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inquiry3-nonenal,(Z)-3-nonenal CAS:31823-43-5 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic
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inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
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inquiryZhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed
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inquiryLower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
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3-NONENAL,(Z)-3-NONENALAppearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
Best quality with low price Storage:ln stock Package:25kg/Barrel Application:Chemicals Transportation:Express/Sea/Air Port:Shanghai
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inquiryfactory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin
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Cas:31823-43-5
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inquiryWatson International Ltd' has a very strong R&D and technical capacity supported by FCAD's platform. The subsidiaries under FCAD Group have accumulated much know-how of different fine chemical branches. For example, Apnoke Scientific L
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inquiryJoyinchem have been committed to chemical supply for several years and have built good cooperation records with multinational chemical corporations and importers from all over the world. Our services include:-Spot goods-Contract manufacturing-Custom
3-Nonenal, (3Z)-Appearance:Off white to slight yellow solid Storage:Store in dry and cool condition Package:25kg or according to cutomer's demand Application:Chemical research/Pharmaceutical intermediates Transportation:By Sea,by Air,By courier like
3-Nonenal, (3Z)-Appearance:Off white to slight yellow solid Storage:Stored in shaded, cool and dry places Package:1L 5L 10L 25L bottle Application:pharma intermediate Transportation:Handle with cares to avoid damaging the packages. Protect them from
(Z)-3-nonenal diisopropyl acetal
(Z)-3-nonenal
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid In tetrahydrofuran for 0.333333h; Heating; | 99% |
With toluene-4-sulfonic acid In tetrahydrofuran for 0.3h; Heating; | |
With toluene-4-sulfonic acid In tetrahydrofuran; water for 0.166667h; Heating; | |
With toluene-4-sulfonic acid In tetrahydrofuran; water for 0.25h; Heating; | |
With toluene-4-sulfonic acid In tetrahydrofuran Heating; |
(Z)-non-3-en-1-ol
(Z)-3-nonenal
Conditions | Yield |
---|---|
With Dess-Martin periodane In dichloromethane at 20℃; for 1h; Dess-Martin oxidation; | 98% |
With Dess-Martin periodane In dichloromethane at 0 - 20℃; | 97% |
With Dess-Martin periodane In dichloromethane at 0 - 20℃; Inert atmosphere; | 96% |
(2RS,4Z)-4-decen-1,2-diol
(Z)-3-nonenal
Conditions | Yield |
---|---|
With lead(IV) acetate; sodium carbonate In dichloromethane at -40 - -30℃; for 0.333333h; Oxidation; | 98% |
With lead(IV) acetate In dichloromethane at -65℃; for 1.5h; | |
With lead(IV) acetate In dichloromethane 1.) -20 deg C, 15 min, 2.) -20 -> 0 deg C, 15 min; |
1,1-dimethoxy-non-3c-ene
(Z)-3-nonenal
Conditions | Yield |
---|---|
