Appearance:Yellow crystal powder Storage:Room temperature Package:25kg/drum Application:UV Photoinitiator Transportation:Express/Sea/Air Port:Any port in China
Cas:75980-60-8
Min.Order:25 Kilogram
FOB Price: $45.0 / 55.0
Type:Lab/Research institutions
inquirySpecifications CAS No.: 75980-60-8 Other Names: TPO MF: C22H21O2P EINECS No.: 278-355-8 Place of Origin: Shandong, China (Mainland) Type: Pharmaceutical Intermediates Purity: 99%min Brand Name: Luyunjia Model Number: luxin-1492 App
Cas:75980-60-8
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryAdvantages: 1. Its photocuringspeed is fast 2. Have light-decolourizatio 3. Can be used for thick coating curing 4. Belongs to low-volatilitymild-smell and environment friendlyproduct 5. Anti-yellowing Appearance:yellowish powder
Chemacure PI-TPO is a photoinitiator for curing styrene-based unsaturated polyesters and acrylic resins. Thanks to Chemacure PI- TPO’s absorption in the long-wave region of the UV spectrum (see plot opposite), even white paints and surfaces
Cas:75980-60-8
Min.Order:1 Metric Ton
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Type:Trading Company
inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At present
Cas:75980-60-8
Min.Order:1 Kilogram
FOB Price: $76.0 / 80.0
Type:Trading Company
inquiryWe provide tailor-made photoinitiator solutions for different performances by custom synthesisi.blends or other technical supports low-odor uv formulations low odor, low yellowing, through-curing non-yellowing uv formulations benzene-free u
Cas:75980-60-8
Min.Order:100 Kilogram
Negotiable
Type:Trading Company
inquiryPhotoinitiators HRcure-TPO CAS NO.: 75980-60-8 Throw curing, LED curing, low-yellowing UV absorption peak: 275nm, 379nm Tianjin Huiren chemtech Co. , Ltd. , established in January 2016, is a national high-tech enterprise t
Cas:75980-60-8
Min.Order:1 Kilogram
FOB Price: $0.1 / 2.0
Type:Lab/Research institutions
inquirywe provide tailor-made photoinitiator solutions for different performances by custom synthesisi.blends or other technical supports low-odor UV formulations Non-yellowing UV formulations Benzene-Free UV formulations Polymeric UV formulations
Cas:75980-60-8
Min.Order:100 Kilogram
Negotiable
Type:Trading Company
inquiryAs a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
Cas:75980-60-8
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:75980-60-8
Min.Order:1 Metric Ton
Negotiable
Type:Manufacturers
inquiryTest Item Requirement Test Result Appearance Yellow crystal Pass Assay ≥99.0%
Cas:75980-60-8
Min.Order:1 Kilogram
FOB Price: $250.0 / 350.0
Type:Manufacturers
inquiryhebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developm
Cas:75980-60-8
Min.Order:1 Metric Ton
FOB Price: $1.0 / 3.0
Type:Manufacturers
inquiryUnique advantages Guaranteed the purity High quality & competitive price Quality control Fast feedback Prompt shipment Appearance:Yellow crystal Storage:Cool dry place Package:20kg/carton Application:Photoinitiator Transportation:By
Cas:75980-60-8
Min.Order:20 Kilogram
FOB Price: $50.0 / 53.0
Type:Trading Company
inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Cas:75980-60-8
Min.Order:1
Negotiable
Type:Other
inquiryProduct description: Product name Photoinitiator TPO CAS number 75980-60-8 Assay >99% Appearance Yellowish crystalline powder Capacity 200mt/year Application Screen printing ink
Cas:75980-60-8
Min.Order:10 Gram
FOB Price: $12.0
Type:Lab/Research institutions
inquiry1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
Cas:75980-60-8
Min.Order:1 Gram
FOB Price: $0.1
Type:Manufacturers
inquiry
Cas:75980-60-8
Min.Order:1 Metric Ton
FOB Price: $1.0
Type:Manufacturers
inquiryTIANFUCHEM-- 75980-60-8--High purity Diphenyl(2,4,6-trimethylbenzoyl)phosphine oxide in stock Our company was built in 2009 with an ISO certificate.In the past 10 years, we have grown up as a famous fine chemicals supplier in China And we
Cas:75980-60-8
Min.Order:1 Metric Ton
FOB Price: $2000.0
Type:Lab/Research institutions
inquiryOur advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva
