Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
Cas:623-51-8
Min.Order:1 Kilogram
FOB Price: $3.0
Type:Lab/Research institutions
inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
Cas:623-51-8
Min.Order:1 Metric Ton
Negotiable
Type:Manufacturers
inquiryUnique advantages of Ethyl Thioglycolate Cas 623-51-8 Guaranteed purity High quality & competitive price Quality control Fast feedback Prompt shipment Appearance:Colorless liquid Storage:Cool dry place Package:25kg/drum,200kg/drum
Cas:623-51-8
Min.Order:25 Kilogram
Negotiable
Type:Trading Company
inquiryhe company has advanced technology, as well as a large number of excellent R & D team, to provide customers from the grams to one hundred kilograms and tons of high-quality products, competitive prices and quality se T rvice Appearance:Whit
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
Cas:623-51-8
Min.Order:1 Gram
FOB Price: $0.1
Type:Manufacturers
inquiryOur main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block
Cas:623-51-8
Min.Order:5 Kiloliter
FOB Price: $1.2 / 5.0
Type:Manufacturers
inquiryETHYL THIOGLYCOLATE Basic information Product Name: ETHYL THIOGLYCOLATE Synonyms: THIOGLYCOLLIC ACID ETHYL ESTER;THIOGLYCOLIC ACID ETHYL ESTER;Ethyl alpha-mercaptoacetate;Ethyl mercaptoa
Cas:623-51-8
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryOur advantages: 1. High quality and competitive price: 1) Standard: BP/USP/EP/ enterprise standard 2) All purity ≥99% 3) We are manufacturers and can provide high quality products at factory prices. 2. Fast and safe delivery 1) The package c
Cas:623-51-8
Min.Order:1 Kilogram
FOB Price: $5.0 / 10.0
Type:Trading Company
inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:623-51-8
Min.Order:1 Kilogram
FOB Price: $139.0 / 210.0
Type:Trading Company
inquiry1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:623-51-8
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryETHYL THIOGLYCOLATE CAS:623-51-8 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic interme
Cas:623-51-8
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:623-51-8
Min.Order:1 Kilogram
Negotiable
Type:Lab/Research institutions
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det
Cas:623-51-8
Min.Order:0 Metric Ton
Negotiable
Type:Lab/Research institutions
inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:623-51-8
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquirySuperior quality, moderate price & quick delivery. Appearance:Colorless liquid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per your request. Application:Pharmaceutical
Cas:623-51-8
Min.Order:1 Gram
Negotiable
Type:Trading Company
inquiryEstablished in May 2015, TaiChem Ltd. is initially invested by a British research and development company and started by PhDs back from aboard. The company is registered in China Medical City (CMC), Taizhou, Jiangsu Province, and the production site
Cas:623-51-8
Min.Order:10 Gram
Negotiable
Type:Lab/Research institutions
inquiryETHYL THIOGLYCOLATE Chemical Properties Melting point -80 °C Boiling point 54 °C/12 mmHg (lit.) density 1.096 g/mL at 25 °C (lit.) refractive index n20/D 1.457(lit.) Fp 118 °F storage temp. Flammables area pka
