DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe
Cas:5117-12-4
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryWelcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our
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inquiryHangzhou Dingyan Chem is a leading manufacturer and supplier of chemicals in China.We develop,produce and distribute high quality pharmaceuticals, intermediates, special chemicals and other fine chemicals. ---------------------------------
Cas:5117-12-4
Min.Order:1 Kilogram
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Type:Trading Company
inquiryGood price Good quality Appearance:white powder Storage:dry condition Package:fiber drum Application:OLED Transportation:by sea Port:Shanghai Port
Cas:5117-12-4
Min.Order:1 Kilogram
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inquiryThe above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Cas:5117-12-4
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inquiry1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
Cas:5117-12-4
Min.Order:1 Gram
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inquiryACMO 4-Acryloylmorpholine Factory CAS 5117-12-4 N-Acryloylmorpholine CAS no 5117-12-4 2-Propen-1-one,1-(4-morpholinyl)- 4-Acryloylmorpholine Manufacturer High quality Best price In stock factory CAS 5117-12-4 4-Acryloylmorpholine COA TDS price
Cas:5117-12-4
Min.Order:5 Kiloliter
FOB Price: $3.5 / 5.0
Type:Manufacturers
inquiryOur company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
Cas:5117-12-4
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryOur advantages: 1. High quality and competitive price: 1) Standard: BP/USP/EP/ enterprise standard 2) All purity ≥99% 3) We are manufacturers and can provide high quality products at factory prices. 2. Fast and safe delivery 1) The package c
Cas:5117-12-4
Min.Order:1 Kilogram
FOB Price: $199.0 / 222.0
Type:Trading Company
inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:5117-12-4
Min.Order:10 Gram
FOB Price: $146.0 / 176.0
Type:Trading Company
inquiryJinlan Pharm-Drugs Technology Co.,Limited (with its export company Hangzhou Royall Import & Export Co.,Ltd.)is located in Hangzhou, Zhejiang Province. Neighboring Ningbo port, Shanghai port, Hangzhou Xiaoshan Int’l Airport and Shanghai Pu
Cas:5117-12-4
Min.Order:1 Gram
FOB Price: $1.0
Type:Manufacturers
inquiryProduct Name 4-Acryloylmorpholine Appearance clear liquid CAS NO. 5117-12-4 Molecular Formula C7H11NO2 Molecular Weight 141.17
1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized
Cas:5117-12-4
Min.Order:1 Kilogram
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inquiry4-Acryloylmorpholine CAS:5117-12-4 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic inter
Cas:5117-12-4
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
Cas:5117-12-4
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiry1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France etc. 3) OEM/ODM Available;
Cas:5117-12-4
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
Cas:5117-12-4
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryBest quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia
4-Acryloylmorpholine CAS 5117-12-4 Our advantage 1.Top quality: Using high quality material and establishing a strict quality control system,assigning specific persons in charge of each part of production,from raw material purchase to assembl
Cas:5117-12-4
Min.Order:1 Kilogram
FOB Price: $10.0 / 50.0
Type:Trading Company
inquiryCompany Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments
Cas:5117-12-4
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiry4-Acryloylmorpholine CAS 5117-12-4 Description Purity: 99% Min Application: Intermediates Appearance: Powder Package: Bag Delivery: 3-5days Our Advantage & Service 1.Top quality: Using high quality material and establishing a stric