Cas:75980-60-8
Min.Order:1 Kilogram
FOB Price: $9.0 / 99.0
Type:Trading Company
inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
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Min.Order:1 Kilogram
FOB Price: $139.0 / 210.0
Type:Trading Company
inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
Cas:75980-60-8
Min.Order:10 Kilogram
Negotiable
Type:Trading Company
inquiryProduct Name 2,4,6-trimethylbenzoyldiphenyl phosphine oxide CAS No. 75980-60-8 Molecular Formula
Cas:75980-60-8
Min.Order:5 Metric Ton
FOB Price: $1.0 / 2.0
Type:Other
inquiryAdvantages: Hubei XinRunde Chemical Co., Ltd is a renowned pharmaceutical manufacturer. We can offer high quality products at competitive price in quick delivery with 100% custom pass guaranteed. Never stop striving to offer our best service is our
Cas:75980-60-8
Min.Order:10 Gram
Negotiable
Type:Other
inquiry1.In No Less 8years exporting experience. forclients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specia
Cas:75980-60-8
Min.Order:25 Kilogram
FOB Price: $1.0
Type:Lab/Research institutions
inquiryWe are the manufacturers and suppliers of API in China, and warehouse in Germany and USA of California, which can quickly and safely deliver to your address 1.High quality and competitive price. 2.Free sample for your evaluation. 3.Promptly delivery
Cas:75980-60-8
Min.Order:10 Gram
FOB Price: $3.5
Type:Trading Company
inquiryBeluga chemical professional supply Diphenyl(2,4,6-trimethylbenzoyl)phosphine oxide CAS75980-60-8 Why choose Beluga chemical 1. Beluga Chemical has a professional RESEARCH and development team and strong technical force to ensure technical supp
Cas:75980-60-8
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryWe have overseas warehouses in California, New Laredo Mexico, Vancouver Canada, Amsterdam Netherlands, and Melbourne Australia. Overseas warehouses can provide some of the best-selling products. We look forward to the cooperation of local powerful
Cas:75980-60-8
Min.Order:0 Metric Ton
Negotiable
Type:Trading Company
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:75980-60-8
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryProduct Detail Minimum Order Qty. 10 Gram Supply Ability 500 Kilograms/Month Storage store in cool, dry, ventilated place 20℃ Delivery Time 3 business days after payment Payment Term TT,western union,Paypal,
Cas:75980-60-8
Min.Order:20 Metric Ton
Negotiable
Type:Trading Company
inquiry1,we produce and sell good chemicals around the world. 2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%. 3,our staff consists of highly qualifie
Cas:75980-60-8
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiry(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
Conditions | Yield |
---|---|
With manganese(IV) oxide In dichloromethane at 20℃; | 98% |
With vanadium(V) oxide; dihydrogen peroxide at 8 - 25℃; for 3.5h; Reagent/catalyst; Green chemistry; | 96% |
With tert.-butylhydroperoxide In dichloromethane at 5 - 20℃; for 6.5h; Reagent/catalyst; | 92.5% |
mesytaldehyde
Diphenylphosphine oxide
(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
Conditions | Yield |
---|---|
Stage #1: mesytaldehyde; Diphenylphosphine oxide In dichloromethane for 6h; Green chemistry; Stage #2: With ammonium metavanadate; dihydrogen peroxide at 8 - 20℃; for 5.5h; Reagent/catalyst; Green chemistry; | 98% |
diphenyl n-pentyloxyphosphine
mesitylene-2-carboxylic acid chloride
(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
Conditions | Yield |
---|---|
at 50 - 90℃; for 9.33333h; | 95.8% |
(sec-butyloxy)di(phenyl)phosphine
mesitylene-2-carboxylic acid chloride
(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
Conditions | Yield |
---|---|
at 50 - 90℃; for 7.33333h; | 95.6% |
Ethyl diphenylphosphinite
mesitylene-2-carboxylic acid chloride
(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
Conditions | Yield |
---|---|
at 40 - 90℃; for 8h; Time; Green chemistry; | 95.1% |
With N,N-dimethyl-cyclohexanamine at 80 - 85℃; Product distribution / selectivity; |
