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Dayang Chem (Hangzhou) Co.,Ltd.

DayangChem exported this product to many countries and regions at best price. If you are looking for the material's manufacturer or supplier in China, DayangChem is your best choice. Pls contact with us freely for getting detailed product spe

(Z)-3-nonen-1-al

Cas:31823-43-5

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

inquiry

Qingdao Beluga Import and Export Co., LTD

3-nonenal,(Z)-3-nonenal CAS:31823-43-5 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic

3-nonenal,(Z)-3-nonenal CAS:31823-43-5

Cas:31823-43-5

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

3-Nonenal, (3Z)-

Cas:31823-43-5

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

3-nonenal,(Z)-3-nonenal

Cas:31823-43-5

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

inquiry

TAIZHOU ZHENYU BIOTECHNOLOGY CO., LTD

Zhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed

3-nonenal,(Z)-3-nonenal

Cas:31823-43-5

Min.Order:1 Kilogram

FOB Price: $2.0

Type:Lab/Research institutions

inquiry

GIHI CHEMICALS CO.,LIMITED

Lower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe

3-Nonenal

Cas:31823-43-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Kono Chem Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou

(3Z)-non-3-enal

Cas:31823-43-5

Min.Order:0

Negotiable

Type:Other

inquiry

Hangzhou Dingyan Chem Co., Ltd

R & D enterprises have their own stock in stock Package:1kg Application:pharmaceutical intermediates

3-Nonenal, (3Z)-

Cas:31823-43-5

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Henan Tianfu Chemical Co., Ltd.

1.Our services:A.Supply sampleB.The packing also can be according the customers` requirmentC.Any inquiries will be replied within 24 hoursD.we provide Commerical Invoice, Packing List, Bill of loading, COA , Health certificate and Origin certificate.

3-Nonenal, (3Z)-

Cas:31823-43-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Antimex Chemical Limied

Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali

3-Nonenal, (3Z)-

Cas:31823-43-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Fandachem Co.,Ltd

3-NONENAL,(Z)-3-NONENALAppearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express

3-NONENAL,(Z)-3-NONENAL

Cas:31823-43-5

Min.Order:0

Negotiable

Type:Other

inquiry

Hangzhou Sartort Biopharma Co., Ltd

Best quality with low price Storage:ln stock Package:25kg/Barrel Application:Chemicals Transportation:Express/Sea/Air Port:Shanghai

(3Z)-non-3-enal

Cas:31823-43-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Henan Kanbei Chemical Co.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

3-nonenal,(Z)-3-nonenal

Cas:31823-43-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

SAGECHEM LIMITED

31823-43-5 Application:intermediate

3-Nonenal, (3Z)-

Cas:31823-43-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

ZHEJIANG JIUZHOU CHEM CO.,LTD

factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

3-nonenal,(Z)-3-nonenal

Cas:31823-43-5

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Amadis Chemical Co., Ltd.

1.Professional synthesis laboratory and production base. 2.Strong synthesis team and service team. 3.Professional data management system. 4.We provide the professional test date and product information ,ex. HNMR ,CNMR,FNMR, HPLC/G

3-nonenal,(Z)-3-nonenal

Cas:31823-43-5

Min.Order:10 Milligram

Negotiable

Type:Lab/Research institutions

inquiry

Watson International Ltd

Watson International Ltd' has a very strong R&D and technical capacity supported by FCAD's platform. The subsidiaries under FCAD Group have accumulated much know-how of different fine chemical branches. For example, Apnoke Scientific L

3-nonenal,(Z)-3-nonenal

Cas:31823-43-5

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Chungking Joyinchem Co., Ltd.

Joyinchem have been committed to chemical supply for several years and have built good cooperation records with multinational chemical corporations and importers from all over the world. Our services include:-Spot goods-Contract manufacturing-Custom

3-Nonenal, (3Z)-

Cas:31823-43-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Nanjing Raymon Biotech Co., Ltd.

