Our Advantage Rich Experience Our products are sold all over Europe,North&South America, Sino-East, Asia and pacific area as well as Africa,we establish long term. Quality service Company cooperates with research institutes. We strictly con
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inquiryAs a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem’s R&D center offer custom synthesis according to the contract research and development services for the fine chemicals, ph
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inquiry2-Mercaptobenzaldehyde CAS:29199-11-9 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic in
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquiryOur Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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inquiryMassive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
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inquiryWe are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov
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inquiry1. Product advantages High purity, all above 98.5%, no impurities after dissolution We will test each batch to ensure quality OEM and private brand services designed for free Various cap colors available We can also provide MT1 peptide powd
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inquiryOur Advantages A. International Top level TechnologyOur company owned biomedicine experts are famous at home and abroad with rich experience in research and development in the field of efficient chiral functional molecules research and development an
factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
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inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
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inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
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inquiryGOLDEN PHARMA CO.,LIMITED.is a professional pharmaceutical company,our team have more than 20years expereince in pharmaceutical production and sales. we are a professional technical enterprise specializing in the R & D, production,QA regulation
We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp
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inquiryLower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
R & D enterprises have their own stock in stock Package:1kg Application:pharmaceutical intermediates
J&H CHEM is one of China's leading providers of integrated fine chemical services including offering, research and development, Custom manufacturing business, as well as other Value-added customer services, for diversified range products of chemicals
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inquiryAnsciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
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inquiry2-Mercaptobenzaldehyde Application:2-Mercaptobenzaldehyde
We are committed to providing our customers with the best products and services at the most competitive prices.Appearance:white powder Storage:Room temperature with sealed well Package:according to the clients requirement Application:Use as primary a
2-MERCAPTOBENZALDEHYDEAppearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
Hangzhou ZeErRui Chemical Co., Ltd. is focused on customization, research and development and production of APIs and advanced intermediates, which can effectively compensate for the deficiencies of traditional CRO and CMO. Priority of high-tech barri
29199-11-9 Application:intermediate
