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inquiryProduct Name 2-Pyridylethylamine Synonyms RARECHEM AL BW 0258; 2-PYRIDYLETHYLAMINE; 2-Pyridineethanamine; 2-(PYRIDIN-2-YL)ETHANAMINE; 2-PYRIDIN-2-YL-ETHYLAMINE; 2-aminoethylpyridine; 2-(2-AMINOETHYL)PYR
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inquiryProduct Name: 2-Pyridylethylamine Synonyms: RARECHEM AL BW 0258;2-PYRIDYLETHYLAMINE;2-Pyridineethanamine;2-(PYRIDIN-2-YL)ETHANAMINE;2-PYRIDIN-2-YL-ETHYLAMINE;2-aminoethylpyridine;Betahistine Impurity 11;2-(2-Aminoethyl)pyridine 98%
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2-(aminoethyl)pyridine
Conditions | Yield |
---|---|
With palladium on activated charcoal; hydrogen In 1,4-dioxane; ethanol at 20℃; for 4h; | 91% |
Conditions | Yield |
---|---|
A 56% B n/a |
2-vinylpyridine
A
2-(aminoethyl)pyridine
B
bis[2-(2-pyridyl)ethyl]amine
Conditions | Yield |
---|---|
With ammonium chloride In methanol; water for 8h; Heating; | A 30% B 50% |
With ammonium chloride In methanol Heating; |
Conditions | Yield |
---|---|
With ammonium chloride In methanol; water for 16h; Reflux; | 29% |
With ammonium chloride |
2-(2-chloroethyl)pyridine
2-(aminoethyl)pyridine
Conditions | Yield |
---|---|
With ethanol; ammonia at 100℃; | |
Multi-step reaction with 2 steps 1: sodium azide / N,N-dimethyl-formamide / 12 h / 70 °C 2: palladium on activated charcoal; hydrogen / ethanol; 1,4-dioxane / 4 h / 20 °C View Scheme |
2-amino-1-[2]pyridyl-ethanone
2-(aminoethyl)pyridine
Conditions | Yield |
---|---|
With hydrogenchloride; platinum Hydrogenation; |
α-(aminomethyl)-2-pyridinemethanol
2-(aminoethyl)pyridine
Conditions | Yield |
---|---|
With hydrogenchloride; platinum Hydrogenation; |
(2-[2]pyridyl-ethyl)-carbamic acid methyl ester
2-(aminoethyl)pyridine
Conditions | Yield |
---|---|
With hydrogenchloride |
Diphenyl-(2-pyridin-2-yl-ethylamino)-methanol
A
2-(aminoethyl)pyridine
B
benzophenone
Conditions | Yield |
---|---|
With water In acetonitrile at 30℃; Rate constant; |
A
2-(aminoethyl)pyridine
Conditions | Yield |
---|---|
With ammonia at 125℃; im Rohr; |
2-(2-bromoethyl)pyridine
2-(aminoethyl)pyridine
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: aqueous ethanol 2: aqueous H2O2; aqueous KOH 3: methanol; bromine 4: aqueous HCl View Scheme |
2-(2-Cyanoethyl)pyridine
2-(aminoethyl)pyridine
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: aqueous H2O2; aqueous KOH 2: methanol; bromine 3: aqueous HCl View Scheme |
3-(pyridin-2-yl)propanoic acid
2-(aminoethyl)pyridine
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: methanol. HCl 2: aqueous NH3 3: methanol; bromine 4: aqueous HCl View Scheme |
3-(pyridin-2-yl)propanamide
2-(aminoethyl)pyridine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: methanol; bromine 2: aqueous HCl View Scheme |
methyl 3-(pyridin-2-yl)propanoate
2-(aminoethyl)pyridine
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: aqueous NH3 2: methanol; bromine 3: aqueous HCl View Scheme |
ethyl 2-pyridylcarbonylacetate
2-(aminoethyl)pyridine
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: aqueous NaOH; NaNO2 2: ethanol; SnCl2+2 H2O; concentrated aqueous HCl 3: platinum; aqueous HCl / Hydrogenation View Scheme |
2-(aminoethyl)pyridine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: ethanol; SnCl2+2 H2O; concentrated aqueous HCl 2: platinum; aqueous HCl / Hydrogenation View Scheme |
2-amino-1-[2]pyridyl-ethanone; dihydrochloride
2-(aminoethyl)pyridine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: palladium; aqueous HCl / Hydrogenation 2: platinum; aqueous HCl / Hydrogenation View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: benzene; thionyl chloride; hydrogen chloride 2: ethanol; NH3 / 100 °C View Scheme | |
Multi-step reaction with 3 steps 1: thionyl chloride / dichloromethane / 1 h / 20 °C 2: sodium azide / N,N-dimethyl-formamide / 12 h / 70 °C 3: palladium on activated charcoal; hydrogen / ethanol; 1,4-dioxane / 4 h / 20 °C View Scheme |
