CHANGZHOU HANGYU PHARMACEUTICAL TECHNOLOGY CO., LTD. founded in 1984, engages in pharmaceutical research, development, production, process design and technical consultation of synthetic and fermentation pharmaceutical products. The organizational s
Cas:1585-16-6
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inquiryDayangChem exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product s
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inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
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inquiryProduct Name: alpha-2-Chloroisodurene Synonyms: 4,6-trimethylbenzyl chloride;Mesitylmethyl chloride;1-(Chloromethyl)-2,4,6-trimethylbenzene;2-(Chloromethyl)mesitylene;alpha-2-Chloroisodurene,98%;2,4,6-Trime
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryalpha-2-Chloroisodurene CAS 1585-16-6 Purity: 99% Min Application: Intermediates Appearance: Powder Package: Bag Delivery: 3-5days Our Advantage & Service 1.Top quality: Using high quality material and establishing a strict quality c
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The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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inquiryWhy Choose Us: 1. Factory direct sales, so we can provide the competitive price and high quality product base on 8 years of production and R&D experience. 2. It is available in stock for quick shipment.Products could be packaged according to cu
We are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov
Cas:1585-16-6
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inquiryProduct Name: alpha-2-Chloroisodurene Synonyms: 4,6-trimethylbenzyl chloride;Mesitylmethyl chloride;1-(Chloromethyl)-2,4,6-trimethylbenzene;2-(Chloromethyl)mesitylene;alpha-2-Chloroisodurene,98%;2,4,6-Trimethylbenzyl chloride;2,4,6-Trimethyl he
Cas:1585-16-6
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inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
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inquiryZhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed
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inquiryWe product this chemical more than 10 years . We are very experience to export it to many countries, Our superior & stable quality , competitive price gain warm reception from our customers. Product Name:alpha-2-Chloroisodurene CAS No:1585-16
Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
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inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
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Triumph has the complete production of G- KG - MT service chain,we can make the new technology into productivity quickly in the research and development of new products. Main Business Custom Synthesis:
High quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use
Superior quality, moderate price & quick delivery. Appearance:white crystalline powder Storage:stored in a cool, dry and ventilated place to provent sun and rain Package:25kg/drum, or as per your request. Application:Used as Pharmaceutical
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inquiryWe are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp
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inquiry1, High quality with competitive price:2, Fast and safe delivery3.Excellent pre-sales and after-sales service4. Well-trained and professional technologist and sales with rich experience in the field for 5-10 yearsAppearance:see detailed specification
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inquiryLower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
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inquiryConditions | Yield |
---|---|
With thionyl chloride In dichloromethane at 0 - 20℃; for 1h; | 100% |