diphenyl n-propoxyphosphine
mesitylene-2-carboxylic acid chloride
(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
Conditions | Yield |
---|---|
at 50 - 90℃; for 7.33333h; | 95.1% |
diphenyl sec-pentyloxyphosphine
mesitylene-2-carboxylic acid chloride
(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
Conditions | Yield |
---|---|
at 50 - 90℃; for 7.33333h; | 94.9% |
(n-butyloxy)di(phenyl)phosphine
mesitylene-2-carboxylic acid chloride
(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
Conditions | Yield |
---|---|
at 50 - 90℃; for 9.33333h; | 94.8% |
(2,4,6-trimethylbenzyl)diphenylphosphine oxide
(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; bis(acetylacetonate)oxovanadium In dichloromethane at 20℃; | 94% |
ethanol
chloro-diphenylphosphine
mesitylene-2-carboxylic acid chloride
(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
Conditions | Yield |
---|---|
Stage #1: ethanol With sodium In toluene at 65 - 70℃; for 2h; Stage #2: chloro-diphenylphosphine In toluene at 5 - 10℃; for 1h; Stage #3: mesitylene-2-carboxylic acid chloride In toluene at 70 - 75℃; for 5h; Temperature; Solvent; | 92.2% |
(trichloromethyl)mesitylene
chloro-diphenylphosphine
(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
Conditions | Yield |
---|---|
Stage #1: chloro-diphenylphosphine With potassium hydroxide In toluene at 20℃; for 2.5h; Inert atmosphere; Stage #2: (trichloromethyl)mesitylene With iron(III) chloride at 90℃; Inert atmosphere; | 91% |
Stage #1: (trichloromethyl)mesitylene; chloro-diphenylphosphine With magnesium In tetrahydrofuran Reflux; Stage #2: With hydrogenchloride; dihydrogen peroxide In water | 87 g |
isopropyl diphenylphosphinite
mesitylene-2-carboxylic acid chloride
(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
Conditions | Yield |
---|---|
at 50 - 90℃; for 7.33333h; | 90.7% |
(trichloromethyl)mesitylene
Diphenylphosphine oxide
(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
Conditions | Yield |
---|---|
Stage #1: (trichloromethyl)mesitylene; Diphenylphosphine oxide With iron(III) chloride In toluene at 90℃; for 3h; Inert atmosphere; Stage #2: With water; sodium hydrogencarbonate In toluene at 20℃; Inert atmosphere; | 89% |
Stage #1: Diphenylphosphine oxide With n-butyllithium In tetrahydrofuran for 0.5h; Cooling with ice; Stage #2: (trichloromethyl)mesitylene In tetrahydrofuran for 0.5h; | 87% |
Diphenylphosphine oxide
mesitylene-2-carboxylic acid chloride
B
(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
Conditions | Yield |
---|---|
With potassium hydroxide In 1,2-dichloro-ethane at -10℃; Solvent; Reagent/catalyst; Temperature; Inert atmosphere; | A 8% B 89% |
Diphenylphosphine oxide
mesitylene-2-carboxylic acid chloride
(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
Conditions | Yield |
---|---|
With dmap at 80℃; | 88.2% |
With Methyltrichlorosilane; triethylamine In 1,4-dioxane at 60℃; Catalytic behavior; Reagent/catalyst; Solvent; Temperature; Schlenk technique; Inert atmosphere; Green chemistry; | 71% |
Stage #1: mesitylene-2-carboxylic acid chloride With aluminum (III) chloride In 1,2-dichloro-ethane at 20℃; for 1h; Inert atmosphere; Stage #2: Diphenylphosphine oxide In 1,2-dichloro-ethane for 5h; Reflux; | 1.6 g |
(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
Conditions | Yield |
---|---|
With dihydrogen peroxide In toluene | 84% |
tetrachloromethane
Diphenylphosphine oxide
1,3,5-trimethyl-benzene
(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
Conditions | Yield |
---|---|
Stage #1: tetrachloromethane; 1,3,5-trimethyl-benzene With aluminum (III) chloride at 40℃; for 3.25h; Inert atmosphere; Stage #2: With hydrogenchloride; water at 20℃; for 0.5h; Inert atmosphere; Stage #3: Diphenylphosphine oxide In toluene Reagent/catalyst; Inert atmosphere; | 84% |
diphenylphosphinous acid methyl ester
2,2,2-trichloro-1-(2,4,6-trimethylphenyl)ethan-1-one
(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
Conditions | Yield |
---|---|
In toluene at 40 - 60℃; | 82% |
Ethyl diphenylphosphinite
