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Cas:29662-90-6
Min.Order:1 Kilogram
FOB Price: $8.0 / 10.0
Type:Trading Company
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Cas:29662-90-6
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
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Cas:29662-90-6
Min.Order:1 Kilogram
FOB Price: $2.0
Type:Lab/Research institutions
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Cas:29662-90-6
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiry2,2-Dimethyloctanoic acid Application:Organic Chemicals
Cas:29662-90-6
Min.Order:0
Negotiable
Type:Lab/Research institutions
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Cas:29662-90-6
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryBest quality with low price Storage:ln stock Package:25kg/Barrel Application:Chemicals Transportation:Express/Sea/Air Port:Shanghai
Cas:29662-90-6
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryfactory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
Conditions | Yield |
---|---|
Stage #1: isobutyric Acid With hydrogenchloride; lithium diisopropyl amide In ethanol at 0℃; for 0.25h; Inert atmosphere; Stage #2: 1-Iodohexane at 0 - 20℃; for 2h; | 63.4% |
Stage #1: isobutyric Acid With lithium diisopropyl amide In tetrahydrofuran at -78 - 20℃; for 1h; Stage #2: 1-Iodohexane In tetrahydrofuran at -78 - 20℃; | |
Stage #1: isobutyric Acid With lithium diisopropyl amide In tetrahydrofuran at -78 - 20℃; Stage #2: 1-Iodohexane In tetrahydrofuran at -78 - 20℃; |
2,2-dimethyloctanamide
dimethyloctanoic acid
Conditions | Yield |
---|---|
With 1,4-dioxane; hydrogenchloride; n-Butyl nitrite | |
With sulfuric acid; sodium nitrite | |
With nitro, sulfate; sulfuric acid; water at 45 - 60℃; |
non-1-ene
carbon monoxide
A
2-methyl-2-ethyl heptanoic acid
B
dimethyloctanoic acid
C
2-methyl-2-propylhexanoic acid
Conditions | Yield |
---|---|
(i) BF3*H2SO4, (ii) H2O; Multistep reaction; |
Conditions | Yield |
---|---|
With di-tert-butyl peroxide |
Conditions | Yield |
---|---|
With sulfuric acid 1.) carbon tetrachloride, 5 deg C, 3 min, 2.) 5 deg C, 4.5 h; Yield given. Multistep reaction; |
non-1-ene
carbon monoxide
A
2-methyl-2-ethyl heptanoic acid
B
dimethyloctanoic acid
C
nonane-3-carboxylic acid
D
2-methyl-2-propylhexanoic acid
Conditions | Yield |
---|---|
With copper(I) oxide; (BF3*H2O)(BF3*H3PO4) at 30℃; under 760 Torr; for 4h; Product distribution; other catalyst; | A 50 % Turnov. B 26 % Turnov. C 15 % Turnov. D 9 % Turnov. |
Conditions | Yield |
---|---|
With oxygen; 1,2-di(benzylidene)hydrazine at 275℃; under 514855 Torr; |
2,2-dimethyl-1-phenyl-octan-1-one
dimethyloctanoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: NaNH2; benzene 2: concentrated H2SO4; NaNO2 View Scheme | |
Multi-step reaction with 2 steps 1: NaNH2; toluene 2: concentrated H2SO4; (NO2)2SO4; water / 45 - 60 °C View Scheme |
dimethyloctanoic acid
Conditions | Yield |
---|---|
With N2; palladium In ethanol |
Conditions | Yield |
---|---|
With n-butyllithium; nitrogen; diisopropylamine In tetrahydrofuran; diethyl ether; hexane; water; mineral oil |
ethyl 2,2-dimethyloctanoate
dimethyloctanoic acid
Conditions | Yield |
---|---|
With sodium hydroxide In methanol; water for 2h; Reflux; |
1-Iodohexane
dimethyloctanoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: lithium diisopropyl amide / tetrahydrofuran / 1 h / -78 °C 1.2: -78 - 20 °C 2.1: sodium hydroxide / water; methanol / 2 h / Reflux View Scheme |
Conditions | Yield |
---|---|
Stage #1: dimethyloctanoic acid With sodium hydroxide In ethanol; water at 20℃; for 1h; Stage #2: neodymium(III) chloride hydrate In ethanol; hexane; water at 20℃; for 15h; | 96% |
dimethyloctanoic acid
4-Benzyloxyphenol
Conditions | Yield |
---|---|
Stage #1: dimethyloctanoic acid With oxalyl dichloride; triethylamine In dichloromethane at 0℃; for 2h; Inert atmosphere; Stage #2: 4-Benzyloxyphenol With triethylamine; N,N-dimethyl-formamide In dichloromethane at 0 - 20℃; for 15h; | 49% |
dimethyloctanoic acid
2,2-dimethyloctanoic acid chloride
Conditions | Yield |
---|---|
With thionyl chloride | |
With thionyl chloride for 1h; Reflux; | |
With oxalyl dichloride; N,N-dimethyl-formamide In dichloromethane at 20℃; | |
With thionyl chloride In benzene for 4h; Reflux; |
Conditions | Yield |
---|---|
at 400℃; |