With oxalyl dichloride In dichloromethane at 20℃; Appel Halogenation; Reflux; | 98% |
With tetrachloromethane; ring-opening metathesis polymer-supported triphenylphosphine In dichloromethane at 45℃; for 6h; | 89% |
formaldehyd
1,3,5-trimethyl-benzene
2-chloromethyl-1,3,5-trimethylbenzene
Conditions | Yield |
---|---|
With hydrogenchloride In water at 65 - 75℃; | 90% |
With hydrogenchloride; acetic acid In water at 37℃; for 1.5h; | 68% |
With hydrogenchloride In water at 60 - 70℃; for 7h; | 36% |
2,4,6-trimethylbenzyl alcohol
benzoyl chloride
B
2-chloromethyl-1,3,5-trimethylbenzene
Conditions | Yield |
---|---|
With 1-methylsulfinyl-2-methoxybenzene In acetonitrile at 20℃; for 14h; Sealed tube; | A n/a B 74% |
chloromethyl isocyanate
1,3,5-trimethyl-benzene
A
2-chloromethyl-1,3,5-trimethylbenzene
B
2-Isocyanatomethyl-1,3,5-trimethyl-benzene
Conditions | Yield |
---|---|
With iron(III) chloride 1.) 40 - 60 deg C, 2.) 100 - 150 deg C, 2 h; | A 15% B 32% |
chloromethyl methyl ether
acetic acid
1,3,5-trimethyl-benzene
2-chloromethyl-1,3,5-trimethylbenzene
Conditions | Yield |
---|---|
at 65℃; ohne Katalysator; Geschwindigkeit dieser Reaktion und der analogen Reaktionen mit anderen aromatischen Kohlenwasserstoffen bei 65grad und 100grad; |
chloromethyl methyl ether
acetic acid
1,3,5-trimethyl-benzene
A
2,4-bis(chloromethyl)mesitylene
B
2-chloromethyl-1,3,5-trimethylbenzene
Conditions | Yield |
---|---|
at 80℃; |
chloromethyl methyl ether
1,3,5-trimethyl-benzene
2-chloromethyl-1,3,5-trimethylbenzene
Conditions | Yield |
---|---|
With acetic acid at 65 - 80℃; |
chloromethyl methyl ether
1,3,5-trimethyl-benzene
A
2,4-bis(chloromethyl)mesitylene
B
2-chloromethyl-1,3,5-trimethylbenzene
ethyl chloromethyl ether
1,3,5-trimethyl-benzene
2-chloromethyl-1,3,5-trimethylbenzene
Conditions | Yield |
---|---|
With carbon disulfide; tin(IV) chloride | |
With tetrachloromethane; tin(IV) chloride at -5℃; | |
With acetic acid |
formaldehyd
1,3,5-trimethyl-benzene
A
2,4-bis(chloromethyl)mesitylene
B
2-chloromethyl-1,3,5-trimethylbenzene
Conditions | Yield |
---|---|
With hydrogenchloride at 65℃; Einleiten von HCl; |
hydrogenchloride
formaldehyd
1,3,5-trimethyl-benzene
A
2,4-bis(chloromethyl)mesitylene
B
2-chloromethyl-1,3,5-trimethylbenzene
Conditions | Yield |
---|---|
at 65℃; Einleiten von HCl; |
hydrogenchloride
2,4,6-trimethylbenzyl acetate
A
methyl-(2,4,6-trimethyl-benzyl)-ether
B
2-chloromethyl-1,3,5-trimethylbenzene
hydrogenchloride
formaldehyd
1,3,5-trimethyl-benzene
A
dimesitylmethane
B
2-chloromethyl-1,3,5-trimethylbenzene
formaldehyd
1,3,5-trimethyl-benzene
A
2,4,6-tris(chloromethyl)-mesitylene
B
2,4-bis(chloromethyl)mesitylene
C
2-chloromethyl-1,3,5-trimethylbenzene
Conditions | Yield |
---|---|
With hydrogenchloride for 2h; Heating; Title compound not separated from byproducts.; |
Conditions | Yield |
---|---|
With hydrogenchloride; formaldehyd for 2h; Heating; |
Conditions | Yield |
---|---|
With tetrachlorosilane; NbCl3(N,N′-bis-(2,6-diisopropylphenyl)-1,4-diaza-2,3-dimethyl-1,3-butadiene) In chloroform-d1 at 80℃; for 24h; | 95 %Spectr. |
sodium cyanide
2-chloromethyl-1,3,5-trimethylbenzene
mesitylacetonitrile
Conditions | Yield |
---|---|
In dimethyl sulfoxide at 80℃; for 0.5h; Substitution; | 100% |
Stage #1: sodium cyanide In ethanol; water Heating / reflux; Stage #2: 2-chloromethyl-1,3,5-trimethylbenzene In ethanol; water for 3h; Heating / reflux; | 72% |
In ethanol |
2-chloromethyl-1,3,5-trimethylbenzene
dimethyl amine
2,4,6-trimethyl-<(dimethylamino)methyl>benzene
Conditions | Yield |
---|---|
In tetrahydrofuran; water at 0 - 20℃; for 3.5h; Substitution; | 100% |
In tetrahydrofuran at 20℃; for 48h; Inert atmosphere; | 94% |
In tetrahydrofuran Ambient temperature; | 92% |
2'-O-acetyl-3-O-descladinosyl-3-O-allyl-6-O-methylerythromycin A 9-(E)-O-acetyloxime 11,12-cyclic carbonate