2,2,2-trichloro-1-(2,4,6-trimethylphenyl)ethan-1-one
(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
Conditions | Yield |
---|---|
In toluene at 40 - 60℃; | 81% |
tetrachloromethane
chloro-diphenylphosphine
1,3,5-trimethyl-benzene
(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
Conditions | Yield |
---|---|
Stage #1: tetrachloromethane; 1,3,5-trimethyl-benzene With aluminum (III) chloride at 40℃; for 3.25h; Inert atmosphere; Stage #2: With hydrogenchloride; water at 20℃; for 0.5h; Inert atmosphere; Stage #3: chloro-diphenylphosphine Further stages; | 81% |
Conditions | Yield |
---|---|
Stage #1: benzene With aluminum (III) chloride; phosphorus trichloride at 70 - 120℃; Stage #2: mesytaldehyde at 5 - 10℃; Stage #3: With tungsten trioxide; tetrabutylammomium bromide; dihydrogen peroxide; sodium hydroxide at 5 - 10℃; pH=2; | 80% |
1,3,5-trimethyl-benzene
(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: aluminum (III) chloride; hydrogenchloride / 2 h / 20 °C 2: magnesium / tetrahydrofuran / Reflux View Scheme | |
Multi-step reaction with 2 steps 1.1: aluminum (III) chloride / 3 h / 20 - 45 °C 2.1: n-butyllithium / tetrahydrofuran / 0.5 h / Cooling with ice 2.2: 0.5 h View Scheme | |
Multi-step reaction with 3 steps 1.1: aluminum (III) chloride / 3 h / 20 - 45 °C 2.1: lithium / tetrahydrofuran / 35 °C / Inert atmosphere 2.2: 20 °C 3.1: dihydrogen peroxide / toluene View Scheme | |
Multi-step reaction with 2 steps 1.1: C8H15N2(1+)*Br(1-)*2AlCl3; titanium tetrachloride; 1-methylimidazole hydrogen sulfate / 20 °C / 22502.3 - 30003 Torr / Autoclave 2.1: water; chlorobenzene / 2 h / 5 - 20 °C 2.2: 20 h / 5 °C / pH 3 View Scheme |
(trichloromethyl)mesitylene
(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: lithium / tetrahydrofuran / 35 °C / Inert atmosphere 1.2: 20 °C 2.1: dihydrogen peroxide / toluene View Scheme |
2,4,6-trimethylbenzyl alcohol
Diphenylphosphine oxide
(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: dipotassium peroxodisulfate / acetone / 20 °C 2: manganese(IV) oxide / dichloromethane / 20 °C View Scheme |
mesitylene-2-carboxylic acid chloride
diphenyl(methyl)phosphine oxide
(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
Conditions | Yield |
---|---|
In toluene at 0 - 80℃; for 3h; Inert atmosphere; | |
In toluene at 0 - 80℃; for 3h; Inert atmosphere; |
benzene
(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: aluminum (III) chloride; trichlorophosphate / 4 h / 70 °C / Inert atmosphere 2: dmap / 80 °C View Scheme | |
Multi-step reaction with 2 steps 1.1: aluminum (III) chloride; trichlorophosphate / 70 - 120 °C 1.2: 0.5 h / 30 °C 2.1: toluene / 40 - 60 °C View Scheme | |
Multi-step reaction with 2 steps 1.1: aluminum (III) chloride; trichlorophosphate / 70 - 130 °C 1.2: 0.5 h / 30 °C 2.1: toluene / 40 - 60 °C View Scheme |
(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
Conditions | Yield |
---|---|
With dihydrogen peroxide In diethyl ether at 30 - 45℃; for 2h; Inert atmosphere; | 59.3g |
With tert.-butylhydroperoxide; vanadia In chlorobenzene at 30℃; under 1500.15 Torr; for 0.00138889h; Temperature; Reagent/catalyst; | |
With 3-chloro-benzenecarboperoxoic acid In tetrahydrofuran at 25℃; for 3h; Inert atmosphere; |
chloro-diphenylphosphine
(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 1-methyl-1H-imidazole / 2 h / 35 - 60 °C 2: 7.33 h / 50 - 90 °C View Scheme | |
Multi-step reaction with 2 steps 1: 1-methyl-1H-imidazole / 2 h / 45 - 65 °C 2: 9.33 h / 50 - 90 °C View Scheme | |
Multi-step reaction with 2 steps 1: 1-methyl-1H-imidazole / 2 h / 50 - 100 °C 2: 7.33 h / 50 - 90 °C View Scheme | |
Multi-step reaction with 2 steps 1: 1-methyl-1H-imidazole / 2 h / 50 - 65 °C 2: 7.33 h / 50 - 90 °C View Scheme | |
Multi-step reaction with 2 steps 1: 1-methyl-1H-imidazole / 3 h / 50 - 80 °C 2: 9.33 h / 50 - 90 °C View Scheme |
mesytaldehyde
chloro-diphenylphosphine
(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: chlorobenzene / 0 h / 30 °C / 1500.15 Torr 2: vanadia; tert.-butylhydroperoxide / chlorobenzene / 0 h / 30 °C / 1500.15 Torr View Scheme | |
