As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch
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inquiryItems Standard Result Appearance White needle crystal Complies Assay,GC 99%min
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inquiryManufacturer supply Phenylmethylsulfonyl fluoride CAS 329-98-6 with attractive price Company profile Wuhan Fortuna Chemical Co.,Ltd established in 2006, is a big integrative chemical enterprise being engaged in Pharmaceutical & its intermedi
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inquiryGood price Appearance:white powder Storage:Sealed, dry, microtherm , avoid light and smell. Package:As per customer's demand Application:Biological buffer Transportation:By Sea or By Air or By Courier Port:shanghai
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inquiry1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s
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inquiryProduct Name: Phenylmethylsulfonyl fluoride Synonyms: benzylsulphonylfluoride;4-TOLUENESULPHONYL FLUORIDE;4-TOLUENESULFONYL FLUORIDE;4-METHYLBENZENESULFONYL FLUORIDE;ALPHA-TOLUENESULPHONYL FLUORIDE;ALPHA-TOLUENESULFONYL FLUORIDE;BENZYL
Cas:329-98-6
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inquiryAbout Product Details Item Specification Test Results Appearance White crystalline powder Conform
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inquiryOur advantages: 1. All inquiries will be replied within 12 hours. 2. Dedication to quality, supply & service. 3. Strictly on selecting raw materials. 4. Reasonable & competitive price, fast lead time. 5. Sample is available for your eva
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Cas:329-98-6
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inquiryProduct Name: Phenylmethylsulfonyl fluoride CAS: 329-98-6 MF: C7H7FO2S MW: 174.19 EINECS: 206-350-2 Mol File: 329-98-6.mol Phenylmethylsulfonyl fluoride Structure Phenylmethylsulfonyl fluoride Chemical Properties Melting point
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inquiryOur company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese
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Cas:329-98-6
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inquiryHello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai
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inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
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Cas:329-98-6
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inquiryPMSFAppearance:white crystalline powder Storage:2-8°C Package:according to customers' requirements Application:pharmical intermediate Transportation:By air(EMS or EUB or FedEx or TNT ect...) or by sea(FOB or CIF or CNF ect...)or according to your dem
moderate price & quick delivery Appearance:White to cream solid Storage:Stored in cool, dry and ventilation place; Away from fire and heat Package:100g/bottle,1kg/bottle,25kg/drum or as per your request Application:PMSF is an irreversible serin
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inquiryName Phenylmethylsulfonyl fluoride Synonyms alpha-Toluenesulfonyl fluoride; PMSF; Benzenemethanesulfonyl fluoride CAS Registry Number 329-98-6 Molecular
Conditions | Yield |
---|---|
With potassium fluoride; triethylamine In dichloromethane; water | 97% |
With Methyl methanesulfonate; hydrogen fluoride at 100℃; for 8h; | 90% |
With potassium fluoride; water Heating; | 54% |
benzylsulfonylhydrazide
phenylmethylsulphonyl fluoride
Conditions | Yield |
---|---|
With Selectfluor In water at 60℃; for 14h; Schlenk technique; | 95% |
With Selectfluor In water at 60℃; for 18h; Schlenk technique; | 80% |
Conditions | Yield |
---|---|
With water; Selectfluor In acetonitrile for 1.5h; Reflux; | 88% |
With Selectfluor In water; acetonitrile at 20℃; for 1.5h; Reflux; | 88% |
Multi-step reaction with 2 steps 1: Selectfluor™ / acetonitrile; water / 0.03 h / 20 °C 2: Selectfluor™ / acetonitrile; water / 1.5 h / 20 °C / Reflux View Scheme |
S-benzyl phenyl-methanethiosulfonate
phenylmethylsulphonyl fluoride
Conditions | Yield |
---|---|