3-Nonenal, (3Z)-Appearance:Off white to slight yellow solid Storage:Store in dry and cool condition Package:25kg or according to cutomer's demand Application:Chemical research/Pharmaceutical intermediates Transportation:By Sea,by Air,By courier like

3-Nonenal, (3Z)-

Cas:31823-43-5

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Hebei Ruishun Trade Co.,Ltd

Supply top quality products with a reasonable price Application:api

31823-43-5

Cas:31823-43-5

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Chemical Co.Ltd

3-Nonenal, (3Z)-Appearance:Off white to slight yellow solid Storage:Stored in shaded, cool and dry places Package:1L 5L 10L 25L bottle Application:pharma intermediate Transportation:Handle with cares to avoid damaging the packages. Protect them from

3-Nonenal, (3Z)-

Cas:31823-43-5

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Synthetic route

(Z)-3-nonenal diisopropyl acetal
120018-49-7

(Z)-3-nonenal diisopropyl acetal

(Z)-3-nonenal
31823-43-5

(Z)-3-nonenal

Conditions
ConditionsYield
With toluene-4-sulfonic acid In tetrahydrofuran for 0.333333h; Heating;99%
With toluene-4-sulfonic acid In tetrahydrofuran for 0.3h; Heating;
With toluene-4-sulfonic acid In tetrahydrofuran; water for 0.166667h; Heating;
With toluene-4-sulfonic acid In tetrahydrofuran; water for 0.25h; Heating;
With toluene-4-sulfonic acid In tetrahydrofuran Heating;
(Z)-non-3-en-1-ol
10340-23-5

(Z)-non-3-en-1-ol

(Z)-3-nonenal
31823-43-5

(Z)-3-nonenal

Conditions
ConditionsYield
With Dess-Martin periodane In dichloromethane at 20℃; for 1h; Dess-Martin oxidation;98%
With Dess-Martin periodane In dichloromethane at 0 - 20℃;97%
With Dess-Martin periodane In dichloromethane at 0 - 20℃; Inert atmosphere;96%
(2RS,4Z)-4-decen-1,2-diol
89616-41-1

(2RS,4Z)-4-decen-1,2-diol

(Z)-3-nonenal
31823-43-5

(Z)-3-nonenal

Conditions
ConditionsYield
With lead(IV) acetate; sodium carbonate In dichloromethane at -40 - -30℃; for 0.333333h; Oxidation;98%
With lead(IV) acetate In dichloromethane at -65℃; for 1.5h;
With lead(IV) acetate In dichloromethane 1.) -20 deg C, 15 min, 2.) -20 -> 0 deg C, 15 min;
1,1-dimethoxy-non-3c-ene
103229-70-5

1,1-dimethoxy-non-3c-ene

(Z)-3-nonenal
31823-43-5

(Z)-3-nonenal

Conditions
ConditionsYield
With trifluoroacetic acid In chloroform for 1.5h;94.5%
With acetic acid for 10h; Ambient temperature;70%
With oxalic acid; benzene-1,2-diol In water; acetone at 45 - 50℃;
With trifluoroacetic acid In chloroform
With water; trifluoroacetic acid In chloroform for 1h;
(3Z)-3-nonenal diethyl acetal
89682-47-3

(3Z)-3-nonenal diethyl acetal

(Z)-3-nonenal
31823-43-5

(Z)-3-nonenal

Conditions
ConditionsYield
With oxalic acid In water; acetone at 60℃; for 1h;93%
With water; oxalic acid In acetone for 1h; Heating;
With 2,5-bis(1,1-dimethylethyl)-1,4-benzenediol; oxalic acid In water; acetone for 2h; Heating; Yield given;
With formic acid In pentane at -40 - 20℃;
1,1-ethylenedioxy-non-3(Z)-ene
77953-94-7

1,1-ethylenedioxy-non-3(Z)-ene

(Z)-3-nonenal
31823-43-5

(Z)-3-nonenal

Conditions
ConditionsYield
With pyridinium p-toluenesulfonate In acetone for 24h; Ambient temperature;90%
With acetic acid for 24h; Ambient temperature;82%
Conditions
ConditionsYield
With Cs-9/13-hydroperoxidelyase In aq. phosphate buffer pH=6; Enzymatic reaction;A 73%
B n/a
(Z)-non-3-en-1-ol
10340-23-5

