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inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
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inquiryLower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
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inquiryAnsciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
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inquiry4-prop-2-enoxybenzoic Acid Application:4-prop-2-enoxybenzoic Acid
We are committed to providing our customers with the best products and services at the most competitive prices.Appearance:white powder Storage:Room temperature with sealed well Package:according to the clients requirement Application:Use as primary a
Best quality with low price Storage:ln stock Package:25kg/Barrel Application:Chemicals Transportation:Express/Sea/Air Port:Shanghai
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inquiryWe are a trading company aiming at providing high-quality services to customers. Established for many years, with good reputation in the industry Storage:Sealed and preserved Application:Fine chemical intermediates, used as the main raw material for
allyl (4-allyloxy)benzoate
4-allyloxybenzoic acid
Conditions | Yield |
---|---|
With 2,2'-azobis(isobutyronitrile) In benzene at 65 - 70℃; for 3h; | 100% |
Stage #1: allyl (4-allyloxy)benzoate With sodium hydroxide for 3h; Heating; Stage #2: With hydrogenchloride at 20℃; pH=3; Further stages.; | 97% |
With sodium hydroxide In water for 6h; Reflux; | 95% |
With potassium hydroxide In methanol at 20℃; | 83% |
4-(2-propenyloxy)benzaldehyde
4-allyloxybenzoic acid
Conditions | Yield |
---|---|
With 2-methyl-but-2-ene; polymer-supported chlorite; acetic acid In tert-butyl alcohol at 25℃; | 98% |
With copper acetylacetonate; oxygen; sodium hydroxide; 1,3-bis(2,4,6-trimethylphenyl)-2-imidazolidinylidene In water at 50℃; under 760.051 Torr; for 12h; Sealed tube; | 93% |
With 4H3N*4H(1+)*CuMo6O18(OH)6(4-); water; oxygen; sodium carbonate at 50℃; under 760.051 Torr; for 12h; | 90% |
allyl bromide
2'-(trimethylsilyl)ethyl-4-hydroxybenzoate
4-allyloxybenzoic acid
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide at 20℃; | 95% |
4-allyloxybenzoic acid
Conditions | Yield |
---|---|
With sodium hydrogen sulfate; silica gel In dichloromethane at 20℃; for 4h; | 94% |
With cerium(III) chloride; sodium iodide In acetonitrile for 2h; Heating; | 87% |
allyl (4-allyloxy)benzoate
A
4-allyloxybenzoic acid
B
4-hydroxy-benzoic acid
Conditions | Yield |
---|---|
With aniline; (ϖ-allyl)palladium triflate based catalyst In toluene at 30℃; for 0.5h; | A 92% B 8% |
Conditions | Yield |
---|---|
With n-Bu4POH In tetrahydrofuran; water at 0 - 20℃; | 91% |
Stage #1: allyl bromide; 4-hydroxy-benzoic acid With potassium carbonate In N,N-dimethyl-formamide at 60℃; for 3h; Stage #2: With sodium hydroxide In 1,4-dioxane; water at 60℃; for 0.25h; | 91% |
With potassium carbonate In N,N-dimethyl-formamide at 40℃; for 10h; | 91% |
Conditions | Yield |
---|---|
With n-Bu4POH In tetrahydrofuran; water at 0 - 20℃; | 86% |
methyl 4-allyloxybenzoate
4-allyloxybenzoic acid
Conditions | Yield |
---|---|
With sodium hydroxide In 1,4-dioxane; water Reflux; | 85.4% |
With sodium hydroxide In methanol; water for 1.5h; Reflux; | 51% |
With sodium hydroxide In tetrahydrofuran; methanol; ethyl acetate | 50% |
With sodium hydroxide In tetrahydrofuran; methanol; ethyl acetate | 50% |
With sodium hydroxide In methanol |
4-allyloxy-benzonitrile
4-allyloxybenzoic acid
Conditions | Yield |
---|---|
Stage #1: 4-allyloxy-benzonitrile With water; sodium hydroxide In ethanol at 20 - 110℃; Sealed; Stage #2: With hydrogenchloride In ethanol; dichloromethane; water pH=1; | 85% |
Stage #1: 4-allyloxy-benzonitrile With sodium hydroxide In ethanol; water at 20 - 110℃; Stage #2: With hydrogenchloride; water In ethanol; dichloromethane pH=1; | 85% |
