CAS No.32767-18-3,OXYGEN-18O2, 97 ATOM % 18O Suppliers

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Synthetic route

: 13709-36-9
xenon difluoride

: 14797-71-8
18O-labeled water

: 32767-18-3
oxygen-18

Conditions

Conditions	Yield
In neat (no solvent, gas phase) byproducts: Xe, HF; at 50°C for 3 h; fractional distn. at low temp.;	99%

: cobalt(III)

: 14797-71-8
18O-labeled water

A: oxygen

B: cobalt(II)

C: 80937-33-3
oxygen

D: hydrogen cation

E: 32767-18-3
oxygen-18

Conditions

Conditions	Yield
In sulfuric acid React. at 23°C.;	A 27% B n/a C <1 D n/a E 73%
In sulfuric acid React. at 23°C.;

...Expand

: Ti((18)O2)(meso-tetra-m-tolyl-porphinato)

: Ti(18)O(meso-tetra-m-tolyl-porphinato)

B: 32767-18-3
oxygen-18

Conditions

Conditions	Yield
In benzene byproducts: C(18)O2, C(18)O; Irradiation (UV/VIS); high-pressure Hg lamp, 30 min; not isolated, (18)O2 detd. by mass spectroscopy;	A n/a B 26%

: 7732-18-5
water

: cobalt(III)

A: oxygen

B: cobalt(II)

C: 80937-33-3
oxygen

D: hydrogen cation

E: 32767-18-3
oxygen-18

Conditions

Conditions	Yield
In sulfuric acid React. at 23°C in aq. CF3CO2H.;	A 9% B n/a C >90 D n/a E <1

...Expand

: 10028-15-6
ozone

: H(18)O(1-)

: 32767-18-3
oxygen-18

Conditions

Conditions	Yield
With sodium hydroxide In water Kinetics; byproducts: HO(1-); evacuation of ampoule with frozen ozone, water labelled with (18)O and NaOH (0.1-2 M) (addn. of natural O2 to some ampoules), ampoules sealing,leaving at 20+/-1°C for 5-20 h; determination of isotopic compn. of liberated oxygen, detection of short living radicals using different acceptors;

: 7732-18-5
water

: 14797-71-8
18O-labeled water

A: oxygen

B: 1333-74-0
hydrogen

C: 80937-33-3
oxygen

D: 32767-18-3
oxygen-18

Conditions

Conditions	Yield
titanium disilicide In water Irradiation (UV/VIS); suspn. of TiSi2 in either tridistilled or tap water with 10% H2(18)O at pH 7 was irradiated at 50 to 85°C with stirring under N2 or Ar; gas chromy., mass-spectrometry;

...Expand

: ice

: 14797-71-8
18O-labeled water

A: oxygen

B: 1173018-52-4
dioxygen-(16)O

C: 1333-74-0
hydrogen

D: 32767-18-3
oxygen-18

Conditions

Conditions	Yield
copper(I) oxide In neat (no solvent) Irradiation (UV/VIS); at room temp. with irradiation by visible light;

...Expand

: ice

: 14797-71-8
18O-labeled water

A: oxygen

B: 1173018-52-4
dioxygen-(16)O

C: 32767-18-3
oxygen-18

Conditions

Conditions	Yield
With ammonium cerium(IV) nitrate In water pH=1.0, 25 °C; monitored by MS;
With sulfuric acid pH=0.0; Catalytic behavior; Electrochemical reaction;
With sodium persulfate; tris(2,2'-bipyridine)ruthenium(II) perchlorate; 27Na(1+)103H2OFe11(H2O)14(OH)2(W3O10)2(SbW9O33)6(27-) at 25℃; pH=10; Irradiation;

...Expand

: ice

: silver sulfate

: 14797-71-8
18O-labeled water

A: oxygen

B: 1173018-52-4
dioxygen-(16)O

C: 7440-22-4
silver

D: 32767-18-3
oxygen-18

Conditions

Conditions	Yield
With titanium(IV) oxide In water Kinetics; byproducts: H(1+); Irradiation (UV/VIS); irradiated under Ar for 5 h;

