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Hunan Longxianng Runhui Trading Co.,Ltd

ProName:Benzene-1,3,5-tricarbaldehyde CasNo:3163-76-6 Molecular Formula:C9H6O3 Appearance:Powder Application:as ligands of porous materials DeliveryTime:2~3days PackAge:1gm, 2gm, 5gm, 10gm and customized pac... Port:S

Benzene-1,3,5-tricarbaldehyde CAS NO.3163-76-6

Cas:3163-76-6

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Dayang Chem (Hangzhou) Co.,Ltd.

Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities

BENZENE-1,3,5-TRICARBALDEHYDE

Cas:3163-76-6

Min.Order:1 Kilogram

FOB Price: $3.0

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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Manufacturer supply CAS 3163-76-6 with best quality

Cas:3163-76-6

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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Hebei Nengqian Chemical Import and Export Co., LTD

With our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin

1,3,5-Benzenetricarboxaldehyde

Cas:3163-76-6

Min.Order:1 Kilogram

FOB Price: $1.0 / 10.0

Type:Trading Company

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Shanghai Upbio Tech Co.,Ltd

1.In No Less 10 years exporting experience. you can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specializ

1,3,5-Benzenetricarboxaldehyde

Cas:3163-76-6

Min.Order:1 Gram

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Wuhan Han Sheng New Material Technology Co.,Ltd

Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We

1,3,5-TRIFORMYLBENZENE

Cas:3163-76-6

Min.Order:10 Kilogram

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Hunan chemfish Pharmaceutical co.,Ltd

Hunan chemfish Pharmaceutical co.,Ltd.located in Lugu High-tech industral park ,Hunan province . with its own R&D center and more than 10000㎡manufacture plant . Chemfish owns 40 reactors from 1000L to 8000L. With complete auxiliary equipment as

1,3,5-Benzenetricarboxaldehyde

Cas:3163-76-6

Min.Order:0 Metric Ton

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Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

CAS NO.:3163-76-6

Cas:3163-76-6

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Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

1,3,5-Benzenetricarboxaldehyde

Cas:3163-76-6

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Shaanxi Cuicheng Biomedical Technology Co., Ltd.

Why Choose Us: 1. Factory direct sales, so we can provide the competitive price and high quality product base on 8 years of production and R&D experience. 2. It is available in stock for quick shipment.Products could be packaged according to cu

1,3,5-Benzenetricarboxaldehyde

Cas:3163-76-6

Min.Order:1 Gram

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Type:Other

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SHANGHAI SYSTEAM BIOCHEM CO., LTD

We are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov

1,3,5-TRIFORMYLBENZENE

Cas:3163-76-6

Min.Order:100 Gram

FOB Price: $100.0 / 2000.0

Type:Lab/Research institutions

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Shanghai Minstar Chemical Co., Ltd

1,3,5-Benzenetricarboxaldehyde Basic information Product Name: 1,3,5-Benzenetricarboxaldehyde Synonyms: 1,3,5-Benzenetricarboxaldehyde;1,3,5-TRIFORMYLBENZENE;1,3,5-Benzenetricarbaldehyde;Benzene-1,3,5-tricarbaldehyde;triforMylbenzene;benzene-1,

1,3,5-Benzenetricarboxaldehyde

Cas:3163-76-6

Min.Order:1 Kilogram

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EAST CHEMSOURCES LIMITED

factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B

1,3,5-TRIFORMYLBENZENE

Cas:3163-76-6

Min.Order:1 Kilogram

FOB Price: $18.0 / 20.0

Type:Trading Company

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Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

1,3,5-TRIFORMYLBENZENE

Cas:3163-76-6

Min.Order:1 Gram

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KAISA GROUP INC

1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer

1,3,5-TRIFORMYLBENZENE

Cas:3163-76-6

Min.Order:1 Metric Ton

FOB Price: $1.5

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Suzhou Health Chemicals Co., Ltd.

High quality,stable supply chain.Appearance:white/off-white or light yellow Storage:Store in cool and dry place, keep away from strong light and heat. Package:aluminum bottle,glass bottle,PTFE bottle,cardboard drum Application:This product can be use

3163-76-6

Cas:3163-76-6

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Bluecrystal chem-union

We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp

1,3,5-TRIFORMYLBENZENE

Cas:3163-76-6

Min.Order:1 Metric Ton

FOB Price: $1.0

Type:Trading Company

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Hebei Mojin Biotechnology Co.,Ltd

1, High quality with competitive price:2, Fast and safe delivery3.Excellent pre-sales and after-sales service4. Well-trained and professional technologist and sales with rich experience in the field for 5-10 yearsAppearance:see detailed specification

1,3,5-Benzenetricarboxaldehyde

Cas:3163-76-6

Min.Order:0

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Win-Win chemical Co.Ltd

Stock products, own laboratory Package:Grams, Kilograms Application:For R&D Transportation:According to customer request Port:Shanghai

Benzene-1,3,5-tricarbaldehyde cas no. 3163-76-6 98%

Cas:3163-76-6

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GIHI CHEMICALS CO.,LIMITED

Lower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe

1,3,5-Benzenetricarboxaldehyde

Cas:3163-76-6

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Hangzhou Dingyan Chem Co., Ltd

R & D enterprises have their own stock in stock Package:1kg Application:pharmaceutical intermediates

1,3,5-Benzenetricarboxaldehyde

Cas:3163-76-6

Min.Order:0

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Type:Manufacturers

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Shanghai Acmec Biochemical Technology Co., Ltd.

