensure quality OEM and private brand services designed for free Various cap colors available We can also provide MT1 peptide powd
Cas:487-68-3
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inquiryProduct Name 2,4,6-Trimethylbenzaldehyde CAS No. 487-68-3 Molecular Formula C10H12O
Cas:487-68-3
Min.Order:5 Metric Ton
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inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:487-68-3
Min.Order:1 Kilogram
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inquiryMesitaldehyde CAS:487-68-3 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic intermediate
Cas:487-68-3
Min.Order:1 Gram
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:487-68-3
Min.Order:1 Kilogram
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inquirySuperiority We can customize and synthesize products that other suppliers may not be able to provide. Advantage cof, mof ligand manufacturer Product Detail
Cas:487-68-3
Min.Order:100 Kilogram
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Type:Trading Company
inquiry1. Timely and efficient service to ensure communication with customers 2. Produce products of different specifications and sizes according to your requirements. 3. Quality procedures and standards recognized by SGS. Advanced plant equipment ensures
Cas:487-68-3
Min.Order:1 Kilogram
FOB Price: $60.0 / 80.0
Type:Lab/Research institutions
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Cas:487-68-3
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inquiryBest quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
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Cas:487-68-3
Min.Order:1 Kilogram
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inquiryHangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:487-68-3
Min.Order:10 Gram
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Type:Lab/Research institutions
inquiryMassive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
Product name: 2,4,6-Trimethylbenzaldehyde CAS No.:487-68-3 Molecule Formula:C10H12O Molecule Weight:148.20 Purity: 99.0% Package: 200kg/drum Description:Colorless transparent liquid Manufacture Standards:Enterprise Standard TESTI
Cas:487-68-3
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiryProduct Details Grade: pharmaceutical grade Purity:99%+ ProductionCapacity: 1000 Kilogram/Month Scope of use: For scientific research only(The product must be used legally) Our Advantage 1. Best quality with competitive price. 2. Quick shipping,
Cas:487-68-3
Min.Order:1 Gram
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Type:Lab/Research institutions
inquiryGMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,
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Cas:487-68-3
Min.Order:1 Kilogram
FOB Price: $18.0 / 20.0
Type:Trading Company
inquiryWe product this chemical more than 10 years . We are very experience to export it to many countries, Our superior & stable quality , competitive price gain warm reception from our customers. Product Name:Mesitaldehyde CAS No:487-68-3 Synonyms
Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
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Conditions | Yield |
---|---|
With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; iodic acid In N,N-dimethyl-formamide at 20℃; for 2h; Reagent/catalyst; Temperature; Inert atmosphere; | 99% |
With 5-nitro-3-oxo-1λ3-benzo[d][1,2]iodaoxol-1(3H)-yl acetate In N,N-dimethyl-formamide at 60℃; for 24h; Reagent/catalyst; | 98% |
With N-Bromosuccinimide; β‐cyclodextrin In methanol; water; acetone at 20℃; for 8h; | 96% |
Conditions | Yield |
---|---|