(Z)-non-3-en-1-ol

B

(Z)-3-nonenal
31823-43-5

(Z)-3-nonenal

Conditions
ConditionsYield
With pyridinium chlorochromate In dichloromethane for 1h; Ambient temperature;A 5%
B 65.4%
(Z)-non-3-en-1-ol
10340-23-5

(Z)-non-3-en-1-ol

A

(E)-2-Nonenal
18829-56-6

(E)-2-Nonenal

B

(Z)-3-nonenal
31823-43-5

(Z)-3-nonenal

Conditions
ConditionsYield
Swern oxidation;
1-Heptyne
628-71-7

1-Heptyne

(Z)-3-nonenal
31823-43-5

(Z)-3-nonenal

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 63 percent / n-BuLi; HMPA / tetrahydrofuran; hexane / 2 h / Heating
2: 83 percent / quinoline; H2 / Lindlar catalyst / ethanol / 2 h
3: HCOOH / pentane / -40 - 20 °C
View Scheme
Multi-step reaction with 3 steps
1: 53 percent / n-BuLi / tetrahydrofuran; hexamethylphosphoric acid triamide / 1.) 0 deg C, 4 h; 2.) 27 deg C, 40 h
2: 83 percent / hydrogen / Pd/BaSO4 / methanol / 30 h
3: 93 percent / oxalic acid / acetone; H2O / 1 h / 60 °C
View Scheme
Multi-step reaction with 3 steps
1: 1) n-butyllithium / 1) THF, hexane, -5 deg C, 1 h, 2) HMPT, a) -5 deg C, 2 h, b) 20 deg C, 18 h
2: 82 percent / NaBH4, H2, Ni(OAc)2 * 4 H2O / ethanol
3: 94.5 percent / 50percent aq. TFA / CHCl3 / 1.5 h
View Scheme
3-nonynal diethyl acetal
90290-02-1

3-nonynal diethyl acetal

(Z)-3-nonenal
31823-43-5

(Z)-3-nonenal

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 83 percent / quinoline; H2 / Lindlar catalyst / ethanol / 2 h
2: HCOOH / pentane / -40 - 20 °C
View Scheme
Multi-step reaction with 2 steps
1: 83 percent / hydrogen / Pd/BaSO4 / methanol / 30 h
2: 93 percent / oxalic acid / acetone; H2O / 1 h / 60 °C
View Scheme
Multi-step reaction with 2 steps
1: 81 percent / i-BuMgBr / Cp2TiCl2 / diethyl ether / 12 h / 26 - 28 °C
2: oxalic acid, 2,5-di-tert-butylhydroquinone / acetone; H2O / 2 h / Heating
View Scheme
Multi-step reaction with 2 steps
1: 77 percent / nickel(II) acetate, NaBH4, H2, ethylenediamine / ethanol
2: oxalic acid dihydrate, water / acetone / 1 h / Heating
View Scheme
hexanal
66-25-1

hexanal

hydrazine hydrochloride

hydrazine hydrochloride

(Z)-3-nonenal
31823-43-5

(Z)-3-nonenal

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: NaN(SiMe3)2 / tetrahydrofuran / -80 °C
2: TsOH / tetrahydrofuran / Heating
View Scheme
3-nonyn-1-ol
31333-13-8

3-nonyn-1-ol

(Z)-3-nonenal
31823-43-5

(Z)-3-nonenal

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 87 percent / H2, quinoline / Lindlar's catalyst / hexane
2: 50.7 percent / pyridinum chlorochromate / CH2Cl2 / 4 h / 0 °C
View Scheme
Multi-step reaction with 2 steps
1: H2, quinoline / Pd/BaSO4 / methanol
2: NCS, Me2S / toluene
View Scheme
Multi-step reaction with 2 steps
1: 99 percent / hydrogen, pyridine / Pd/BaSO4 / methanol
2: 50 percent / CrO3(Py)2 / L.H. Sarett, J. Chem. Soc., 35, 4000 (1970)
View Scheme
1-Bromopentane
110-53-2