Acmec is a leading manufacturer and supplier of biochemical reagents and life science products. We have over 40,000 items in stock (real-time inventory) and offer discounted prices to registered members of the online store ( www.acmec.com.cn ) Appea

Acmec Benzene-1,3,5-tricarbaldehyde 25g

Cas:3163-76-6

Min.Order:1 bottle

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Shanghai Finebiotech Co.,Ltd.

Shanghai Finebiotech Co.,Ltd.was established in 2020, which providing professional chemical services. As a customer-oriented company, we have distinguished ourself from others in providing worldwide customers with cost-effective and efficient service

1,3,5-Benzenetricarboxaldehyde

Cas:3163-76-6

Min.Order:0

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Wuxi TAA Chemical Industry Co.,LTD.

1.A strong technical force and advanced processing equipments. The quality of the products has been strictly inspected and all kinds of index have reached or exceeded domestic and international standards.2. Now we have established long-term stable re

1,3,5-Benzenetricarboxaldehyde

Cas:3163-76-6

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Henan Tianfu Chemical Co., Ltd.

1.Our services:A.Supply sampleB.The packing also can be according the customers` requirmentC.Any inquiries will be replied within 24 hoursD.we provide Commerical Invoice, Packing List, Bill of loading, COA , Health certificate and Origin certificate.

1,3,5-Benzenetricarboxaldehyde

Cas:3163-76-6

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Xian Changyue Biological Technology Co., Ltd.

best seller Application:API

1,3,5-Benzenetricarboxaldehyde

Cas:3163-76-6

Min.Order:0

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Type:Manufacturers

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Hebei Sankai Chemical Technology Co., Ltd

1. Product advantages? High purity, all above 98.5%, no impurities after dissolution? We will test each batch to ensure quality? OEM and private brand services designed for free? Various cap colors available? We can also provide MT1 peptide powder2.

1,3,5-Benzenetricarboxaldehyde

Cas:3163-76-6

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Antimex Chemical Limied

Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali

1,3,5-Benzenetricarboxaldehyde

Cas:3163-76-6

Min.Order:0

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Type:Lab/Research institutions

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Qingdao Beluga Import and Export Co., LTD

We are a trading company aiming at providing high-quality services to customers. Established for many years, with good reputation in the industry Storage:Sealed and preserved Application:Fine chemical intermediates, used as the main raw material for

1,3,5-TRIFORMYLBENZENE

Cas:3163-76-6

Min.Order:0

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HANGZHOU TIANYE CHEMICALS CO., LTD.

We product this chemical more than 10 years . We are very experience to export it to many countries, Our superior & stable quality , competitive price gain warm reception from our customers. Application:Chemical intermediate

Benzene-1,3,5-tricarbaldehyde

Cas:3163-76-6

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Synthetic route

1,3,5-tris(hydroxymethyl)benzene
4464-18-0

1,3,5-tris(hydroxymethyl)benzene

benzene-1,3,5-trialdehyde
3163-76-6

benzene-1,3,5-trialdehyde

Conditions
ConditionsYield
With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione In tert-butyl alcohol for 5h; Reflux;100%
With pyridinium chlorochromate99%
With Dess-Martin periodane In dichloromethane for 15h;98%
triformylmethane
18655-47-5

triformylmethane

benzene-1,3,5-trialdehyde
3163-76-6

benzene-1,3,5-trialdehyde

Conditions
ConditionsYield
In water at 20℃; for 168h;96%
1,3,5-trimethyl-benzene
108-67-8

1,3,5-trimethyl-benzene

benzene-1,3,5-trialdehyde
3163-76-6

benzene-1,3,5-trialdehyde

Conditions
ConditionsYield
With 1,4-dichloro-1,4-diazoniabicyclo[2,2,2]octane bis-chloride; water at 40℃; for 0.333333h; pH=7;90%
(i) (irradiation), Br2, (ii) aq. H2SO4; Multistep reaction;
Multi-step reaction with 4 steps
1: bromine / 160 °C / Irradiation.UV-Licht
2: tetrachloromethane; dibenzoyl peroxide; <α,α'>azoisobutyronitrile; N-bromo-succinimide
3: methanol / Behandeln der Reaktionsloesung mit warmer wss. Natriumperchlorat-Loesung
4: N,N-dimethyl-4-nitroso-aniline / Hydrolysieren des Reaktionsprodukts
View Scheme
Multi-step reaction with 3 steps
1: bromine / 160 °C / Irradiation.UV-Licht
2: tetrachloromethane; dibenzoyl peroxide; <α,α'>azoisobutyronitrile; N-bromo-succinimide
3: hexamethylenetetramine
View Scheme
Multi-step reaction with 2 steps
1: N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) / tetrachloromethane / 15 h / 85 °C
2: sodium methylate; 2-nitropropane / methanol; ethyl acetate / 6 h / 30 °C
View Scheme
1,3,5-Tris(bromomethyl)benzene
18226-42-1