...Expand

: 14797-71-8
18O-labeled water

A: hydrogen cation

B: 32767-18-3
oxygen-18

Conditions

Conditions	Yield
With manganese(II) sulfate In water Kinetics; Irradiation (UV/VIS); catalytic oxidn. of H2(18)O in a three-chamber glass vessel while shaking deaerated aq. solns. of reagents (Ru- and Mn-compds., vesicles and a buffer soln.), photocatalytic liberation of (18)O2; detn. of (18)O2 by gas chromy.;

: 14797-71-8
18O-labeled water

A: 1333-74-0
hydrogen

B: 32767-18-3
oxygen-18

Conditions

Conditions	Yield
With cat: Pt/TiO2 In neat (no solvent) Kinetics; Irradiation (UV/VIS); 23°C; mass-spectrometry;

: 14797-71-8
18O-labeled water

: 32767-18-3
oxygen-18

Conditions

Conditions	Yield
With potassium fluoride In water Electrolysis; electrolysis of (18)O-enriched water (platinum electrodes, dil. KF soln.as electrolyte, current 2 A, isolated anode and cathode compartments);
With ammonium cerium(IV) nitrate; ruthenium-red In further solvent(s) byproducts: (16)O2, (18)O(16)O; oxidation of water using Ru-red; detd. by GC-MS;
With glassy carbon/nafion/Mn4O4(O2P(C6H4CH2OH)2)6(1+) In water Irradiation (UV/VIS); photooxidation of water, Mn4O4(O2P(C6H4CH3OH)6(1+) doped nafion as photocatalyst at 0.8-1.2 V vs Ag/AgCl, light wavelength > 395 nm; detd. by MAS;

: 32767-18-3
hydrogen (18)O-peroxide

: 7722-84-1
dihydrogen peroxide

A: 80937-33-3
oxygen

B: 32767-18-3
oxygen-18

Conditions

Conditions	Yield
{(bis(salicylideneaminato)propane)(μ2-O)manganese(IV)}2 In not given (N2); raction is run on a Schlenk line; analyzed by MS;

...Expand

: 10028-15-6
ozone

A: oxygen

B: 1173018-52-4
dioxygen-(16)O

C: 32767-18-3
oxygen-18

Conditions

Conditions	Yield
In neat (no solvent, gas phase) Irradiation (UV/VIS); photodissociation of isotopical enriched O3 (ratio (16)O:(18)O 1:1, 266nm); not isolated;

...Expand

: 14390-96-6
ammonia

: 10028-15-6
ozone

A: 113321-73-6
(15)NH2(18)OH

B: 32767-18-3
oxygen-18

Conditions

Conditions	Yield
In solid matrix Irradiation (UV/VIS); codeposition of NH3, O3, and Ar (Ar/NH3 = Ar/O3 = 300:1) at 10-14 K and photodissociation of the NH3-O3 complex in the Ar matrix by exposure to 290-1000 nm radiation; reaction studied by IR spectroscopy;

...Expand

: 21424-26-0
ozone

: 13550-49-7
ammonia-d3

A: 113321-74-7
(2)H3N(18)O

B: 32767-18-3
oxygen-18

Conditions

Conditions	Yield
In solid matrix Irradiation (UV/VIS); codeposition of ND3, O3, and Ar (Ar/ND3 = Ar/O3 = 300:1) at 10-14 K and photodissociation of the ND3-O3 complex in the Ar matrix by exposure to 290-1000 nm radiation; reaction studied by IR spectroscopy;

...Expand

: 13780-28-4
ammonia-d2

: 21424-26-0
ozone

: 15123-00-9
ammonia

A: 113321-75-8
H(2)H2N(18)O

B: 113321-77-0
H(2)H2N(18)O

C: 113321-76-9
H2(2)HN(18)O

D: H2(2)HN(18)O

E: 32767-18-3
oxygen-18

Conditions

Conditions	Yield
In solid matrix Irradiation (UV/VIS); codeposition of NH3, O3, and Ar (Ar/NH3 = Ar/O3 = 300:1) at 10-14 K and photodissociation of the NH3-O3 complex in the Ar matrix by exposure to 290-1000 nm radiation; reaction studied by IR spectroscopy;

...Expand

: 21424-26-0
ozone

: 7664-41-7
ammonia

A: 113321-72-5
NH2(18)OH

B: 32767-18-3
oxygen-18

Conditions

Conditions	Yield
In solid matrix Irradiation (UV/VIS); codeposition of NH3, O3, and Ar (Ar/NH3 = Ar/O3 = 300:1) at 10-14 K and photodissociation of the NH3-O3 complex in the Ar matrix by exposure to 290-1000 nm radiation; reaction studied by IR spectroscopy;

