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Dayang Chem (Hangzhou) Co.,Ltd.

DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe

4-Cyanobenzamide Manufacturer/High quality/Best price/In stock

Cas:3034-34-2

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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Henan Tianfu Chemical Co., Ltd.

Product Name: 4-CYANOBENZAMIDE Synonyms: 4-cyanobenamide;4-cyano-benzamid;Benzamide, 4-cyano-;cyanobenzamide;p-cyano-benzamid;P-CYANO BENZAMIDE;4-CYANOBENZAMIDE;Benzamide, 4-cyano- (9CI) CAS: 3034-34-2 MF: C8H6N2O MW:

3034-34-2 4-CYANOBENZAMIDE

Cas:3034-34-2

Min.Order:1 Kilogram

FOB Price: $8900.0

Type:Lab/Research institutions

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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Pharmaceutical Grade CAS 3034-34-2 with competitive price

Cas:3034-34-2

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

CAS NO.:3034-34-2

Cas:3034-34-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

4-CYANOBENZAMIDE

Cas:3034-34-2

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

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Ality Chemical Corporation

The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi

Factory Supply Cyanobenzamide; 95%

Cas:3034-34-2

Min.Order:0 Metric Ton

Negotiable

Type:Other

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Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

4-Cyanobenzamide

Cas:3034-34-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

HANGZHOU YUNUO CHEMICAL CO.,LTD

superior quality moderate price & quick delivery Appearance:Beige powder Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:1kg/bag, 1kg/drum or 25kg/drum or as per your request. Application:Used to make other

Benzamide,4-cyano-

Cas:3034-34-2

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

inquiry

Kono Chem Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou

Cyanobenzamide; 95%

Cas:3034-34-2

Min.Order:0

Negotiable

Type:Other

inquiry

GIHI CHEMICALS CO.,LIMITED

high purity,in stock Package:25kg/drum,or as per customers'demand Application:API,Pharmaceutical intermediates Transportation:air,sea,courier

4-Cyanobenzamide

Cas:3034-34-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Henan Allgreen Chemical Co.,Ltd

high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea

4-CyanobenzaMide

Cas:3034-34-2

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Antimex Chemical Limied

Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali

4-CyanobenzaMide

Cas:3034-34-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Hangzhou Fandachem Co.,Ltd

4-Cyanobenzamide cas 3034-34-2Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express

4-Cyanobenzamide cas 3034-34-2

Cas:3034-34-2

Min.Order:0

Negotiable

Type:Other

inquiry

Hangzhou Sartort Biopharma Co., Ltd

Best quality with low priceAppearance:Beige powder Storage:ln stock Package:25kg/Barrel Application:Chemicals Transportation:Express/Sea/Air Port:Shanghai

Cyanobenzamide;95%

Cas:3034-34-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

SAGECHEM LIMITED

3034-34-2 Application:intermediate

Benzamide, 4-cyano-

Cas:3034-34-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

ZHEJIANG JIUZHOU CHEM CO.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

4-CYANOBENZAMIDE

Cas:3034-34-2

Min.Order:0

Negotiable

Type:Trading Company

inquiry

LEAP CHEM Co., Ltd.

Best Seller, High Quality, Competitive Price, Fast Delivery, Quick ResponseAppearance:powder, or liquid Storage:Stored in room temperature, ventilated place Package:Bottle, barrel, cargo, container, etc. Application:Pharmaceuticals, intermediates, AP

4-Cyanobenzamide

Cas:3034-34-2

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Amadis Chemical Co., Ltd.