1-Bromopentane

silver fluoride

silver fluoride

(Z)-3-nonenal
31823-43-5

(Z)-3-nonenal

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 61 percent / lithium amide / liquid ammonia; tetrahydrofuran / 3 h
2: 87 percent / H2, quinoline / Lindlar's catalyst / hexane
3: 50.7 percent / pyridinum chlorochromate / CH2Cl2 / 4 h / 0 °C
View Scheme
hexanal
66-25-1

hexanal

(Z)-3-nonenal
31823-43-5

(Z)-3-nonenal

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 100 percent / NaN(SiMe3)2 / tetrahydrofuran / 12 h / -100 deg C to RT
2: p-TsOH / H2O; tetrahydrofuran / 0.17 h / Heating
View Scheme
1-allyl-2-pentylacetylene
24948-66-1

1-allyl-2-pentylacetylene

(Z)-3-nonenal
31823-43-5

(Z)-3-nonenal

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 2.) hydrogen, triethylamine / 2.) Lindlar catalyst / 2.) THF, 23 deg C, 1 atm, 4.5 h
2: lead tetracetate / CH2Cl2 / 1.) -20 deg C, 15 min, 2.) -20 -> 0 deg C, 15 min
View Scheme
1,1-dimethoxy-non-3-yne
87745-62-8

1,1-dimethoxy-non-3-yne

(Z)-3-nonenal
31823-43-5

(Z)-3-nonenal

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 82 percent / NaBH4, H2, Ni(OAc)2 * 4 H2O / ethanol
2: 94.5 percent / 50percent aq. TFA / CHCl3 / 1.5 h
View Scheme
Multi-step reaction with 2 steps
1: 82 percent / hydrogen / P-2 Ni / ethanol
2: trifluoroacetic acid, water / CHCl3 / 1 h
View Scheme
Multi-step reaction with 2 steps
1: 82 percent / NaBH4 / nickel acetate tetrahydrate / aq. ethanol
2: 50percent aq. TFA / CHCl3
View Scheme
Multi-step reaction with 2 steps
1: H2 / Lindlar catalyst / hexane
2: oxalic acid, benzene-1,2-diol / acetone; H2O / 45 - 50 °C
View Scheme
1-heptynyllithium
42017-07-2

1-heptynyllithium

(Z)-3-nonenal
31823-43-5

(Z)-3-nonenal

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 70 percent / HMPT / tetrahydrofuran / -5 °C
2: 82 percent / hydrogen / P-2 Ni / ethanol
3: trifluoroacetic acid, water / CHCl3 / 1 h
View Scheme
hexanal
66-25-1

hexanal

magnesium aluminium-isopropylate

magnesium aluminium-isopropylate

(Z)-3-nonenal
31823-43-5

(Z)-3-nonenal

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 1.) NaN(SiMe3)2 / 1.) THF, toluene, RT, 1 h, 2.) from -100 to 0 deg C, 4 h
2: 0.1 M aq. p-toluenesulfonic acid / tetrahydrofuran / 0.3 h / Heating
View Scheme
(Z)-oct-2-en-1-ol
26001-58-1

(Z)-oct-2-en-1-ol

(Z)-3-nonenal
31823-43-5

(Z)-3-nonenal

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: 70 percent / pyridinium chlorochromate / CH2Cl2 / 2 h / Ambient temperature
2: 70 percent / dimethylsulfoxide / 1. cooling, 2h 2. room temperature, 12h 3. 50 deg C, 3h
3: 75 percent / PTS / benzene / 6 h / Heating; in a Dean and Stark water seperator
4: 90 percent / PTS / acetone / 24 h / Ambient temperature
View Scheme
2-octyn-1-ol
20739-58-6

2-octyn-1-ol

(Z)-3-nonenal
31823-43-5

(Z)-3-nonenal

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: 95 percent / H2 / Lindlars'catalyst / hexane
2: 70 percent / pyridinium chlorochromate / CH2Cl2 / 2 h / Ambient temperature
3: 70 percent / dimethylsulfoxide / 1. cooling, 2h 2. room temperature, 12h 3. 50 deg C, 3h
4: 75 percent / PTS / benzene / 6 h / Heating; in a Dean and Stark water seperator
5: 90 percent / PTS / acetone / 24 h / Ambient temperature
View Scheme
cis-2-octene oxide
20664-46-4

cis-2-octene oxide

(Z)-3-nonenal
31823-43-5

(Z)-3-nonenal

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 70 percent / dimethylsulfoxide / 1. cooling, 2h 2. room temperature, 12h 3. 50 deg C, 3h
2: 75 percent / PTS / benzene / 6 h / Heating; in a Dean and Stark water seperator
3: 90 percent / PTS / acetone / 24 h / Ambient temperature
View Scheme
1-methoxy-nona-1,3(Z)-diene
77953-93-6, 77953-95-8