...Expand

: 1173018-52-4
dioxygen-(16)O

: superoxide

: 32767-18-3
oxygen-18

Conditions

Conditions	Yield
Kinetics; in He buffer, pressure: 0.4 Torr;

: 7732-18-5
water

: 14797-71-8
18O-labeled water

A: 17410-58-1
oxygen-18O,16O

B: 80937-33-3
oxygen

C: 32767-18-3
oxygen-18

Conditions

Conditions	Yield
With Ce(IV); (H2O)(terpy)Mn(O)(terpy)Mn(H2O)(3+)/Kaolin clay In water adsorption of ((H2O)(terpy)Mn(μ-O)2Mn(terpy)(H2O))(3+) onto Kaolin clay; addn. of excess Ce(IV) to suspn. in H2(18)O; monitoring by EIMS;
With Ce(4+); ([Ru(NC5H3(C5H4N)2)(H2O)]2(C3HN2(C5H4N)2))(3+) In water mixing ruthenium compd. with Ce(4+), dilution with H2O, (18)OH2; not isolated, detected by mass spectrometry;
With ammonium cerium (IV) nitrate; Fe(N,N'-dimethyl-N,N'-bis(8-quinolyl)-ethane-1,2-diamine)(OTf)2; nitric acid Mechanism;

...Expand

: 1173018-52-4
dioxygen-(16)O

: 14797-71-8
18O-labeled water

A: oxygen

B: 32767-18-3
oxygen-18

Conditions

Conditions	Yield
With ethanol; titanium(IV) oxide In gaseous matrix Irradiation (UV/VIS); photocatalytic reactor (six 4 W UV lapms), He carrier gas;
titanium(IV) oxide In gaseous matrix Irradiation (UV/VIS); photocatalytic reactor (six 4 W UV lapms), He carrier gas;

...Expand

: 32767-18-3
hydrogen (18)O-peroxide

: 32767-18-3
oxygen-18

Conditions

Conditions	Yield
[Mn4O6(N,N-bis(2-pyridylmethyl)ethylamine)4](ClO4)3 In water; acetonitrile byproducts: H2O; Electrolysis; at 22°C; bulk electrolysis; MAS; video recording displacement of mineral oil in gas buret;
{(bis(salicylideneaminato)propane)(μ2-O)manganese(IV)}2 In not given (N2); reaction is run on a Schlenk line; analyzed by MS;

: ozone

: 37006-04-5
hydroperoxy radical

A: (16)O(1)H

B: 32767-18-3
oxygen-18

Conditions

Conditions	Yield
In gas Kinetics; reacting H(18)O2 (generated by recation of Cl, CH3OH, and (18)O2) with O3 in a flow tube (flow velocity for 350 to 800 cm/s, H(18)O2 concn. ca 310E11 cm*-3);; detd. by laser magnetic resonance detection; not isolated;;

...Expand

: ozone

: 37006-04-5
hydroperoxy radical

A: 1173018-52-4
hydroperoxy radical

B: 32767-18-3
oxygen-18

Conditions

Conditions	Yield
In gas Kinetics; reacting H(18)O2 (generated by reaction of Cl, CH3OH, and (18)O2) with O3 in a flow tube (flow velocity for 350 to 800 cm/s, H(18)O2 concn. ca 310E11 cm*-3); detd. by laser magnetic resonance detection; not isolated;;

...Expand

: 15917-79-0
nitric oxide

A: 29817-79-6
nitrogen-15

B: 20259-33-0
nitrous oxide

C: 32767-18-3
oxygen-18

Conditions

Conditions	Yield
With Pt In neat (no solvent) decomposition of NO on Pt(410);

...Expand

: Ti((18)O2)(meso-tetra-m-tolyl-porphinato)

: 75489-54-2
Ti(O2)(meso-tetra-m-tolyl-porphinato)

A: 1173018-52-4
dioxygen-(16)O

: (tetra(m-tolyl)porphinato)TiO

: Ti(18)O(meso-tetra-m-tolyl-porphinato)