ethyl 4-(n-prop-2'-enyloxy)benzoate
4-allyloxybenzoic acid
Conditions | Yield |
---|---|
With sodium hydroxide In ethanol; water Heating; | 82% |
With potassium carbonate | |
Stage #1: ethyl 4-(n-prop-2'-enyloxy)benzoate With potassium hydroxide In ethanol for 4h; Reflux; Stage #2: With hydrogenchloride In water |
4-allyloxybenzoic acid
Conditions | Yield |
---|---|
With oxygen; sodium methylate; silver trifluoromethanesulfonate In tetrahydrofuran; methanol at 37℃; under 760.051 Torr; for 12h; Sealed tube; | 77% |
4-allyloxybenzyl alcohol
A
4-(2-propenyloxy)benzaldehyde
B
4-allyloxybenzoic acid
Conditions | Yield |
---|---|
With 2.9-dimethyl-1,10-phenanthroline; oxygen; sodium hydrogencarbonate; gold(I) chloride In water at 100℃; under 38002.6 Torr; for 24h; | A 49% B 35% |
Ethyl 4-hydroxybenzoate
4-allyloxybenzoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 81 percent / K2CO3 / ethanol / Heating 2: 82 percent / NaOH / H2O; ethanol / Heating View Scheme | |
Multi-step reaction with 2 steps 1: alcoholic KOH-solution / 120 - 130 °C / Destillation des Reaktionsprodukts 2: aqueous potash View Scheme | |
Multi-step reaction with 2 steps 1: potassium carbonate / acetonitrile / 10 h / 85 °C / Reflux 2: potassium hydroxide / ethanol; water / 5 h / 105 °C / Reflux View Scheme |
4-cyanophenol
4-allyloxybenzoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 0 °C 1.2: 5 h / 20 °C 2.1: sodium hydroxide; water / ethanol / 20 - 110 °C / Sealed 2.2: pH 1 View Scheme | |
Multi-step reaction with 2 steps 1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 0 °C 1.2: 5 h / 20 °C 2.1: sodium hydroxide / ethanol; water / 20 - 110 °C 2.2: pH 1 View Scheme |
allyl bromide
4-hydroxy-benzoic acid
A
4-allyloxybenzoic acid
B
allyl (4-allyloxy)benzoate
Conditions | Yield |
---|---|
With sodium hydroxide In ethanol; water Reflux; | A 305 mg B 570 mg |
4-hydroxy-benzoic acid
4-allyloxybenzoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: potassium carbonate / N,N-dimethyl-formamide / 16 h / 20 °C 2: potassium hydroxide / methanol / 20 °C View Scheme | |
Multi-step reaction with 2 steps 1.1: potassium carbonate / N,N-dimethyl-formamide / 17.5 h / 40 - 70 °C 1.2: 1 h / 70 °C 2.1: sodium hydroxide / water / 6 h / Reflux View Scheme |
methyl 4-hydroxylbenzoate
4-allyloxybenzoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: potassium carbonate / butanone / 24 h / Reflux 2: sodium hydroxide / water; methanol / 1.5 h / Reflux View Scheme | |
Multi-step reaction with 2 steps 1: potassium carbonate / N,N-dimethyl-formamide / 80 °C 2: sodium hydroxide / water; 1,4-dioxane / Reflux View Scheme |
Conditions | Yield |
---|---|
Stage #1: Ethyl 4-hydroxybenzoate; allyl bromide With potassium carbonate In acetone for 24h; Reflux; Inert atmosphere; Stage #2: With sodium hydroxide In diethyl ether |
4-allyloxybenzoic acid
4-allyloxybenzoyl chloride
Conditions | Yield |
---|---|
With thionyl chloride at 20 - 55℃; for 7h; | 98% |
With oxalyl dichloride In dichloromethane at 20℃; for 3h; | 91% |
With thionyl chloride; N,N-dimethyl-formamide 1) room temperature, overnight, 2) 60 deg C, 2 h; | 90% |
4-allyloxybenzoic acid
4-hydroxy-benzaldehyde
4-(4-allyloxyphenylcarboxy)benzaldehyde
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In dichloromethane for 4h; Ambient temperature; | 95% |
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 0 - 20℃; for 4.5h; | 95% |
Stage #1: 4-allyloxybenzoic acid; 4-hydroxy-benzaldehyde With dmap In N,N-dimethyl-formamide at 20℃; for 0.25h; Stage #2: With dicyclohexyl-carbodiimide In N,N-dimethyl-formamide at 20℃; | 81.8% |
4-allyloxybenzoic acid
4-hydroxy-benzoic acid
Conditions | Yield |
---|---|
With cerium(III) chloride; sodium iodide In acetonitrile for 4h; deallylation; Heating; | 93% |
With cerium(III) chloride; sodium iodide In acetonitrile for 20h; Heating; | 13 % Chromat. |
cholesterol
4-allyloxybenzoic acid