Cas:5117-12-4
Min.Order:1 Kilogram
FOB Price: $10.0 / 50.0
Type:Trading Company
inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
Cas:5117-12-4
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:5117-12-4
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquirySuperior quality, moderate price & quick delivery. Appearance:Clear liquid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:25kg/drum;200kg/drum as per your request Application:Used as Pharmaceutical Intermedia
Cas:5117-12-4
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiryProduct name: 4-Acryloylmorpholine CAS No.:5117-12-4 Molecule Formula:C10H12N2O2 Molecule Weight:192.21 Purity: 99.0% Package: 200kg/drum Description:Colorless transparent liquid Manufacture Standards:Enterprise Standard
Cas:5117-12-4
Min.Order:1 Kilogram
Negotiable
Type:Trading Company
inquiryOur Advantages A. International Top level TechnologyOur company owned biomedicine experts are famous at home and abroad with rich experience in research and development in the field of efficient chiral functional molecules research and development an
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Min.Order:0
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Type:Trading Company
inquiry4-Acryloylmorpholine Chemical Properties Melting point −35 °C(lit.) Boiling point 158°C 50mm density 1.122 g/mL at 25 °C(lit.) refractive index n20/D 1.512(lit.) Fp >230 °F storage temp. 2-8°C pka
Cas:5117-12-4
Min.Order:1 Gram
FOB Price: $66.0
Type:Lab/Research institutions
inquiryHebei yanxi chemical co., LTD who registered capital of 10 million yuan, nearly to $2 million, we have a pharmaceutical raw materials factory production of pharmaceutical raw materials, and a reagent r&d center, and we do research and developmen
Cas:5117-12-4
Min.Order:1 Kilogram
FOB Price: $30.0 / 50.0
Type:Trading Company
inquiryZhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed
Cas:5117-12-4
Min.Order:1 Kilogram
FOB Price: $2.0
Type:Lab/Research institutions
inquiryMy Company Changchun Artel Import and Export trade companyImport and Export Trade Co., Ltd.is located in Changchun, a national historical and cultural city, Jilin Province, China. It covers an area of 22,000 square meters, construction area
Cas:5117-12-4
Min.Order:20 Metric Ton
Negotiable
Type:Trading Company
inquiryN-Acryloylmorpholine
Conditions | Yield |
---|---|
With 10H-phenothiazine; sodium methylate In glycerol at 200℃; Pyrolysis; | 97% |
(+/-)-2-hydroxy-1-morpholinopropan-1-one
N-Acryloylmorpholine
Conditions | Yield |
---|---|
With sulfuric acid; acetic anhydride at 550℃; Temperature; | 96.1% |
4-(3-methoxy-propionyl)-morpholine
N-Acryloylmorpholine
Conditions | Yield |
---|---|
With sodium methylate; 4-methoxy-phenol at 200℃; Pyrolysis; | 96% |
With lithium phosphate at 390℃; Pyrolysis; |
β-morpholinyl-N,N-morpholinylpropionic acid amide
acetic anhydride
A
4-acetylmorpholine
B
N-Acryloylmorpholine
Conditions | Yield |
---|---|
Stage #1: β-morpholinyl-N,N-morpholinylpropionic acid amide; acetic anhydride In toluene at 20 - 80℃; for 2h; Inert atmosphere; Stage #2: With 2,6-di-tert-butyl-4-methyl-phenol; N-ethyl-N,N-diisopropylamine for 18h; Reagent/catalyst; Temperature; Reflux; | A 84% B 95% |
N-Acryloylmorpholine
Conditions | Yield |
---|---|
Stage #1: 3-(diethylamino)-1-morpholinopropan-1-one With acetic anhydride In toluene at 20 - 80℃; for 2h; Inert atmosphere; Stage #2: With 2,6-di-tert-butyl-4-methyl-phenol; triethylamine Reflux; | 94% |
With 4-methoxy-phenol | 11.8 g |
Conditions | Yield |
---|---|
With 10H-phenothiazine; sulfuric acid for 2h; Reagent/catalyst; Heating; | 93.12% |
N-Acryloylmorpholine