With 1-dodecyl-3-methylimidazolium iron chloride; periodic acid at 30℃; for 1.5h; | 98% |
With 4Na(1+)*6H(1+)*NiMo6O24(10-)=Na4H6NiMo6O24; oxygen In water; acetonitrile at 20℃; under 760.051 Torr; for 12h; Irradiation; | 91% |
With sodium nitrate; acetic acid In water for 8h; Reflux; | 83% |
With potassium hydroxide; cetyltrimethylammonim bromide; potassium nitrate In water for 7.5h; pH=10 - 11; Reflux; | 82% |
With (NH4)4[ZnMo6O18(OH)6]; oxygen In water; acetonitrile at 60℃; under 760.051 Torr; for 12h; | 81% |
Conditions | Yield |
---|---|
Stage #1: 1,3,5-trimethyl-benzene With titanium tetrachloride In dichloromethane at 0℃; for 1h; Inert atmosphere; Stage #2: Dichloromethyl methyl ether In dichloromethane at 0℃; for 0.75h; Inert atmosphere; regioselective reaction; | 96% |
With silver trifluoromethanesulfonate In dichloromethane at -78℃; for 0.333333h; Inert atmosphere; | 69% |
With dichloromethane; titanium tetrachloride |
2,4,6-trimethylbenzaldehyde oxime
mesytaldehyde
Conditions | Yield |
---|---|
With chromium trioxide-kieselghur reagent In dichloromethane for 3h; Reflux; | 92% |
With 2-iodoxybenzoic acid; β‐cyclodextrin In water; acetone at 20℃; for 12h; | 90% |
With iodobenzene; β‐cyclodextrin; potassium bromide In water; acetone at 20℃; for 12h; | 90% |
Conditions | Yield |
---|---|
Stage #1: N,N-dimethyl-formamide With trichlorophosphate In dichloromethane at -10℃; for 0.333333h; Stage #2: 1,3,5-trimethyl-benzene In dichloromethane at -5℃; for 6.16667h; Solvent; Reflux; | 90.3% |
mesytaldehyde
Conditions | Yield |
---|---|
With water at 20℃; | 89% |
Conditions | Yield |
---|---|
With sodium periodate In N,N-dimethyl-formamide at 150℃; for 0.833333h; | 87% |
With sodium periodate; N,N-dimethyl-formamide at 150℃; for 0.833333h; | 87% |
With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione In dimethyl sulfoxide at 65℃; for 2.5h; | 80% |
With potassium hydroxide; 2-nitropropane In isopropyl alcohol at 40 - 45℃; for 0.333333h; | 75% |
With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione In dimethyl sulfoxide at 60℃; |
mesytaldehyde
Conditions | Yield |
---|---|
With Bromoform; potassium tert-butylate In hexane at -78℃; for 3h; | 87% |
Multi-step reaction with 2 steps 1: chloroform; water / 24 h / 20 °C 2: air / 20 °C View Scheme |
Dichloromethyl methyl ether
1,3,5-trimethyl-benzene
A
mesytaldehyde
B
1-(dichloromethyl)-2,4,6-trimethylbenzene
C
3-dichloromethyl-2,4,6-trimethylbenzaldehyde
D
1,3-bis(dichloromethyl)mesitylene
Conditions | Yield |
---|---|
With titanium tetrachloride In dichloromethane at 20 - 25℃; for 0.25h; Further byproducts given; | A 84% B 3 % Chromat. C 3 % Chromat. D 1 % Chromat. |
With titanium tetrachloride In dichloromethane for 0.25h; Ambient temperature; Yields of byproduct given; | A 84% B n/a C n/a D n/a |
With aluminium trichloride In dichloromethane at 20 - 25℃; for 0.25h; Further byproducts given; | A 55 % Chromat. B 10% C 10 % Chromat. D 25 % Chromat. |
Conditions | Yield |
---|---|
With C25H19(1+)*BF4(1-) In dichloromethane at 20℃; for 3.5h; Reagent/catalyst; Schlenk technique; Inert atmosphere; | A 79% B 65% |
2,4,6-trimethylbenzyl mercaptan
mesytaldehyde
Conditions | Yield |
---|---|
With dipotassium peroxodisulfate; tetrakis(pyridine)silver(II) peroxodisulfate; oxygen In N,N-dimethyl-formamide at 23℃; under 760.051 Torr; Irradiation; | 76% |
2,4,6-trimethylphenyl bromide
N,N-dimethyl-formamide
mesytaldehyde
Conditions | Yield |
---|---|
Stage #1: 2,4,6-trimethylphenyl bromide With n-butyllithium In tetrahydrofuran at -78℃; for 1.5h; Stage #2: N,N-dimethyl-formamide In tetrahydrofuran at -78 - 20℃; | 75% |