1.Professional synthesis laboratory and production base. 2.Strong synthesis team and service team. 3.Professional data management system. 4.We provide the professional test date and product information ,ex. HNMR ,CNMR,FNMR, HPLC/G

4-Cyanobenzamide

Cas:3034-34-2

Min.Order:10 Milligram

Negotiable

Type:Lab/Research institutions

inquiry

Jilin haofei import and export trade Co.,Ltd

Price, service, company and transport advantage: 1.Best service, high quality and reasonable price. 2. It's customers' right to choose the package (EMS, DHL, FEDEX, UPS). ? 3. It's customers' right to choose the packing way for his products fro

Best price/ 4-CyanobenzaMide CAS NO.3034-34-2

Cas:3034-34-2

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Hangzhou Share Chemical Co., Ltd

At Share Chemical Company, we scrupulously abide by our policy of “Excellent Quality at a Reasonable Price”. We strive to satisfy all of our customers by providing the finest quality products supported by the finest in customer servi

4-CyanobenzaMide

Cas:3034-34-2

Min.Order:1 Gram

Negotiable

Type:Other

inquiry

Nanjing Norris Pharm Technology Co., Ltd.

R & D enterprises have their own stock in stockAppearance:To be subject to the object Package:Customized Application:pharmaceutical intermediates Transportation:Air Port:Shanghai;Guangzhou

4-CyanobenzaMide

Cas:3034-34-2

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Chemical Technology Co.,LTD

1. Production capacity: we have three production base with high-tech production equipment and instruments, equipped with professional production personnel, meet your requirements.2. Quality assurance: we have a first-class testing equipment and testi

4-CYANOBENZAMIDE

Cas:3034-34-2

Min.Order:0

Negotiable

Type:Other

inquiry

Finetech Industry Limited

FINETECH INDUSTRY LIMITED is a LONDON based CRO company providing drug discovery & development services to worldwide clients. FINETECH INDUSTRY LIMITED supplies the 4-CYANOBENZAMIDE, CAS:3034-34-2 with the most competitive price and the best quality.

4-CYANOBENZAMIDE

Cas:3034-34-2

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Antaeus Bio-technology Co., LTD

Antaeus-biotech with Established in July 15833 is a high-technical enterprise which focus on the development of health products. We have excellent professionals, first-class facilities and perfect management system. Through persistent efforts, we con

4-CYANOBENZAMIDE

Cas:3034-34-2

Min.Order:0

Negotiable

Type:Other

inquiry

NovaChemistry

high purity Application:Drug intermediates Materials intermediates and active molecules

4-Cyanobenzamide

Cas:3034-34-2

Min.Order:0

Negotiable

Type:Trading Company

inquiry

ENDOTHERM GmbH

1 g - 135 €

4-Cyanobenzamide

Cas:3034-34-2

Min.Order:0

Negotiable

Type:Trading Company

inquiry

SYNPHABASE

more information,pls contact with us!

4-Cyanobenzamide

Cas:3034-34-2

Min.Order:0

Negotiable

Type:Trading Company

inquiry

ENDOTHERM GmbH

4-Cyanobenzamide

Cas:3034-34-2

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Synthetic route

4-cyanobenzaldehyde oxime
52707-54-7, 52707-59-2, 64847-77-4

4-cyanobenzaldehyde oxime

4-cyanobenzamide
3034-34-2

4-cyanobenzamide

Conditions
ConditionsYield
With Cu(II) on nano silica functionalized triazine dendrimer In water at 20℃; for 0.5h; Beckmann Rearrangement; Green chemistry;98%
With Cu(II)-metformin immobilized ongraphene oxide In water at 100℃; for 0.5h; Beckmann Rearrangement; Green chemistry;96%
With [Ru(κ(3)-tpy)(κ(1)-P-PPh2Py)Cl2] In toluene for 12h; Beckmann rearrangement; Reflux;80%
With Cu(II) complex on SiO2-coated Fe3O4 nanoparticles at 80℃; for 1h; Beckmann Rearrangement; Green chemistry;80%
4-cyanobenzaldehyde
105-07-7

4-cyanobenzaldehyde

4-cyanobenzamide
3034-34-2

4-cyanobenzamide

Conditions
ConditionsYield
Stage #1: 4-cyanobenzaldehyde With hydroxylamine hydrochloride; sodium hydrogencarbonate In water
Stage #2: In water at 100℃; for 10h;
98%
With hydroxylamine hydrochloride; sodium carbonate In water at 80℃; for 48h;96%
With hydroxylamine hydrochloride; sodium carbonate In water at 80℃; for 22h; Green chemistry;95%
tert-butylisonitrile
119072-55-8, 7188-38-7

tert-butylisonitrile

4-iodobenzamide
3956-07-8

4-iodobenzamide

4-cyanobenzamide
3034-34-2

4-cyanobenzamide

Conditions
ConditionsYield
With copper (II) trifluoroacetate hydrate; palladium diacetate In dimethyl sulfoxide at 130℃; for 10h; Sealed tube; Inert atmosphere;98%
4-Cyanobenzyl alcohol
874-89-5

