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Hangzhou Sartort Biopharma Co., Ltd

Appearance:Yellow crystal powder Storage:Room temperature Package:25kg/drum Application:UV Photoinitiator Transportation:Express/Sea/Air Port:Any port in China

UV Photoinitiator TPO Omnirad TPO Irgacure TPO CAS No 75980-60-8

Cas:75980-60-8

Min.Order:25 Kilogram

FOB Price: $45.0 / 55.0

Type:Lab/Research institutions

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Luyunjia Chemistry Xiamen Limited

Specifications CAS No.: 75980-60-8 Other Names: TPO MF: C22H21O2P EINECS No.: 278-355-8 Place of Origin: Shandong, China (Mainland) Type: Pharmaceutical Intermediates Purity: 99%min Brand Name: Luyunjia Model Number: luxin-1492 App

lower price TPO 75980-60-8 Diphenyl(2,4,6-trimethylbenzoyl)phosphine oxide

Cas:75980-60-8

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Wuhan Kemi-Works Chemical Co., Ltd

Advantages: 1. Its photocuringspeed is fast 2. Have light-decolourizatio 3. Can be used for thick coating curing 4. Belongs to low-volatilitymild-smell and environment friendlyproduct 5. Anti-yellowing Appearance:yellowish powder

Photoinitiator-TPO

Cas:75980-60-8

Min.Order:1 Kilogram

Negotiable

Type:Other

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King Brother Chem Co., Ltd

Chemacure PI-TPO is a photoinitiator for curing styrene-based unsaturated polyesters and acrylic resins. Thanks to Chemacure PI- TPO’s absorption in the long-wave region of the UV spectrum (see plot opposite), even white paints and surfaces

Diphenyl(2,4,6-trimethylbenzoyl)phosphine oxide(75980–60–8)

Cas:75980-60-8

Min.Order:1 Metric Ton

FOB Price: $45.0

Type:Trading Company

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Baoji Guokang Healthchem co.,ltd

Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At present

diphenyl(2,4,6-trimethylbenzoyl)phosphine oxide CAS:75980-60-8

Cas:75980-60-8

Min.Order:1 Kilogram

FOB Price: $76.0 / 80.0

Type:Trading Company

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Guangdong Juda Chemical Industrial Co.,Limited

We provide tailor-made photoinitiator solutions for different performances by custom synthesisi.blends or other technical supports low-odor uv formulations low odor, low yellowing, through-curing non-yellowing uv formulations benzene-free u

TPO CAS NO.75980-60-8 Factory Low Price High Quality

Cas:75980-60-8

Min.Order:100 Kilogram

Negotiable

Type:Trading Company

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Tianjin Huiren Chemtech Co., Ltd

Photoinitiators HRcure-TPO CAS NO.: 75980-60-8 Throw curing, LED curing, low-yellowing UV absorption peak: 275nm, 379nm Tianjin Huiren chemtech Co. , Ltd. , established in January 2016, is a national high-tech enterprise t

Photoinitiators HRcure-TPO

Cas:75980-60-8

Min.Order:1 Kilogram

FOB Price: $0.1 / 2.0

Type:Lab/Research institutions

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Hunan Russell Chemicals Technology Co.,Ltd

we provide tailor-made photoinitiator solutions for different performances by custom synthesisi.blends or other technical supports low-odor UV formulations Non-yellowing UV formulations Benzene-Free UV formulations Polymeric UV formulations

factory low price high quality TPO

Cas:75980-60-8

Min.Order:100 Kilogram

Negotiable

Type:Trading Company

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Dayang Chem (Hangzhou) Co.,Ltd.