1-(2,4,6-trimethylphenyl)prop-2-en-1-ol
A
mesytaldehyde
B
E-3-(2,4,6-trimethylphenyl)propenal
Conditions | Yield |
---|---|
With periodic acid; pyridinium chlorochromate In acetonitrile at 0 - 20℃; for 2h; stereoselective reaction; | A 12% B 74% |
2,4,6-trimethylbenzaldehyde azine
mesytaldehyde
Conditions | Yield |
---|---|
With ammonium cerium(IV) nitrate In water; acetonitrile at 50℃; for 18h; Oxidation; | 71% |
N,N,N',N'-tetraformylhydrazine
1,3,5-trimethyl-benzene
A
mesytaldehyde
B
2,4,6-trimethylbenzaldehyde azine
Conditions | Yield |
---|---|
Stage #1: N,N,N',N'-tetraformylhydrazine; 1,3,5-trimethyl-benzene With aluminium trichloride In 1,2-dichloro-ethane at -11 - 0℃; for 18h; Stage #2: With water | A 21% B 68% |
Conditions | Yield |
---|---|
With aluminium trichloride In chlorobenzene at -15 - -7℃; for 16h; Formylation; | 67% |
3-pyridinecarboxylic acid ethyl ester
A
mesytaldehyde
B
ethyl 4-chloronicotinate
Conditions | Yield |
---|---|
With (trichloromethyl)mesitylene In chloroform for 576h; Ambient temperature; | A n/a B 64% |
Conditions | Yield |
---|---|
With α,α,α,2,4,6-hexachlorotoluene In chloroform for 720h; Ambient temperature; | A 64% B 49% |
Conditions | Yield |
---|---|
With 3-Methylpyridine In chloroform for 720h; Ambient temperature; | A 64% B 49% |
Conditions | Yield |
---|---|
With 1,2,3,4-tetrahydroisoquinoline In acetonitrile at 20℃; Green chemistry; | 63% |
1,3-dichloro-2,4,6-trimethylbenzene
N,N-dimethyl-formamide
A
mesytaldehyde
B
2,4,6-trimethylisophthalic dialdehyde
Conditions | Yield |
---|---|
Stage #1: 1,3-dichloro-2,4,6-trimethylbenzene With naphthalene; lithium In diethyl ether at 20℃; for 4.55h; Stage #2: N,N-dimethyl-formamide In diethyl ether at 20℃; Cooling with ice; | A 12% B 61% |
Dichloromethyl methyl ether
dimesitylmethane
A
mesytaldehyde
B
2,4,6-trimethyl-3-(chloromethyl)benzaldehyde
C
3-chloromethyl-2,4,6-trimethylbenzylidene dichloride
D
dimesitylmethane-3,3'-dicarbaldehyde
Conditions | Yield |
---|---|
With aluminium trichloride In dichloromethane for 0.25h; Further byproducts given; | A 20 % Chromat. B 10 % Chromat. C 10 % Chromat. D 60% |
trifluoromethanesulphonyloxy-methylene-N,N-dimethyliminium trifluoromethanesulphonate
1,3,5-trimethyl-benzene
mesytaldehyde
Conditions | Yield |
---|---|
at 125℃; for 96h; | 60% |
Conditions | Yield |
---|---|
With rhodium(III) chloride trihydrate; hydrogen; triethylamine; triphenylphosphine In N,N-dimethyl acetamide at 90℃; under 7500.75 Torr; for 12h; Autoclave; | 60% |
Conditions | Yield |
---|---|
With aluminum (III) chloride In chlorobenzene at -12 - 18℃; for 22h; | 57% |
Conditions | Yield |
---|---|
With trifuran-2-yl-phosphane; palladium diacetate In tetrahydrofuran; toluene at 0℃; for 15h; Schlenk technique; | 57% |
2-(2,4,6-trimethylphenyl)-2-hydroxyacetonitrile
A
mesytaldehyde
B
mesitylenecarboxylic acid
Conditions | Yield |
---|---|
Stage #1: 2-hydroxy-2-(2,4,6-trimethylphenyl)acetonitrile With (η(6)-benzene)chloro[1,2-bis(diphenylphosphino)ethane]ruthenium(II) chloride In benzene at 120℃; for 24h; Inert atmosphere; Schlenk technique; Stage #2: With water In dichloromethane; ethyl acetate; benzene for 24h; | A 40% B 55% |
Conditions | Yield |
---|---|
With polymer(resin Amberlyst A-26)-supported tetracarbonylhydridoferrate anion In dichloromethane for 1h; Heating; | 53% |
With Pd-BaSO4; xylene Hydrogenation; | |
With hydrogen; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal In ethyl acetate at 25℃; under 760 Torr; for 2h; Yield given; | |
With triethylsilane; bis-triphenylphosphine-palladium(II) chloride; (Z)-N,N-diisopropyl-2-styrylbenzamide In tetrahydrofuran at 65℃; for 24h; Inert atmosphere; chemoselective reaction; |