1-methoxy-nona-1,3(Z)-diene

(Z)-3-nonenal
31823-43-5

(Z)-3-nonenal

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 75 percent / PTS / benzene / 6 h / Heating; in a Dean and Stark water seperator
2: 90 percent / PTS / acetone / 24 h / Ambient temperature
View Scheme
1-pentyl tosylate
4450-76-4

1-pentyl tosylate

(Z)-3-nonenal
31823-43-5

(Z)-3-nonenal

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: (i) EtMgBr, THF, CH2Cl2, (ii) /BRN= 1879859/
2: NaOMe / 24 h / 110 - 115 °C
3: H2 / Lindlar catalyst / hexane
4: oxalic acid, benzene-1,2-diol / acetone; H2O / 45 - 50 °C
View Scheme
1c-methoxy-non-1-en-3-yne
91819-64-6

1c-methoxy-non-1-en-3-yne

(Z)-3-nonenal
31823-43-5

(Z)-3-nonenal

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: NaOMe / 24 h / 110 - 115 °C
2: H2 / Lindlar catalyst / hexane
3: oxalic acid, benzene-1,2-diol / acetone; H2O / 45 - 50 °C
View Scheme
linoleic acid
60-33-3

linoleic acid

A

azelaic acid semialdehyde
2553-17-5

azelaic acid semialdehyde

B

(Z)-3-nonenal
31823-43-5

(Z)-3-nonenal

Conditions
ConditionsYield
With Cs-9/13-hydroperoxidelyase; St-lipoxygenase1 In aq. phosphate buffer pH=6; Enzymatic reaction;
(Z)-3-nonenal
31823-43-5

(Z)-3-nonenal

lithium acetylide
70277-75-7

lithium acetylide

(+/-)-(5Z)-5-undecen-1-yn-3-ol
129030-85-9

(+/-)-(5Z)-5-undecen-1-yn-3-ol

Conditions
ConditionsYield
In tetrahydrofuran at -78℃; for 1h;95%
In tetrahydrofuran for 1h; -78 to 20 deg C; Yield given;
(Z)-3-nonenal
31823-43-5

(Z)-3-nonenal

trimethylsilylacetylene
1066-54-2

trimethylsilylacetylene

(E/Z)-1-trimethylsilylundec-5-en-1-yn-3-ol
118789-62-1

(E/Z)-1-trimethylsilylundec-5-en-1-yn-3-ol

Conditions
ConditionsYield
Stage #1: trimethylsilylacetylene With n-butyllithium In tetrahydrofuran; hexane at -78℃; Inert atmosphere;
Stage #2: (Z)-3-nonenal In tetrahydrofuran; hexane at -78℃; for 2h; Inert atmosphere;
95%
(Z)-3-nonenal
31823-43-5

(Z)-3-nonenal

3,3-diethoxypropyl triphenylphosphonium iodide

3,3-diethoxypropyl triphenylphosphonium iodide

(Z,Z)-dodeca-3,6-dien-1-al diethylacetal
118207-20-8

(Z,Z)-dodeca-3,6-dien-1-al diethylacetal

Conditions
ConditionsYield
Stage #1: 3,3-diethoxypropyl triphenylphosphonium iodide With sodium hexamethyldisilazane In tetrahydrofuran; toluene at 20℃; for 2h;
Stage #2: (Z)-3-nonenal In tetrahydrofuran; toluene at -90 - 20℃; Wittig olefination;
88%
(Z)-3-nonenal
31823-43-5

(Z)-3-nonenal

[3-[(tert-butyldimethylsilyl)oxy]propyl]triphenylphosphonium bromide
120379-76-2

[3-[(tert-butyldimethylsilyl)oxy]propyl]triphenylphosphonium bromide

tert-butyl-dodeca-3,6-dienyloxy-dimethylsilane
125198-05-2

tert-butyl-dodeca-3,6-dienyloxy-dimethylsilane

Conditions
ConditionsYield
With lithium hexamethyldisilazane In tetrahydrofuran at -78 - 20℃; Condensation;85%
C32H34(2)H4O2PS(1+)*Br(1-)