2-chloromethyl-1,3,5-trimethylbenzene
C46H72N2O12
Conditions | Yield |
---|---|
Stage #1: 2'-O-acetyl-3-O-descladinosyl-3-O-allyl-6-O-methylerythromycin A 9-(E)-O-acetyloxime 11,12-cyclic carbonate With potassium tert-butylate In N,N-dimethyl-formamide at 20℃; for 0.25h; Stage #2: 2-chloromethyl-1,3,5-trimethylbenzene With potassium tert-butylate In N,N-dimethyl-formamide at 20℃; for 1h; | 100% |
2-chloromethyl-1,3,5-trimethylbenzene
(2S,3S)-1,4-bis(allyloxy)-2,3-dihydroxybutane
(2S,3S)-2,3-bis(2,4,6-trimethyl-phenylmethoxy)-1,4-bis(allyloxy)butane
Conditions | Yield |
---|---|
Stage #1: (2S,3S)-1,4-bis(allyloxy)-2,3-dihydroxybutane With sodium hydride In N,N-dimethyl-formamide at 20℃; for 0.333333h; Stage #2: 2-chloromethyl-1,3,5-trimethylbenzene In N,N-dimethyl-formamide at 50℃; for 7h; | 99% |
2-chloromethyl-1,3,5-trimethylbenzene
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 50 - 60℃; | 99% |
2-chloromethyl-1,3,5-trimethylbenzene
Conditions | Yield |
---|---|
In tetrahydrofuran addn. of 111 μmol of the benzylchloride to a soln. of 111 μmol of the bis(imido) compound in 7 ml THF at -40°C and evaporation;; extraction with pentane, filtration and concentration; coupling product present as an impurity; detn. by (1)H-NMR- and (13)C-NMR spectroscopy;; | 99% |
Conditions | Yield |
---|---|
With triethylamine for 1h; Heating; Inert atmosphere; Ionic liquid; | 99% |
sodium cyanide
2-chloromethyl-1,3,5-trimethylbenzene
mesitylacetonitrile
Conditions | Yield |
---|---|
With trimethyldodecylammonium chloride In toluene at 68 - 72℃; for 6h; Reagent/catalyst; Temperature; | 98.8% |
Conditions | Yield |
---|---|
With iron(III) sulfate; water In toluene at 110℃; for 0.7h; Ionic liquid; | 98% |
With potassium carbonate; acetone | |
Multi-step reaction with 2 steps 1: silver acetate; glacial acetic acid 2: aqueous KOH View Scheme |
1,4-dichloro-5-hydroxy-9,10-anthracenedione
2-chloromethyl-1,3,5-trimethylbenzene
1,4-dichloro-5-<(2,4,6-trimethylphenyl)methoxy>-9,10-anthracenedione
Conditions | Yield |
---|---|
With caesium carbonate | 98% |
With caesium carbonate In N,N-dimethyl-formamide; acetone for 23h; Heating; | 78% |
With caesium carbonate In N,N-dimethyl-formamide; acetone |
2-chloromethyl-1,3,5-trimethylbenzene
triphenylphosphine
Triphenyl<(2,4,6-trimethylphenyl)methyl>phosphoniumchlorid
Conditions | Yield |
---|---|
In benzene for 120h; Ambient temperature; | 98% |
In toluene for 12h; Heating; | 95% |
In benzene at 70℃; for 48h; | 80% |
2-chloromethyl-1,3,5-trimethylbenzene
Re{NC6H3(CH(CH3)2)2}3(CH2C6H2(CH3)3)
Conditions | Yield |
---|---|
In tetrahydrofuran addn. of 0.06 mmol of the benzyl compound (in 2 ml THF) to a soln. of 0.06 mmol of the tris(imido) compound in 8 ml THF and evaporation after 20 minutes;; extraction with pentane and cooling to -40°C; small amounts of the dibenzyl coupling product; detn. by (1)H-NMR- and (13)C-NMR spectroscopy;; | 98% |
2-chloromethyl-1,3,5-trimethylbenzene
Conditions | Yield |
---|---|
In tetrahydrofuran addn. of 116 μmol of 2,4,6-trimethylbenzylchloride to a soln. of 116 μmol of the Na(THF)2 salt in 10 ml THF at -40°C and evaporation;; extraction with pentane, filtration, evaporation, solvation in pentane and concentration; contamination with the dibenzyl coupling product; detn. by (1)H-NMR- and (13)C-NMR spectroscopy;; | 98% |
Conditions | Yield |
---|---|
With 1-dodecyl-3-methylimidazolium iron chloride; periodic acid at 30℃; for 1.5h; | 98% |
With 4Na(1+)*6H(1+)*NiMo6O24(10-)=Na4H6NiMo6O24; oxygen In water; acetonitrile at 20℃; under 760.051 Torr; for 12h; Irradiation; | 91% |
With sodium nitrate; acetic acid In water for 8h; Reflux; | 83% |
With potassium hydroxide; cetyltrimethylammonim bromide; potassium nitrate In water for 7.5h; pH=10 - 11; Reflux; | 82% |
With (NH4)4[ZnMo6O18(OH)6]; oxygen In water; acetonitrile at 60℃; under 760.051 Torr; for 12h; | 81% |