D: 32767-18-3
oxygen-18

Conditions

Conditions	Yield
In benzene byproducts: C(18)O2, C(18)O; Irradiation (UV/VIS); high-pressure Hg lamp, 30 min; not isolated, (18)O2 and (16)O2 detd. by mass spectroscopy; total yieldof O2-isotopes 54%;

...Expand

: Ca(18)O

: nitrogen oxide

A: 15917-78-9
nitric oxide

B: 32767-18-3
oxygen-18

Conditions

Conditions	Yield
In gaseous matrix Kinetics; CaO/quartz sand mixt. in fixed bed reactor exposing to NO/Ar at const. temp. in range of 573-1073 K; mass spectrometric monitoring;

...Expand

: carbon monoxide

: Ca(18)O

A: 55125-78-5
carbon monoxide

B: 32767-18-3
oxygen-18

Conditions

Conditions	Yield
In gaseous matrix Kinetics; CaO/quartz sand mixt. in fixed bed reactor exposing to CO/Ar at const. temp. in range of 573-1073 K; mass spectrometric monitoring;

...Expand

: 132156-02-6
tetra n-butylammonium (18)O-hydroxide

: Mn(OH)O[(C4H2N)C(C6H2(CH3)3)]3(C4H2N)C(C6H4)C(C4H2N)[(C4H2N)C(C6H2(CH3)3)]3Mn(OH)O

: 14797-71-8
18O-labeled water

: Mn(OH)[(C4H2N)C(C6H2(CH3)3)]3(C4H2N)C(C6H4)C(C4H2N)[(C4H2N)C(C6H2(CH3)3)]3Mn(1+)*NO3(1-)*5H2O=[Mn2(C100H87N8O)]NO3*5H2O

B: 32767-18-3
oxygen-18

Conditions

Conditions	Yield
With trifluorormethanesulfonic acid In dichloromethane; acetonitrile under Ar; addn. 40 equiv. of CF3SO3H for each Mn(V)-ion in CH2Cl2/CH3CN (1:3 v/v) with 10 % H2(18)O; few s;

...Expand

: 18955-01-6, 104759-03-7, 24162-13-8
tris-2,2'-bipyridyl ruthenium(III) ion

: 14797-71-8
18O-labeled water

A: 52389-25-0, 24162-12-7, 15158-62-0
ruthenium(II) tris(2,2’-bipyridyl)

B: 32767-18-3
oxygen-18

Conditions

Conditions	Yield
Rb8K2[Ru4O4(OH)2(H2O)4(γ-SiW10O36)2]*25H2O In water-d2 byproducts: H(1+); H2(18)O reacted with Ru(NC5H4C5H4N)3(3+) in presence of small amt. of Ru-W complex; monitored by chromy.;

...Expand

: trans-[Ir(4-C5F4N)(CNtBu)(PiPr3)2]

: 32767-18-3
oxygen-18

: trans-[Ir(4-C5F4N)(18O2)(CNtBu)(PiPr3)2]

Conditions

Conditions	Yield
In tetrahydrofuran at 20℃; for 16h; Inert atmosphere; Schlenk technique;	99%

: [Ir(Cl){Mes-N=CH-CH=N-2,6-Mes}(CNtBu)]

: 32767-18-3
oxygen-18

: [Ir(Cl)(18O2){2,4,6-Me3C6H2-N=CH-CH=N-2,4,6-Me3C6H2}(CNtBu)]

Conditions

Conditions	Yield
In benzene at -196.16 - 19.84℃; for 0.666667h;	96%

: (tetra(m-tolyl)porphinato)TiO

: 32767-18-3
oxygen-18

: Ti((18)O2)(meso-tetra-m-tolyl-porphinato)

Conditions

Conditions	Yield
With N,N-Dimethylhydrazine In tetrahydrofuran twofold excess of >99% (18)O2, stirring; recrystn. (CH2Cl2/MeOH);	94%

: C31H29B2CoN9

: 32767-18-3
oxygen-18

: C62H58B4Co2N18(18)O2

Conditions

Conditions	Yield
In tetrahydrofuran under 760.051 Torr; Sealed tube;	93%

: [FeII(2-[bis(pyridin-2-ylmethyl)]amino-N-quinolin-8-yl-acetamido)(MeCN)]ClO4*0.5CH2Cl2