C32H34(2)H4O2PS(1+)*Br(1-)

(Z)-3-nonenal
31823-43-5

(Z)-3-nonenal

tert-butyl 7-thia(5,6,8,9-2H4)arachidonate
947264-17-7

tert-butyl 7-thia(5,6,8,9-2H4)arachidonate

Conditions
ConditionsYield
Stage #1: C32H34(2)H4O2PS(1+)*Br(1-) With sodium hexamethyldisilazane In tetrahydrofuran; benzene at -78℃; for 0.75h;
Stage #2: (Z)-3-nonenal In tetrahydrofuran; benzene at -78 - 20℃; Wittig reaction; Further stages.;
85%
(Z)-3-nonenal
31823-43-5

(Z)-3-nonenal

(1E,3E,5Z)-1-bromo-7,7-diethoxyhepta-1,3,5-triene
420112-17-0

(1E,3E,5Z)-1-bromo-7,7-diethoxyhepta-1,3,5-triene

(2Z,4E,6E,10Z)-1,1-diethoxyhexadeca-2,4,6,10-tetraen-8-ol

(2Z,4E,6E,10Z)-1,1-diethoxyhexadeca-2,4,6,10-tetraen-8-ol

Conditions
ConditionsYield
Stage #1: (1E,3E,5Z)-1-bromo-7,7-diethoxyhepta-1,3,5-triene With tert.-butyl lithium In diethyl ether; pentane at -75℃; for 1.5h;
Stage #2: (Z)-3-nonenal In diethyl ether; pentane at -75℃; for 2h;
76%
(Z)-3-nonenal
31823-43-5

(Z)-3-nonenal

hexylidenetriphenylphosphoran
16666-79-8, 19493-12-0

hexylidenetriphenylphosphoran

cis,cis-6,9-pentadecadiene
114832-58-5

cis,cis-6,9-pentadecadiene

Conditions
ConditionsYield
With sodium hexamethyldisilazane In tetrahydrofuran at -80℃;75%
(Z)-3-nonenal
31823-43-5

(Z)-3-nonenal

((3Z,6Z)-dodeca-3,6-dien-1-yl)triphenylphosphonium bromide
83606-41-1

((3Z,6Z)-dodeca-3,6-dien-1-yl)triphenylphosphonium bromide

heneicosa-6c,9c,12c,15c-tetraene
54542-68-6

heneicosa-6c,9c,12c,15c-tetraene

Conditions
ConditionsYield
With N,N,N,N,N,N-hexamethylphosphoric triamide; lithium hexamethyldisilazane In tetrahydrofuran at -78 - 20℃; Condensation;75%
(Z)-3-nonenal
31823-43-5

(Z)-3-nonenal

(13)C2HLi

(13)C2HLi

C9(13)C2H18O
376591-07-0

C9(13)C2H18O

Conditions
ConditionsYield
In tetrahydrofuran71%
Vinyl bromide
593-60-2

Vinyl bromide

(Z)-3-nonenal
31823-43-5

(Z)-3-nonenal

(5Z)-1,5-undecadien-3-ol
56722-23-7

(5Z)-1,5-undecadien-3-ol

Conditions
ConditionsYield
With magnesium In tetrahydrofuran 1.) r.t., 6 h; 2.) reflux, 2 h;70.6%
(Z)-3-nonenal
31823-43-5

(Z)-3-nonenal

vinyl magnesium bromide
1826-67-1

vinyl magnesium bromide

(5Z)-1,5-undecadien-3-ol
56722-23-7

(5Z)-1,5-undecadien-3-ol

Conditions
ConditionsYield
In tetrahydrofuran 1. room temp., 8h 2. reflux, 2h;70%
In diethyl ether at 0℃; for 0.25h; Yield given;
In diethyl ether at 20℃; for 0.5h; Grignard reaction;2.54 g
In tetrahydrofuran at 0 - 20℃; Grignard Reaction;
In tetrahydrofuran at 0 - 20℃;
(Z)-3-nonenal
31823-43-5