As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch

Diphenyl(2,4,6-trimethylbenzoyl)phosphine oxide

Cas:75980-60-8

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

inquiry

Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality 2,4,6-Trimethylbenzoyldiphenylphosphine Oxide supplier in China

Cas:75980-60-8

Min.Order:1 Metric Ton

Negotiable

Type:Manufacturers

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Hangzhou Dingyan Chem Co., Ltd

Test Item Requirement Test Result Appearance Yellow crystal Pass Assay ≥99.0%

High quality Diphenyl(2,4,6-trimethylbenzoyl)phosphine oxide with best price cas:75980-60-8

Cas:75980-60-8

Min.Order:1 Kilogram

FOB Price: $250.0 / 350.0

Type:Manufacturers

inquiry

Hebei yanxi chemical co.,LTD.

hebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developm

Diphenyl(2,4,6-trimethylbenzoyl)phosphine oxide CAS NO.75980-60-8

Cas:75980-60-8

Min.Order:1 Metric Ton

FOB Price: $1.0 / 3.0

Type:Manufacturers

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Wuhan Fortuna Chemical Co.,Ltd

Unique advantages Guaranteed the purity High quality & competitive price Quality control Fast feedback Prompt shipment Appearance:Yellow crystal Storage:Cool dry place Package:20kg/carton Application:Photoinitiator Transportation:By

High quality Diphenyl(2,4,6-trimethylbenzoyl)phosphine oxide Cas 75980-60-8 with best price

Cas:75980-60-8

Min.Order:20 Kilogram

FOB Price: $50.0 / 53.0

Type:Trading Company

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply Diphenyl(2,4,6-trimethylbenzoyl)phosphine oxide

Cas:75980-60-8

Min.Order:1

Negotiable

Type:Other

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Jinan Finer Chemical Co., Ltd

Product description: Product name Photoinitiator TPO CAS number 75980-60-8 Assay >99% Appearance Yellowish crystalline powder Capacity 200mt/year Application Screen printing ink

Photoinitiator TPO

Cas:75980-60-8

Min.Order:10 Gram

FOB Price: $12.0

Type:Lab/Research institutions

inquiry

Xi'an Xszo Chem Co., Ltd.

1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s

Factory price Cosmetic TRIMETHYLBENZOYL DIPHENYLPHOSPHINE OXIDE 75980-60-8 Manufacturer

Cas:75980-60-8

Min.Order:1 Gram

FOB Price: $0.1

Type:Manufacturers

inquiry

Chemwill Asia Co., Ltd.

Photoinitiator-TPO CAS 75980-60-8 In stock

Cas:75980-60-8

Min.Order:1 Metric Ton

FOB Price: $1.0

Type:Manufacturers

inquiry

Henan Tianfu Chemical Co., Ltd.

TIANFUCHEM-- 75980-60-8--High purity Diphenyl(2,4,6-trimethylbenzoyl)phosphine oxide in stock Our company was built in 2009 with an ISO certificate.In the past 10 years, we have grown up as a famous fine chemicals supplier in China And we

TIANFUCHEM-- 75980-60-8--High purity Diphenyl(2,4,6-trimethylbenzoyl)phosphine oxide in stock

Cas:75980-60-8

Min.Order:1 Metric Ton

FOB Price: $2000.0

Type:Lab/Research institutions

inquiry

Hebei Nengqian Chemical Import and Export Co., LTD

Our advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva

Diphenyl(2,4,6-trimethylbenzoyl)phosphine oxide

Cas:75980-60-8

Min.Order:1 Kilogram

FOB Price: $9.0 / 99.0

Type:Trading Company

inquiry

Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Manufacturer supply CAS 75980-60-8 with best quality

Cas:75980-60-8

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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Wuhan Han Sheng New Material Technology Co.,Ltd

Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We

Photoinitiator TPO,cas:75980-60-8 fandachem

Cas:75980-60-8

Min.Order:10 Kilogram

Negotiable

Type:Trading Company

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Henan Sinotech Import&Export Corporation

Product Name 2,4,6-trimethylbenzoyldiphenyl phosphine oxide CAS No. 75980-60-8 Molecular Formula

2,4,6-trimethylbenzoyldiphenyl phosphine oxide

Cas:75980-60-8

Min.Order:5 Metric Ton

FOB Price: $1.0 / 2.0

Type:Other

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Hubei Langyou International Trading Co., Ltd

Advantages: Hubei XinRunde Chemical Co., Ltd is a renowned pharmaceutical manufacturer. We can offer high quality products at competitive price in quick delivery with 100% custom pass guaranteed. Never stop striving to offer our best service is our

UV Photoinitiator Tpo 99% CAS No. 75980-60-8

Cas:75980-60-8

Min.Order:10 Gram

Negotiable

Type:Other

inquiry

Shanghai Upbio Tech Co.,Ltd

1.In No Less 8years exporting experience. forclients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specia

Top Supplier Photoinitiator-TPO CAS NO.75980-60-8

Cas:75980-60-8

Min.Order:25 Kilogram

FOB Price: $1.0

Type:Lab/Research institutions

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Xi'an Faithful Biotech Co., Ltd.