1,3,5-Tris(bromomethyl)benzene

benzene-1,3,5-trialdehyde
3163-76-6

benzene-1,3,5-trialdehyde

Conditions
ConditionsYield
Stage #1: 1,3,5-Tris(bromomethyl)benzene With 2-nitropropane; sodium methylate In methanol; ethyl acetate at 30℃; for 6h;
Stage #2: With water In methanol; ethyl acetate
80.8%
With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione In dimethyl sulfoxide at 20℃;57%
With 2-nitropropane; sodium ethanolate In ethanol; dimethyl sulfoxide for 3h; Ambient temperature;52%
α,α,α',α',α'',α''-hexabromomesitylene
1889-66-3

α,α,α',α',α'',α''-hexabromomesitylene

benzene-1,3,5-trialdehyde
3163-76-6

benzene-1,3,5-trialdehyde

Conditions
ConditionsYield
With sulfuric acid In water for 1h;80%
With morpholine for 4h; Reflux;60%
With sulfuric acid
(i) Mor, (ii) aq. HCl; Multistep reaction;
(E)-3-(dimethylamino)acrolein
927-63-9, 692-32-0

(E)-3-(dimethylamino)acrolein

benzene-1,3,5-trialdehyde
3163-76-6

benzene-1,3,5-trialdehyde

Conditions
ConditionsYield
With acetic acid for 10h; Heating;60%
1,3,5-benzene tris(carbonyl chloride)
4422-95-1

1,3,5-benzene tris(carbonyl chloride)

A

Isophthalaldehyde
626-19-7

Isophthalaldehyde

B

benzene-1,3,5-trialdehyde
3163-76-6

benzene-1,3,5-trialdehyde

Conditions
ConditionsYield
With hydrogen; thiourea; Pd-BaSO4 In xylene for 10h; Heating;A 19%
B 59%
1,3,5-(N-methyl-N-methoxy)trimellitamide

1,3,5-(N-methyl-N-methoxy)trimellitamide

benzene-1,3,5-trialdehyde
3163-76-6

benzene-1,3,5-trialdehyde

Conditions
ConditionsYield
With sodium bis(2-methoxyethoxy)aluminium hydride In toluene at 0 - 20℃; for 6h;55%
sorbic Acid
110-44-1

sorbic Acid

N,N-dimethyl-formamide
68-12-2, 33513-42-7

N,N-dimethyl-formamide

A

benzene-1,3,5-trialdehyde
3163-76-6

benzene-1,3,5-trialdehyde

B

2-chlorobenzene-1,3,5-tricarboxaldehyde
102626-20-0

2-chlorobenzene-1,3,5-tricarboxaldehyde

Conditions
ConditionsYield
With trichlorophosphate at 80 - 90℃;A 37%
B 5%
3-penten-2-ol
1569-50-2

3-penten-2-ol

N,N-dimethyl-formamide
68-12-2, 33513-42-7

N,N-dimethyl-formamide

A

Isophthalaldehyde
626-19-7

Isophthalaldehyde

B

benzene-1,3,5-trialdehyde
3163-76-6

benzene-1,3,5-trialdehyde

Conditions
ConditionsYield
With trichlorophosphate for 6h; Heating;A 26%
B 6%
With trichlorophosphate for 6h; Heating; other 3-buten-2-ols;A 26%
B 6%
1,3,5-benzene tris(carbonyl chloride)
4422-95-1

1,3,5-benzene tris(carbonyl chloride)

benzene-1,3,5-trialdehyde
3163-76-6

benzene-1,3,5-trialdehyde

Conditions
ConditionsYield
With hydrogen; thiourea; Pd-BaSO4 In xylene for 10h;12%
With lithium aluminium tetrahydride; tert-butyl alcohol In diethyl ether; diethylene glycol dimethyl ether
With lithium tri-t-butoxyaluminum hydride
Multi-step reaction with 2 steps
1: benzene; pyridine
2: LiAlH4
View Scheme
1,3,5-tris(3,5-dimethylpyrazolyl-1-carbonyl)benzene
118927-16-5

1,3,5-tris(3,5-dimethylpyrazolyl-1-carbonyl)benzene

benzene-1,3,5-trialdehyde
3163-76-6

benzene-1,3,5-trialdehyde

Conditions
ConditionsYield
With lithium aluminium tetrahydride
1,3,5-tris-pyridiniomethyl-benzene; triperchlorate

1,3,5-tris-pyridiniomethyl-benzene; triperchlorate

benzene-1,3,5-trialdehyde
3163-76-6

benzene-1,3,5-trialdehyde

Conditions
ConditionsYield
With p-dimethylaminonitrosobenzene Hydrolysieren des Reaktionsprodukts;
Propargylic aldehyde
624-67-9

Propargylic aldehyde

benzene-1,3,5-trialdehyde
3163-76-6

benzene-1,3,5-trialdehyde

Conditions
ConditionsYield
With tetracarbonyl nickel
3,3-diethoxypropanal
6367-37-9