Cas:623-51-8
Min.Order:1 Gram
FOB Price: $66.0
Type:Lab/Research institutions
inquiryAppearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea
SAGECHEM is a chemical R&D, manufacturing and distribution company in China since 2009, including pharmaceutical intermediates, agrochemical, dyestuff intermediates, organosilicone, API and etc. We also offer a full range of services in custom synthe
Cas:623-51-8
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryStock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai
Cas:623-51-8
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryName: Ethyl thioglycolate CASNo. 623-51-8 EINECS No. 210-800-3 MF C4H8O2S Appearance:Colorless transparent liquid, Storage: Preserve in well-closed, light-resis
high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
R & D enterprises have their own stock in stockAppearance:To be subject to the object Package:Customized Application:pharmaceutical intermediates Transportation:Air Port:Shanghai;Guangzhou
high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,or Intermediates,fine chemicals Transportation:air,sea,courier
Acmec is a leading manufacturer and supplier of biochemical reagents and life science products. We have over 40,000 items in stock (real-time inventory) and offer discounted prices to registered members of the online store ( www.acmec.com.cn ) Appea
Cas:623-51-8
Min.Order:1 bottle
Negotiable
Type:Lab/Research institutions
inquiryOur clients, like BASF,CHEMO,Brenntag,ASR,Evonik,Merck and etc.Appearance:COA Storage:in stock Application:MSDS/TDS
TAIHO Unique Advantages:1.We're factory2.Free samples available3.Commodity inspection can be done4.ISO9001,Kosher certifications5.10 years experiences Storage:Store in cool &dry place Package:aluminium foil bag/fiber can/plastic drum Application:comp
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In chloroform esterified azeotropically; | 72% |
With LEWATIT K2621 In toluene for 72h; Heating; | 58% |
With magnesium sulfate; toluene-4-sulfonic acid for 16h; Inert atmosphere; Reflux; | 36% |
thiocyanato-acetic acid ethyl ester
1-(ethoxycarbonylmethyl)pyridinium chloride
A
pyridinium cyanoi(ethoxycarbonyl)methylide
B
ethyl 2-sulfanylacetate
Conditions | Yield |
---|---|
With potassium carbonate In chloroform Ambient temperature; | A 63% B n/a |
thiocyanato-acetic acid ethyl ester
1-(2-oxopropyl)pyridinium chloride
A
Cyano-acetyl-pyridinium-methylid
B
ethyl 2-sulfanylacetate
Conditions | Yield |
---|---|
With potassium carbonate In chloroform Ambient temperature; | A 58% B n/a |
thiocyanato-acetic acid ethyl ester
1-ethoxycarbonylmethyl-4-methylpyridinium chloride
A
C11H12N2O2
B
ethyl 2-sulfanylacetate
Conditions | Yield |
---|---|
With potassium carbonate In chloroform Ambient temperature; | A 53% B n/a |
thiocyanato-acetic acid ethyl ester
1-Ethoxycarbonylmethyl-3,5-dimethyl-pyridinium; chloride
A
C12H14N2O2
B
ethyl 2-sulfanylacetate
Conditions | Yield |
---|---|
With potassium carbonate In chloroform Ambient temperature; | A 51% B n/a |