Conditions | Yield |
---|---|
With V2O5/TiO2; dihydrogen peroxide In water; acetonitrile at 30℃; for 4h; Sealed tube; | 52% |
Conditions | Yield |
---|---|
In benzene for 10h; Heating; | 100% |
Conditions | Yield |
---|---|
With lithium tetrafluoroborate at 25℃; for 3h; | 100% |
With iodine In chloroform at 20℃; for 0.166667h; | 90% |
mesytaldehyde
acetylenemagnesium bromide
1-(2,4,6-trimethylphenyl)prop-2-yn-1-ol
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; for 2h; | 100% |
Conditions | Yield |
---|---|
In water at 20℃; Inert atmosphere; | 100% |
mesytaldehyde
1-propynylmagnesium bromide
chloromethyl methyl ether
Conditions | Yield |
---|---|
Stage #1: mesytaldehyde; 1-propynylmagnesium bromide In tetrahydrofuran at 0 - 20℃; for 1.5h; Schlenk technique; Inert atmosphere; Stage #2: chloromethyl methyl ether In tetrahydrofuran at 20℃; Schlenk technique; Inert atmosphere; | 100% |
mesytaldehyde
(1,3-dioxolan-2-yl-methyl)triphenylphosphonium bromide
Conditions | Yield |
---|---|
Stage #1: (1,3-dioxolan-2-yl-methyl)triphenylphosphonium bromide With sodium hydride In tetrahydrofuran; mineral oil at 0℃; for 1h; Inert atmosphere; Stage #2: mesytaldehyde In tetrahydrofuran; mineral oil at 20℃; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
With trimethylamine-N-oxide; sodium formate; C34H44FeN4O4(2+)*2I(1-) In water at 80℃; for 24h; Inert atmosphere; Schlenk technique; | 99% |
With sodium formate; N-tosylethylenediamine; bis[dichloro(pentamethylcyclopentadienyl)iridium(III)] at 80℃; for 0.7h; | 97% |
With formic acid; C20H29ClIrN4(1+)*Cl(1-) In water at 80℃; for 0.25h; chemoselective reaction; | 97% |
Conditions | Yield |
---|---|
With palladium on activated charcoal; hydrogen In methanol at 25℃; under 760.051 Torr; for 0.833333h; | 99% |
Clemensen redn.; | |
With [Ru(OH2)3(4'-phenyl-2,2':6',2''-terpy)](OTf)2; hydrogen In sulfolane; water at 175℃; under 56887.8 Torr; for 3h; | 8 %Chromat. |
Conditions | Yield |
---|---|
With C32H39Br2MgN2(1-)*C16H32LiO4(1+) In chloroform-d1 at 20℃; for 0.5h; Inert atmosphere; Glovebox; | 99% |
With [[{(2,6-iPr2C6H3N)P(Ph2)}2N]AlMe]+[MeB(C6F5)3]- In neat (no solvent) at 25 - 28℃; for 0.0833333h; chemoselective reaction; | 98% |
With C29H38AlN4O2(1+)*CF3O3S(1-) at 20℃; for 0.333333h; Catalytic behavior; Inert atmosphere; Schlenk technique; | 95% |
Conditions | Yield |
---|---|
With C4H11FeMo6NO24(3-)*3C16H36N(1+); water; oxygen; sodium carbonate at 50℃; under 760.051 Torr; for 8h; Green chemistry; | 99% |
With 4H3N*4H(1+)*CuMo6O18(OH)6(4-); water; oxygen; sodium carbonate at 50℃; under 760.051 Torr; for 12h; | 99% |
With tris[2-(4,6-difluorophenyl)pyridinato-C2,N]-iridium(III); oxygen In acetonitrile at 20℃; Irradiation; Sealed tube; Green chemistry; chemoselective reaction; | 90% |
mesytaldehyde
α-fluoro-α-(phenylselanyl)acetic acid ethyl ester
Conditions | Yield |
---|---|
With 2,2,6,6-tetramethylpiperidinyl-lithium; methanesulfonyl chloride In tetrahydrofuran at -78℃; | 99% |
mesytaldehyde
(trifluoromethyl)trimethylsilane
Conditions | Yield |
---|---|
With dmap; tetrabutylammonium tricarbonylnitrosylferrate In tetrahydrofuran at 30℃; for 14h; Schlenk technique; Inert atmosphere; Sealed tube; | 99% |
With 4 A molecular sieve In dimethyl sulfoxide at 20℃; for 0.25h; | 100 % Spectr. |
With cesium fluoride In tetrahydrofuran at 20℃; for 1h; Inert atmosphere; |
Conditions | Yield |
---|---|
With camphor-10-sulfonic acid In methanol at 23℃; for 12h; | 99% |
With CSA In methanol at 20℃; for 12h; Inert atmosphere; | 92% |
Conditions | Yield |
---|---|