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inquiry2,2'-dithiodibenzaldehyde
2-formylthiophenol
Conditions | Yield |
---|---|
With tris-(2-carboxyethyl)-phosphine hydrochloride In dimethyl sulfoxide | 100% |
With triphenylphosphine In methanol; water; N,N-dimethyl-formamide 1.) room temp., 30 min; 2.) ice-water bath, 30 min; | 80% |
With water; triphenylphosphine In methanol; N,N-dimethyl-formamide at 20℃; for 0.5h; | 80% |
o-hydroxymethyl thiophenol
2-formylthiophenol
Conditions | Yield |
---|---|
With dihydrogen peroxide In neat (no solvent) at 80℃; for 4h; Green chemistry; | 100% |
Multi-step reaction with 2 steps 1: 54 percent / pyridinium chlorochromate / CH2Cl2 / 4 h / 20 °C 2: 80 percent / triphenylphosphine; water / methanol; dimethylformamide / 0.5 h / 20 °C View Scheme | |
Multi-step reaction with 2 steps 1: 54 percent / PCC / CH2Cl2 / 4 h / Ambient temperature 2: 80 percent / Ph3P / dimethylformamide; H2O; methanol / 1.) room temp., 30 min; 2.) ice-water bath, 30 min View Scheme |
2-(2-bromophenyl)-1,3-dioxolan
2-formylthiophenol
Conditions | Yield |
---|---|
Stage #1: 2-(2-bromophenyl)-1,3-dioxolan With magnesium In tetrahydrofuran at 0℃; for 1h; Reflux; Stage #2: With sulfur In tetrahydrofuran at 20℃; Stage #3: With hydrogenchloride; water In tetrahydrofuran; water for 2h; Reflux; | 91% |
Conditions | Yield |
---|---|
Stage #1: thiophenol With n-butyllithium; N,N,N,N,-tetramethylethylenediamine Stage #2: N,N-dimethyl-formamide | 83% |
Stage #1: thiophenol With n-butyllithium; N,N,N,N,-tetramethylethylenediamine In hexane Stage #2: N,N-dimethyl-formamide In hexane | 66% |
Stage #1: thiophenol With n-butyllithium; N,N,N,N,-tetramethylethylenediamine In hexane at 0 - 20℃; for 16h; Inert atmosphere; Stage #2: N,N-dimethyl-formamide In hexane at 0 - 20℃; for 20h; Inert atmosphere; | 48% |
o-Thioacetoxybenzaldehyde
2-formylthiophenol
Conditions | Yield |
---|---|
With titanium tetrachloride; zinc In dichloromethane at 25℃; for 0.166667h; | 82% |
o-rhodano-benzaldehyde
2-formylthiophenol
Conditions | Yield |
---|---|
With sodium hydroxide for 0.0833333h; | 70% |
With sodium sulfide; water das Natriumsalz entsteht; |
2-hydroxy-5-phenylcyclohex-1-enecarbaldehyde
A
mer-hydrido(1-carbonyl-2-oxo-5-phenylyclohexenediyl)tris(trimethylphosphine)cobalt(III)
B
2-formylthiophenol
Conditions | Yield |
---|---|
In diethyl ether at -80 - 20℃; for 14h; Mechanism; Inert atmosphere; Schlenk technique; | A 69% B n/a |
ethyl 2-sulfanylacetate
ortho-bromobenzaldehyde
A
ethyl benzo[b]thiophene-2-carboxylate
B
2-formylthiophenol
Conditions | Yield |
---|---|
With potassium tert-butylate In ammonia for 180h; Irradiation; | A 55% B 10% |
With potassium tert-butylate 1.) NH3, irradiation, 180 min,; Yield given. Multistep reaction. Yields of byproduct given; |
Conditions | Yield |
---|---|
With triphenylphosphine In chloroform at 20℃; for 96h; | A 9% B 52% C 33.5% |
2-[(phenylmethyl)thio]benzaldehyde
2-formylthiophenol
Conditions | Yield |
---|---|
Stage #1: 2-[(phenylmethyl)thio]benzaldehyde With aluminum (III) chloride In benzene at 20℃; for 48.5h; Inert atmosphere; Stage #2: With water In benzene Cooling with ice; | 24% |
A
2-formylthiophenol
B
S-(2-formylphenyl) N,N-dimethylthiocarbamate
Conditions | Yield |
---|---|
In 1-methyl-pyrrolidin-2-one at 230℃; for 15h; Miyazaki-Newman-Kwart rearrangement; Microwave irradiation; | A 10% B n/a |
2-mercapto-N-methyl-N-phenylbenzamide
2-formylthiophenol
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride |
Conditions | Yield |
---|---|