: 32767-18-3
oxygen-18

: [FeIV(18O)(2-[bis(pyridin-2-ylmethyl)]amino-N-quinolin-8-yl-acetamido)]ClO4

Conditions

Conditions	Yield
In acetonitrile at 25℃;	92%

: C17H29CuN3O2(1+)*F6P(1-)

: 32767-18-3
oxygen-18

: C38H68Cu2N4O6(18)O2(2+)*2F6P(1-)

Conditions

Conditions	Yield
In tetrahydrofuran at -82℃; for 24h; Inert atmosphere;	92%

: 918621-91-7
tetrabutylammonium tris[(N'-tert-butylureayl)-N-ethyl]aminatocobaltate(II)

: 32767-18-3
oxygen-18

: potassium tris[(N'-tert-butylureayl)-N-ethyl]aminato(hydroxo-(18)O)cobaltate(III)

Conditions

Conditions	Yield
In acetonitrile under N2; soln. of Co complex in MeCN treated with (18)O2 (0.5 equiv.) at 295.5 K and 0.98 atm; stirred for 1 h; vol. reduced under vac.; Et2O added; filtered; ppt. washed with Et2O; dried;	90%

: Cu2(C5H4NCH2CH2)2NCH2C6H4CH2N(CH3)CH2CH2C5H4N(2+)*2ClO4(1-)=[Cu2(C5H4NCH2CH2)2NCH2C6H4CH2N(CH3)CH2CH2C5H4N][ClO4]2

: 32767-18-3
oxygen-18

: Cu2((18)OH)(CH3CN)(C5H4NCH2CH2)2NCH2C6H3(18)OCH2N(CH3)CH2CH2C5H4N(2+)*2ClO4(1-)=[C32H38Cu2N6(18)O2][ClO4]2

Conditions

Conditions	Yield
In N,N-dimethyl-formamide under Ar using Schlenk techniques; soln. of Cu-complex in Ar saturated DMF exposed to an atmosphere of (18)O2 at 0°C; stirred overnight at room temp.; solvent removed (vac., 40°C); residue dissolved (CH2Cl2); filtered; pptn. by Et2O; washed (ether); dried (air);	85%

: (C2H5)4N(1+)*{Ni(CN)(SCH2CH2)2NCH2CH2SCH3}(1-)={(C2H5)4N}{Ni(CN)(SCH2CH2)2NCH2CH2SCH3}

: 13435-20-6
tetraethylammoniumcyanide

: 32767-18-3
oxygen-18

: (C2H5)4N(1+)*{Ni(CN)((18)O2SCH2CH2N(CH2CH2S)CH2CH2SCH3)}(1-)={(C2H5)4N}{Ni(CN)((18)O2SCH2CH2N(CH2CH2S)CH2CH2SCH3)}

Conditions

Conditions	Yield
In N,N-dimethyl-formamide (18)O2 bubbled for 15 min, allowed to stand under an (18)O2 atmosphere overnight; toluene layered on the soln., filtered after two days;	84%

...Expand

: 91-01-0
1,1-Diphenylmethanol

: 865-47-4
potassium tert-butylate

: 32767-18-3
oxygen-18

: {(18)O}-potassium hydroperoxide

Conditions

Conditions	Yield
In diethyl ether at 0°C, 60 min; sepn. by filtration, washing with dry, cold ether, dried in vac. at 0°C;	83%

...Expand

: 865255-93-2
bis[(N'-tert-butylureayl)-N-ethyl]-(N''-isopropylcarbamoyl-methyl)amine

: 71-48-7, 917-69-1, 5931-89-5, 55881-15-7, 68931-68-0, 68931-69-1, 93029-27-7
cobalt(II) acetate

: potassium hydride

: 32767-18-3
oxygen-18

: 918621-77-9
potassium bis[(N'-tert-butylureayl)-N-ethyl]-(N''-isopropylcarbamoylmethyl)aminato(hydroxo-(18)O)cobaltate(III)

Conditions

Conditions	Yield
In N,N-dimethyl acetamide byproducts: potassium acetate; under Ar; soln. of ligand in anhyd. DMA treated with solid KH; stirred until gas evolution ceased; Co acetate added; stirred for 30 min; treatedwith (18)O2 (0.55 equiv.) at 293.5 K and 0.99 atm; stirred for 1 h; placed under vac. for a few min; filtered; filtrate concd. in vac.; treated with Et2O; filtered; ppt. washed with Et2O; dried under vac.;	82%