Conditions | Yield |
---|---|
With 10H-phenothiazine; sodium methylate; 4-methoxy-phenol In glycerol at 160℃; Pyrolysis; | 92% |
Conditions | Yield |
---|---|
With sodium ethanolate In ethanol at 78℃; for 5h; Temperature; | 91.5% |
1-morpholinopropane-1-one
N-Acryloylmorpholine
Conditions | Yield |
---|---|
With potassium tert-butylate; oxygen; palladium diacetate In dimethyl sulfoxide at 90 - 120℃; under 760.051 Torr; for 36h; Reagent/catalyst; Temperature; | 90% |
Conditions | Yield |
---|---|
With triethylamine at 0 - 3℃; for 2h; Reagent/catalyst; Temperature; | 89.95% |
Conditions | Yield |
---|---|
With 10H-phenothiazine; copper(II) bis(trifluoromethanesulfonate) at 135℃; for 2h; Inert atmosphere; | 89% |
With 4-methoxy-phenol | 8.46 g |
With 10H-phenothiazine; sulfuric acid; 4-methoxy-phenol at 180 - 220℃; under 450.045 Torr; for 6h; Reagent/catalyst; | |
With 10H-phenothiazine In glycerol at 150℃; under 52.5053 Torr; for 0.5h; Reagent/catalyst; Solvent; Inert atmosphere; |
N-Acryloylmorpholine
Conditions | Yield |
---|---|
With sodium ethanolate In ethanol at 85℃; for 3h; | 88.7% |
Conditions | Yield |
---|---|
With sodium hydroxide at 85 - 90℃; | 85.5% |
With potassium tert-butylate In water at 120℃; for 3h; Reagent/catalyst; Temperature; | 20.7% |
β-morpholinyl-N,N-morpholinylpropionic acid amide
benzyl bromide
A
N-Acryloylmorpholine
B
4-benzyl-morpholine
Conditions | Yield |
---|---|
Stage #1: β-morpholinyl-N,N-morpholinylpropionic acid amide; benzyl bromide In toluene at 20 - 80℃; for 2h; Inert atmosphere; Stage #2: With 2,6-di-tert-butyl-4-methyl-phenol; triethylamine for 12h; Reflux; | A 77% B 84% |
Conditions | Yield |
---|---|
With 4-methoxy-phenol; trichlorophosphate In dichloromethane at 0 - 5℃; for 1h; Reagent/catalyst; Concentration; Solvent; | 81% |
With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride In dichloromethane at 20℃; for 12h; | 21% |
N-Acryloylmorpholine
Conditions | Yield |
---|---|
With copper(II) bis(trifluoromethanesulfonate); hydroquinone at 100℃; for 10h; Inert atmosphere; | 80% |
Conditions | Yield |
---|---|
With triethylamine In dichloromethane 1 h, 0 deg C then 1 h, room temp.; | 78% |
With triethylamine 1.) 0 deg C, 1 h; 2.) r.t., 1 h; | 78% |
In dichloromethane at 0 - 20℃; for 3h; Inert atmosphere; | 63% |
N-Acryloylmorpholine
Conditions | Yield |
---|---|
With phosphorus pentoxide In N,N-dimethyl-formamide at 135℃; Temperature; Solvent; | 77.6% |
Conditions | Yield |
---|---|
In dichloromethane 1.) 0 deg C, 483 min; 2.) 25 deg C, 1 h; | 76% |
Conditions | Yield |
---|---|
With triethylamine In acetonitrile at 20℃; for 16h; | 75% |
Conditions | Yield |
---|---|
With sulfuric acid at 120℃; for 3h; Inert atmosphere; | 28.2% |
morpholine
acryloyl chloride
A
N-Acryloylmorpholine
B
β-morpholinyl-N,N-morpholinylpropionic acid amide
Conditions | Yield |
---|---|
With triethylamine; benzene |
Conditions | Yield |
---|---|
With tetracarbonyl nickel; acrylic acid; toluene |
Conditions | Yield |
---|---|
With triethylamine In ethanol for 1h; Heating; | A 40 % Chromat. B 60 % Chromat. |
N-prop-2-ynylmorpholine N-oxide
A
morpholine
B
N-Acryloylmorpholine
C
N-propargylmorpholine
D
3-(3-oxapentane-1,5-diyl)aminoacrylaldehyde
Conditions | Yield |
---|---|
With triethylamine In tert-butyl alcohol at 50 - 79℃; Product distribution; Activation energy; Kinetics; Further Variations:; Solvents; Temperatures; Reagents; pH-values; |
2-chloro-1-(4-morpholino)propan-1-one
N-Acryloylmorpholine
Conditions | Yield |
---|---|
With sodium ethanolate In ethanol at 70℃; for 8h; | 569 g |
N-Acryloylmorpholine
Conditions | Yield |
---|---|
With 4-methoxy-phenol | 19.2 g |
morpholine
acrylic acid methyl ester
acrylic acid
N-Acryloylmorpholine
Conditions | Yield |
---|---|
