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Cas:26960-77-0
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
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Cas:26960-77-0
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inquirysodium dodecane-1-thiolate CAS:26960-77-0 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organ
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Min.Order:10 Gram
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inquiryAnsciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
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inquiryGood Quality Package:1kg/bag Application:Medical or chemical Transportation:Air/Train/Sea Port:Shenzhen
factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
1-Dodecanethiol, sodiumsalt (1:1)Appearance:Off white to slight yellow solid Storage:Store in dry and cool condition Package:25kg or according to cutomer's demand Application:Chemical research/Pharmaceutical intermediates Transportation:By Sea,by Air
Cas:26960-77-0
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inquiryCas:26960-77-0
Min.Order:0
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inquiry1-dodecylthiol
sodium dodecanethiolate
Conditions | Yield |
---|---|
With sodium hydride In diethyl ether | |
With sodium hydride In N,N-dimethyl-formamide at 5 - 25℃; for 1h; Inert atmosphere; Schlenk technique; | |
With sodium hydride In diethyl ether; mineral oil at 5℃; for 0.166667h; |
Conditions | Yield |
---|---|
In methanol at 20℃; for 0.25h; |
Conditions | Yield |
---|---|
In various solvent(s) at 180℃; for 20h; | 96% |
In various solvent(s) at 180℃; for 20h; Product distribution; Mechanism; var. temp.; var. solvents; other subst. chlorobenzenes; other thiolates; |
9,10-dichloroanthracene
sodium dodecanethiolate
Conditions | Yield |
---|---|
In various solvent(s) at 169℃; for 23h; | 95% |
hexachlorobenzene
sodium dodecanethiolate
hexakis(n-dodecylthio)benzene
Conditions | Yield |
---|---|
In various solvent(s) at 128℃; for 24h; | 95% |
In N,N,N,N,N,N-hexamethylphosphoric triamide Yield given; |
sodium dodecanethiolate
1-nitro-1,2-diphenyl-2-phenylthioethene
Conditions | Yield |
---|---|
In methanol at 20℃; for 1.25h; | 91% |
carbon monoxide
4-iodo-biphenyl
sodium dodecanethiolate
S-dodecyl biphenyl-4-carbothioate
Conditions | Yield |
---|---|
With bis-triphenylphosphine-palladium(II) chloride; 1-dodecylthiol In tetrahydrofuran at 60℃; under 7600.51 Torr; for 24h; Autoclave; | 90% |
carbon monoxide
para-iodoanisole
sodium dodecanethiolate
S-(n-dodecyl) 4-methoxybenzothioate
Conditions | Yield |
---|---|
With bis-triphenylphosphine-palladium(II) chloride; 1-dodecylthiol In tetrahydrofuran at 60℃; under 7600.51 Torr; for 24h; Autoclave; | 88% |
1,2,4,5-tetrachlorobenzene
sodium dodecanethiolate
Conditions | Yield |
---|---|
In various solvent(s) at 162℃; for 22h; | 86% |
sodium dodecanethiolate
2,3-dibromopropionic acid ethyl ester
Conditions | Yield |
---|---|
In ethanol at 70℃; for 4h; Substitution; | 82% |
Conditions | Yield |
---|---|
In tetrahydrofuran-d8 at 20℃; for 3h; Inert atmosphere; Glovebox; | 82% |
Conditions | Yield |
---|---|
In various solvent(s) at 175℃; for 22h; | 81% |
sodium dodecanethiolate