Conditions | Yield |
---|---|
With ammonium hydroxide; chloro(1,5-cyclooctadiene)rhodium(I) dimer; hydrogen at 100℃; under 20686.5 Torr; for 24h; Autoclave; Green chemistry; chemoselective reaction; | |
With aluminum (III) chloride; sodium tetrahydroborate In diethyl ether at 20℃; for 6h; | 0.6 g |
2-(bromomethyl)pyridine hydrobromide
2-(aminoethyl)pyridine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: sodium hydrogencarbonate / water 1.2: 24 h / 75 °C 2.1: sodium tetrahydroborate; aluminum (III) chloride / diethyl ether / 6 h / 20 °C View Scheme |
2-(aminoethyl)pyridine
2-hydroxy-isophthalaldehyde
2,6-bis-1-hydroxybenzene
Conditions | Yield |
---|---|
In methanol for 1h; Heating; | 100% |
In dichloromethane for 1h; |
2-(aminoethyl)pyridine
3,6-diformylpyridazine
Conditions | Yield |
---|---|
In acetonitrile | 100% |
2-(aminoethyl)pyridine
tert-butyl 2-(1-oxidopyridin-2-yl)ethylcarbamate
Conditions | Yield |
---|---|
Stage #1: 2-(aminoethyl)pyridine With di-tert-butyl dicarbonate In N,N-dimethyl-formamide at 20℃; for 1h; Stage #2: With 3-chloro-benzenecarboperoxoic acid In chloroform at 0℃; for 3.5h; | 100% |
Multi-step reaction with 2 steps 1: tetrahydrofuran / 3.5 h / 0 - 20 °C 2: 3-chloro-benzenecarboperoxoic acid / ethyl acetate / 15 h / 20 °C View Scheme |
2-(aminoethyl)pyridine
Conditions | Yield |
---|---|
In methanol for 72h; Inert atmosphere; Reflux; | 100% |
2-(aminoethyl)pyridine
N-(2-(pyridin-2-yl)ethyl)pyrazine-2-carboxamide
Conditions | Yield |
---|---|
In methanol at 20℃; for 22h; Reflux; | 100% |
2-(aminoethyl)pyridine
N-methyl-2-imidazolcarboxaldehyde
2-(2-(((1'-methyl-2'-imidazolyl)methylene)amino)ethyl)pyridine
Conditions | Yield |
---|---|
In methanol Reflux; | 100% |
In methanol for 4h; Reflux; | 65% |
In methanol at 60℃; for 4h; | 60% |
In ethanol at 60℃; for 4h; |
pyridine-2-carbaldehyde
2-(aminoethyl)pyridine
(2-pyridin-2-yl-ethyl)-pyridin-2-ylmethyl-amine
Conditions | Yield |
---|---|
With sodium tetrahydroborate In methanol | 100% |
Stage #1: pyridine-2-carbaldehyde; 2-(aminoethyl)pyridine In dichloromethane at 20℃; for 12h; Sealed tube; Molecular sieve; Stage #2: With methanol; sodium tetrahydroborate at 0℃; for 5h; Inert atmosphere; | 100% |
With sodium tris(acetoxy)borohydride In 1,2-dichloro-ethane at 20℃; for 2.5h; Inert atmosphere; | 97% |
2-(aminoethyl)pyridine
di-tert-butyl dicarbonate
tert-butyl (2-(pyridin-2-yl)ethyl)carbamate
Conditions | Yield |
---|---|
In tetrahydrofuran at 0 - 20℃; for 3.5h; | 99% |
In dichloromethane Ambient temperature; | |
With triethylamine In N-methyl-acetamide |
2-(aminoethyl)pyridine
[PdCl(Me)(2-(2-aminoethyl)pyridine-N,N')]
Conditions | Yield |
---|---|
In dichloromethane byproducts: COD; N2-atmosphere; stirring at room temp. for 3 h; evapn., washing (Et2O), drying; can be recrystallized (Et2O diffusion into MeCN soln.); elem. anal.; | 99% |
2-(aminoethyl)pyridine
Conditions | Yield |
---|---|
In water addn. of the amine to the Ni salt in H2O, filtration, addn. of aq. NaN3; slow evapn. (room temp.); | 99% |
2-pyrrole aldehyde
2-(aminoethyl)pyridine
N-(1H-pyrrol-2-ylmethylene)-2-(pyridin-2-yl)ethanamine
Conditions | Yield |
---|---|
In ethanol | 99% |
pyridine-2-carbaldehyde
2-(aminoethyl)pyridine
cobalt(II) tetrafluoroborate hexahydrate
Conditions | Yield |
---|---|
With glacial acetic acid In ethanol ligands dissolved in EtOH (2 drops of glacial acetic acid), refluxed for2 h, cooled to room temp., Fe compd. added (2:2:1 molar ratio), stirred for 1 h; ppt. filtered off, dried (vac.), elem. anal.; | 99% |
2-(aminoethyl)pyridine
(Z)-ethyl 2-hydroxy-4-oxo-4-(pyridin-2-yl)but-2-enoate
methyl 4-formylbenzoate
Conditions | Yield |
---|---|
With pyridinium p-toluenesulfonate In methanol; diethyl ether at -10℃; for 1h; | 99% |