thiocyanato-acetic acid ethyl ester
1-(2-oxo-2-phenylethyl)pyridin-1-ium chloride
A
1-(1-cyano-2-oxo-2-phenyl-ethyl)-pyridinium betaine
B
ethyl 2-sulfanylacetate
Conditions | Yield |
---|---|
With potassium carbonate In chloroform Ambient temperature; | A 45% B n/a |
thiocyanato-acetic acid ethyl ester
1-acetonyl-3,5-dimethylpyridinium chloride
A
ethyl 2-sulfanylacetate
Conditions | Yield |
---|---|
With potassium carbonate In chloroform Ambient temperature; | A n/a B 42% |
thiocyanato-acetic acid ethyl ester
1-acetonyl-4-methylpyridinium chloride
A
ethyl 2-sulfanylacetate
Conditions | Yield |
---|---|
With potassium carbonate In chloroform Ambient temperature; | A n/a B 40% |
thiocyanato-acetic acid ethyl ester
1-[2-oxo-2-(phenyl)ethyl]-4-methylpyridinium chloride
A
ethyl 2-sulfanylacetate
Conditions | Yield |
---|---|
With potassium carbonate In chloroform Ambient temperature; | A n/a B 37% |
Conditions | Yield |
---|---|
With potassium carbonate In chloroform Ambient temperature; | A n/a B 28% |
thiocyanato-acetic acid ethyl ester
1-(cyanomethyl)-3,5-dimethylpyridinium chloride
A
3,5-dimethylpyridinium dicyanomethylide
B
ethyl 2-sulfanylacetate
Conditions | Yield |
---|---|
With potassium carbonate In chloroform Ambient temperature; | A 18% B n/a |
thiocyanato-acetic acid ethyl ester
A
4-methylpyridinium dicyanomethylide
B
ethyl 2-sulfanylacetate
Conditions | Yield |
---|---|
With potassium carbonate In chloroform Ambient temperature; | A 15% B n/a |
thiocyanato-acetic acid ethyl ester
2-pyridin-1-ium-1-ylacetonitrile chloride
A
pyridinium 1-dicyanomethylide
B
ethyl 2-sulfanylacetate
Conditions | Yield |
---|---|
With potassium carbonate In chloroform Ambient temperature; | A 7% B n/a |
Conditions | Yield |
---|---|
With phosphoric acid beim Destillieren; |
Conditions | Yield |
---|---|
With ethanol; 6-methyl-2,4-dinitrophenol durch Oxydations-Reduktionsfermente im Sonnenlicht bei pH 7.2; |
Conditions | Yield |
---|---|
zerfaellt in der Waerme; |
4,4-diethyl-3,5-dithia-heptanedioic acid diethyl ester
B
ethyl 2-sulfanylacetate
Conditions | Yield |
---|---|
Destillation im Vakuum; | |
Destillation im Vakuum; |
4,4-dipropyl-3,5-dithia-heptanedioic acid diethyl ester
B
ethyl 2-sulfanylacetate
Conditions | Yield |
---|---|
Destillation im Vakuum; |
4,4-dibutyl-3,5-dithia-heptanedioic acid diethyl ester
B
ethyl 2-sulfanylacetate
Conditions | Yield |
---|---|
Destillation im Vakuum; |
formamide
ethyl bromoacetate
ethyl 2-sulfanylacetate
Conditions | Yield |
---|---|
With pyridine; phosphorous (V) sulfide anschliessend Behandeln mit Wasser; |
Conditions | Yield |
---|---|
Veresterung; |
Conditions | Yield |
---|---|
With ethanol; potassium hydrosulfide | |
With hydrosulfide exchange resin (from Amberlite IRA-400); triethylamine hydrochloride In methanol for 1h; Ambient temperature; | 97 % Chromat. |
Conditions | Yield |
---|---|
With ethanol |
1-(ethoxycarbonylmethylthio)-4-methylphthalazine
A
1-methyl-3,4-dihydro-4-oxophthalazine
B
ethyl 2-sulfanylacetate
Conditions | Yield |
---|---|
With hydrogenchloride |
Conditions | Yield |