4-Cyanobenzyl alcohol

4-cyanobenzamide
3034-34-2

4-cyanobenzamide

Conditions
ConditionsYield
With [1,1'-bis(diphenylphosphino)ferrocene]nickel(II) chloride; silver trifluoroacetate; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione In N,N-dimethyl-formamide at 8℃; for 9h; Reagent/catalyst; Solvent;96.2%
With iron(III) chloride; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; hydroxylamine hydrochloride; iodine; potassium carbonate In 1,2-dichloro-ethane at 90℃; for 32h;83%
terephthalonitrile
623-26-7

terephthalonitrile

4-cyanobenzamide
3034-34-2

4-cyanobenzamide

Conditions
ConditionsYield
Stage #1: terephthalonitrile With Br(1-)*C24H30N4Rh(1+); water In isopropyl alcohol at 25℃; for 0.5h; Inert atmosphere;
Stage #2: With potassium tert-butylate In isopropyl alcohol at 25℃; for 12h; Inert atmosphere;
96%
With water In dimethyl sulfoxide at 100℃; Green chemistry;96%
With sodium tetrahydroborate In ethanol; water at 80℃; for 4h; regioselective reaction;94%
4-cyano-N-phenyl-N-tosylbenzamide

4-cyano-N-phenyl-N-tosylbenzamide

4-cyanobenzamide
3034-34-2

4-cyanobenzamide

Conditions
ConditionsYield
With ammonium carbonate In dimethyl sulfoxide at 25℃; for 6h;85%
potassiumhexacyanoferrate(II) trihydrate

potassiumhexacyanoferrate(II) trihydrate

p-bromobenzamide
698-67-9

p-bromobenzamide

4-cyanobenzamide
3034-34-2

4-cyanobenzamide

Conditions
ConditionsYield
With tris-(dibenzylideneacetone)dipalladium(0); tris(2-morpholinophenyl)phosphine; potassium carbonate In water; tert-butyl alcohol at 85℃; for 10h; Schlenk technique; Inert atmosphere;82%
zinc(II) cyanide
557-21-1

zinc(II) cyanide

p-bromobenzamide
698-67-9

p-bromobenzamide

4-cyanobenzamide
3034-34-2

4-cyanobenzamide

Conditions
ConditionsYield
With dmap; 1,1'-bis-(diphenylphosphino)ferrocene; nickel(II) chloride hexahydrate; zinc In acetonitrile at 80℃; for 6h; Schlenk technique; Inert atmosphere; Sealed tube;82%
para-methylbenzamide
619-55-6

para-methylbenzamide

4-cyanobenzamide
3034-34-2

4-cyanobenzamide

Conditions
ConditionsYield
With hydroxylamine hydrochloride; 2,4,6-triphenylpyrylium tetrafluoroborate; oxygen; ammonium bromide In acetonitrile at 40℃; under 750.075 Torr; for 24h; Molecular sieve; Irradiation;82%
zinc(II) cyanide
557-21-1

zinc(II) cyanide

4-chlorobenzamide
619-56-7

4-chlorobenzamide

4-cyanobenzamide
3034-34-2

4-cyanobenzamide

Conditions
ConditionsYield
With dmap; 1,1'-bis-(diphenylphosphino)ferrocene; nickel(II) chloride hexahydrate; zinc In acetonitrile at 80℃; for 6h; Schlenk technique; Inert atmosphere; Sealed tube;80%
With dmap; 1,1'-bis-(diphenylphosphino)ferrocene; nickel(II) chloride hexahydrate; zinc In acetonitrile at 80℃; for 6h; Inert atmosphere; Sealed tube;80%
4-cyanobenzaldehyde
105-07-7