(Z)-3-nonenal

(1E,3E,5Z)-1,6-dibromohexa-1,3,5-triene
179681-29-9

(1E,3E,5Z)-1,6-dibromohexa-1,3,5-triene

A

(1E,3E,5Z,9Z)-1-bromo-7-hydroxypentadeca-1,3,5,9-tetraene

(1E,3E,5Z,9Z)-1-bromo-7-hydroxypentadeca-1,3,5,9-tetraene

B

(1Z,3E,5E,9Z)-1-bromo-7-hydroxy-pentadeca-1,3,5,9-tetraene

(1Z,3E,5E,9Z)-1-bromo-7-hydroxy-pentadeca-1,3,5,9-tetraene

C

(6Z,10E,12E,14Z,18Z)-9,16-dihydroxytetraeicosa-6,10,12,14,18-pentaene

(6Z,10E,12E,14Z,18Z)-9,16-dihydroxytetraeicosa-6,10,12,14,18-pentaene

Conditions
ConditionsYield
Stage #1: (1E,3E,5Z)-1,6-dibromohexa-1,3,5-triene With tert.-butyl lithium In diethyl ether; pentane at -75℃; for 1.5h;
Stage #2: (Z)-3-nonenal In diethyl ether; pentane at 0℃; for 1.5h;
A 8%
B 65%
C 10%
(Z)-3-nonenal
31823-43-5

(Z)-3-nonenal

acetylene
74-86-2

acetylene

(+/-)-(5Z)-5-undecen-1-yn-3-ol
129030-85-9

(+/-)-(5Z)-5-undecen-1-yn-3-ol

Conditions
ConditionsYield
With n-butyllithium In tetrahydrofuran at -78℃; for 1h;62%
With n-butyllithium 1.) THF, hexane, -78 deg C, 20 min, 2.) THF, -78 deg C, 20 min; Yield given. Multistep reaction;
With n-butyllithium 1) THF, hexane, -78 deg C, 30 min., 2) THF, a) -78 deg C, 20 min., b) room temperature, 1 h; Yield given. Multistep reaction;
With n-butyllithium 1.) THF, hexane, -78 deg C, 30 min, 2.a) -78 deg C, 20 min, b) to rt, 1 h; Yield given. Multistep reaction;
(Z)-3-nonenal
31823-43-5

(Z)-3-nonenal

ethyl 3-lithiopropiolate
72036-30-7

ethyl 3-lithiopropiolate

ethyl 4-hydroxy-6-(Z)-dodecen-2-ynoate
76695-83-5

ethyl 4-hydroxy-6-(Z)-dodecen-2-ynoate

Conditions
ConditionsYield
60%
C32H38O2PS(1+)*Br(1-)

C32H38O2PS(1+)*Br(1-)

(Z)-3-nonenal
31823-43-5

(Z)-3-nonenal

tert-butyl 7-thiaarachidonate
947264-07-5

tert-butyl 7-thiaarachidonate

Conditions
ConditionsYield
Stage #1: C32H38O2PS(1+)*Br(1-) With sodium hexamethyldisilazane In tetrahydrofuran; benzene at -78℃; for 0.75h;
Stage #2: (Z)-3-nonenal In tetrahydrofuran; benzene at -78 - 20℃; Wittig reaction; Further stages.;
58%
(Z)-3-nonenal
31823-43-5

(Z)-3-nonenal

(1,1-[2H2]-10-methoxycarbonyl-deca-cis,cis-3,6-dienyl)-triphenylphosphonium bromide

(1,1-[2H2]-10-methoxycarbonyl-deca-cis,cis-3,6-dienyl)-triphenylphosphonium bromide

methyl 11-[2H]-arachidonate

methyl 11-[2H]-arachidonate

Conditions
ConditionsYield
Stage #1: (1,1-[2H2]-10-methoxycarbonyl-deca-cis,cis-3,6-dienyl)-triphenylphosphonium bromide With sodium hexamethyldisilazane In tetrahydrofuran at -70℃; for 1h; Wittig reaction;
Stage #2: (Z)-3-nonenal In tetrahydrofuran at 0℃; for 6h; Wittig reaction; Further stages.;
54%
(Z)-3-nonenal
31823-43-5