With trifluoroacetic acid In chloroform for 1.5h; | 94.5% |
With acetic acid for 10h; Ambient temperature; | 70% |
With oxalic acid; benzene-1,2-diol In water; acetone at 45 - 50℃; | |
With trifluoroacetic acid In chloroform | |
With water; trifluoroacetic acid In chloroform for 1h; |
(3Z)-3-nonenal diethyl acetal
(Z)-3-nonenal
Conditions | Yield |
---|---|
With oxalic acid In water; acetone at 60℃; for 1h; | 93% |
With water; oxalic acid In acetone for 1h; Heating; | |
With 2,5-bis(1,1-dimethylethyl)-1,4-benzenediol; oxalic acid In water; acetone for 2h; Heating; Yield given; | |
With formic acid In pentane at -40 - 20℃; |
1,1-ethylenedioxy-non-3(Z)-ene
(Z)-3-nonenal
Conditions | Yield |
---|---|
With pyridinium p-toluenesulfonate In acetone for 24h; Ambient temperature; | 90% |
With acetic acid for 24h; Ambient temperature; | 82% |
9(S)-hydroperoxyoctadeca-10Z,12E-dienoic acid
A
azelaic acid semialdehyde
B
(Z)-3-nonenal
Conditions | Yield |
---|---|
With Cs-9/13-hydroperoxidelyase In aq. phosphate buffer pH=6; Enzymatic reaction; | A 73% B n/a |
(Z)-non-3-en-1-ol
A
non-2-enal
B
(Z)-3-nonenal
Conditions | Yield |
---|---|
With pyridinium chlorochromate In dichloromethane for 1h; Ambient temperature; | A 5% B 65.4% |
Conditions | Yield |
---|---|
Swern oxidation; |
1-Heptyne
(Z)-3-nonenal
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 63 percent / n-BuLi; HMPA / tetrahydrofuran; hexane / 2 h / Heating 2: 83 percent / quinoline; H2 / Lindlar catalyst / ethanol / 2 h 3: HCOOH / pentane / -40 - 20 °C View Scheme | |
Multi-step reaction with 3 steps 1: 53 percent / n-BuLi / tetrahydrofuran; hexamethylphosphoric acid triamide / 1.) 0 deg C, 4 h; 2.) 27 deg C, 40 h 2: 83 percent / hydrogen / Pd/BaSO4 / methanol / 30 h 3: 93 percent / oxalic acid / acetone; H2O / 1 h / 60 °C View Scheme | |
Multi-step reaction with 3 steps 1: 1) n-butyllithium / 1) THF, hexane, -5 deg C, 1 h, 2) HMPT, a) -5 deg C, 2 h, b) 20 deg C, 18 h 2: 82 percent / NaBH4, H2, Ni(OAc)2 * 4 H2O / ethanol 3: 94.5 percent / 50percent aq. TFA / CHCl3 / 1.5 h View Scheme |
3-nonynal diethyl acetal
(Z)-3-nonenal
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 83 percent / quinoline; H2 / Lindlar catalyst / ethanol / 2 h 2: HCOOH / pentane / -40 - 20 °C View Scheme | |
Multi-step reaction with 2 steps 1: 83 percent / hydrogen / Pd/BaSO4 / methanol / 30 h 2: 93 percent / oxalic acid / acetone; H2O / 1 h / 60 °C View Scheme | |
Multi-step reaction with 2 steps 1: 81 percent / i-BuMgBr / Cp2TiCl2 / diethyl ether / 12 h / 26 - 28 °C 2: oxalic acid, 2,5-di-tert-butylhydroquinone / acetone; H2O / 2 h / Heating View Scheme | |
Multi-step reaction with 2 steps 1: 77 percent / nickel(II) acetate, NaBH4, H2, ethylenediamine / ethanol 2: oxalic acid dihydrate, water / acetone / 1 h / Heating View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: NaN(SiMe3)2 / tetrahydrofuran / -80 °C 2: TsOH / tetrahydrofuran / Heating View Scheme |
3-nonyn-1-ol
(Z)-3-nonenal
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 87 percent / H2, quinoline / Lindlar's catalyst / hexane 2: 50.7 percent / pyridinum chlorochromate / CH2Cl2 / 4 h / 0 °C View Scheme | |