2-p-chlorophenylthio-1-nitro-1,2-diphenylethene
Conditions | Yield |
---|---|
In methanol at 20℃; for 1.08333h; | 81% |
sodium dodecanethiolate
Conditions | Yield |
---|---|
In methanol at 20℃; for 1.58333h; | 80% |
Conditions | Yield |
---|---|
With potassium hydroxide In dimethyl sulfoxide at 20 - 80℃; Inert atmosphere; Sealed tube; | 80% |
ortho-methylphenyl iodide
carbon monoxide
sodium dodecanethiolate
S-(n-dodecyl) 2-methylbenzothioate
Conditions | Yield |
---|---|
With bis-triphenylphosphine-palladium(II) chloride; 1-dodecylthiol In tetrahydrofuran at 60℃; under 7600.51 Torr; for 24h; Autoclave; | 79% |
iodobenzene
carbon monoxide
sodium dodecanethiolate
S-(n-dodecyl) benzothioate
Conditions | Yield |
---|---|
With bis-triphenylphosphine-palladium(II) chloride; 1-dodecylthiol In tetrahydrofuran at 60℃; under 7600.51 Torr; for 24h; Autoclave; | 78% |
sodium dodecanethiolate
Conditions | Yield |
---|---|
In methanol at 20℃; for 1h; | 76% |
Conditions | Yield |
---|---|
In various solvent(s) at 150℃; for 19h; | 75% |
Conditions | Yield |
---|---|
In various solvent(s) at 157℃; for 20h; | 68% |
sodium dodecanethiolate
2-(6-ethoxy-2-benzothiazolylthio)-1-nitro-1-phenylethene
Conditions | Yield |
---|---|
In methanol at 20℃; for 0.5h; | 68% |
sodium dodecanethiolate
Conditions | Yield |
---|---|
In methanol at 20℃; for 1h; | 67% |
1,3-dibromo-2-hydroxypropane
sodium dodecanethiolate
B
1,3-bis-(dodecylmercapto)-2-propanol
Conditions | Yield |
---|---|
In N-methyl-acetamide | A 67% B n/a |
pentaerythritol tetrabromide
sodium dodecanethiolate
1,3-bis-dodecylmercapto-2,2-bis-(dodecylmercapto-methyl)-propane
Conditions | Yield |
---|---|
In methanol; water for 5h; Heating; | 63% |
para-dichlorobenzene
sodium dodecanethiolate
1,4-bis(n-dodecylthio)benzene
Conditions | Yield |
---|---|
In various solvent(s) at 157℃; for 20h; | 63% |
sodium dodecanethiolate
3-(bromomethyl)-3-(dodecylthiomethyl)thietane
3,3-bis(dodecylthiomethyl)thietane
Conditions | Yield |
---|---|
In ethanol | 60% |
1-Chloro-4-iodobenzene
carbon monoxide
sodium dodecanethiolate
S-(n-dodecyl) 4-chlorobenzothioate
Conditions | Yield |
---|---|
With bis-triphenylphosphine-palladium(II) chloride; 1-dodecylthiol In tetrahydrofuran at 60℃; under 7600.51 Torr; for 24h; Autoclave; | 54% |
sodium dodecanethiolate
N,N-didesmethylvenlafaxine
A
N,N-Didesmethyldesvenlafaxine
B
dodecyl methyl sulfide
C
O-desmethylvenlafaxine
D
1-dodecylthiol
Conditions | Yield |
---|---|
In decaethylene glycol at 190℃; for 3h; Product distribution / selectivity; | A 52% B n/a C n/a D n/a |
Conditions | Yield |
---|---|
at 20℃; for 5h; Inert atmosphere; Glovebox; | 51.1% |
sodium dodecanethiolate
2-(4-chlorophenylthio)-1-nitro-1-phenylethene
A
didodecyl disulfide
Conditions | Yield |
---|---|
In methanol at -10 - 0℃; for 1h; | A 40% B 50% |
Umemoto's reagent
sodium dodecanethiolate
A
didodecyl disulfide
B
1-[(trifluoromethyl)thio]dodecane
Conditions | Yield |
---|---|
In tetrahydrofuran for 0.5h; Ambient temperature; | A 30% B 47% |
sodium dodecanethiolate
2-(4-chlorophenylthio)-1-nitro-1-phenylethene
A
didodecyl disulfide
Conditions | Yield |
---|---|
In methanol at 20℃; for 0.0833333h; | A 7% B 33% C 44% |
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