Yield

In N,N-dimethyl acetamide byproducts: potassium acetate; under Ar; soln. of ligand in anhyd. DMA treated with solid KH; stirred until gas evolution ceased; Co acetate added; stirred for 30 min; treatedwith (18)O2 (0.55 equiv.) at 293.5 K and 0.99 atm; stirred for 1 h; placed under vac. for a few min; filtered; filtrate concd. in vac.; treated with Et2O; filtered; ppt. washed with Et2O; dried under vac.;

82%

...Expand

: (4,4'-di-tert-butyl-2,2'-bipyridine)(tert-butylisocyanide)chloridorhodium(I)

: 32767-18-3
oxygen-18

: (4,4'-di-tert-butyl-2,2'-bipyridine)(tert-butylisocyanide)(peroxido)chloridorhodium(III)

Conditions

Conditions	Yield
In neat (no solvent, solid phase) Rh complex stirred at -196°C (vac.), (18)O2 added (0.1 bar) for 30 min; washed (n-hexane, benzene), dried (vac.);	80%

: [Rh(Cl){Mes-N=CH-CH=N-2,6-Mes}(CNtBu)]

: 32767-18-3
oxygen-18

: [Rh(Cl)(18O2){2,4,6-Me3C6H2-N=CH-CH=N-2,4,6-Me3C6H2}(CNtBu)]

Conditions

Conditions	Yield
In tetrahydrofuran at -196.16 - 19.84℃; for 12h;	78%

: 14221-02-4
tetrakis(triphenylphosphine)platinum

: 32767-18-3
oxygen-18

: 87118-08-9
(PPh3)2Pt(18)O2

Conditions

Conditions	Yield
In diethyl ether suspn. Pt complex in Et2O was frozen at -196 °C, evacuated, (18)O2 was added, warmed to room temp. and stirred for 2 h; ppt. was collected, washed with Et2O, dried under reduced pressure;	77%

: Co3NO(1+)

: 32767-18-3
oxygen-18

A: Co3(18)OO(1+)

B: Co3((18)O)2(1+)

Conditions

Conditions	Yield
In gas Kinetics; byproducts: N(16)O, N(18)O; reaction in the gas phase with a pressure of dioxygen of < 5E-8, products: Co3((18)O)2 + N(16)O and Co3(18)O(16)O + N(18)O; expt. was performed on a mass spectrometer;	A 76% B 24%

...Expand

: {(C5Me5)2Mo2S4}

: 32767-18-3
oxygen-18

A: 2C5(CH3)5(1-)*2Mo(5+)*2(18)O(2-)*2S(2-)=(C5(CH3)5)2Mo2(18)O2S2

B: (C5Me5)2Mo2(μ-S2)(μ-S)(μ-SSO2(18)O)

C: (C5Me5)2Mo2(μ-S2)(μ-S)(μ-S2O3)

D: 2C5(CH3)5(1-)*2Mo(5+)*(18)O(2-)*3S(2-)=(C5(CH3)5)2Mo2(18)OS3

Conditions

Conditions	Yield
With SO2; N(C2H5)3 In chloroform under inert atmosphere, reaction time: 18 h;	A n/a B n/a C 75% D n/a

...Expand

: Co4NO(1+)

: 32767-18-3
oxygen-18

A: Co4((18)OO)(1+)

B: Co4((18)O)2(1+)

Conditions

Conditions	Yield
In gaseous matrix Kinetics; byproducts: N(16)O, N(18)O; reaction in gas phase with dioxygen pressure of < 5E-8, results: Co4((18)O)2(1+) + N(16)O and Co4((18)O)((16)O)(1+) + N(18)O; expt. was performed on a mass spectrometer;	A 63% B 37%

...Expand

: 58452-28-1
tetrakis(acetonitrile)copper(I) trifluoromethanesulfonate

: 586344-21-0
(10,15,20-tris(2,4,6-trimethylphenyl)-5-(2'-bis(5''-methyl-2''-pyridylmethyl)aminomethyl)pyridine-5'-carboxyamidophenyl)-porpyrinatoiron(III)