---|---|
In 1,4-dioxane; water at 25℃; Rate constant; var. pH; |
(1-Hydroxy-2-oxo-2-phenyl-ethylsulfanyl)-acetic acid ethyl ester
A
2,2-dihydroxy-1-phenyl-ethanone
B
ethyl 2-sulfanylacetate
Conditions | Yield |
---|---|
With 1,4-diaza-bicyclo[2.2.2]octane In water; acetonitrile at 30℃; Equilibrium constant; |
thiocyanato-acetic acid ethyl ester
phosphoric acid
water
ethyl 2-sulfanylacetate
2-(acetylthio)acetate ethyl ester
ethyl 2-sulfanylacetate
Conditions | Yield |
---|---|
With water |
A
diethyl 2,2'-disulfanediyldiacetate
B
ethyl 2-sulfanylacetate
C
[5,6]fullerene-C70
Conditions | Yield |
---|---|
at 50℃; Temperature; |
2-chloro-3-pyridinecarbonitrile
ethyl 2-sulfanylacetate
ethyl 3-aminothieno[2,3-b]pyridine-2-carboxylate
Conditions | Yield |
---|---|
Stage #1: ethyl 2-sulfanylacetate With sodium hydride In dimethyl sulfoxide; mineral oil at 20℃; for 0.25h; Stage #2: 2-chloro-3-pyridinecarbonitrile In dimethyl sulfoxide; mineral oil at 20℃; for 3h; | 100% |
With sodium carbonate In ethanol at 90℃; for 2.5h; | 94% |
With sodium carbonate In ethanol for 4.5h; Heating / reflux; | 93.2% |
N,N-Dimethyl-2,4-bis(trifluoroacetyl)-1-naphthylamine
ethyl 2-sulfanylacetate
2-ethoxycarbonyl-5-trifluoroacetyl-3-trifluoromethylnaphtho<1,2-b>thiophene
Conditions | Yield |
---|---|
In acetonitrile for 2h; Heating; | 100% |
3-bromo-2-thiophenecarboxaldehyde
ethyl 2-sulfanylacetate
ethyl thieno[3,2,-b]thiophene-2-carboxylate
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 60 - 70℃; | 100% |
With potassium carbonate In N,N-dimethyl-formamide at 25 - 30℃; Inert atmosphere; Large scale; | 97.9% |
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 72h; | 91% |
2,3-Dichloro-1,4-naphthoquinone
ethyl 2-sulfanylacetate
ethyl 2-(3-chloro-1,4-dioxo-1,4-dihydronaphthalen-2-ylthio)acetate
Conditions | Yield |
---|---|
With water at 50℃; for 2h; | 100% |
In water at 50℃; for 2h; | 100% |
In ethanol at 80 - 90℃; | 97% |
4-chloro-3-cyano-5-fluoropyridine
ethyl 2-sulfanylacetate
3-amino-7-fluoro-thieno[3,2-c]pyridine-2-carboxylic acid ethyl ester
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 0 - 40℃; for 1h; | 100% |
2-fluoro-5-nitrobenzonitrile
ethyl 2-sulfanylacetate
ethyl (3-amino-5-nitrobenzothiophen)-2-carboxylate
Conditions | Yield |
---|---|
With triethylamine In dimethyl sulfoxide | 100% |
Stage #1: ethyl 2-sulfanylacetate With sodium hydride In dimethyl sulfoxide; mineral oil at 20℃; for 0.333333h; Stage #2: 2-fluoro-5-nitrobenzonitrile In dimethyl sulfoxide; mineral oil at 20℃; for 3h; | 93% |
With triethylamine In dimethyl sulfoxide at 20℃; for 3h; | 90% |
1-benzoyl-4-oxo-piperidine-3-carboxylic acid methyl ester
ethyl 2-sulfanylacetate
A
1-benzoyl-4-ethoxycarbonylmethylsulfanyl-1,2,5,6-tetrahydro-pyridine-3-carboxylic acid methyl ester
B
5-benzoyl-3-hydroxy-4,5,6,7-tetrahydro-thieno[3,2-c]pyridine-2-carboxylic acid ethyl ester
Conditions | Yield |
---|---|
In ethanol | A n/a B 100% |
ethyl 2-sulfanylacetate
6-amino-5-bromo-pyridine-2-carboxylic acid methyl ester
methyl 3-oxo-3,4-dihydro-2H-pyrido[3,2-b][1,4]thiazine-6-carboxylate
Conditions | Yield |