4-cyanobenzaldehyde

A

4-cyanobenzamide
3034-34-2

4-cyanobenzamide

B

sodium 4-cyanobenzoate
17264-66-3

sodium 4-cyanobenzoate

Conditions
ConditionsYield
Stage #1: 4-cyanobenzaldehyde With ammonia at -33℃; for 1h; Inert atmosphere;
Stage #2: With potassium permanganate at -33℃; for 1h; Inert atmosphere; Reflux;
Stage #3: With sodium sulfite
A 78%
B 20%
4-cyanobenzaldehyde
105-07-7

4-cyanobenzaldehyde

A

4-cyanobenzoic Acid
619-65-8

4-cyanobenzoic Acid

B

4-cyanobenzamide
3034-34-2

4-cyanobenzamide

Conditions
ConditionsYield
Stage #1: 4-cyanobenzaldehyde With ammonia at -33℃; for 1h; Inert atmosphere;
Stage #2: With potassium permanganate for 1h; Inert atmosphere; Reflux;
A n/a
B 78%
4-cyanobenzoic Acid
619-65-8

4-cyanobenzoic Acid

4-cyanobenzamide
3034-34-2

4-cyanobenzamide

Conditions
ConditionsYield
With ammonium chloride; N-ethyl-N,N-diisopropylamine; 2-(1-oxypyridin-2-yl)-1,1,3,3-tetramethylisothiouronium tetrafluoroborate In N,N-dimethyl-formamide at 20℃; for 0.5h;77%
With tris[2-phenylpyridinato-C2,N]iridium(III); dipotassium hydrogenphosphate; borane-ammonia complex; di-tert-butyl dicarbonate; magnesium chloride In acetonitrile at 20℃; for 36h; Schlenk technique; Irradiation; Green chemistry;58%
Multi-step reaction with 2 steps
1: (COCl)2, DMF / CH2Cl2 / Heating
2: conc. NH4OH / ethyl acetate / 0.17 h
View Scheme
4-cyanobenzoyl chlorIde
6068-72-0

4-cyanobenzoyl chlorIde

methylamine
74-89-5

methylamine

4-cyanobenzamide
3034-34-2

4-cyanobenzamide

Conditions
ConditionsYield
With triethylamine In dichloromethane at 20℃; for 1h; Cooling with ice;76%
4-(2,6-dioxopiperidine-1-carbonyl)benzonitrile

4-(2,6-dioxopiperidine-1-carbonyl)benzonitrile

4-cyanobenzamide
3034-34-2

4-cyanobenzamide

Conditions
ConditionsYield
With lithium hydroxide monohydrate In water at 20℃; for 2h;76%
terephthalonitrile
623-26-7

terephthalonitrile

A

4-cyanobenzamide
3034-34-2

4-cyanobenzamide

B

terephthalamide
3010-82-0

terephthalamide

Conditions
ConditionsYield
With water; palladium diacetate; acetic acid; scandium tris(trifluoromethanesulfonate) at 30℃; for 24h;A 65%
B 18%
With chitosan-supported ruthenium catalyst (ChRu) In water at 120℃; for 1h; Microwave irradiation; Sealed tube; Overall yield = 7 %;
With nitrile hydratase from Rhodococcus rhodochrous J1 W72Y mutant In aq. phosphate buffer at 35℃; for 4h; pH=7.4; Reagent/catalyst; Enzymatic reaction; regioselective reaction;
4-Cyanochlorobenzene
623-03-0

4-Cyanochlorobenzene

carbon monoxide
201230-82-2

carbon monoxide

4-cyanobenzamide
3034-34-2

4-cyanobenzamide

Conditions
ConditionsYield
With (1,3-(dicyclohexylphosphino)propane )Pd(ethylene); ammonia; potassium carbonate In dimethyl sulfoxide at 110℃; under 450 Torr; for 24h; Schlenk technique; Inert atmosphere;60%
With ammonia; palladium diacetate; catacxium A In 1,4-dioxane at 130℃; under 3000.3 Torr; for 20h; Autoclave;32 %Chromat.
With 1,1'-bis-(diphenylphosphino)ferrocene; ammonia; palladium diacetate In 1,4-dioxane at 130℃; under 1500.15 Torr; for 20h;30 %Chromat.
terephthalaldehyde oxime
69386-99-8, 18705-39-0