: 143-66-8
sodium tetraphenyl borate

: 32767-18-3
oxygen-18

: [(10,15,20-tris(2,4,6-trimethylphenyl)-5-(2'-bis(5''-methyl-2''-pyridylmethyl)amino(copper(II))methyl)pyridine-5'-carboxyamidophenyl)-porphyrinato(η1:η2-peroxo)iron(III)] tetraphenylborate

Conditions

Conditions	Yield
In acetonitrile soln. in CH3CN cooled to -30°C, exposed to dry O2 for 30 min, stored at -30°C for 5 d; elem. anal.;	60%

...Expand

: [RuII(η5-C5Me5)(bpy)(CH3CN)](NO3)

: 143-66-8
sodium tetraphenyl borate

: 32767-18-3
oxygen-18

: [RuIV(η2-18O2)(η5-C5Me5)(bpy)](BPh4)

Conditions

Conditions	Yield
In diethyl ether; acetonitrile at -40 - 20℃; Glovebox; Schlenk technique;	58%

...Expand

: 27903-26-0
[Pd{P(p-tol)3}3]

: 32767-18-3
oxygen-18

: 945402-71-1
(P(p-tolyl)3)2Pd(18)O2

Conditions

Conditions	Yield
In diethyl ether suspn. Pd complex in Et2O was frozen at -196 °C, evacuated, (18)O2 was added, warmed to room temp. and stirred for 20 min; ppt. was collected, washed with Et2O, dried under reduced pressure;	56%

: 1311994-23-6
[RhCl(di-ortho-xylyl-α-diketimine)(tert-butyl isocyanide)]

: 32767-18-3
oxygen-18

: [Rh((18)O)2Cl(di-ortho-xylyl-α-diketimine)(tert-butyl isocyanide)]

Conditions

Conditions	Yield
In benzene cooled to 77 K benzene soln. of metal compd. treated with (18)O2 for 10 min, warmed to room temp., mixt. stirred for 2 h; dried (vac.);	55%

: 1121-60-4
pyridine-2-carbaldehyde

: 14057-91-1
tetrakis(acetonitrile)copper(I) perchlorate

: N,N-bis(2-pyridylmethyl)-1,2-di(2-pyridyl)ethylamine

: 32767-18-3
oxygen-18

: C60H56Cl2Cu3N12O10(18)O2(3+)*C12H8Cl2CuN2O12(2-)*ClO4(1-)

Conditions

Conditions	Yield
In acetonitrile at 20℃; for 1h;	55%

...Expand

: 1477516-76-9
(i-Pr2Ph)2nacnacCr(η2-C2(SiMe3)2)

: 32767-18-3
oxygen-18

: C29H41CrN2(18)O2

Conditions

Conditions	Yield
In tetrahydrofuran at -78℃; for 1h; Schlenk technique; Glovebox;	52%

: C20H27FeN2NiOSSe(1+)

: 32767-18-3
oxygen-18

: C20H27FeN2NiO(18)OSSe(1+)

Conditions

Conditions	Yield
In dichloromethane at 22℃; for 2h;	50%

: ammonium hexafluorophosphate

: 439587-65-2
[Fe(II)(η2-OAc)(1,4,7-((MeO)2C6H3CH2)3-1,4,7-triazacyclononane)](1+)

: 127-09-3
sodium acetate

: 32767-18-3
oxygen-18

A: [Fe(III)2(μ-O)(μ-OAc)2(1,4,7-((MeO)2C6H3CH2)3-1,4,7-triazacyclononane)2](PF6)2

B: [Fe(III)2(μ-(18)O)(μ-OAc)2(1,4,7-((MeO)2C6H3CH2)3-1,4,7-triazacyclononane)2](PF6)2

Conditions

Conditions	Yield
In ethanol; dichloromethane Kinetics; under Ar; EtOH solns. of NaOAc and NH4PF6 added successively to CH2Cl2 soln. of Fe complex; (18)O2 introduced; stirred at 20°C for 24 h; evapd. to dryness; dissolved in CHCl3; chromd. with preparative SEC (twopolystyragel columns, CHCl3, room temp.); detd. by Raman spectra;	A n/a B 49%

...Expand

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Hazard Codes	O
Risk Statements	8
Safety Statements	17
RIDADR	UN 1072 2.2
WGK Germany	3

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