With n-butyllithium; N,N,N,N,-tetramethylethylenediamine 1.) hexane, a) 0 deg C, 0.5 h, b) RT, 17 h, 2.) hexane, 25 deg C, 18 h; Yield given; Multistep reaction; |
Thiosalicylic acid
2-formylthiophenol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 96 percent / LiAlH4 / tetrahydrofuran / 20 °C 2: 54 percent / pyridinium chlorochromate / CH2Cl2 / 4 h / 20 °C 3: 80 percent / triphenylphosphine; water / methanol; dimethylformamide / 0.5 h / 20 °C View Scheme | |
With lithium aluminium tetrahydride In tetrahydrofuran at 0℃; Reflux; | |
Multi-step reaction with 3 steps 1: lithium aluminium tetrahydride / tetrahydrofuran / 24 h / 20 °C / Inert atmosphere 2: pyridinium chlorochromate / dichloromethane / 4 h / 20 °C / Inert atmosphere 3: triphenylphosphine / water; N,N-dimethyl-formamide; methanol / 0.5 h / 20 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 3 steps 1: lithium aluminium tetrahydride / tetrahydrofuran / 20 °C 2: pyridinium chlorochromate / dichloromethane / 5 h / 20 °C 3: tris-(2-carboxyethyl)-phosphine hydrochloride / dimethyl sulfoxide View Scheme | |
Multi-step reaction with 3 steps 1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C 2: pyridinium chlorochromate / dichloromethane / 20 °C 3: triphenylphosphine / methanol; N,N-dimethyl-formamide; water / 1 h / 0 - 20 °C View Scheme |
1,2-bis(2-(hydroxymethyl)phenyl)disulfane
2-formylthiophenol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 16 percent / PCC 2: 80 percent / Ph3P / dimethylformamide; H2O; methanol / 1.) room temp., 30 min; 2.) ice-water bath, 30 min View Scheme | |
With triphenylphosphine In methanol; water; N,N-dimethyl-formamide for 1h; |
2-aminobenzaldehyde
2-formylthiophenol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 1) sodium nitrite / 1) sulphuric acid, water, 0 deg C, 2) water, room temp., 1 h, 60 deg C, 30 min 2: 70 percent / sodium hydroxide / 0.08 h View Scheme | |
Multi-step reaction with 2 steps 1: Diazotization.durch Umsetzung mit CuCNS 2: sodium sulfide; water / das Natriumsalz entsteht View Scheme |
2-formylthiophenol
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 2: Diazotization.durch Umsetzung mit CuCNS 3: sodium sulfide; water / das Natriumsalz entsteht View Scheme |
2-Fluorobenzaldehyde
2-formylthiophenol
Conditions | Yield |
---|---|
With sodium sulfide |
2-chloro-benzaldehyde
2-formylthiophenol
Conditions | Yield |
---|---|
With sodium sulfide nonahydrate In N,N-dimethyl acetamide at 80℃; for 0.5h; Inert atmosphere; | |
Multi-step reaction with 3 steps 1.1: potassium hydroxide / dimethyl sulfoxide / 0.33 h / 20 °C / Inert atmosphere 1.2: 1.5 h / 110 °C / Inert atmosphere 2.1: acetic acid; hydrogen bromide; dimethyl sulfoxide / water / 20 °C / Cooling with ice 3.1: triphenylphosphine / tetrahydrofuran / 0.33 h / 20 °C / Inert atmosphere 3.2: 0.17 h / Inert atmosphere View Scheme |
salicylaldehyde
2-formylthiophenol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: potassium carbonate / acetonitrile / 0.17 h / 20 °C / Inert atmosphere 1.2: 24 h / 80 °C / Inert atmosphere 2.1: 1-methyl-pyrrolidin-2-one / 15 h / 230 °C / Microwave irradiation View Scheme |
ortho-bromobenzaldehyde
2-formylthiophenol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: toluene-4-sulfonic acid / toluene / Dean-Stark 2.1: magnesium / tetrahydrofuran / 1 h / 0 °C / Reflux 2.2: 20 °C 2.3: 2 h / Reflux View Scheme |
2-(tert-butylthio)benzaldehyde
2-formylthiophenol
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: acetic acid; hydrogen bromide; dimethyl sulfoxide / water / 20 °C / Cooling with ice 2.1: triphenylphosphine / tetrahydrofuran / 0.33 h / 20 °C / Inert atmosphere 2.2: 0.17 h / Inert atmosphere View Scheme |