Stage #1: methyl 1-(1-ethynyl)-2-naphthoate With n-butyllithium Stage #2: mesytaldehyde Further stages.; | 99% |
Conditions | Yield |
---|---|
With zinc In dimethyl sulfoxide for 2h; Barbier Coupling Reaction; Milling; | 99% |
With water; tin(ll) chloride at 20℃; for 2h; | 97% |
With ammonium chloride; zinc In tetrahydrofuran at 20℃; for 1h; | 92% |
Stage #1: allyl bromide With magnesium In tetrahydrofuran for 8h; Sealed tube; Inert atmosphere; Stage #2: mesytaldehyde In tetrahydrofuran Sealed tube; Inert atmosphere; |
mesytaldehyde
(R,R)-1,2-diphenylethylenediamine
(1R,2R)-1,2-diphenyl-N1-(2,4,6-trimethylbenzylidene)ethane-1,2-diamine
Conditions | Yield |
---|---|
In water at 20℃; for 16h; | 99% |
mesytaldehyde
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane
4,4,5,5-tetramethyl-2-((2,4,6-trimethylbenzyl)oxy)-1,3,2-dioxaborolane
Conditions | Yield |
---|---|
With C45H69NdO3*2C4H8O In tetrahydrofuran at 20℃; for 0.166667h; Inert atmosphere; | 99% |
With [Ag((cyclohexyl)3P)(HMDS)] In benzene-d6 at 20℃; for 8h; Inert atmosphere; | 97% |
With C19H25AsN2O In benzene-d6 at 20℃; for 0.5h; Inert atmosphere; Glovebox; Schlenk technique; | 90% |
Conditions | Yield |
---|---|
With titanium(IV) tetrabutoxide; triethylsilyl chloride In dichloromethane at 20℃; | A n/a B 99% |
Conditions | Yield |
---|---|
With carbon dioxide In ethanol at 20℃; under 760.051 Torr; for 18h; Sealed tube; | 99% |
With sodium hydrogensulfite In water; ethyl acetate at 40℃; for 20h; Inert atmosphere; Schlenk technique; Sealed tube; |
mesytaldehyde
Conditions | Yield |
---|---|
In ethanol for 2h; Reflux; | 99% |
mesytaldehyde
N-methylhydroxyamine hydrochloride
C-mesityl-N-methylnitrone
Conditions | Yield |
---|---|
With triethylamine In chloroform for 22h; | 98% |
Conditions | Yield |
---|---|
Stage #1: 1-ethynylnaphthalene With n-butyllithium Stage #2: mesytaldehyde Further stages.; | 98% |
mesytaldehyde
Chloroiodomethane
2-chloro-1-(2,4,6-trimethylphenyl)ethanol
Conditions | Yield |
---|---|
With methyllithium In tetrahydrofuran at -40℃; Flow reactor; | 98% |
Stage #1: Chloroiodomethane With TurboGrignard In tetrahydrofuran at -20℃; for 0.000277778h; Flow reactor; Stage #2: mesytaldehyde In tetrahydrofuran at -20℃; for 0.000444444h; Flow reactor; | 95% |
Conditions | Yield |
---|---|
With cerium(III) chloride heptahydrate In ethanol at 20℃; for 0.0166667h; Green chemistry; diastereoselective reaction; | 98% |
With water; acetic acid In neat (no solvent) at 20℃; for 0.0833333h; Green chemistry; stereoselective reaction; | 94% |
mesytaldehyde
Diphenylphosphine oxide
(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
Conditions | Yield |
---|---|
Stage #1: mesytaldehyde; Diphenylphosphine oxide In dichloromethane for 6h; Green chemistry; Stage #2: With ammonium metavanadate; dihydrogen peroxide at 8 - 20℃; for 5.5h; Reagent/catalyst; Green chemistry; | 98% |
mesytaldehyde
C6H5NHBO2C2(CH3)4
N-(2,4,6-trimethylbenzylidene)aniline
Conditions | Yield |
---|---|
In benzene-d6 at 25℃; for 1h; Inert atmosphere; Schlenk technique; | 98% |
mesytaldehyde
acetophenone
(E)-1-phenyl-3-[(2,4,6-trimethylphenyl)]prop-2-en-1-one
Conditions | Yield |
---|---|
Stage #1: mesytaldehyde; acetophenone With potassium hydroxide In ethanol; water at 20℃; for 12h; Claisen Schmidt condensation; Stage #2: With hydrogenchloride In ethanol; water pH=3 - 4; | 97% |
With sodium hydroxide In ethanol; water at 20℃; for 0.0833333h; | 72% |
With sodium hydroxide at 0℃; | |
Stage #1: acetophenone With sodium hydroxide In ethanol; water at 0 - 20℃; for 1.33333h; Stage #2: mesytaldehyde In ethanol; water at 20℃; |
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