3,3-diethoxypropanal

A

benzene-1,3,5-trialdehyde
3163-76-6

benzene-1,3,5-trialdehyde

B

(E)-3-[2-((Z)-2-Hydroxy-vinyl)-furan-3-yloxy]-propenal
111008-70-9

(E)-3-[2-((Z)-2-Hydroxy-vinyl)-furan-3-yloxy]-propenal

C

5-(1,4,6-Trioxa-azulen-5-yl)-benzene-1,3-dicarbaldehyde

5-(1,4,6-Trioxa-azulen-5-yl)-benzene-1,3-dicarbaldehyde

D

(3Z,13Z)-5-(2,6,10,12,16-Pentaoxa-tricyclo[13.3.0.05,9]octadeca-1(15),3,5(9),7,13,17-hexaen-11-yl)-benzene-1,3-dicarbaldehyde

(3Z,13Z)-5-(2,6,10,12,16-Pentaoxa-tricyclo[13.3.0.05,9]octadeca-1(15),3,5(9),7,13,17-hexaen-11-yl)-benzene-1,3-dicarbaldehyde

E

(E)-3-[2-((Z)-2-{(E)-1-Hydroxy-3-[2-((Z)-2-hydroxy-vinyl)-furan-3-yloxy]-allyloxy}-vinyl)-furan-3-yloxy]-propenal
111008-72-1

(E)-3-[2-((Z)-2-{(E)-1-Hydroxy-3-[2-((Z)-2-hydroxy-vinyl)-furan-3-yloxy]-allyloxy}-vinyl)-furan-3-yloxy]-propenal

F

(E)-3-[2-((Z)-2-{(E)-1-Hydroxy-3-[2-((Z)-2-{(E)-1-hydroxy-3-[2-((Z)-2-hydroxy-vinyl)-furan-3-yloxy]-allyloxy}-vinyl)-furan-3-yloxy]-allyloxy}-vinyl)-furan-3-yloxy]-propenal
111008-73-2

(E)-3-[2-((Z)-2-{(E)-1-Hydroxy-3-[2-((Z)-2-{(E)-1-hydroxy-3-[2-((Z)-2-hydroxy-vinyl)-furan-3-yloxy]-allyloxy}-vinyl)-furan-3-yloxy]-allyloxy}-vinyl)-furan-3-yloxy]-propenal

Conditions
ConditionsYield
In water for 240h;
1,4-dihydrobenzoic acid
4794-04-1

1,4-dihydrobenzoic acid

N,N-dimethyl-formamide
68-12-2, 33513-42-7

N,N-dimethyl-formamide

benzene-1,3,5-trialdehyde
3163-76-6

benzene-1,3,5-trialdehyde

Conditions
ConditionsYield
With trichlorophosphate 1.) room temp., 1 h; Yield given. Multistep reaction;
cyclohexadieneacetyl chloride
3217-88-7

cyclohexadieneacetyl chloride

N,N-dimethyl-formamide
68-12-2, 33513-42-7

N,N-dimethyl-formamide

benzene-1,3,5-trialdehyde
3163-76-6

benzene-1,3,5-trialdehyde

Conditions
ConditionsYield
With trichlorophosphate 1.) room temp., 1 h; Yield given. Multistep reaction;
penta-1,3-diene
504-60-9

penta-1,3-diene

N,N-dimethyl-formamide
68-12-2, 33513-42-7

N,N-dimethyl-formamide

benzene-1,3,5-trialdehyde
3163-76-6

benzene-1,3,5-trialdehyde

Conditions
ConditionsYield
(i) PCl5, (ii) H2O; Multistep reaction;
N,N-dimethyl-formamide
68-12-2, 33513-42-7

N,N-dimethyl-formamide

(7-dimethylamino-2,4,6-heptatrienylidene)dimethylammonium perchlorate

(7-dimethylamino-2,4,6-heptatrienylidene)dimethylammonium perchlorate

benzene-1,3,5-trialdehyde
3163-76-6

benzene-1,3,5-trialdehyde

Conditions
ConditionsYield
(i) chloromethylene-dimethyl-ammonium chloride, CHCl3, (ii) H2O; Multistep reaction;
tetrahydrofuran
109-99-9

tetrahydrofuran

1,3,5-tris(3,5-dimethylpyrazolyl-1-carbonyl)benzene
118927-16-5

1,3,5-tris(3,5-dimethylpyrazolyl-1-carbonyl)benzene

LiAlH4

LiAlH4

benzene-1,3,5-trialdehyde
3163-76-6

benzene-1,3,5-trialdehyde

trimesinic acid-trichloride

trimesinic acid-trichloride

benzene-1,3,5-trialdehyde
3163-76-6

benzene-1,3,5-trialdehyde

Conditions
ConditionsYield
With Pd-BaSO4 Hydrogenation;
benzene-1,3,5-tricarboxylic acid
554-95-0