With Selectfluor In water; acetonitrile at 20℃; for 1.5h; Reflux; | 88% |
dibenzyl disulphide
A
phenylmethylsulphonyl fluoride
B
S-benzyl phenyl-methanethiosulfonate
Conditions | Yield |
---|---|
With water; Selectfluor In acetonitrile at 20℃; for 0.0333333h; | A 10% B 82% |
With Selectfluor In water; acetonitrile at 20℃; for 0.0333333h; | A 10% B 82% |
Conditions | Yield |
---|---|
With potassium fluoride In dichloromethane; water | 77% |
phenylmethylsulphonyl fluoride
Conditions | Yield |
---|---|
With N-fluorobis(benzenesulfon)imide In tetrahydrofuran at 0 - 20℃; for 3h; | 64% |
phenylmethanesulfonyl bromide
phenylmethylsulphonyl fluoride
Conditions | Yield |
---|---|
With tetrabutyl ammonium fluoride In tetrahydrofuran at 0 - 20℃; Inert atmosphere; | 59% |
Conditions | Yield |
---|---|
With pyridine; hydrogenchloride; potassium fluoride; water In acetonitrile at 20℃; for 40h; Electrochemical reaction; Green chemistry; | 45% |
Multi-step reaction with 2 steps 1: N-Bromosuccinimide; isopropyl alcohol / dichloromethane / 1 h / 20 °C 2: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 1,4-diazabicyclo [2.2.2] octane-1,4-diium-1,4-disulfinate / tetrahydrofuran / 0.75 h / 20 °C 2: N-fluorobis(benzenesulfon)imide / tetrahydrofuran / 3 h / 0 - 20 °C View Scheme |
Conditions | Yield |
---|---|
In toluene for 8h; Menshutkin Reaction; Inert atmosphere; Sealed tube; Reflux; | 100% |
4-(trimethylsilyl)morpholine
phenylmethylsulphonyl fluoride
4-(phenylmethane)sulfonylmorpholine
Conditions | Yield |
---|---|
In acetonitrile for 1h; Reflux; Inert atmosphere; | 97% |
phenylmethylsulphonyl fluoride
benzylsulfonyl azide
Conditions | Yield |
---|---|
With dmap; trimethylsilylazide In acetonitrile at 50℃; for 2h; Reagent/catalyst; Temperature; | 97% |
phenylmethylsulphonyl fluoride
[(benzylsulfonyl)(4-methoxyphenyl)methylene](triphenyl)phosphorane
Conditions | Yield |
---|---|
Stage #1: 4-methoxybenzyltriphenylphosphonium halide With n-butyllithium In tetrahydrofuran; hexane at 20℃; for 1h; Stage #2: phenylmethylsulphonyl fluoride In tetrahydrofuran; hexane at 20℃; | 86% |
Conditions | Yield |
---|---|
Stage #1: phenylmethylsulphonyl fluoride; C7H11NOS With triethylamine In acetonitrile at 20℃; Combinatorial reaction / High throughput screening (HTS); Sealed tube; Stage #2: In acetonitrile at 80℃; for 4h; Combinatorial reaction / High throughput screening (HTS); Sealed tube; Sonication; | 86% |
Conditions | Yield |
---|---|
With dibenzo-18-crown-6; potassium carbonate In acetonitrile for 3h; Ambient temperature; | 84% |
β-(2-methylphenoxy)ethylamine
phenylmethylsulphonyl fluoride
C16H19NO3S
Conditions | Yield |
---|---|
Stage #1: β-(2-methylphenoxy)ethylamine; phenylmethylsulphonyl fluoride With triethylamine In acetonitrile at 20℃; Combinatorial reaction / High throughput screening (HTS); Sealed tube; Stage #2: In acetonitrile at 80℃; for 4h; Combinatorial reaction / High throughput screening (HTS); Sealed tube; Sonication; | 82% |
phenylmethylsulphonyl fluoride
(3-chlorobenzyl)triphenylphosphonium chloride
[(benzylsulfonyl)(3-chlorophenyl)methylene](triphenyl)phosphorane
Conditions | Yield |
---|---|
Stage #1: (3-chlorobenzyl)triphenylphosphonium chloride With n-butyllithium In tetrahydrofuran; hexane at 20℃; for 1h; Stage #2: phenylmethylsulphonyl fluoride In tetrahydrofuran; hexane at 20℃; | 80% |
phenylmethylsulphonyl fluoride
Conditions | Yield |
---|---|
With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile) In acetonitrile Reflux; | 80% |
phenylmethylsulphonyl fluoride
(RS)-1-methyl-3-phenylpropylamine
N-(1-methyl-3-phenylpropyl)-C-phenylmethanesulfonamide
Conditions | Yield |
---|---|
Stage #1: phenylmethylsulphonyl fluoride; (RS)-1-methyl-3-phenylpropylamine With triethylamine In acetonitrile at 20℃; Combinatorial reaction / High throughput screening (HTS); Sealed tube; Stage #2: In acetonitrile at 80℃; for 4h; Combinatorial reaction / High throughput screening (HTS); Sealed tube; Sonication; | 79% |
phenylmethylsulphonyl fluoride
4-nitrobenzaldehdye
4-nitrostilbene
Conditions | Yield |
---|---|
With dibenzo-18-crown-6; potassium carbonate In acetonitrile for 3h; Ambient temperature; | 78% |