Conditions | Yield |
---|---|
Stage #1: 2,2'-dithiodibenzaldehyde With triphenylphosphine In tetrahydrofuran at 20℃; for 0.333333h; Inert atmosphere; Stage #2: acrylonitrile In tetrahydrofuran for 0.166667h; Inert atmosphere; |
2-formylthiophenol
2,2'-dithiodibenzaldehyde
Conditions | Yield |
---|---|
With triethylamine; phenylacetylene; copper(l) iodide In acetonitrile at 20℃; for 8h; | 100% |
With oxygen; SiO2-Cl In dichloromethane at 0℃; for 0.166667h; | 98% |
MoO2Cl2(DMSO)2 In dimethyl sulfoxide at 20℃; for 0.5h; | 91% |
nitrostyrene
2-formylthiophenol
(2R,3R,4S)-3-nitro-2-phenylthiochroman-4-ol
Conditions | Yield |
---|---|
With 2-{[(1S)-N-{[(4S,5S)-4,5-dihydro-4,5-diphenyl-1-tosyl-1H-imidazol-2-yl]methyl}-1-phenylethanamino]methyl}-4,6-dibromophenol; nickel(II) acetate tetrahydrate In toluene at -40 - 20℃; for 15h; Solvent; Temperature; Reagent/catalyst; Inert atmosphere; enantioselective reaction; | 99% |
With 2-{[(1S)-N-{[(4S,5S)-4,5-dihydro-4,5-diphenyl-1-tosyl-1H-imidazol-2-yl]methyl}-1-phenylethanamino]methyl}-4,6-dibromophenol; nickel diacetate In toluene at -40℃; for 15h; | 99% |
1-chloro-4-(2-nitrovinyl)benzene
2-formylthiophenol
(2R,3R,4S)-2-(4-chlorophenyl)-3-nitrothiochroman-4-ol
Conditions | Yield |
---|---|
With 2-{[(1S)-N-{[(4S,5S)-4,5-dihydro-4,5-diphenyl-1-tosyl-1H-imidazol-2-yl]methyl}-1-phenylethanamino]methyl}-4,6-dibromophenol; nickel(II) acetate tetrahydrate In toluene at -40 - 20℃; for 15h; Inert atmosphere; enantioselective reaction; | 99% |
3-chloroβ-nitrostyrene
2-formylthiophenol
(2R,3R,4S)-2-(3-chlorophenyl)-3-nitrothiochroman-4-ol
Conditions | Yield |
---|---|
With 2-{[(1S)-N-{[(4S,5S)-4,5-dihydro-4,5-diphenyl-1-tosyl-1H-imidazol-2-yl]methyl}-1-phenylethanamino]methyl}-4,6-dibromophenol; nickel(II) acetate tetrahydrate In toluene at -40 - 20℃; for 15h; Inert atmosphere; enantioselective reaction; | 99% |
4-bromo-β-nitrostyrene
2-formylthiophenol
(2R,3R,4S)-2-(4-bromophenyl)-3-nitrothiochroman-4-ol
Conditions | Yield |
---|---|
With 2-{[(1S)-N-{[(4S,5S)-4,5-dihydro-4,5-diphenyl-1-tosyl-1H-imidazol-2-yl]methyl}-1-phenylethanamino]methyl}-4,6-dibromophenol; nickel(II) acetate tetrahydrate In toluene at -40 - 20℃; for 15h; Inert atmosphere; enantioselective reaction; | 99% |
3-bromo-β-nitro-styrene
2-formylthiophenol
(2R,3R,4S)-2-(3-bromophenyl)-3-nitrothiochroman-4-ol
Conditions | Yield |
---|---|
With 2-{[(1S)-N-{[(4S,5S)-4,5-dihydro-4,5-diphenyl-1-tosyl-1H-imidazol-2-yl]methyl}-1-phenylethanamino]methyl}-4,6-dibromophenol; nickel(II) acetate tetrahydrate In toluene at -40 - 20℃; for 15h; Inert atmosphere; enantioselective reaction; | 99% |
4-fluoro-β-nitrostyrene
2-formylthiophenol
(2R,3R,4S)-2-(4-fluorophenyl)-3-nitrothiochroman-4-ol
Conditions | Yield |
---|---|
With 2-{[(1S)-N-{[(4S,5S)-4,5-dihydro-4,5-diphenyl-1-tosyl-1H-imidazol-2-yl]methyl}-1-phenylethanamino]methyl}-4,6-dibromophenol; nickel(II) acetate tetrahydrate In toluene at -40 - 20℃; for 15h; Inert atmosphere; enantioselective reaction; | 99% |
3-nitro-β-nitrostyrene
2-formylthiophenol
(2S,3R,4R)-3-nitro-2-(3-nitrophenyl)thiochroman-4-ol
Conditions | Yield |
---|---|
With 2-{[(1S)-N-{[(4S,5S)-4,5-dihydro-4,5-diphenyl-1-tosyl-1H-imidazol-2-yl]methyl}-1-phenylethanamino]methyl}-4,6-dibromophenol; nickel(II) acetate tetrahydrate In toluene at -40 - 20℃; for 15h; Inert atmosphere; enantioselective reaction; | 99% |
1-methoxy-3-(2-nitrovinyl)benzene
2-formylthiophenol
(2R,3R,4S)-2-(3-methoxyphenyl)-3-nitrothiochroman-4-ol
Conditions | Yield |