We are the manufacturers and suppliers of API in China, and warehouse in Germany and USA of California, which can quickly and safely deliver to your address 1.High quality and competitive price. 2.Free sample for your evaluation. 3.Promptly delivery

Qingdao Beluga Import and Export Co., LTD

Beluga chemical professional supply Diphenyl(2,4,6-trimethylbenzoyl)phosphine oxide CAS75980-60-8 Why choose Beluga chemical 1. Beluga Chemical has a professional RESEARCH and development team and strong technical force to ensure technical supp

Diphenyl(2,4,6-trimethylbenzoyl)phosphine oxide CAS75980-60-8

Cas:75980-60-8

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Shanghai Terui OP New Material Technology Co., Ltd.

We have overseas warehouses in California, New Laredo Mexico, Vancouver Canada, Amsterdam Netherlands, and Melbourne Australia. Overseas warehouses can provide some of the best-selling products. We look forward to the cooperation of local powerful

CAS 75980-60-8 Diphenyl(2,4,6-trimethylbenzoyl)phosphine oxide

Cas:75980-60-8

Min.Order:0 Metric Ton

Negotiable

Type:Trading Company

inquiry

Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

Diphenyl(2,4,6-trimethylbenzoyl)phosphine oxide

Cas:75980-60-8

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Changchun Artel lmport and Export trade company

Product Detail Minimum Order Qty. 10 Gram Supply Ability 500 Kilograms/Month Storage store in cool, dry, ventilated place 20℃ Delivery Time 3 business days after payment Payment Term TT,western union,Paypal,

Photoinitiator TPOCAS NO.: 75980-60-8

Cas:75980-60-8

Min.Order:20 Metric Ton

Negotiable

Type:Trading Company

inquiry

Hubei Jiutian Bio-medical Technology Co., Ltd

1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highly qualifie

CAS 75980-60-8 CAS 75980-60-8 Diphenyl(2,4,6-trimethylbenzoyl)phosphine oxide

Cas:75980-60-8

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Synthetic route

α-hydroxy-(2,4,6-trimethylbenzyl)diphenyl phosphine oxide

α-hydroxy-(2,4,6-trimethylbenzyl)diphenyl phosphine oxide

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

Conditions
ConditionsYield
With manganese(IV) oxide In dichloromethane at 20℃;98%
With vanadium(V) oxide; dihydrogen peroxide at 8 - 25℃; for 3.5h; Reagent/catalyst; Green chemistry;96%
With tert.-butylhydroperoxide In dichloromethane at 5 - 20℃; for 6.5h; Reagent/catalyst;92.5%
mesytaldehyde
487-68-3

mesytaldehyde

Diphenylphosphine oxide
4559-70-0

Diphenylphosphine oxide

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

Conditions
ConditionsYield
Stage #1: mesytaldehyde; Diphenylphosphine oxide In dichloromethane for 6h; Green chemistry;
Stage #2: With ammonium metavanadate; dihydrogen peroxide at 8 - 20℃; for 5.5h; Reagent/catalyst; Green chemistry;
98%
diphenyl n-pentyloxyphosphine
39150-04-4

diphenyl n-pentyloxyphosphine

mesitylene-2-carboxylic acid chloride
938-18-1

mesitylene-2-carboxylic acid chloride

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

Conditions
ConditionsYield
at 50 - 90℃; for 9.33333h;95.8%
(sec-butyloxy)di(phenyl)phosphine
65119-90-6