---|---|
Stage #1: ethyl 2-sulfanylacetate With sodium hydride In N,N-dimethyl-formamide at 0℃; for 1h; Stage #2: 6-amino-5-bromo-pyridine-2-carboxylic acid methyl ester In N,N-dimethyl-formamide at 20℃; | 100% |
Stage #1: ethyl 2-sulfanylacetate With sodium hydride In N,N-dimethyl-formamide at 0℃; for 1h; Stage #2: 6-amino-5-bromo-pyridine-2-carboxylic acid methyl ester In N,N-dimethyl-formamide at 20℃; for 16h; | |
Stage #1: ethyl 2-sulfanylacetate With sodium hydride In DMF (N,N-dimethyl-formamide) at 0℃; for 1h; Stage #2: 6-amino-5-bromo-pyridine-2-carboxylic acid methyl ester In DMF (N,N-dimethyl-formamide) at 20℃; for 16h; |
allyldimethylethoxysilane
ethyl 2-sulfanylacetate
[3-(ethoxydimethylsilanyl)propylsulfanyl]acetic acid ethyl ester
Conditions | Yield |
---|---|
at 100℃; for 16h; Inert atmosphere; | 100% |
3-bromo-6-(furan-2-yl)pyrazine-2-carbonitrile
ethyl 2-sulfanylacetate
ethyl 7-amino-2-(furan-2-yl)thieno[2,3-b]pyrazine-6-carboxylate
Conditions | Yield |
---|---|
With sodium carbonate In ethanol at 20 - 50℃; for 3h; | 100% |
With sodium carbonate In ethanol at 20 - 50℃; for 3h; | 10% |
3-bromobenzo[b]thiophene-2-carbaldehyde
ethyl 2-sulfanylacetate
ethyl thieno[3,2-b][1]benzothiophene 2-carboxylate
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 50h; | 100% |
With potassium carbonate In N,N-dimethyl-formamide at 0 - 20℃; for 72h; | 92% |
With potassium carbonate In N,N-dimethyl-formamide | |
With potassium carbonate In N,N-dimethyl-formamide |
3-nitro-4-fluorobenzoic acid
ethyl 2-sulfanylacetate
4-ethoxycarbonylmethylsulfanyl-3-nitrobenzoic acid
Conditions | Yield |
---|---|
With sodium acetate In water at 90℃; for 24h; Inert atmosphere; | 100% |
(2-amino-3-methylphenyl) (benzotriazole-1-yl)methanone
ethyl 2-sulfanylacetate
ethyl 2-(2-amino-3-methylbenzoylthio)acetate
Conditions | Yield |
---|---|
With dmap In dichloromethane at 20℃; | 100% |
ethyl 2-sulfanylacetate
Conditions | Yield |
---|---|
With N,N,N',N'-tetramethylguanidine In N,N-dimethyl-formamide at 23℃; for 16h; | 100% |
3-bromo-5-(4-methoxyphenyl)thiophene-2-carbaldehyde
ethyl 2-sulfanylacetate
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 50h; | 100% |
3-bromo-5-(4-(trifluoromethyl)phenyl)thiophene-2-carbaldehyde
ethyl 2-sulfanylacetate
Conditions | Yield |
---|---|
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 50h; | 100% |
ethyl 2-sulfanylacetate
Conditions | Yield |
---|---|
With sodium hydroxide In N,N-dimethyl-formamide at 0 - 20℃; | 100% |
With potassium tert-butylate In N,N-dimethyl-formamide at 0 - 20℃; for 1.5h; | 100% |
ethyl 2-sulfanylacetate
2-bromo-4-methyl-5-nitrobenzaldehyde
ethyl 6-methyl-5-nitrobenzo[b]thiophene-2-carboxylate
Conditions | Yield |
---|---|
With sodium In ethanol for 3h; Inert atmosphere; Reflux; | 99.8% |
With sodium ethanolate 1.) EtOH, 5 deg C, 20 min, 2.) EtOH, reflux, 3 h; Yield given. Multistep reaction; |
ethyl 2-sulfanylacetate
dimethyl N-cyanodithioiminocarbonate
ethyl 4-amino-2-(methylthio)thiazol-5-carboxylate
Conditions | Yield |
---|---|
With diisopropylamine In N,N-dimethyl-formamide at 100℃; for 5h; | 99% |