Conditions | Yield |
---|---|
Stage #1: Boc-D-Trp-OH With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 0℃; for 0.166667h; Inert atmosphere; Stage #2: 2-(aminoethyl)pyridine With triethylamine In dichloromethane at 0 - 20℃; Inert atmosphere; | 99% |
2-(aminoethyl)pyridine
Biphenyl-2,2'-dicarbaldehyde
(2-Pyridin-2-yl-ethyl)-[1-(2'-{[(E)-2-pyridin-2-yl-ethylimino]-methyl}-biphenyl-2-yl)-meth-(E)-ylidene]-amine
Conditions | Yield |
---|---|
With magnesium sulfate In chloroform at 20℃; for 4h; Inert atmosphere; | 98% |
In chloroform Condensation; Heating; |
2-(aminoethyl)pyridine
3-[8-(2,6-difluorophenyl)-2-(methylsulfinyl)-7-oxo-5,6,7,8-tetrahydropyrimido[4,5-d]pyrimidin-4-yl]-4-methyl-N-(1-methylethyl)benzamide
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In tetrahydrofuran; chloroform at 20℃; | 98% |
2-(aminoethyl)pyridine
2,7-diacetyl-1,8-dihydroxy-3,6-dimethylnaphthalene
C10H2(CH3)2(OH)(COCH3)C(CH3)N(CH2)2C5H4NPd(Cl)O
Conditions | Yield |
---|---|
With LiCl In methanol heating suspn. of PdCl2, LiCl and dihydroxynaphthalene (reflux) until complete dissoln., addn. of aminoethylpyridine; concg. by boiling at atm. pressure until crystn. commences, cooling, collecting crystals, washing with MeOH; | 98% |
2-(aminoethyl)pyridine
5-bromosalicyclaldehyde
N-(pyridine-2-ylethyl)-2-hydroxy-5-bromo-benzylideneamine
Conditions | Yield |
---|---|
In methanol for 5h; Reflux; | 98% |
In methanol Reflux; | 52% |
In methanol for 3h; Reflux; |
Conditions | Yield |
---|---|
With triethylamine In acetonitrile for 12h; Inert atmosphere; Reflux; | 98% |
2-(aminoethyl)pyridine
2,9‐bis(4-formylphenyl)‐1,10‐phenanthroline
Conditions | Yield |
---|---|
In toluene at 20℃; for 24h; Molecular sieve; | 98% |
2-(aminoethyl)pyridine
terephthalaldehyde,
(2-Pyridin-2-yl-ethyl)-[1-(4-{[(E)-2-pyridin-2-yl-ethylimino]-methyl}-phenyl)-meth-(E)-ylidene]-amine
Conditions | Yield |
---|---|
In ethanol Heating; | 97% |
In benzene at 20℃; for 24h; |
2-(aminoethyl)pyridine
o-hydroxyacetophenone
N-(2-hydroxyacetophenonyl)-2-iminoethylpyridine
Conditions | Yield |
---|---|
With 4 A molecular sieve In methanol for 0.5h; | 97% |
In ethanol Reflux; |
2-(aminoethyl)pyridine
Isopropyl isocyanate
1-isopropyl-3-(2-pyridylethyl)urea
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 2h; Addition; | 97% |
Conditions | Yield |
---|---|
With triethylamine In dichloromethane | 97% |
With triethylamine In dichloromethane at 20℃; for 20h; | 97% |
Conditions | Yield |
---|---|
In methanol; water addn. of methanolic soln. of 1 equiv. of pyridine deriv. into hot methanolic soln. of 1 equiv. of cadmium compd., addn. of aq. soln. of dicyanamide salt, stirring for 2 h; filtration, keeping in desiccator with CaCl2 for few wks., isolation of crystals, elem. anal.; | A 97% B 0% |
2-(aminoethyl)pyridine
4-chloro-2-(3,4-difluorophenyl)pyrimidine-5-carboxylic acid ethyl ester
ethyl 2-(3,4-difluorophenyl)-4-(2-(pyridin-2-yl)ethylamino)pyrimidine-5-carboxylate
Conditions | Yield |
---|---|
With triethylamine In N,N-dimethyl-formamide at 20℃; for 0.5h; | 97% |
2-(aminoethyl)pyridine
5-Nitrosalicylaldehyde
N-(pyridine-2-ylethyl)-2-hydroxy-5-nitro-benzylideneamine
Conditions | Yield |
---|---|
In methanol for 5h; Reflux; | 97% |
In methanol Reflux; | 86% |
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In chloroform for 48h; Reflux; | 97% |
With magnesium sulfate In chloroform at 20℃; for 4h; Inert atmosphere; | 90% |
2-(aminoethyl)pyridine
dimethyl 1-[3-(diethoxyphosphoryl)ethyl]-1H-1,2,3-triazole-4,5-dicarboxylate
diethyl [2-[4,5-bis[[[2-(2-pyridinyl)ethyl]amino]carbonyl]-1H-1,2,3-triazol-1-yl]ethyl]phosphonate
Conditions | Yield |
---|---|
In methanol at 20℃; for 14h; | 97% |
Conditions | Yield |
---|---|
With magnesium sulfate In chloroform at 20℃; for 4h; Inert atmosphere; | 97% |
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