benzene-1,3,5-tricarboxylic acid

A

Isophthalaldehyde
626-19-7

Isophthalaldehyde

B

benzene-1,3,5-trialdehyde
3163-76-6

benzene-1,3,5-trialdehyde

Conditions
ConditionsYield
With hydrogen; 2,2-dimethylpropanoic anhydride; tetrakis(triphenylphosphine) palladium(0) In tetrahydrofuran at 80℃; under 22501.8 Torr; for 24h;A 6 % Chromat.
B 86 % Spectr.
triformylmethane
18655-47-5

triformylmethane

adenosine
58-61-7

adenosine

A

benzene-1,3,5-trialdehyde
3163-76-6

benzene-1,3,5-trialdehyde

B

6-(3,5-diformyl-4-hydroxy-1,4-dihydropyridin-1-yl)-9-(β-D-ribofuranosyl)purine

6-(3,5-diformyl-4-hydroxy-1,4-dihydropyridin-1-yl)-9-(β-D-ribofuranosyl)purine

C

6-(3,5-diformyl-2-hydroxy-1,2-dihydropyridin-1-yl)-9-(β-D-ribofuranosyl)purine

6-(3,5-diformyl-2-hydroxy-1,2-dihydropyridin-1-yl)-9-(β-D-ribofuranosyl)purine

Conditions
ConditionsYield
In 1,4-dioxane; water at 70℃; for 3h;
1,3,5-tris-(methoxycarbonyl)benzene
2672-58-4

1,3,5-tris-(methoxycarbonyl)benzene

benzene-1,3,5-trialdehyde
3163-76-6

benzene-1,3,5-trialdehyde

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 79 percent / LiAlH4
2: 98 percent / Dess-Martin reagent / CH2Cl2 / 15 h
View Scheme
Multi-step reaction with 2 steps
1: lithium aluminium tetrahydride / tetrahydrofuran / 14 h / 0 - 20 °C / Inert atmosphere
2: 2-iodoxybenzoic acid / tert-butyl alcohol / 2 h / 95 °C / Reflux; Inert atmosphere
View Scheme
Multi-step reaction with 2 steps
1: lithium aluminium tetrahydride / tetrahydrofuran / 16 h / 0 - 70 °C / Inert atmosphere
2: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / acetonitrile / 1 h / 80 °C / Inert atmosphere
View Scheme
Multi-step reaction with 2 steps
1: lithium aluminium tetrahydride / tetrahydrofuran / Reflux
2: pyridinium chlorochromate
View Scheme
benzene-1,3,5-tricarboxylic acid
554-95-0

benzene-1,3,5-tricarboxylic acid

benzene-1,3,5-trialdehyde
3163-76-6

benzene-1,3,5-trialdehyde

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 90 percent / SOCl2, DMF / 2.5 h / Heating
2: 12 percent / H2, thiourea / Pd/BaSO4 / xylene / 10 h
View Scheme
Multi-step reaction with 3 steps
1: SOCl2
2: benzene; pyridine
3: LiAlH4
View Scheme
Stage #1: benzene-1,3,5-tricarboxylic acid With sulfuric acid In methanol for 12h; Reflux;
Stage #2: With lithium aluminium tetrahydride In tetrahydrofuran at 0℃; for 12h; Inert atmosphere;
Stage #3: With pyridinium chlorochromate In diethyl ether; dichloromethane
Stage #1: benzene-1,3,5-tricarboxylic acid With sulfuric acid In methanol for 12h; Reflux;
Stage #2: With lithium aluminium tetrahydride In tetrahydrofuran at 0℃; for 12h; Inert atmosphere;
Multi-step reaction with 3 steps
1.1: sulfuric acid / 24 h / Reflux
2.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / Inert atmosphere
2.2: 24 h / Reflux
3.1: pyridinium chlorochromate / dichloromethane / 6 h / 20 °C
View Scheme
3,5-bis(bromomethyl)toluene
19294-04-3

3,5-bis(bromomethyl)toluene

benzene-1,3,5-trialdehyde
3163-76-6

benzene-1,3,5-trialdehyde

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: tetrachloromethane; dibenzoyl peroxide; <α,α'>azoisobutyronitrile; N-bromo-succinimide
2: methanol / Behandeln der Reaktionsloesung mit warmer wss. Natriumperchlorat-Loesung
3: N,N-dimethyl-4-nitroso-aniline / Hydrolysieren des Reaktionsprodukts
View Scheme
Multi-step reaction with 2 steps
1: tetrachloromethane; dibenzoyl peroxide; <α,α'>azoisobutyronitrile; N-bromo-succinimide
2: hexamethylenetetramine
View Scheme
1,3,5-trimethyl-benzene
108-67-8