(sec-butyloxy)di(phenyl)phosphine

mesitylene-2-carboxylic acid chloride
938-18-1

mesitylene-2-carboxylic acid chloride

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

Conditions
ConditionsYield
at 50 - 90℃; for 7.33333h;95.6%
Ethyl diphenylphosphinite
719-80-2

Ethyl diphenylphosphinite

mesitylene-2-carboxylic acid chloride
938-18-1

mesitylene-2-carboxylic acid chloride

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

Conditions
ConditionsYield
at 40 - 90℃; for 8h; Time; Green chemistry;95.1%
With N,N-dimethyl-cyclohexanamine at 80 - 85℃; Product distribution / selectivity;
diphenyl n-propoxyphosphine
92556-46-2

diphenyl n-propoxyphosphine

mesitylene-2-carboxylic acid chloride
938-18-1

mesitylene-2-carboxylic acid chloride

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

Conditions
ConditionsYield
at 50 - 90℃; for 7.33333h;95.1%
diphenyl sec-pentyloxyphosphine
38011-61-9

diphenyl sec-pentyloxyphosphine

mesitylene-2-carboxylic acid chloride
938-18-1

mesitylene-2-carboxylic acid chloride

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

Conditions
ConditionsYield
at 50 - 90℃; for 7.33333h;94.9%
(n-butyloxy)di(phenyl)phosphine
13360-94-6

(n-butyloxy)di(phenyl)phosphine

mesitylene-2-carboxylic acid chloride
938-18-1

mesitylene-2-carboxylic acid chloride

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

Conditions
ConditionsYield
at 50 - 90℃; for 9.33333h;94.8%
(2,4,6-trimethylbenzyl)diphenylphosphine oxide
149731-53-3

(2,4,6-trimethylbenzyl)diphenylphosphine oxide

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

Conditions
ConditionsYield
With tert.-butylhydroperoxide; bis(acetylacetonate)oxovanadium In dichloromethane at 20℃;94%
ethanol
64-17-5

ethanol

chloro-diphenylphosphine
1079-66-9

chloro-diphenylphosphine

mesitylene-2-carboxylic acid chloride
938-18-1

mesitylene-2-carboxylic acid chloride

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

Conditions
ConditionsYield
Stage #1: ethanol With sodium In toluene at 65 - 70℃; for 2h;
Stage #2: chloro-diphenylphosphine In toluene at 5 - 10℃; for 1h;
Stage #3: mesitylene-2-carboxylic acid chloride In toluene at 70 - 75℃; for 5h; Temperature; Solvent;
92.2%
(trichloromethyl)mesitylene
707-74-4

(trichloromethyl)mesitylene

chloro-diphenylphosphine
1079-66-9

chloro-diphenylphosphine

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

Conditions
ConditionsYield
Stage #1: chloro-diphenylphosphine With potassium hydroxide In toluene at 20℃; for 2.5h; Inert atmosphere;
Stage #2: (trichloromethyl)mesitylene With iron(III) chloride at 90℃; Inert atmosphere;
91%
Stage #1: (trichloromethyl)mesitylene; chloro-diphenylphosphine With magnesium In tetrahydrofuran Reflux;
Stage #2: With hydrogenchloride; dihydrogen peroxide In water
87 g
isopropyl diphenylphosphinite
27350-46-5

isopropyl diphenylphosphinite

mesitylene-2-carboxylic acid chloride
938-18-1

mesitylene-2-carboxylic acid chloride

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

Conditions
ConditionsYield
at 50 - 90℃; for 7.33333h;90.7%
(trichloromethyl)mesitylene
707-74-4

(trichloromethyl)mesitylene

Diphenylphosphine oxide
4559-70-0

Diphenylphosphine oxide

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

Conditions
ConditionsYield
Stage #1: (trichloromethyl)mesitylene; Diphenylphosphine oxide With iron(III) chloride In toluene at 90℃; for 3h; Inert atmosphere;
Stage #2: With water; sodium hydrogencarbonate In toluene at 20℃; Inert atmosphere;
89%
Stage #1: Diphenylphosphine oxide With n-butyllithium In tetrahydrofuran for 0.5h; Cooling with ice;
Stage #2: (trichloromethyl)mesitylene In tetrahydrofuran for 0.5h;
87%
Diphenylphosphine oxide
4559-70-0