---|---|
With 2-{[(1S)-N-{[(4S,5S)-4,5-dihydro-4,5-diphenyl-1-tosyl-1H-imidazol-2-yl]methyl}-1-phenylethanamino]methyl}-4,6-dibromophenol; nickel(II) acetate tetrahydrate In toluene at -40 - 20℃; for 15h; Inert atmosphere; enantioselective reaction; | 99% |
1-methyl-3-(2-nitrovinyl)benzene
2-formylthiophenol
(2S,3R,4R)-3-nitro-2-(m-tolyl)thiochroman-4-ol
Conditions | Yield |
---|---|
With 2-{[(1S)-N-{[(4S,5S)-4,5-dihydro-4,5-diphenyl-1-tosyl-1H-imidazol-2-yl]methyl}-1-phenylethanamino]methyl}-4,6-dibromophenol; nickel(II) acetate tetrahydrate In toluene at -40 - 20℃; for 15h; Inert atmosphere; enantioselective reaction; | 99% |
1-(2-thienyl)-2-nitroethene
2-formylthiophenol
(2R,3R,4R)-3-nitro-2-(thiophen-2-yl)thiochroman-4-ol
Conditions | Yield |
---|---|
With 2-{[(1S)-N-{[(4S,5S)-4,5-dihydro-4,5-diphenyl-1-tosyl-1H-imidazol-2-yl]methyl}-1-phenylethanamino]methyl}-4,6-dibromophenol; nickel(II) acetate tetrahydrate In toluene at -40 - 20℃; for 15h; Inert atmosphere; enantioselective reaction; | 99% |
3-(2-bromobenzylidene)oxindole
2-formylthiophenol
Conditions | Yield |
---|---|
With 2C2H3O2(1-)*Ni(2+)*C49H45N5 In toluene at -40 - 20℃; for 30h; stereoselective reaction; | 99% |
2-formylthiophenol
3-benzylidene-6-chloroindol-2-one
Conditions | Yield |
---|---|
With 2C2H3O2(1-)*Ni(2+)*C49H45N5 In toluene at -40 - 20℃; for 30h; stereoselective reaction; | 99% |
(E)-1-methoxy-4-(2-nitrovinyl)benzene
2-formylthiophenol
B
(2R,3R,4S)-2-(4-methoxyphenyl)-3-nitrothiochroman-4-ol
Conditions | Yield |
---|---|
With 2-{[(1S)-N-{[(4S,5S)-4,5-dihydro-4,5-diphenyl-1-tosyl-1H-imidazol-2-yl]methyl}-1-phenylethanamino]methyl}-4,6-dibromophenol; nickel diacetate In toluene at -40℃; for 15h; | A n/a B 99% |
2-formylthiophenol
Conditions | Yield |
---|---|
With C31H26F6N4O2 In dichloromethane at 0℃; Solvent; enantioselective reaction; | 99% |
2-formylthiophenol
Conditions | Yield |
---|---|
With C31H26F6N4O2 In dichloromethane at 0℃; enantioselective reaction; | 99% |
2-formylthiophenol
Conditions | Yield |
---|---|
With C31H26F6N4O2 In dichloromethane at 0℃; enantioselective reaction; | 99% |
2-formylthiophenol
Conditions | Yield |
---|---|
With C31H26F6N4O2 In dichloromethane at 0℃; enantioselective reaction; | 99% |
2-formylthiophenol
Conditions | Yield |
---|---|
With C31H26F6N4O2 In dichloromethane at 0℃; enantioselective reaction; | 99% |
2-formylthiophenol
Conditions | Yield |
---|---|
With C31H26F6N4O2 In dichloromethane at 0℃; enantioselective reaction; | 99% |
2-formylthiophenol
Conditions | Yield |
---|---|
With C31H26F6N4O2 In dichloromethane at 0℃; enantioselective reaction; | 99% |
2-formylthiophenol
Conditions | Yield |
---|---|
With C31H26F6N4O2 In dichloromethane at 0℃; enantioselective reaction; | 99% |
2-formylthiophenol
Conditions | Yield |
---|---|
With C31H26F6N4O2 In dichloromethane at 0℃; enantioselective reaction; | 99% |
2-formylthiophenol
Conditions | Yield |
---|---|
With C31H26F6N4O2 In dichloromethane at 0℃; enantioselective reaction; | 99% |
2-formylthiophenol
Conditions | Yield |
---|---|
With C31H26F6N4O2 In dichloromethane at 0℃; enantioselective reaction; | 99% |
2-formylthiophenol
Conditions | Yield |
---|---|
With C31H26F6N4O2 In dichloromethane at 0℃; enantioselective reaction; | 99% |
2-formylthiophenol
Conditions | Yield |
---|---|
With C31H26F6N4O2 In dichloromethane at 0℃; enantioselective reaction; | 99% |
2-formylthiophenol
Conditions | Yield |
---|---|
With C31H26F6N4O2 In dichloromethane at 0℃; enantioselective reaction; | 99% |
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