Stage #1: mesytaldehyde; chloro-diphenylphosphine In water; chlorobenzene at 5 - 20℃; for 2h; Stage #2: With ammonium molibdate; tetrabutylammomium bromide; dihydrogen peroxide; sodium hydroxide In water; chlorobenzene at 5℃; for 20h; pH=3; |
(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
2-chloropropionyl chloride
Conditions | Yield |
---|---|
With aluminum (III) chloride In dichloromethane at 10 - 35℃; for 7h; | 99% |
1-iodoperfluorododecane
(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
pentacosafluorododecyldiphenylphosphine
Conditions | Yield |
---|---|
With Diphenylphosphine oxide at 20℃; for 6h; Inert atmosphere; Irradiation; | 98% |
(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
diphenyl(2,4,6-trimethylphenyl)phosphine oxide
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); tricyclohexylphosphine In 5,5-dimethyl-1,3-cyclohexadiene at 130℃; for 16h; Schlenk technique; Inert atmosphere; | 97% |
1-Iodo-perfluorodecane
(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
Conditions | Yield |
---|---|
With Diphenylphosphine oxide at 20℃; for 1.5h; Wavelength; Reagent/catalyst; Time; Inert atmosphere; Irradiation; | 96% |
With diphenylphosphane at 20℃; for 3.5h; Wavelength; Irradiation; Inert atmosphere; Sealed tube; | 81 %Spectr. |
In chloroform-d1 at 15 - 25℃; for 3.5h; Solvent; Irradiation; Sealed tube; | 41 %Spectr. |
dodecafluoro-1,6-diiodohexane
(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
1,6-bis(diphenylthiophosphinyl)perfluorohexane
Conditions | Yield |
---|---|
Stage #1: dodecafluoro-1,6-diiodohexane; (2,4,6-trimethylbenzoyl)diphenylphosphine oxide With Diphenylphosphine oxide at 20℃; for 6h; Inert atmosphere; Irradiation; Stage #2: With sulfur at 80℃; for 5h; Inert atmosphere; | 96% |
4,4'-dimethoxyphenyl disulfide
(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
B
S-(4-methoxyphenyl)thiodiphenylphosphorus oxide
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 6h; Inert atmosphere; Sealed tube; Irradiation; | A 87% B 96% |
(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
diphenyldisulfane
A
S-phenyl 2,4,6-trimethylthiobenzoate
B
diphenylthiophosphinic acid-S-phenyl ester
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 6h; Inert atmosphere; Sealed tube; Irradiation; | A 78% B 95% |
1-Iodo-perfluorodecane
(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
diphenylphosphane
Conditions | Yield |
---|---|
at 20℃; for 1.5h; Irradiation; | 95% |
In chloroform-d1 at 15 - 25℃; for 1.5h; Irradiation; Sealed tube; | 88% |
di(p-tolyl) disulfide
(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
A
S-(4-methylphenyl)thiodiphenylphosphorus oxide
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 6h; Inert atmosphere; Sealed tube; Irradiation; | A 94% B 94% |
bis(p-chlorophenyl) diselenide
(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 6h; Inert atmosphere; Sealed tube; Irradiation; | A 94% B 92% |
dibutyl diselenide
(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 6h; Inert atmosphere; Sealed tube; Irradiation; | A 91% B 94% |
diphenyl diselenide
(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
A
Se-phenyl diphenylselenophosphinate
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 6h; Inert atmosphere; Sealed tube; Irradiation; | A 92% B 88% |
(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
chloroacetyl chloride
Conditions | Yield |
---|---|
With aluminum (III) chloride In dichloromethane at 10 - 35℃; for 7h; | 92% |
dibenzyl disulphide
(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
A
diphenylphosphinothioic acid S-benzyl ester
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 6h; Inert atmosphere; Sealed tube; Irradiation; | A 91% B 40 %Spectr. |
1-Iodo-perfluorodecane
(2,4,6-trimethylbenzoyl)diphenylphosphine oxide
Diphenylphosphine oxide
Conditions | Yield |
---|---|
at 20℃; for 1.5h; Irradiation; | 90% |
In chloroform-d1 at 15 - 25℃; for 1.5h; Irradiation; | 90% |
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