(S)-4-benzyl-1-(2,6-diisopropylphenyl)-4,5-dihydro-1H-imidazole
2-chloromethyl-1,3,5-trimethylbenzene
(S)-4-benzyl-1-(2,6-diisopropylphenyl)-3-(2,4,6-trimethylbenzyl)-4,5-dihydro-1H-imidazol-3-ium chloride
Conditions | Yield |
---|---|
In toluene at 100℃; for 1h; | 98% |
In acetonitrile at 110℃; for 5h; | 85% |
2-chloromethyl-1,3,5-trimethylbenzene
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 80℃; for 16h; Schlenk technique; | 98% |
Conditions | Yield |
---|---|
With Ni(1,3-bis(2,6-bis(diphenylmethyl)-4-methylphenyl)imidazol-2-ylidene)(PPh3)Br2; magnesium In tetrahydrofuran at 0 - 60℃; for 24.5h; Glovebox; Inert atmosphere; Schlenk technique; | 98% |
Dichloromethyl methyl ether
2-chloromethyl-1,3,5-trimethylbenzene
2,4,6-trimethyl-3-(chloromethyl)benzaldehyde
Conditions | Yield |
---|---|
Stage #1: Dichloromethyl methyl ether; 2-chloromethyl-1,3,5-trimethylbenzene With titanium tetrachloride In dichloromethane at 17 - 20℃; for 0.333333h; Inert atmosphere; Stage #2: With water In dichloromethane for 0.25h; Inert atmosphere; | 97% |
With titanium tetrachloride In dichloromethane at 20℃; for 0.5h; | 84% |
With titanium tetrachloride In dichloromethane at 20℃; for 0.25h; | 64% |
2-chloromethyl-1,3,5-trimethylbenzene
thiophenol
2,4,6-trimethylbenzyl phenyl sulfide
Conditions | Yield |
---|---|
With tetra(n-butyl)ammonium hydroxide In chloroform; water for 16h; Ambient temperature; | 97% |
1-Methylbenzimidazole
2-chloromethyl-1,3,5-trimethylbenzene
1-methyl-3-(2,4,6-trimethylbenzyl)benzimidazolium chloride
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 95℃; for 4h; Inert atmosphere; Schlenk technique; | 97% |
In N,N-dimethyl-formamide at 80℃; Inert atmosphere; Schlenk technique; |
2-chloromethyl-1,3,5-trimethylbenzene
1-(2,4,6-trimethylbenzyl)-4,5-dihydroimidazole
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 25℃; for 6h; | 96% |
2-chloromethyl-1,3,5-trimethylbenzene
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 70℃; Schlenk technique; | 96% |
2-chloromethyl-1,3,5-trimethylbenzene
2-(fluoromethyl)-1,3,5-trimethylbenzene
Conditions | Yield |
---|---|
With tetrabutyl ammonium fluoride In acetonitrile for 2h; Reflux; | 95% |
With potassium fluoride; 18-crown-6 ether In acetonitrile at 80℃; for 90h; |
4-Benzyloxyphenol
2-chloromethyl-1,3,5-trimethylbenzene
1-benzyloxy-4-(2,4,6-trimethylbenzyloxy)benzene
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide at 20℃; | 95% |
4-cyclohexyl-2-mercapto-6-oxo-1,6-dihydro-pyrimidine-5-carbonitrile
2-chloromethyl-1,3,5-trimethylbenzene
4-cyclohexyl-6-oxo-2-(2,4,6-trimethyl-benzylsulfanyl)-1,6-dihydro-pyrimidine-5-carbonitrile
Conditions | Yield |
---|---|
With potassium carbonate In acetone at 0 - 20℃; for 36h; | 95% |
piperazine
2-chloromethyl-1,3,5-trimethylbenzene
1-(2,4,6-trimethylbenzyl)-piperazine
Conditions | Yield |
---|---|
In tetrahydrofuran for 4h; Reflux; | 94.3% |
In tetrahydrofuran for 4h; Reflux; Inert atmosphere; | 49% |
2-chloromethyl-1,3,5-trimethylbenzene
benzonitrile
N-(2,4,6-trimethylbenzyl)benzamide
Conditions | Yield |
---|---|
With iron(III) chloride for 8h; Ritter reaction; Heating; | 94% |
2-chloromethyl-1,3,5-trimethylbenzene
N-(isobutyl)benzimidazole
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide at 80℃; for 24h; Inert atmosphere; Schlenk technique; | 94% |
In N,N-dimethyl-formamide at 80℃; for 24h; Inert atmosphere; Schlenk technique; | 94% |
In N,N-dimethyl-formamide at 80℃; for 24h; Inert atmosphere; Schlenk technique; | 94% |
In N,N-dimethyl-formamide at 80℃; for 24h; | 94% |
Conditions | Yield |
---|---|
Stage #1: 5,6-dimethyl-1H-benzo[d]imida-zole With potassium hydroxide In ethanol at 20℃; for 0.25h; Stage #2: 2-chloromethyl-1,3,5-trimethylbenzene In ethanol at 20℃; for 17h; Reflux; | 94% |
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