(Z)-3-nonenal

9-(Triphenyl-λ5-phosphanylidene)-nonanoic acid ethyl ester
135924-65-1

9-(Triphenyl-λ5-phosphanylidene)-nonanoic acid ethyl ester

ethyl (9Z,12Z)-9,12-octadecadienoate
544-35-4

ethyl (9Z,12Z)-9,12-octadecadienoate

(Z)-3-nonenal
31823-43-5

(Z)-3-nonenal

tributyl[(E)-2-trimethylsilylethenyl]stannane
58207-97-9

tributyl[(E)-2-trimethylsilylethenyl]stannane

1-(trimethylsilyl)-1(E),5(Z)-undecadien-3(R)-ol
115418-86-5

1-(trimethylsilyl)-1(E),5(Z)-undecadien-3(R)-ol

Conditions
ConditionsYield
With n-butyllithium 1) THF, hexane, -60 deg C, 1h, 2) 0 deg C, 1h; Yield given. Multistep reaction;
(Z)-3-nonenal
31823-43-5

(Z)-3-nonenal

lithium trimethylsilylacetylenide
54655-07-1

lithium trimethylsilylacetylenide

(E/Z)-1-trimethylsilylundec-5-en-1-yn-3-ol
118789-62-1

(E/Z)-1-trimethylsilylundec-5-en-1-yn-3-ol

Conditions
ConditionsYield
In diethyl ether at -30 - 20℃;
(Z)-3-nonenal
31823-43-5

(Z)-3-nonenal

Triphenyl-[(Z)-6-(tetrahydro-pyran-2-yloxy)-hex-3-enyl]-phosphonium; iodide
88730-62-5

Triphenyl-[(Z)-6-(tetrahydro-pyran-2-yloxy)-hex-3-enyl]-phosphonium; iodide

2-((3Z,6Z,9Z)-pentadeca-3,6,9-trienyloxy)tetrahydro-2H-pyran
120379-60-4

2-((3Z,6Z,9Z)-pentadeca-3,6,9-trienyloxy)tetrahydro-2H-pyran

Conditions
ConditionsYield
With N,N,N,N,N,N-hexamethylphosphoric triamide; lithium diisopropyl amide 1.) THF, -78 deg C, 1 h, 2.) THF, -78 deg C, 5 min then 0 deg C, 1.5 h; Yield given. Multistep reaction;
(Z)-3-nonenal
31823-43-5

(Z)-3-nonenal

Triphenyl-[(1S,4S)-4-(tetrahydro-pyran-2-yloxymethyl)-cyclohex-2-enylmethyl]-phosphonium; iodide
131721-09-0

Triphenyl-[(1S,4S)-4-(tetrahydro-pyran-2-yloxymethyl)-cyclohex-2-enylmethyl]-phosphonium; iodide

2-[(1S,4R)-((1Z,4Z)-4-Deca-1,4-dienyl)-cyclohex-2-enylmethoxy]-tetrahydro-pyran
131721-10-3

2-[(1S,4R)-((1Z,4Z)-4-Deca-1,4-dienyl)-cyclohex-2-enylmethoxy]-tetrahydro-pyran

Conditions
ConditionsYield
With n-butyllithium 1.) THF; Multistep reaction;
(Z)-3-nonenal
31823-43-5

(Z)-3-nonenal

Triphenyl-[(1S,4R)-4-(tetrahydro-pyran-2-yloxymethyl)-cyclohex-2-enylmethyl]-phosphonium; iodide
131721-09-0

Triphenyl-[(1S,4R)-4-(tetrahydro-pyran-2-yloxymethyl)-cyclohex-2-enylmethyl]-phosphonium; iodide

2-[(1S,4S)-((1Z,4Z)-4-Deca-1,4-dienyl)-cyclohex-2-enylmethoxy]-tetrahydro-pyran
131721-10-3

2-[(1S,4S)-((1Z,4Z)-4-Deca-1,4-dienyl)-cyclohex-2-enylmethoxy]-tetrahydro-pyran

Conditions
ConditionsYield
With n-butyllithium 1.) THF; Yield given. Multistep reaction;

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