Stage #1: morpholine; acrylic acid methyl ester With 2,6-di-tert-butyl-4-methyl-phenol at 20 - 55℃; for 3h; Inert atmosphere; Stage #2: With sodium methylate In methanol at 55 - 75℃; for 6.5h; Stage #3: acrylic acid With 2,6-di-tert-butyl-4-methyl-phenol In 5,5-dimethyl-1,3-cyclohexadiene at 140 - 145℃; for 2h; |
S-1-butyl-S'-(α-methyl-α'-acetic acid)trithiocarbonate
N-Acryloylmorpholine
Conditions | Yield |
---|---|
With 2,2’-azobis[2-(2-imidazolin-2-yl)propane] dihydrochloride In 1,4-dioxane; water at 70℃; for 2h; Inert atmosphere; | 99% |
With 4,4'-dicyano-4,4'-azo-di-valeric acid In 1,4-dioxane; water at 70℃; for 24h; |
pyrrolidine
N-Acryloylmorpholine
1-morpholino-3-(pyrrolidin-1-yl)propan-1-one
Conditions | Yield |
---|---|
In dichloromethane for 1h; Inert atmosphere; Reflux; | 98% |
With [DABCO-PDO][OAc] In neat (no solvent) at 20℃; for 2h; Michael Addition; Green chemistry; | 90% |
With triethylamine In water at 20℃; for 2h; Michael Addition; Green chemistry; | 89% |
N-Acryloylmorpholine
3-chloro-8-methyl-6-trifluoromethylsulfonyloxy-8H-quino[4,3,2-kl]acridine
(E)-3-(3-chloro-8-methyl-8H-quino[4,3,2-kl]acridin-6-yl)acrylic acid (morpholin-1-yl)amide
Conditions | Yield |
---|---|
With triethylamine; triphenylphosphine; tris(dibenzylideneacetone)dipalladium (0) In 1,4-dioxane at 100℃; for 18h; Heck reaction; | 98% |
Conditions | Yield |
---|---|
With C29H26N2O5Ru; sodium acetate In 1,4-dioxane at 100℃; for 96h; Inert atmosphere; | 98% |
N-Acryloylmorpholine
5,5'-dibromo-2,2'-bisthiophene
4,4′-{2,2′-bithiene-5,5′-diylbis-[(1E)-3-oxoprop-1-ene-1,3-diyl]}dimorpholine
Conditions | Yield |
---|---|
With dichloro{bis[1,1’,1’’-(phosphinetriyl)tripiperidine]}palladium(II); tetrabutylammomium bromide; potassium carbonate In tetrahydrofuran; 1-methyl-pyrrolidin-2-one at 100℃; for 24h; Heck Reaction; Schlenk technique; Glovebox; Inert atmosphere; Green chemistry; | 98% |
N-Acryloylmorpholine
Conditions | Yield |
---|---|
With C33H30N2O In dichloromethane at -78 - -30℃; for 44h; Michael Addition; Inert atmosphere; enantioselective reaction; | 98% |
Conditions | Yield |
---|---|
With palladium(II) trifluoroacetate; N,N'-bis(2,6-dimethylphenyl)butane-2,3-diimine; toluene-4-sulfonic acid; p-benzoquinone In tetrahydrofuran at 20℃; under 3000.3 Torr; for 67h; Autoclave; | 98% |
N-Acryloylmorpholine
Conditions | Yield |
---|---|
In tetrahydrofuran | 97% |
Conditions | Yield |
---|---|
With copper(l) iodide; N,N,N',N'',N'''-pentamethyldiethylenetriamine In acetonitrile at 80℃; for 12h; Schlenk technique; Inert atmosphere; stereoselective reaction; | 97% |
Conditions | Yield |
---|---|
With potassium tert-butylate In neat (no solvent) at 20℃; for 0.333333h; Michael Addition; Inert atmosphere; | 96% |
tert-butyl 5-iodo-1H-indole-1-carboxylate
N-Acryloylmorpholine
Conditions | Yield |
---|---|
With potassium phosphate; sodium chloride In water; N,N-dimethyl-formamide at 45℃; for 16h; Micellar solution; | 96% |
Conditions | Yield |
---|---|
at 70 - 100℃; for 3.16667h; | 95% |
N-Acryloylmorpholine
1-Bromonaphthalene
(E)-1-morpholino-3-(naphthalen-1-yl)prop-2-en-1-one
Conditions | Yield |
---|---|
With dichloro{bis[1,1’,1’’-(phosphinetriyl)tripiperidine]}palladium(II); tetrabutylammomium bromide; potassium carbonate In tetrahydrofuran; 1-methyl-pyrrolidin-2-one at 100℃; for 6h; Heck Reaction; Schlenk technique; Glovebox; Inert atmosphere; Green chemistry; | 95% |
Conditions | Yield |
---|---|
With potassium tert-butylate In neat (no solvent) at 20℃; for 0.333333h; Michael Addition; Inert atmosphere; | 95% |
N-Acryloylmorpholine
4-Bromodiphenyl ether
(E)-1-morpholino-3-(4-phenoxyphenyl)prop-2-en-1-one
Conditions | Yield |
---|---|