Diphenylphosphine oxide

mesitylene-2-carboxylic acid chloride
938-18-1

mesitylene-2-carboxylic acid chloride

A

C34H32O3P2

C34H32O3P2

B

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

Conditions
ConditionsYield
With potassium hydroxide In 1,2-dichloro-ethane at -10℃; Solvent; Reagent/catalyst; Temperature; Inert atmosphere;A 8%
B 89%
Diphenylphosphine oxide
4559-70-0

Diphenylphosphine oxide

mesitylene-2-carboxylic acid chloride
938-18-1

mesitylene-2-carboxylic acid chloride

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

Conditions
ConditionsYield
With dmap at 80℃;88.2%
With Methyltrichlorosilane; triethylamine In 1,4-dioxane at 60℃; Catalytic behavior; Reagent/catalyst; Solvent; Temperature; Schlenk technique; Inert atmosphere; Green chemistry;71%
Stage #1: mesitylene-2-carboxylic acid chloride With aluminum (III) chloride In 1,2-dichloro-ethane at 20℃; for 1h; Inert atmosphere;
Stage #2: Diphenylphosphine oxide In 1,2-dichloro-ethane for 5h; Reflux;
1.6 g
C22H21Cl2P

C22H21Cl2P

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

Conditions
ConditionsYield
With dihydrogen peroxide In toluene84%
tetrachloromethane
56-23-5

tetrachloromethane

Diphenylphosphine oxide
4559-70-0

Diphenylphosphine oxide

1,3,5-trimethyl-benzene
108-67-8

1,3,5-trimethyl-benzene

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

Conditions
ConditionsYield
Stage #1: tetrachloromethane; 1,3,5-trimethyl-benzene With aluminum (III) chloride at 40℃; for 3.25h; Inert atmosphere;
Stage #2: With hydrogenchloride; water at 20℃; for 0.5h; Inert atmosphere;
Stage #3: Diphenylphosphine oxide In toluene Reagent/catalyst; Inert atmosphere;
84%
diphenylphosphinous acid methyl ester
4020-99-9

diphenylphosphinous acid methyl ester

2,2,2-trichloro-1-(2,4,6-trimethylphenyl)ethan-1-one
81759-79-7

2,2,2-trichloro-1-(2,4,6-trimethylphenyl)ethan-1-one

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

Conditions
ConditionsYield
In toluene at 40 - 60℃;82%
Ethyl diphenylphosphinite
719-80-2

Ethyl diphenylphosphinite

2,2,2-trichloro-1-(2,4,6-trimethylphenyl)ethan-1-one
81759-79-7

2,2,2-trichloro-1-(2,4,6-trimethylphenyl)ethan-1-one

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

Conditions
ConditionsYield
In toluene at 40 - 60℃;81%
tetrachloromethane
56-23-5

tetrachloromethane

chloro-diphenylphosphine
1079-66-9

chloro-diphenylphosphine

1,3,5-trimethyl-benzene
108-67-8

1,3,5-trimethyl-benzene

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

Conditions
ConditionsYield
Stage #1: tetrachloromethane; 1,3,5-trimethyl-benzene With aluminum (III) chloride at 40℃; for 3.25h; Inert atmosphere;
Stage #2: With hydrogenchloride; water at 20℃; for 0.5h; Inert atmosphere;
Stage #3: chloro-diphenylphosphine Further stages;
81%
mesytaldehyde
487-68-3

mesytaldehyde

benzene
71-43-2

benzene

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

Conditions
ConditionsYield
Stage #1: benzene With aluminum (III) chloride; phosphorus trichloride at 70 - 120℃;
Stage #2: mesytaldehyde at 5 - 10℃;
Stage #3: With tungsten trioxide; tetrabutylammomium bromide; dihydrogen peroxide; sodium hydroxide at 5 - 10℃; pH=2;
80%
1,3,5-trimethyl-benzene
108-67-8