Multi-step reaction with 2 steps 1: H2, quinoline / Pd/BaSO4 / methanol 2: NCS, Me2S / toluene View Scheme | |
Multi-step reaction with 2 steps 1: 99 percent / hydrogen, pyridine / Pd/BaSO4 / methanol 2: 50 percent / CrO3(Py)2 / L.H. Sarett, J. Chem. Soc., 35, 4000 (1970) View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 61 percent / lithium amide / liquid ammonia; tetrahydrofuran / 3 h 2: 87 percent / H2, quinoline / Lindlar's catalyst / hexane 3: 50.7 percent / pyridinum chlorochromate / CH2Cl2 / 4 h / 0 °C View Scheme |
hexanal
(Z)-3-nonenal
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 100 percent / NaN(SiMe3)2 / tetrahydrofuran / 12 h / -100 deg C to RT 2: p-TsOH / H2O; tetrahydrofuran / 0.17 h / Heating View Scheme |
1-allyl-2-pentylacetylene
(Z)-3-nonenal
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 2.) hydrogen, triethylamine / 2.) Lindlar catalyst / 2.) THF, 23 deg C, 1 atm, 4.5 h 2: lead tetracetate / CH2Cl2 / 1.) -20 deg C, 15 min, 2.) -20 -> 0 deg C, 15 min View Scheme |
1,1-dimethoxy-non-3-yne
(Z)-3-nonenal
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 82 percent / NaBH4, H2, Ni(OAc)2 * 4 H2O / ethanol 2: 94.5 percent / 50percent aq. TFA / CHCl3 / 1.5 h View Scheme | |
Multi-step reaction with 2 steps 1: 82 percent / hydrogen / P-2 Ni / ethanol 2: trifluoroacetic acid, water / CHCl3 / 1 h View Scheme | |
Multi-step reaction with 2 steps 1: 82 percent / NaBH4 / nickel acetate tetrahydrate / aq. ethanol 2: 50percent aq. TFA / CHCl3 View Scheme | |
Multi-step reaction with 2 steps 1: H2 / Lindlar catalyst / hexane 2: oxalic acid, benzene-1,2-diol / acetone; H2O / 45 - 50 °C View Scheme |
1-heptynyllithium
(Z)-3-nonenal
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 70 percent / HMPT / tetrahydrofuran / -5 °C 2: 82 percent / hydrogen / P-2 Ni / ethanol 3: trifluoroacetic acid, water / CHCl3 / 1 h View Scheme |
hexanal
(Z)-3-nonenal
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 1.) NaN(SiMe3)2 / 1.) THF, toluene, RT, 1 h, 2.) from -100 to 0 deg C, 4 h 2: 0.1 M aq. p-toluenesulfonic acid / tetrahydrofuran / 0.3 h / Heating View Scheme |
(Z)-oct-2-en-1-ol
(Z)-3-nonenal
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: 70 percent / pyridinium chlorochromate / CH2Cl2 / 2 h / Ambient temperature 2: 70 percent / dimethylsulfoxide / 1. cooling, 2h 2. room temperature, 12h 3. 50 deg C, 3h 3: 75 percent / PTS / benzene / 6 h / Heating; in a Dean and Stark water seperator 4: 90 percent / PTS / acetone / 24 h / Ambient temperature View Scheme |
2-octyn-1-ol
(Z)-3-nonenal
Conditions | Yield |
---|---|
Multi-step reaction with 5 steps 1: 95 percent / H2 / Lindlars'catalyst / hexane 2: 70 percent / pyridinium chlorochromate / CH2Cl2 / 2 h / Ambient temperature 3: 70 percent / dimethylsulfoxide / 1. cooling, 2h 2. room temperature, 12h 3. 50 deg C, 3h 4: 75 percent / PTS / benzene / 6 h / Heating; in a Dean and Stark water seperator 5: 90 percent / PTS / acetone / 24 h / Ambient temperature View Scheme |
cis-2-octene oxide
(Z)-3-nonenal
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 70 percent / dimethylsulfoxide / 1. cooling, 2h 2. room temperature, 12h 3. 50 deg C, 3h 2: 75 percent / PTS / benzene / 6 h / Heating; in a Dean and Stark water seperator 3: 90 percent / PTS / acetone / 24 h / Ambient temperature View Scheme |