phenylmethylsulphonyl fluoride
[(benzylsulfonyl)(phenyl)methylene](triphenyl)phosphorane
Conditions | Yield |
---|---|
Stage #1: benzyltriphenylphosphonium halide With n-butyllithium In tetrahydrofuran; hexane at 20℃; for 1h; Stage #2: phenylmethylsulphonyl fluoride In tetrahydrofuran; hexane at 20℃; | 78% |
phenylmethylsulphonyl fluoride
2-methyl-1-phenyl-propylamine
N-(2-methyl-1-phenylpropyl)-C-phenylmethanesulfonamide
Conditions | Yield |
---|---|
Stage #1: phenylmethylsulphonyl fluoride; 2-methyl-1-phenyl-propylamine With triethylamine In acetonitrile at 20℃; Combinatorial reaction / High throughput screening (HTS); Sealed tube; Stage #2: In acetonitrile at 80℃; for 4h; Combinatorial reaction / High throughput screening (HTS); Sealed tube; Sonication; | 78% |
phenylmethylsulphonyl fluoride
α-bromoacetophenone
1,3-diphenyl-propen-3-one
Conditions | Yield |
---|---|
With dibenzo-18-crown-6; potassium carbonate In acetonitrile for 10h; Heating; | 77% |
With dibenzo-18-crown-6; potassium carbonate In acetonitrile for 10h; Heating; other arylmethanesulfonyl fluorides and activated haloalkanes; competition reaction with benzaldehyde and other aldehydes; | 77% |
With potassium carbonate; 1,4,7,10,13,20-Hexaoxa<13.1>(1,2)benzenophan In acetonitrile |
phenylmethylsulphonyl fluoride
cyclohexylmethylamine
N-(cyclohexylmethyl)-1-phenylmethanesulfonamide
Conditions | Yield |
---|---|
Stage #1: phenylmethylsulphonyl fluoride; cyclohexylmethylamine With triethylamine In acetonitrile at 20℃; Combinatorial reaction / High throughput screening (HTS); Sealed tube; Stage #2: In acetonitrile at 80℃; for 4h; Combinatorial reaction / High throughput screening (HTS); Sealed tube; Sonication; | 76% |
phenylmethylsulphonyl fluoride
2-allyl-phenylamine
Conditions | Yield |
---|---|
With pyridine In dichloromethane at 0 - 50℃; Inert atmosphere; | 75% |
phenylmethylsulphonyl fluoride
[(benzylsulfonyl)(4-methylphenyl)methylene](triphenyl)phosphorane
Conditions | Yield |
---|---|
Stage #1: 4-methylbenzyltriphenylphosphonium halide With n-butyllithium In tetrahydrofuran; hexane at 20℃; for 1h; Stage #2: phenylmethylsulphonyl fluoride In tetrahydrofuran; hexane at 20℃; | 74% |
phenylmethylsulphonyl fluoride
(p-nitrobenzyl)triphenylphosphonium bromide
[(benzylsulfonyl)(4-nitrophenyl)methylene](triphenyl)phosphorane
Conditions | Yield |
---|---|
Stage #1: (p-nitrobenzyl)triphenylphosphonium bromide With n-butyllithium In tetrahydrofuran; hexane at 20℃; for 1h; Stage #2: phenylmethylsulphonyl fluoride In tetrahydrofuran; hexane at 20℃; for 5h; | 72% |
(i) nBuLi, (ii) /BRN= 2088311/; Multistep reaction; |
phenylmethylsulphonyl fluoride
1-(4-bromophenyl)-cyclopropylamine
C16H16BrNO2S
Conditions | Yield |
---|---|
Stage #1: phenylmethylsulphonyl fluoride; 1-(4-bromophenyl)-cyclopropylamine With triethylamine In acetonitrile at 20℃; Combinatorial reaction / High throughput screening (HTS); Sealed tube; Stage #2: In acetonitrile at 80℃; for 4h; Combinatorial reaction / High throughput screening (HTS); Sealed tube; Sonication; | 72% |
phenylmethylsulphonyl fluoride
para-bromophenacyl bromide
(E)-1-(4-bromophenyl)-3-phenylprop-2-en-1-one
Conditions | Yield |
---|---|
With dibenzo-18-crown-6; potassium carbonate In acetonitrile for 10h; Heating; | 71% |
Conditions | Yield |
---|---|
Stage #1: 4-(morpholinomethyl)piperidin-4-ol; phenylmethylsulphonyl fluoride With triethylamine In acetonitrile at 20℃; Combinatorial reaction / High throughput screening (HTS); Sealed tube; Stage #2: In acetonitrile at 80℃; for 4h; Combinatorial reaction / High throughput screening (HTS); Sealed tube; Sonication; | 71% |
Conditions | Yield |
---|---|
With potassium carbonate In N,N,N,N,N,N-hexamethylphosphoric triamide for 3h; Ambient temperature; | 70% |
With dibenzo-18-crown-6; potassium carbonate In acetonitrile for 3h; Product distribution; Mechanism; Ambient temperature; other substituted methanesulphonyl fluorides, other aldehydes and ketones; var. times, temp. and solvents; | 69% |
Conditions | Yield |
---|---|
With triethylamine In water; acetone at 4℃; sulfonylation; | 69% |
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