1,3,5-trimethyl-benzene

nitrosyl chloride

nitrosyl chloride

benzene-1,3,5-trialdehyde
3163-76-6

benzene-1,3,5-trialdehyde

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: Br2 / Irradiation
2: H2SO4
View Scheme
Multi-step reaction with 2 steps
1: Br2 / 155 - 180 °C / Irradiation
2: (i) Mor, (ii) aq. HCl
View Scheme
triethyl benzene-1,3,5-tricarboxylate
4105-92-4

triethyl benzene-1,3,5-tricarboxylate

benzene-1,3,5-trialdehyde
3163-76-6

benzene-1,3,5-trialdehyde

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: lithium borohydride / tetrahydrofuran
2: pyridinium chlorochromate
View Scheme
trimethyl 1,3,5-benzenetricarboxylate

trimethyl 1,3,5-benzenetricarboxylate

benzene-1,3,5-trialdehyde
3163-76-6

benzene-1,3,5-trialdehyde

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / Inert atmosphere
1.2: 24 h / Reflux
2.1: pyridinium chlorochromate / dichloromethane / 6 h / 20 °C
View Scheme
benzene-1,3,5-trialdehyde
3163-76-6

benzene-1,3,5-trialdehyde

(1R,2R)-1,2-diaminocyclohexane
20439-47-8

(1R,2R)-1,2-diaminocyclohexane

CC3-R

CC3-R

Conditions
ConditionsYield
In dichloromethane at 20℃; for 12h;100%
With trifluoroacetic acid In dichloromethane at 20℃; for 120h;83%
With trifluoroacetic acid In dichloromethane at 20℃;83%
With trifluoroacetic acid In dichloromethane at 20℃;83%
In dichloromethane at 20℃;70%
benzene-1,3,5-trialdehyde
3163-76-6

benzene-1,3,5-trialdehyde

2,2-diethoxy-ethanamine
645-36-3

2,2-diethoxy-ethanamine

C27H45N3O6

C27H45N3O6

Conditions
ConditionsYield
In methanol; chloroform at 20℃; for 1h; Inert atmosphere;98%
benzene-1,3,5-trialdehyde
3163-76-6

benzene-1,3,5-trialdehyde

malononitrile
109-77-3

malononitrile

1,3,5-tris(2',2'-ethenyldicarbonnitrile)benzene
186508-05-4

1,3,5-tris(2',2'-ethenyldicarbonnitrile)benzene

Conditions
ConditionsYield
With 1,2,4,5-tetramethylbenzene; C193H176N12O6Zn2(4+) In chloroform-d1; [D3]acetonitrile at 20℃; for 48h; Reagent/catalyst; Knoevenagel Condensation;97%
With piperidine In 1,2-dimethoxyethane at 20℃; for 0.5h;95%
With piperidine In butan-1-ol at 50℃; for 8h;87%
With boron trioxide In ethanol for 2h; Heating;15%
3,6-dioxa-1,8-diaminooctane
929-59-9

3,6-dioxa-1,8-diaminooctane

C96H118N2O2(2+)*2F6P(1-)

C96H118N2O2(2+)*2F6P(1-)

benzene-1,3,5-trialdehyde
3163-76-6

benzene-1,3,5-trialdehyde

C36H48N6O6*C96H118N2O2(2+)*2F6P(1-)

C36H48N6O6*C96H118N2O2(2+)*2F6P(1-)

Conditions
ConditionsYield
Stage #1: 3,6-dioxa-1,8-diaminooctane; benzene-1,3,5-trialdehyde In chloroform-d1 at 20℃; for 1h;
Stage #2: C96H118N2O2(2+)*2F6P(1-) In chloroform-d1 at 20℃; for 2h;
97%
benzene-1,3,5-trialdehyde
3163-76-6

benzene-1,3,5-trialdehyde

ethylenediamine
107-15-3

ethylenediamine

propane-1,3-diamine

propane-1,3-diamine

Conditions
ConditionsYield
In dichloromethane at 20℃; Cooling with ice;96%
In ethyl acetate at 22℃; for 72.5h;74%
In methanol Inert atmosphere; Cooling with ice;
benzene-1,3,5-trialdehyde
3163-76-6

benzene-1,3,5-trialdehyde

3-amino-2,4,6-trinitrotoluene
22603-58-3

3-amino-2,4,6-trinitrotoluene

3,3',3''-((1E,1'E,1''E)-benzene-1,3,5-triyltris(ethene-2,1-diyl))tris(2,4,6-trinitroaniline)

3,3',3''-((1E,1'E,1''E)-benzene-1,3,5-triyltris(ethene-2,1-diyl))tris(2,4,6-trinitroaniline)

Conditions
ConditionsYield
With piperidine In benzene for 16h; Knoevenagel Condensation; Dean-Stark; Reflux;96%
benzene-1,3,5-trialdehyde
3163-76-6

benzene-1,3,5-trialdehyde

3,4,5-trimethoxybenzohydrazide
3291-03-0

3,4,5-trimethoxybenzohydrazide

N'1,N'3,N'5-tris(3,4,5-trimethoxybenzylidene)benzene-1,3,5-tricarbohydrazide

N'1,N'3,N'5-tris(3,4,5-trimethoxybenzylidene)benzene-1,3,5-tricarbohydrazide

Conditions
ConditionsYield
With trifluoroacetic acid In chloroform for 4h; Reflux;95%
benzene-1,3,5-trialdehyde
3163-76-6

benzene-1,3,5-trialdehyde

1,3,5-tris(aminomethyl)-2,4,6-trifluorobenzene

1,3,5-tris(aminomethyl)-2,4,6-trifluorobenzene

C72H48F12N12

C72H48F12N12

Conditions
ConditionsYield
In methanol at 20℃; for 49h; Solvent;95%
1,2-Dihydro-N-methylcyclohepta[b]pyrrol-2-one
3336-87-6