terephthalaldehyde oxime

A

terephthalonitrile
623-26-7

terephthalonitrile

B

4-cyanobenzamide
3034-34-2

4-cyanobenzamide

Conditions
ConditionsYield
With nickel(II) chloride dihydrate In acetonitrile at 80℃; Molecular sieve; Inert atmosphere;A 58%
B 42%
formic acid
64-18-6

formic acid

4-iodobenzonitrile
3058-39-7

4-iodobenzonitrile

4-cyanobenzamide
3034-34-2

4-cyanobenzamide

Conditions
ConditionsYield
With palladium diacetate; ammonium bicarbonate; dicyclohexyl-carbodiimide; triphenylphosphine In acetonitrile at 100℃; Inert atmosphere;55%
4-cyanophenyl methyl ketone
1443-80-7

4-cyanophenyl methyl ketone

4-cyanobenzamide
3034-34-2

4-cyanobenzamide

Conditions
ConditionsYield
With sodium azide; iodine; sodium hydrogencarbonate In water at 100℃; for 2h;53%
4-cyanobenzamide
3034-34-2

4-cyanobenzamide

4-cyanobenzoic Acid
619-65-8

4-cyanobenzoic Acid

Conditions
ConditionsYield
96%
With sodium nitrite In sulfuric acid95%
94%
With acetic anhydride; acetic acid; sodium nitrite In water92%
With sulfuric acid; acetic acid; sodium nitrite In water86%
4-cyanobenzamide
3034-34-2

4-cyanobenzamide

1-(4-cyanophenyl)urea
86065-51-2

1-(4-cyanophenyl)urea

Conditions
ConditionsYield
With [bis(acetoxy)iodo]benzene; ammonium carbamate In 2,2,2-trifluoroethanol at 0 - 20℃; for 23.5h; Reagent/catalyst; Solvent; Hofmann Rearrangement; Inert atmosphere;95%
4-chloro-2-(trichloromethyl)quinazoline
3137-63-1

4-chloro-2-(trichloromethyl)quinazoline

4-cyanobenzamide
3034-34-2

4-cyanobenzamide

4-cyano-N-(2-trichloromethylquinazolin-4-yl)benzamide

4-cyano-N-(2-trichloromethylquinazolin-4-yl)benzamide

Conditions
ConditionsYield
With sodium hydride In N,N-dimethyl-formamide at 0 - 20℃; Inert atmosphere;95%
4-cyanobenzamide
3034-34-2

4-cyanobenzamide

4-(aminomethyl)benzamide
369-53-9

4-(aminomethyl)benzamide

Conditions
ConditionsYield
With ammonia; hydrogen In toluene at 120℃; under 22502.3 Torr; for 16h; Autoclave;91%
With formic acid; palladium 10% on activated carbon; triethylamine In tetrahydrofuran at 40℃; for 3h;98 %Chromat.
4-cyanobenzamide
3034-34-2

4-cyanobenzamide

diphenyl acetylene
501-65-5

diphenyl acetylene

C36H22N2O
1253388-71-4

C36H22N2O

Conditions
ConditionsYield
With dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; silver carbonate In acetonitrile at 115℃; for 10h; Inert atmosphere;90%
4-cyanobenzamide
3034-34-2

4-cyanobenzamide

terephthalonitrile
623-26-7

terephthalonitrile

Conditions
ConditionsYield
With iron(II) chloride tetrahydrate; N-methyl-N-trimethylsilyl-2,2,2-trifluoroacetamide In tetrahydrofuran at 70℃; for 2h;90%
With diethyl chlorophosphate at 120℃; for 0.25h; Neat (no solvent);86%
Stage #1: 4-cyanobenzamide With N-methylbenzamide; phenylsilane; C28H18ClMnN2O2; potassium tert-butylate In tetrahydrofuran at 50℃; Inert atmosphere; Glovebox; Sealed tube;
Stage #2: With sodium hydroxide In tetrahydrofuran for 2h; Inert atmosphere; Glovebox; Sealed tube;
Stage #3: Glovebox; Inert atmosphere;
82%
at 315℃; for 1h; Temperature;72%
With N-methyl-N-trimethylsilyl-2,2,2-trifluoroacetamide; zinc trifluoromethanesulfonate In tetrahydrofuran at 70℃; for 24h; chemoselective reaction;
4-cyanobenzamide
3034-34-2