cholesteryl 4-(2-propenyloxy)benzoate
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 20℃; for 24h; | 91% |
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane for 8h; Reflux; | 25% |
With dmap; dicyclohexyl-carbodiimide Steglich Esterification; | |
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 20℃; |
4-allyloxybenzoic acid
4-methoxy-phenol
<4-(allyloxy)benzoyloxy>-4-methoxybenzene
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 20℃; for 24h; | 91% |
With dmap; dicyclohexyl-carbodiimide In dichloromethane at 20℃; for 24h; Inert atmosphere; | 72% |
With dmap; dicyclohexyl-carbodiimide Steglich Esterification; |
4-allyloxybenzoic acid
meta-hydroxybenzaldehyde
Conditions | Yield |
---|---|
Stage #1: 4-allyloxybenzoic acid; meta-hydroxybenzaldehyde With dmap In N,N-dimethyl-formamide at 20℃; for 0.25h; Stage #2: With dicyclohexyl-carbodiimide In N,N-dimethyl-formamide at 20℃; | 90.9% |
2-(4-hydroxyphenyl)benzoxazole
4-allyloxybenzoic acid
Conditions | Yield |
---|---|
Stage #1: 4-allyloxybenzoic acid With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In tetrahydrofuran at 20℃; for 0.25h; Stage #2: 2-(4-hydroxyphenyl)benzoxazole In tetrahydrofuran at 20℃; for 3h; | 87.4% |
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In tetrahydrofuran at 0 - 20℃; for 4h; | 85% |
4-allyloxybenzoic acid
A
4-propoxybenzoic acid
B
4-hydroxy-benzoic acid
Conditions | Yield |
---|---|
With potassium hydroxide In methanol at 20℃; for 10h; | A 3% B 82% |
1,3,5-tri-O-benzylphloroglucinol
4-allyloxybenzoic acid
4'-allyloxy-2,4,6-tribenzyloxybenzophenone
Conditions | Yield |
---|---|
Stage #1: 4-allyloxybenzoic acid With trifluoroacetic anhydride In dichloromethane at 0℃; Stage #2: 1,3,5-tri-O-benzylphloroglucinol In dichloromethane at 20℃; for 48h; | 82% |
Conditions | Yield |
---|---|
Stage #1: 4-allyloxybenzoic acid With 1-hydroxy-pyrrolidine-2,5-dione; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In N,N-dimethyl-formamide at 20℃; for 1h; Stage #2: 3-Amino-1,2-propanediol In N,N-dimethyl-formamide at 20℃; | 82% |
Conditions | Yield |
---|---|
With dmap; dicyclohexyl-carbodiimide In tetrahydrofuran at 30℃; for 24h; | 79% |
N-hydroxyphthalimide
4-allyloxybenzoic acid
Conditions | Yield |
---|---|
With dicyclohexyl-carbodiimide In ethyl acetate at 20℃; for 3h; Inert atmosphere; | 78% |
4-allyloxybenzoic acid
Conditions | Yield |
---|---|
Stage #1: (Z)-4-(cyclopentyloxy)-N’-hydroxybenzimidamide With 1,1'-carbonyldiimidazole In N,N-dimethyl-formamide at 50 - 100℃; for 0.25h; Stage #2: 4-allyloxybenzoic acid In tetrahydrofuran; N,N-dimethyl-formamide at 100℃; for 14h; | 78% |
2-((trifluoromethyl)thio)isoindoline-1,3-dione
4-allyloxybenzoic acid
Conditions | Yield |
---|---|
With iron(III) chloride; triphenylphosphine In tetrahydrofuran at 20℃; for 0.5h; | 75% |
3,3,3-trifluoro-2-phenylpropene
4-allyloxybenzoic acid
Conditions | Yield |
---|---|
With [4,4’-bis(1,1-dimethylethyl)-2,2’-bipyridine-N1,N1‘]bis [3,5-difluoro-2-[5-(trifluoromethyl)-2-pyridinyl-N]phenyl-C]iridium(III) hexafluorophosphate; sodium hydrogencarbonate; triphenylphosphine In N,N-dimethyl-formamide at 20℃; for 48h; Molecular sieve; Inert atmosphere; Sealed tube; Irradiation; | 74% |
2-(3-hydroxyphenyl)-1,3-benzoxazole
4-allyloxybenzoic acid
Conditions | Yield |
---|---|
Stage #1: 4-allyloxybenzoic acid With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In tetrahydrofuran at 20℃; for 0.25h; Stage #2: 2-(3-hydroxyphenyl)-1,3-benzoxazole In tetrahydrofuran at 20℃; for 3h; | 73.6% |
1-(4-hydroxyphenyl)piperazine
4-allyloxybenzoic acid
Conditions | Yield |
---|---|
Stage #1: 4-allyloxybenzoic acid With dmap; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine In N,N-dimethyl-formamide for 0.25h; Stage #2: 1-(4-hydroxyphenyl)piperazine In N,N-dimethyl-formamide at 20℃; for 12h; | 72% |
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