With dichloro{bis[1,1’,1’’-(phosphinetriyl)tripiperidine]}palladium(II); tetrabutylammomium bromide; potassium carbonate In tetrahydrofuran; 1-methyl-pyrrolidin-2-one at 100℃; for 24h; Heck Reaction; Schlenk technique; Glovebox; Inert atmosphere; Green chemistry; | 94% |
3-phenyl-4-iodo-5-methylisoxazole
N-Acryloylmorpholine
Conditions | Yield |
---|---|
With tetrabutyl-ammonium chloride; sodium carbonate; palladium diacetate In N,N-dimethyl-formamide at 85℃; for 24h; Heck cross-coupling; | 93% |
N-Acryloylmorpholine
tert-butyl 4-(4-chloro-2-methoxyphenyl)-3,6-dihydropyridine-1(2H)-carboxylate
tert-butyl 4-{2-methoxy-4-[(1E)-3-morpholin-4-yl-3-oxoprop-1-enyl]phenyl}-3,6-dihydropyridine-1(2H)-carboxylate
Conditions | Yield |
---|---|
With N-Methyldicyclohexylamine; tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine In 1,4-dioxane at 120℃; | 93% |
N-Acryloylmorpholine
diethyl (N-benzylideneaminomethyl)phosphonate
diethyl ((2S,4S,5S)-4-(morpholine-4-carbonyl)-5-phenylpyrrolidine-2-yl)phosphonate
Conditions | Yield |
---|---|
With (R)-((4,4’-bi-1,3-benzodioxole)-5,5’-diyl)bis(bis(3,5-di-t-butyl-4-methoxyphenyl))phosphine; silever triflate; potassium hexamethylsilazane In toluene at 25℃; for 2h; Inert atmosphere; optical yield given as %ee; enantioselective reaction; | 93% |
With (R)-((4,4’-bi-1,3-benzodioxole)-5,5’-diyl)bis(bis(3,5-di-t-butyl-4-methoxyphenyl))phosphine; silver bis(trimethylsilyl)amide In toluene at 25℃; for 2h; Inert atmosphere; optical yield given as %ee; stereoselective reaction; | 93% |
With (R)-((4,4’-bi-1,3-benzodioxole)-5,5’-diyl)bis(bis(3,5-di-t-butyl-4-methoxyphenyl))phosphine; silver bis(trimethylsilyl)amide In toluene at 25℃; enantioselective reaction; | 93% |
Conditions | Yield |
---|---|
With copper(l) iodide; benzyl tri-n-butylammonium bromide; tris[(2-pyridylmethyl)amine]; diisopropylamine In toluene at 100℃; for 20h; Inert atmosphere; | 93% |
Conditions | Yield |
---|---|
With potassium phosphate; tris-(dibenzylideneacetone)dipalladium(0); tetramethylammonium formiate; P(p-C6H4F)3 In 1,4-dioxane; water at 80℃; for 4h; Sealed tube; | 93% |
N-Acryloylmorpholine
3-chloro-8-methyl-8H-quino[4,3,2-kl]acridine
(E)-3-(8-methyl-8H-quino[4,3,2-kl]acridin-3-yl)acrylic acid (morpholin-4-yl)amide
Conditions | Yield |
---|---|
With potassium phosphate; tri-tert-butyl phosphine; tris(dibenzylideneacetone)dipalladium (0) In 1,4-dioxane at 170℃; for 48h; Heck reaction; | 92% |
N-Acryloylmorpholine
methyl 2-(benzylideneamino)acetate
(2R,4S,5S)-methyl 4-(morpholine-4-carbonyl)-5-phenylpyrrolidine-2-carboxylate
Conditions | Yield |
---|---|
With (R)-DTBM-segphos; silver trifluoromethanesulfonate; potassium hexamethylsilazane In diethyl ether at 0℃; for 24h; Inert atmosphere; optical yield given as %ee; enantioselective reaction; | 92% |
With (R)-((4,4’-bi-1,3-benzodioxole)-5,5’-diyl)bis(bis(3,5-di-t-butyl-4-methoxyphenyl))phosphine; silver bis(trimethylsilyl)amide In diethyl ether at 0℃; for 24h; Inert atmosphere; optical yield given as %ee; stereoselective reaction; | 92% |
With (R)-((4,4’-bi-1,3-benzodioxole)-5,5’-diyl)bis(bis(3,5-di-t-butyl-4-methoxyphenyl))phosphine; silver bis(trimethylsilyl)amide In diethyl ether at 0℃; for 24h; enantioselective reaction; | 92% |
N-Acryloylmorpholine
3-((7-chloro-3-iodoimidazo[1,2-a]pyridin-2-yl)methyl)-1-cyclopropyl-1H-imidazo[4,5-c]pyridin-2(3H)-one
(E)-3-((7-chloro-3-(3-morpholino-3-oxoprop-1-enyl)imidazo[1,2-a]pyridin-2-yl)methyl)-1-cyclopropyl-1H-imidazo[4,5-c]pyridin-2(3H)-one
Conditions | Yield |
---|---|
Stage #1: N-Acryloylmorpholine; 3-((7-chloro-3-iodoimidazo[1,2-a]pyridin-2-yl)methyl)-1-cyclopropyl-1H-imidazo[4,5-c]pyridin-2(3H)-one With triphenylphosphine; palladium diacetate In tetrahydrofuran at 80℃; for 2h; Inert atmosphere; Stage #2: With water for 1h; | 92% |
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