4-cyanobenzamide

4-Amidinobenzamide
54050-86-1

4-Amidinobenzamide

Conditions
ConditionsYield
With sodium amide In dimethyl sulfoxide Reagent/catalyst; Solvent; Sealed tube;85%
With hydrogenchloride; ethanol; benzene Behandeln des Reaktionsprodukts mit aethanol. Ammoniak;
ethylthioacetic acid methyl ester
2432-51-1

ethylthioacetic acid methyl ester

4-cyanobenzamide
3034-34-2

4-cyanobenzamide

N-butyryl-4-cyanobenzamide
1181384-68-8

N-butyryl-4-cyanobenzamide

Conditions
ConditionsYield
Stage #1: 4-cyanobenzamide With N-Bromosuccinimide; iron(II) chloride In acetonitrile at 20℃; for 0.0166667h;
Stage #2: ethylthioacetic acid methyl ester In acetonitrile at 45℃; for 20h;
85%
di-tert-butyl dicarbonate
24424-99-5

di-tert-butyl dicarbonate

4-cyanobenzamide
3034-34-2

4-cyanobenzamide

N,N-Boc2-4-cyanobenzamide

N,N-Boc2-4-cyanobenzamide

Conditions
ConditionsYield
With dmap In dichloromethane at 0 - 20℃; Inert atmosphere;85%
With dmap In acetonitrile at 20℃; for 15h; Inert atmosphere; Sealed tube;85%
With dmap In dichloromethane at 0 - 23℃; Inert atmosphere;84.5%
4-cyanobenzamide
3034-34-2

4-cyanobenzamide

N-(4-cyanobenzoyl)-N'-(4-cyanophenyl)urea

N-(4-cyanobenzoyl)-N'-(4-cyanophenyl)urea

Conditions
ConditionsYield
With tetra-N-butylammonium tribromide; 1,8-diazabicyclo[5.4.0]undec-7-ene In dichloromethane for 1h; Ambient temperature;83%
1-iodocyclohexane
626-62-0

1-iodocyclohexane

4-cyanobenzamide
3034-34-2

4-cyanobenzamide

4-cyano-N-cyclohexylbenzamide

4-cyano-N-cyclohexylbenzamide

Conditions
ConditionsYield
Stage #1: Cyclohexyl iodide; 4-cyanobenzamide With copper(l) iodide; lithium tert-butoxide In N,N-dimethyl-formamide; acetonitrile at 20℃; for 0.0833333h; Inert atmosphere;
Stage #2: In N,N-dimethyl-formamide; acetonitrile at 20℃; for 24h; Inert atmosphere; Irradiation;
83%
4-cyanobenzamide
3034-34-2

4-cyanobenzamide

terephthalamide
3010-82-0

terephthalamide

Conditions
ConditionsYield
With water; sodium hydroxide In ethanol at 90℃; for 17h;82%
With potassium tert-butylate In tert-butyl alcohol at 20℃; for 12h; Solvent; Inert atmosphere;78%
4-cyanobenzamide
3034-34-2

4-cyanobenzamide

Hexafluoroacetone
684-16-2

Hexafluoroacetone

4-cyano-N-(1,1,1,3,3,3-hexafluoropropan-2-ylidene)benzamide

4-cyano-N-(1,1,1,3,3,3-hexafluoropropan-2-ylidene)benzamide

Conditions
ConditionsYield
Stage #1: 4-cyanobenzamide; Hexafluoroacetone With pyridine In benzene at 20℃; for 0.5h;
Stage #2: With thionyl chloride In benzene at 20℃; for 2h;
82%

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