1-methoxy-nona-1,3(Z)-diene
(Z)-3-nonenal
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 75 percent / PTS / benzene / 6 h / Heating; in a Dean and Stark water seperator 2: 90 percent / PTS / acetone / 24 h / Ambient temperature View Scheme |
1-pentyl tosylate
(Z)-3-nonenal
Conditions | Yield |
---|---|
Multi-step reaction with 4 steps 1: (i) EtMgBr, THF, CH2Cl2, (ii) /BRN= 1879859/ 2: NaOMe / 24 h / 110 - 115 °C 3: H2 / Lindlar catalyst / hexane 4: oxalic acid, benzene-1,2-diol / acetone; H2O / 45 - 50 °C View Scheme |
1c-methoxy-non-1-en-3-yne
(Z)-3-nonenal
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: NaOMe / 24 h / 110 - 115 °C 2: H2 / Lindlar catalyst / hexane 3: oxalic acid, benzene-1,2-diol / acetone; H2O / 45 - 50 °C View Scheme |
Conditions | Yield |
---|---|
With Cs-9/13-hydroperoxidelyase; St-lipoxygenase1 In aq. phosphate buffer pH=6; Enzymatic reaction; |
Conditions | Yield |
---|---|
In tetrahydrofuran at -78℃; for 1h; | 95% |
In tetrahydrofuran for 1h; -78 to 20 deg C; Yield given; |
(Z)-3-nonenal
trimethylsilylacetylene
(E/Z)-1-trimethylsilylundec-5-en-1-yn-3-ol
Conditions | Yield |
---|---|
Stage #1: trimethylsilylacetylene With n-butyllithium In tetrahydrofuran; hexane at -78℃; Inert atmosphere; Stage #2: (Z)-3-nonenal In tetrahydrofuran; hexane at -78℃; for 2h; Inert atmosphere; | 95% |
(Z)-3-nonenal
(Z,Z)-dodeca-3,6-dien-1-al diethylacetal
Conditions | Yield |
---|---|
Stage #1: 3,3-diethoxypropyl triphenylphosphonium iodide With sodium hexamethyldisilazane In tetrahydrofuran; toluene at 20℃; for 2h; Stage #2: (Z)-3-nonenal In tetrahydrofuran; toluene at -90 - 20℃; Wittig olefination; | 88% |
(Z)-3-nonenal
[3-[(tert-butyldimethylsilyl)oxy]propyl]triphenylphosphonium bromide
tert-butyl-dodeca-3,6-dienyloxy-dimethylsilane
Conditions | Yield |
---|---|
With lithium hexamethyldisilazane In tetrahydrofuran at -78 - 20℃; Condensation; | 85% |
(Z)-3-nonenal
tert-butyl 7-thia(5,6,8,9-2H4)arachidonate
Conditions | Yield |
---|---|
Stage #1: C32H34(2)H4O2PS(1+)*Br(1-) With sodium hexamethyldisilazane In tetrahydrofuran; benzene at -78℃; for 0.75h; Stage #2: (Z)-3-nonenal In tetrahydrofuran; benzene at -78 - 20℃; Wittig reaction; Further stages.; | 85% |
(Z)-3-nonenal
(1E,3E,5Z)-1-bromo-7,7-diethoxyhepta-1,3,5-triene
Conditions | Yield |
---|---|
Stage #1: (1E,3E,5Z)-1-bromo-7,7-diethoxyhepta-1,3,5-triene With tert.-butyl lithium In diethyl ether; pentane at -75℃; for 1.5h; Stage #2: (Z)-3-nonenal In diethyl ether; pentane at -75℃; for 2h; | 76% |
(Z)-3-nonenal
hexylidenetriphenylphosphoran
cis,cis-6,9-pentadecadiene
Conditions | Yield |
---|---|
With sodium hexamethyldisilazane In tetrahydrofuran at -80℃; | 75% |
(Z)-3-nonenal
((3Z,6Z)-dodeca-3,6-dien-1-yl)triphenylphosphonium bromide
heneicosa-6c,9c,12c,15c-tetraene
Conditions | Yield |
---|---|
With N,N,N,N,N,N-hexamethylphosphoric triamide; lithium hexamethyldisilazane In tetrahydrofuran at -78 - 20℃; Condensation; | 75% |
Conditions | Yield |
---|---|
In tetrahydrofuran | 71% |
Conditions | Yield |
---|---|
With magnesium In tetrahydrofuran 1.) r.t., 6 h; 2.) reflux, 2 h; | 70.6% |
Conditions | Yield |
---|---|