1,3,5-trimethyl-benzene

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: aluminum (III) chloride; hydrogenchloride / 2 h / 20 °C
2: magnesium / tetrahydrofuran / Reflux
View Scheme
Multi-step reaction with 2 steps
1.1: aluminum (III) chloride / 3 h / 20 - 45 °C
2.1: n-butyllithium / tetrahydrofuran / 0.5 h / Cooling with ice
2.2: 0.5 h
View Scheme
Multi-step reaction with 3 steps
1.1: aluminum (III) chloride / 3 h / 20 - 45 °C
2.1: lithium / tetrahydrofuran / 35 °C / Inert atmosphere
2.2: 20 °C
3.1: dihydrogen peroxide / toluene
View Scheme
Multi-step reaction with 2 steps
1.1: C8H15N2(1+)*Br(1-)*2AlCl3; titanium tetrachloride; 1-methylimidazole hydrogen sulfate / 20 °C / 22502.3 - 30003 Torr / Autoclave
2.1: water; chlorobenzene / 2 h / 5 - 20 °C
2.2: 20 h / 5 °C / pH 3
View Scheme
(trichloromethyl)mesitylene
707-74-4

(trichloromethyl)mesitylene

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: lithium / tetrahydrofuran / 35 °C / Inert atmosphere
1.2: 20 °C
2.1: dihydrogen peroxide / toluene
View Scheme
2,4,6-trimethylbenzyl alcohol
4170-90-5

2,4,6-trimethylbenzyl alcohol

Diphenylphosphine oxide
4559-70-0

Diphenylphosphine oxide

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: dipotassium peroxodisulfate / acetone / 20 °C
2: manganese(IV) oxide / dichloromethane / 20 °C
View Scheme
mesitylene-2-carboxylic acid chloride
938-18-1

mesitylene-2-carboxylic acid chloride

diphenyl(methyl)phosphine oxide
2129-89-7

diphenyl(methyl)phosphine oxide

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

Conditions
ConditionsYield
In toluene at 0 - 80℃; for 3h; Inert atmosphere;
In toluene at 0 - 80℃; for 3h; Inert atmosphere;
benzene
71-43-2

benzene

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: aluminum (III) chloride; trichlorophosphate / 4 h / 70 °C / Inert atmosphere
2: dmap / 80 °C
View Scheme
Multi-step reaction with 2 steps
1.1: aluminum (III) chloride; trichlorophosphate / 70 - 120 °C
1.2: 0.5 h / 30 °C
2.1: toluene / 40 - 60 °C
View Scheme
Multi-step reaction with 2 steps
1.1: aluminum (III) chloride; trichlorophosphate / 70 - 130 °C
1.2: 0.5 h / 30 °C
2.1: toluene / 40 - 60 °C
View Scheme
diphenylphosphanyl(2,4,6-trimethylphenyl)methanone

diphenylphosphanyl(2,4,6-trimethylphenyl)methanone

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

Conditions
ConditionsYield
With dihydrogen peroxide In diethyl ether at 30 - 45℃; for 2h; Inert atmosphere;59.3g
With tert.-butylhydroperoxide; vanadia In chlorobenzene at 30℃; under 1500.15 Torr; for 0.00138889h; Temperature; Reagent/catalyst;
With 3-chloro-benzenecarboperoxoic acid In tetrahydrofuran at 25℃; for 3h; Inert atmosphere;
chloro-diphenylphosphine
1079-66-9

chloro-diphenylphosphine

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 1-methyl-1H-imidazole / 2 h / 35 - 60 °C
2: 7.33 h / 50 - 90 °C
View Scheme
Multi-step reaction with 2 steps
1: 1-methyl-1H-imidazole / 2 h / 45 - 65 °C
2: 9.33 h / 50 - 90 °C
View Scheme
Multi-step reaction with 2 steps
1: 1-methyl-1H-imidazole / 2 h / 50 - 100 °C
2: 7.33 h / 50 - 90 °C
View Scheme
Multi-step reaction with 2 steps
1: 1-methyl-1H-imidazole / 2 h / 50 - 65 °C
2: 7.33 h / 50 - 90 °C
View Scheme
Multi-step reaction with 2 steps
1: 1-methyl-1H-imidazole / 3 h / 50 - 80 °C
2: 9.33 h / 50 - 90 °C
View Scheme
mesytaldehyde
487-68-3