dimethyloctanoic acid
2,2-dimethyloctanamide
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: thionyl chloride 2: water; ammonia View Scheme |
dimethyloctanoic acid
2,2-dimethyl-octanoic acid anilide
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: thionyl chloride View Scheme |
dimethyloctanoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 6 steps 1: thionyl chloride / 1 h / Reflux 2: pyridine / dichloromethane / 0 - 20 °C 3: tetrahydrofuran / -78 - 20 °C 4: C7H16AuO3S; water / methanol / 12 h / 70 °C 5: triethylamine; 4-toluenesulfonyl azide / acetonitrile / 4 h / 0 - 20 °C 6: t-BuBrettPhosAuNTf2; 8-isopropyl-quinoline-N-oxide / 1,2-dichloro-ethane / 96 h / 20 °C View Scheme |
dimethyloctanoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: thionyl chloride / 1 h / Reflux 2: pyridine / dichloromethane / 0 - 20 °C 3: tetrahydrofuran / -78 - 20 °C 4: C33H48NP*Au(1+)*Cl(1-); silver(I) triflimide; 8-isopropyl-quinoline-N-oxide / fluorobenzene / 2 h / 20 °C View Scheme |
dimethyloctanoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: thionyl chloride / 1 h / Reflux 2: pyridine / dichloromethane / 0 - 20 °C 3: tetrahydrofuran / -78 - 20 °C 4: t-BuBrettPhosAuNTf2; 8-isopropyl-quinoline-N-oxide / 1,2-dichloro-ethane / 2 h / 20 °C View Scheme | |
Multi-step reaction with 4 steps 1: thionyl chloride / 1 h / Reflux 2: pyridine / dichloromethane / 0 - 20 °C 3: tetrahydrofuran / -78 - 20 °C 4: 8-methylquinoline 1-oxide; C33H48NP*Au(1+)*Cl(1-) / fluorobenzene / 12 h / 20 °C View Scheme | |
Multi-step reaction with 4 steps 1: thionyl chloride / 1 h / Reflux 2: pyridine / dichloromethane / 0 - 20 °C 3: tetrahydrofuran / -78 - 20 °C 4: 8-methylquinoline 1-oxide; silver(I) triflimide; (1,3-dimesitylimidazol-2-ylidene)gold(I) chloride / fluorobenzene / 2 h / 20 °C View Scheme | |
Multi-step reaction with 4 steps 1: thionyl chloride / 1 h / Reflux 2: pyridine / dichloromethane / 0 - 20 °C 3: tetrahydrofuran / -78 - 20 °C 4: 8-methylquinoline 1-oxide; C33H48NP*Au(1+)*Cl(1-); silver(I) triflimide / fluorobenzene / 2 h / 20 °C View Scheme |
dimethyloctanoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: thionyl chloride / 1 h / Reflux 2: pyridine / dichloromethane / 0 - 20 °C 3: tetrahydrofuran / -78 - 20 °C View Scheme |
dimethyloctanoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: thionyl chloride / 1 h / Reflux 2: pyridine / dichloromethane / 0 - 20 °C 3: tetrahydrofuran / -78 - 20 °C View Scheme |
dimethyloctanoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: thionyl chloride / 1 h / Reflux 2: pyridine / dichloromethane / 0 - 20 °C View Scheme | |
Multi-step reaction with 2 steps 1: N,N-dimethyl-formamide; oxalyl dichloride / dichloromethane / 20 °C 2: dmap; pyridine / dichloromethane / 0 - 20 °C View Scheme |
dimethyloctanoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: thionyl chloride / 1 h / Reflux 2: pyridine / dichloromethane / 0 - 20 °C 3: tetrahydrofuran / -78 - 20 °C 4: C7H16AuO3S; water / methanol / 12 h / 70 °C 5: triethylamine; 4-toluenesulfonyl azide / acetonitrile / 4 h / 0 - 20 °C View Scheme |
dimethyloctanoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: thionyl chloride / 1 h / Reflux 2: pyridine / dichloromethane / 0 - 20 °C 3: tetrahydrofuran / -78 - 20 °C 4: C7H16AuO3S; water / methanol / 12 h / 70 °C View Scheme |
dimethyloctanoic acid
1,1-dimethyl-heptyl isocyanate
Conditions | Yield |
---|---|
With diphenylphosphoranyl azide; triethylamine In toluene at 0 - 100℃; for 14h; Inert atmosphere; |
dimethyloctanoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: diphenylphosphoranyl azide; triethylamine / toluene / 14 h / 0 - 100 °C / Inert atmosphere 2: hydrogenchloride / water; acetic acid / 20 °C View Scheme |
dimethyloctanoic acid
1,1-dimethylheptylamine
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: diphenylphosphoranyl azide; triethylamine / toluene / 14 h / 0 - 100 °C / Inert atmosphere 2: hydrogenchloride / water; acetic acid / 20 °C View Scheme |
dimethyloctanoic acid
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: diphenylphosphoranyl azide; triethylamine / toluene / 14 h / 0 - 100 °C / Inert atmosphere 2: hydrogenchloride / water; acetic acid / 20 °C 3: tetrahydrofuran; toluene / 2 h / 0 - 20 °C / Inert atmosphere View Scheme |
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