In tetrahydrofuran 1. room temp., 8h 2. reflux, 2h; | 70% |
In diethyl ether at 0℃; for 0.25h; Yield given; | |
In diethyl ether at 20℃; for 0.5h; Grignard reaction; | 2.54 g |
In tetrahydrofuran at 0 - 20℃; Grignard Reaction; | |
In tetrahydrofuran at 0 - 20℃; |
(Z)-3-nonenal
(1E,3E,5Z)-1,6-dibromohexa-1,3,5-triene
Conditions | Yield |
---|---|
Stage #1: (1E,3E,5Z)-1,6-dibromohexa-1,3,5-triene With tert.-butyl lithium In diethyl ether; pentane at -75℃; for 1.5h; Stage #2: (Z)-3-nonenal In diethyl ether; pentane at 0℃; for 1.5h; | A 8% B 65% C 10% |
Conditions | Yield |
---|---|
With n-butyllithium In tetrahydrofuran at -78℃; for 1h; | 62% |
With n-butyllithium 1.) THF, hexane, -78 deg C, 20 min, 2.) THF, -78 deg C, 20 min; Yield given. Multistep reaction; | |
With n-butyllithium 1) THF, hexane, -78 deg C, 30 min., 2) THF, a) -78 deg C, 20 min., b) room temperature, 1 h; Yield given. Multistep reaction; | |
With n-butyllithium 1.) THF, hexane, -78 deg C, 30 min, 2.a) -78 deg C, 20 min, b) to rt, 1 h; Yield given. Multistep reaction; |
(Z)-3-nonenal
ethyl 3-lithiopropiolate
ethyl 4-hydroxy-6-(Z)-dodecen-2-ynoate
Conditions | Yield |
---|---|
60% |
Conditions | Yield |
---|---|
Stage #1: C32H38O2PS(1+)*Br(1-) With sodium hexamethyldisilazane In tetrahydrofuran; benzene at -78℃; for 0.75h; Stage #2: (Z)-3-nonenal In tetrahydrofuran; benzene at -78 - 20℃; Wittig reaction; Further stages.; | 58% |
(Z)-3-nonenal
Conditions | Yield |
---|---|
Stage #1: (1,1-[2H2]-10-methoxycarbonyl-deca-cis,cis-3,6-dienyl)-triphenylphosphonium bromide With sodium hexamethyldisilazane In tetrahydrofuran at -70℃; for 1h; Wittig reaction; Stage #2: (Z)-3-nonenal In tetrahydrofuran at 0℃; for 6h; Wittig reaction; Further stages.; | 54% |
(Z)-3-nonenal
9-(Triphenyl-λ5-phosphanylidene)-nonanoic acid ethyl ester
ethyl (9Z,12Z)-9,12-octadecadienoate
(Z)-3-nonenal
tributyl[(E)-2-trimethylsilylethenyl]stannane
1-(trimethylsilyl)-1(E),5(Z)-undecadien-3(R)-ol
Conditions | Yield |
---|---|
With n-butyllithium 1) THF, hexane, -60 deg C, 1h, 2) 0 deg C, 1h; Yield given. Multistep reaction; |
(Z)-3-nonenal
lithium trimethylsilylacetylenide
(E/Z)-1-trimethylsilylundec-5-en-1-yn-3-ol
Conditions | Yield |
---|---|
In diethyl ether at -30 - 20℃; |
(Z)-3-nonenal
Triphenyl-[(Z)-6-(tetrahydro-pyran-2-yloxy)-hex-3-enyl]-phosphonium; iodide
2-((3Z,6Z,9Z)-pentadeca-3,6,9-trienyloxy)tetrahydro-2H-pyran
Conditions | Yield |
---|---|
With N,N,N,N,N,N-hexamethylphosphoric triamide; lithium diisopropyl amide 1.) THF, -78 deg C, 1 h, 2.) THF, -78 deg C, 5 min then 0 deg C, 1.5 h; Yield given. Multistep reaction; |
(Z)-3-nonenal
Triphenyl-[(1S,4S)-4-(tetrahydro-pyran-2-yloxymethyl)-cyclohex-2-enylmethyl]-phosphonium; iodide
2-[(1S,4R)-((1Z,4Z)-4-Deca-1,4-dienyl)-cyclohex-2-enylmethoxy]-tetrahydro-pyran
Conditions | Yield |
---|---|
With n-butyllithium 1.) THF; Multistep reaction; |
(Z)-3-nonenal
Triphenyl-[(1S,4R)-4-(tetrahydro-pyran-2-yloxymethyl)-cyclohex-2-enylmethyl]-phosphonium; iodide
2-[(1S,4S)-((1Z,4Z)-4-Deca-1,4-dienyl)-cyclohex-2-enylmethoxy]-tetrahydro-pyran
Conditions | Yield |
---|---|
With n-butyllithium 1.) THF; Yield given. Multistep reaction; |
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