1,2-Dihydro-N-methylcyclohepta[b]pyrrol-2-one

benzene-1,3,5-trialdehyde
3163-76-6

benzene-1,3,5-trialdehyde

1,3,5-tris[bis(1,2-dihydro-2-oxo-N-methylcyclohepta[b]pyrrol-3-yl)methyl]benzene

1,3,5-tris[bis(1,2-dihydro-2-oxo-N-methylcyclohepta[b]pyrrol-3-yl)methyl]benzene

Conditions
ConditionsYield
With trifluoroacetic acid In dichloromethane at 20℃; for 48h;94%
1,3-bis(α-aminoisopropyl)benzene
19937-49-6

1,3-bis(α-aminoisopropyl)benzene

benzene-1,3,5-trialdehyde
3163-76-6

benzene-1,3,5-trialdehyde

C54H60N6

C54H60N6

Conditions
ConditionsYield
With acetic acid In acetonitrile at 20℃; for 168h;92%
2,4,6-Trinitrotoluene
118-96-7

2,4,6-Trinitrotoluene

benzene-1,3,5-trialdehyde
3163-76-6

benzene-1,3,5-trialdehyde

1,3,5-tris(2,4,6-trinitrostyryl)benzene

1,3,5-tris(2,4,6-trinitrostyryl)benzene

Conditions
ConditionsYield
With piperidine In benzene for 14h; Knoevenagel Condensation; Dean-Stark; Reflux;90.3%
benzene-1,3,5-trialdehyde
3163-76-6

benzene-1,3,5-trialdehyde

1,2-Dihydro-N-phenylcyclohepta[b]pyrrol-2-one
303730-52-1

1,2-Dihydro-N-phenylcyclohepta[b]pyrrol-2-one

1,3,5-tris[bis(1,2-dihydro-2-oxo-N-phenylcyclohepta[b]pyrrol-3-yl)methyl]benzene

1,3,5-tris[bis(1,2-dihydro-2-oxo-N-phenylcyclohepta[b]pyrrol-3-yl)methyl]benzene

Conditions
ConditionsYield
With trifluoroacetic acid In dichloromethane at 20℃; for 48h;90%
benzene-1,3,5-trialdehyde
3163-76-6

benzene-1,3,5-trialdehyde

thiosemicarbazide
79-19-6

thiosemicarbazide

2,2′,2″-(benzene-1,3,5-triyltris(methanylylidene))tris(hydrazinecarbothioamide)
67002-24-8

2,2′,2″-(benzene-1,3,5-triyltris(methanylylidene))tris(hydrazinecarbothioamide)

Conditions
ConditionsYield
With acetic acid In methanol for 4h; Reflux;90%
benzene-1,3,5-trialdehyde
3163-76-6

benzene-1,3,5-trialdehyde

girard's reagent T
123-46-6

girard's reagent T

2,2',2''-((2E,2'E,2''E)-2,2',2''-(benzene-1,3,5-triyltris(methanylylidene))tris(hydrazin-1-yl-2-ylidene))tris(N,N,N-trimethyl-2-oxoethanaminium) chloride

2,2',2''-((2E,2'E,2''E)-2,2',2''-(benzene-1,3,5-triyltris(methanylylidene))tris(hydrazin-1-yl-2-ylidene))tris(N,N,N-trimethyl-2-oxoethanaminium) chloride

Conditions
ConditionsYield
In methanol for 24h; Reflux;90%
benzene-1,3,5-trialdehyde
3163-76-6

benzene-1,3,5-trialdehyde

1,3-bis[1-(4-aminophenyl)-1-methylethylidene]benzene
2687-27-6

1,3-bis[1-(4-aminophenyl)-1-methylethylidene]benzene

C90H84N6

C90H84N6

Conditions
ConditionsYield
With acetic acid In acetonitrile at 20℃; for 36h; Concentration;90%
benzene-1,3,5-trialdehyde
3163-76-6

benzene-1,3,5-trialdehyde

4-(Trifluoromethyl)phenylacetonitrile
2338-75-2

4-(Trifluoromethyl)phenylacetonitrile

C36H18F9N3

C36H18F9N3

Conditions
ConditionsYield
With sodium ethanolate In ethanol for 3h; Knoevenagel Condensation; Reflux;90%
(S,S)-N-methyl-1,2-diphenylethylenediamine
203923-04-0