mesytaldehyde

chloro-diphenylphosphine
1079-66-9

chloro-diphenylphosphine

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: chlorobenzene / 0 h / 30 °C / 1500.15 Torr
2: vanadia; tert.-butylhydroperoxide / chlorobenzene / 0 h / 30 °C / 1500.15 Torr
View Scheme
Stage #1: mesytaldehyde; chloro-diphenylphosphine In water; chlorobenzene at 5 - 20℃; for 2h;
Stage #2: With ammonium molibdate; tetrabutylammomium bromide; dihydrogen peroxide; sodium hydroxide In water; chlorobenzene at 5℃; for 20h; pH=3;
(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

2-chloropropionyl chloride
625-36-5

2-chloropropionyl chloride

C25H24ClO3P

C25H24ClO3P

Conditions
ConditionsYield
With aluminum (III) chloride In dichloromethane at 10 - 35℃; for 7h;99%
1-iodoperfluorododecane
307-60-8

1-iodoperfluorododecane

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

pentacosafluorododecyldiphenylphosphine
1424373-37-4

pentacosafluorododecyldiphenylphosphine

Conditions
ConditionsYield
With Diphenylphosphine oxide at 20℃; for 6h; Inert atmosphere; Irradiation;98%
(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

diphenyl(2,4,6-trimethylphenyl)phosphine oxide
91239-43-9

diphenyl(2,4,6-trimethylphenyl)phosphine oxide

Conditions
ConditionsYield
With tris-(dibenzylideneacetone)dipalladium(0); tricyclohexylphosphine In 5,5-dimethyl-1,3-cyclohexadiene at 130℃; for 16h; Schlenk technique; Inert atmosphere;97%
1-Iodo-perfluorodecane
423-62-1

1-Iodo-perfluorodecane

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

henicosafluorodecyldiphenylphosphine

henicosafluorodecyldiphenylphosphine

Conditions
ConditionsYield
With Diphenylphosphine oxide at 20℃; for 1.5h; Wavelength; Reagent/catalyst; Time; Inert atmosphere; Irradiation;96%
With diphenylphosphane at 20℃; for 3.5h; Wavelength; Irradiation; Inert atmosphere; Sealed tube;81 %Spectr.
In chloroform-d1 at 15 - 25℃; for 3.5h; Solvent; Irradiation; Sealed tube;41 %Spectr.
dodecafluoro-1,6-diiodohexane
375-80-4

dodecafluoro-1,6-diiodohexane

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

1,6-bis(diphenylthiophosphinyl)perfluorohexane
1424373-26-1

1,6-bis(diphenylthiophosphinyl)perfluorohexane

Conditions
ConditionsYield
Stage #1: dodecafluoro-1,6-diiodohexane; (2,4,6-trimethylbenzoyl)diphenylphosphine oxide With Diphenylphosphine oxide at 20℃; for 6h; Inert atmosphere; Irradiation;
Stage #2: With sulfur at 80℃; for 5h; Inert atmosphere;
96%
4,4'-dimethoxyphenyl disulfide
5335-87-5

4,4'-dimethoxyphenyl disulfide

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

A

S-(4-methoxyphenyl) 2,4,6-trimethylthiobenzoate

S-(4-methoxyphenyl) 2,4,6-trimethylthiobenzoate

B

S-(4-methoxyphenyl)thiodiphenylphosphorus oxide
99234-85-2

S-(4-methoxyphenyl)thiodiphenylphosphorus oxide

Conditions
ConditionsYield
In dichloromethane at 20℃; for 6h; Inert atmosphere; Sealed tube; Irradiation;A 87%
B 96%
(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

diphenyldisulfane
882-33-7

diphenyldisulfane

A

S-phenyl 2,4,6-trimethylthiobenzoate
50404-53-0

S-phenyl 2,4,6-trimethylthiobenzoate

B

diphenylthiophosphinic acid-S-phenyl ester
5510-78-1

diphenylthiophosphinic acid-S-phenyl ester

Conditions
ConditionsYield
In dichloromethane at 20℃; for 6h; Inert atmosphere; Sealed tube; Irradiation;A 78%
B 95%
1-Iodo-perfluorodecane
423-62-1