With N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 100℃; | 89% |
With triethylamine In N,N-dimethyl-formamide | |
With triethylamine In N,N-dimethyl-formamide at 100℃; for 2h; |
cyclohexane-1,2-epoxide
ethyl 2-sulfanylacetate
trans-2-hydroxycyclohexyl(carboethoxy)methyl sulfide
Conditions | Yield |
---|---|
With sodium ethanolate In ethanol for 25h; Heating; | 99% |
2-((R)-oxiran-2-ylmethoxy)tetrahydro-2H-pyran
ethyl 2-sulfanylacetate
[(R)-2-Hydroxy-3-(tetrahydro-pyran-2-yloxy)-propylsulfanyl]-acetic acid ethyl ester
Conditions | Yield |
---|---|
sodium ethanolate In ethanol at 22℃; | 99% |
ethyl 2-sulfanylacetate
α-bromoacetophenone
ethyl 2-((2-oxo-2-phenylethyl)thio)acetate
Conditions | Yield |
---|---|
With potassium carbonate In tetrahydrofuran at 20℃; Inert atmosphere; | 99% |
With sodium hydroxide In methanol for 4h; | 60% |
With sodium carbonate In ethanol at 20℃; |
[Bis(methylthio)methylene]malononitrile
ethyl 2-sulfanylacetate
3-amino-4-cyano-5-(methylthio)thiophene-2-carboxylic acid ethyl ester
Conditions | Yield |
---|---|
With triethylamine In methanol for 2h; Reflux; | 99% |
With triethylamine In methanol for 2h; Reflux; | 99% |
With triethylamine In ethanol at 0 - 20℃; for 12h; | 72.6% |
3-chloroisonicotinic acid ethyl ester
ethyl 2-sulfanylacetate
ethyl 3-hydroxythieno [2,3-c]pyridine-2-carboxylate
Conditions | Yield |
---|---|
With sodium hydride In N,N-dimethyl-formamide at 5 - 20℃; for 18.67h; | 99% |
In N,N-dimethyl-formamide; mineral oil at 20℃; for 3.25h; Cooling with ice; | 70% |
2-fluoro-6-(trifluoromethyl)benzonitrile
ethyl 2-sulfanylacetate
Conditions | Yield |
---|---|
With sodium hydroxide In N,N-dimethyl-formamide at 0 - 20℃; | 99% |
With potassium tert-butylate In N,N-dimethyl-formamide at 0 - 20℃; for 1.5h; | 99% |
ethyl 2-sulfanylacetate
Conditions | Yield |
---|---|
Stage #1: ethyl 2-sulfanylacetate With sodium hydride In tetrahydrofuran at 0 - 20℃; for 0.333333h; Inert atmosphere; Stage #2: N-(benzyloxy)formimidoyl chloride In tetrahydrofuran at 20℃; for 5h; Inert atmosphere; | 99% |
ethyl 2-sulfanylacetate
Conditions | Yield |
---|---|
With Trimethylsilanol; (S)-N-(2-pyridinesulfonyl)-(6-methoxyquinolin-4-yl)(8-vinylquinuclidin-2-yl)methanamine In toluene at -80℃; for 8h; Inert atmosphere; enantioselective reaction; | 99% |
ethyl 2-sulfanylacetate
Conditions | Yield |
---|---|
With Trimethylsilanol; (S)-N-(2-pyridinesulfonyl)-(6-methoxyquinolin-4-yl)(8-vinylquinuclidin-2-yl)methanamine In toluene at -80℃; for 8h; Inert atmosphere; enantioselective reaction; | 99% |
ethyl 2-sulfanylacetate
Conditions | Yield |
---|---|
With Trimethylsilanol; (S)-N-(2-pyridinesulfonyl)-(6-methoxyquinolin-4-yl)(8-vinylquinuclidin-2-yl)methanamine In toluene at -80℃; for 8h; Inert atmosphere; enantioselective reaction; | 99% |
ethyl 2-sulfanylacetate
Conditions | Yield |
---|---|
With Trimethylsilanol; (S)-N-(2-pyridinesulfonyl)-(6-methoxyquinolin-4-yl)(8-vinylquinuclidin-2-yl)methanamine In toluene at -80℃; for 8h; Inert atmosphere; enantioselective reaction; | 99% |
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