(S,S)-N-methyl-1,2-diphenylethylenediamine

benzene-1,3,5-trialdehyde
3163-76-6

benzene-1,3,5-trialdehyde

C54H48N6
1208333-07-6

C54H48N6

Conditions
ConditionsYield
Stage #1: (S,S)-N-methyl-1,2-diphenylethylenediamine; benzene-1,3,5-trialdehyde In dichloromethane at 20℃; for 3h; Inert atmosphere;
Stage #2: With N-Bromosuccinimide In dichloromethane at 0 - 20℃; Inert atmosphere;
88%
benzene-1,3,5-trialdehyde
3163-76-6

benzene-1,3,5-trialdehyde

3,5-bis(trifluoromethyl)phenylacetonitrile
85068-32-2

3,5-bis(trifluoromethyl)phenylacetonitrile

C39H15F18N3

C39H15F18N3

Conditions
ConditionsYield
With sodium ethanolate In ethanol for 3h; Knoevenagel Condensation; Reflux;88%
benzene-1,3,5-trialdehyde
3163-76-6

benzene-1,3,5-trialdehyde

(1S, 2S)-trans-diaminocyclopentane dihydrochloride

(1S, 2S)-trans-diaminocyclopentane dihydrochloride

C66H72N12

C66H72N12

Conditions
ConditionsYield
With triethylamine In methanol; dichloromethane at 20℃; for 240h;87%
benzene-1,3,5-trialdehyde
3163-76-6

benzene-1,3,5-trialdehyde

2,2-Dimethyl-1,3-propanediol
126-30-7

2,2-Dimethyl-1,3-propanediol

5-(5,5-Dimethyl-[1,3]dioxan-2-yl)-benzene-1,3-dicarbaldehyde
950608-82-9

5-(5,5-Dimethyl-[1,3]dioxan-2-yl)-benzene-1,3-dicarbaldehyde

Conditions
ConditionsYield
With toluene-4-sulfonic acid86%
benzene-1,3,5-trialdehyde
3163-76-6

benzene-1,3,5-trialdehyde

(1R,2R)-1,2-diaminocyclohexane
20439-47-8

(1R,2R)-1,2-diaminocyclohexane

rac-CC3

rac-CC3

Conditions
ConditionsYield
In dichloromethane at 20℃; for 120h;85%
benzene-1,3,5-trialdehyde
3163-76-6

benzene-1,3,5-trialdehyde

N-benzylhydroxylamine hydrochloride
29601-98-7

N-benzylhydroxylamine hydrochloride

(1Z,1'Z,1''Z)-1,1',1''-(benzene-1,3,5-triyl)tris(N-benzylmethanimine oxide)

(1Z,1'Z,1''Z)-1,1',1''-(benzene-1,3,5-triyl)tris(N-benzylmethanimine oxide)

Conditions
ConditionsYield
With sodium hydrogencarbonate; sodium sulfate In tetrahydrofuran at 90℃; under 11251.1 Torr; for 6h; Microwave irradiation;85%
benzene-1,3,5-trialdehyde
3163-76-6

benzene-1,3,5-trialdehyde

(1R,2R)-1,2-diaminocyclohexane
20439-47-8

(1R,2R)-1,2-diaminocyclohexane

Conditions
ConditionsYield
With trifluoroacetic acid In dichloromethane at 20℃; for 120h;83%
benzene-1,3,5-trialdehyde
3163-76-6

benzene-1,3,5-trialdehyde

1,2-bis(4-(bis(4-methoxyphenyl)amino)phenyl)ethane-1,2-dione

1,2-bis(4-(bis(4-methoxyphenyl)amino)phenyl)ethane-1,2-dione

N,N',N'',N"',N"",N""'-(4,4',4'',4"',4"",4""'-(2,2',2''-(benzene-1,3,5-triyl)tris(1H-imidazole-5,4,2-triyl))hexakis(4,1-phenylene))hexakis(4-methoxy-N-(4-methoxyphenyl)benzenamine)

N,N',N'',N"',N"",N""'-(4,4',4'',4"',4"",4""'-(2,2',2''-(benzene-1,3,5-triyl)tris(1H-imidazole-5,4,2-triyl))hexakis(4,1-phenylene))hexakis(4-methoxy-N-(4-methoxyphenyl)benzenamine)

Conditions
ConditionsYield
With ammonium acetate; acetic acid at 140℃; for 15h;83%
benzene-1,3,5-trialdehyde
3163-76-6

benzene-1,3,5-trialdehyde

4-methoxybenzoic acid hydrazide
3290-99-1

4-methoxybenzoic acid hydrazide

N'1,N'3,N'5-tris(4-methoxybenzylidene)benzene-1,3,5-tricarbohydrazide

N'1,N'3,N'5-tris(4-methoxybenzylidene)benzene-1,3,5-tricarbohydrazide

Conditions
ConditionsYield
With trifluoroacetic acid In chloroform for 4h; Reflux;82%
benzene-1,3,5-trialdehyde
3163-76-6

benzene-1,3,5-trialdehyde

[(p-methylphenyl)sulfonylmethyl]isonitrile
38622-91-2, 36635-61-7

[(p-methylphenyl)sulfonylmethyl]isonitrile

C15H9N3O3
1006055-17-9

C15H9N3O3

Conditions
ConditionsYield
With potassium carbonate In methanol at 70℃; van Leusen oxazole synthesis;81%
benzene-1,3,5-trialdehyde
3163-76-6

benzene-1,3,5-trialdehyde

1,1-dimethylethylenediamine
811-93-8

1,1-dimethylethylenediamine

C60H72N12

C60H72N12

Conditions
ConditionsYield
In dichloromethane at 20℃; for 96h; Cooling with ice;81%

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