1-Iodo-perfluorodecane

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

diphenylphosphane
829-85-6

diphenylphosphane

henicosafluorodecyldiphenylphosphine

henicosafluorodecyldiphenylphosphine

Conditions
ConditionsYield
at 20℃; for 1.5h; Irradiation;95%
In chloroform-d1 at 15 - 25℃; for 1.5h; Irradiation; Sealed tube;88%
di(p-tolyl) disulfide
103-19-5

di(p-tolyl) disulfide

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

A

S-(4-methylphenyl)thiodiphenylphosphorus oxide
5510-81-6

S-(4-methylphenyl)thiodiphenylphosphorus oxide

B

S-(4-methylphenyl) 2,4,6-trimethylthiobenzoate

S-(4-methylphenyl) 2,4,6-trimethylthiobenzoate

Conditions
ConditionsYield
In dichloromethane at 20℃; for 6h; Inert atmosphere; Sealed tube; Irradiation;A 94%
B 94%
bis(p-chlorophenyl) diselenide
20541-49-5

bis(p-chlorophenyl) diselenide

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

A

Se-(4-chlorophenyl) 2,4,6-trimethylselenobenzoate

Se-(4-chlorophenyl) 2,4,6-trimethylselenobenzoate

B

Se-(4-chlorophenyl) diphenylselenophosphinate

Se-(4-chlorophenyl) diphenylselenophosphinate

Conditions
ConditionsYield
In dichloromethane at 20℃; for 6h; Inert atmosphere; Sealed tube; Irradiation;A 94%
B 92%
dibutyl diselenide
20333-40-8

dibutyl diselenide

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

A

P,P-diphenylphosphinoselenoic acid Se-butyl ester

P,P-diphenylphosphinoselenoic acid Se-butyl ester

B

Se-(n-butyl) 2,4,6-trimethylselenobenzoate

Se-(n-butyl) 2,4,6-trimethylselenobenzoate

Conditions
ConditionsYield
In dichloromethane at 20℃; for 6h; Inert atmosphere; Sealed tube; Irradiation;A 91%
B 94%
diphenyl diselenide
1666-13-3

diphenyl diselenide

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

A

Se-phenyl diphenylselenophosphinate
2049-62-9

Se-phenyl diphenylselenophosphinate

B

Se-phenyl 2,4,6-trimethylselenobenzoate

Se-phenyl 2,4,6-trimethylselenobenzoate

Conditions
ConditionsYield
In dichloromethane at 20℃; for 6h; Inert atmosphere; Sealed tube; Irradiation;A 92%
B 88%
(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

chloroacetyl chloride
79-04-9

chloroacetyl chloride

C24H22ClO3P

C24H22ClO3P

Conditions
ConditionsYield
With aluminum (III) chloride In dichloromethane at 10 - 35℃; for 7h;92%
dibenzyl disulphide
150-60-7

dibenzyl disulphide

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

A

diphenylphosphinothioic acid S-benzyl ester
3096-05-7

diphenylphosphinothioic acid S-benzyl ester

B

C17H18OS

C17H18OS

Conditions
ConditionsYield
In dichloromethane at 20℃; for 6h; Inert atmosphere; Sealed tube; Irradiation;A 91%
B 40 %Spectr.
1-Iodo-perfluorodecane
423-62-1

1-Iodo-perfluorodecane

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
75980-60-8

(2,4,6-trimethylbenzoyl)diphenylphosphine oxide

Diphenylphosphine oxide
4559-70-0

Diphenylphosphine oxide

henicosafluorodecyldiphenylphosphine

henicosafluorodecyldiphenylphosphine

Conditions
ConditionsYield
at 20℃; for 1.5h; Irradiation;90%
In chloroform-d1 at 15 - 25℃; for 1.5h; Irradiation;90%
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