Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
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Cas:3294-03-9
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inquiry2,2'-Thiodi(4-tert-octylphenol) CAS:3294-03-9 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quali
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inquiryJ&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
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inquiryLower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
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Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
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2,2'-Thiodi(4-tert-octylphenol) cas 3294-03-9Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
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2,2'-Thiodi(4-tert-octylphenol) Basic information Product Name: 2,2'-Thiodi(4-tert-octylphenol) Synonyms: 2,2’-thiobis[4-(1,1,3,3-tetramethylbutyl)-ph
Cas:3294-03-9
Min.Order:100 Kilogram
Negotiable
Type:Trading Company
inquiryHenan Wising Chem specializes in sourcing chemicals in China. We are associated with many trusted manufacturers each having different areas of expertise required for meeting the needs of our local as well as overseas buyers. We have access to custom
Cas:3294-03-9
Min.Order:500 Gram
Negotiable
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inquiryPrice, service, company and transport advantage: 1. Best service, place of origin China, high quality, and reasonable price. 2. It's customers' right to choose the package (EMS, DHL, FEDEX, UPS). 3. It's customers' right
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Min.Order:1 Kilogram
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inquiryProduct quality is the lifeline for our company. We obtained ISO9001 quality certificate. We are always focusing on upgrading the quality system and improving the whole product quality. We have built the quality inspection center which is equipp
Conditions | Yield |
---|---|
With sulfur dichloride In hexane at 0 - 20℃; | 43.9% |
methanol
2,2'-thiobis-4,4'-(1,1,3,3-tetramethylbutyl)phenol
[Ti2(μ-methylato)2(methylato)2(κ3-2,2'-thiobis[4-(1,1,3,3-tetramethylbutyl)phenolato])2]
Conditions | Yield |
---|---|
In methanol byproducts: CH3OH; N2, equimol., Ti compd. added to a soln. of S compd., stirred at room temp. for 12 h; ppt. filtered, washed (methanol), dried (vac.); elem. anal.; | 95% |
Vanadium (III) chloride-(tris-tetrahydrofuran)
2,2'-thiobis-4,4'-(1,1,3,3-tetramethylbutyl)phenol
acetonitrile
Conditions | Yield |
---|---|
In toluene byproducts: HCl; (N2, Schlenk) to a soln. of complex in toluene was added thio-compound, the mixt. was stirred at room temp. for 48 h, volatiles were removed in vac., the solid was dissolved in CH3CN, stirred for 3 h; ppt. was filtered off, washed with cold CH3CN, dried under vac.; elem. anal.; | 92% |
Conditions | Yield |
---|---|
In toluene byproducts: C2H5OH; (N2, Schlenk) to a soln. of V-compound in toluene was added thio-compound, the mixt. was stirred at room temp. for 2 h; volatiles were removed, the residue was dissolved in hot n-hexane, ppt. was filtered off, washed with n-hexane, dried in vac.; elem. anal.; | 91% |
ethanol
2,2'-thiobis-4,4'-(1,1,3,3-tetramethylbutyl)phenol
[Ti2(μ-ethylato)2(ethylato)2(κ3-2,2'-thiobis[4-(1,1,3,3-tetramethylbutyl)phenolato])2]
Conditions | Yield |
---|---|
In ethanol byproducts: ethanol; N2, equimol., Ti compd. added to a soln. of S compd., stirred at room temp. for 12 h; ppt. filtered, washed (methanol), dried (vac.); elem. anal.; | 90% |
2,2'-thiobis-4,4'-(1,1,3,3-tetramethylbutyl)phenol
[TaCp*Me2(κ3-2,2'-thiobis(6-tert-octylphenolato)]
Conditions | Yield |
---|---|
In toluene byproducts: CH4; (N2); stirring a mixt. of Ta complex and ligand in toluene at 100°C for 8 h; evapn.; elem. anal.; | 89% |
Conditions | Yield |
---|---|
In hexane byproducts: HCl; under N2; S compd. (1.5 equiv.) added to soln. of TiCl4 in n-hexane, mixt. stirred at room temp. for 48 h; volatiles removed under vac., residue washed with hexane, ppt. filtered off, washed with hexane, dried under vac.; elem. anal.; | 86% |
2,2'-thiobis-4,4'-(1,1,3,3-tetramethylbutyl)phenol
trimethylaluminum
[Al2(μ-κ3-O,S,O-2,2'-thiobis(4-(1,1,3,3-tetramethylbutyl)phenolato))2Me2]
Conditions | Yield |
---|---|
In toluene byproducts: methane; under N2; toluene soln. of AlMe3 added to cooled (273 K) soln. of ligand(1 equiv.) in toluene; warmed to room temp.; stirred for 12 h; filtered; ppt. washed with hexane; dried under vac.; elem. anal.; | 84% |
2,2'-thiobis-4,4'-(1,1,3,3-tetramethylbutyl)phenol
hafnium tetrachloride
[Hf(2,2'-thiobis(4-(1,1,3,3-tetramethylbutyl)phenolato)-κ3O,S,O)2]
Conditions | Yield |
---|---|
In toluene byproducts: HCl; (N2); addn. of ligand to a suspn. of metal salt in toluene, reflux for 48 h; filtration, evapn. in vac.; elem. anal.; | 82% |
2,2'-thiobis-4,4'-(1,1,3,3-tetramethylbutyl)phenol
hafnium tetrachloride
[Hf2(μ-2,2'-thiobis(4-(1,1,3,3-tetramethyl-butyl)phenolate)-κ3O,S,O)2Cl4]
Conditions | Yield |
---|---|
In toluene byproducts: HCl; (N2); to suspn. of HfCl4 in toluene was added thiobisphenol, stirred at room temp. for 48 h; evapd. in vac., elem. anal.; | 82% |
2,2'-thiobis-4,4'-(1,1,3,3-tetramethylbutyl)phenol
titanium tetrachloride
bis(μ-2,2'-thiobis[4-(1,1,3,3-tetramethylbutyl)phenolato]-κ3O,S,O)tetrachlorodititanium(IV)
Conditions | Yield |
---|---|
In hexane byproducts: HCl; under N2; S compd. (1 equiv.) added to soln. of TiCl4 in n-hexane, mixt.refluxed for 48 h; ppt. filtered off, washed with cold Et2O, dried under vac.; elem. anal.; | 80% |
In diethyl ether byproducts: HCl; under N2; S compd. (1 equiv.) added to soln. of TiCl4 in Et2O, mixt. refluxed for 48 h; ppt. filtered off, washed with cold Et2O, dried under vac.; elem. anal.; | 80% |
2,2'-thiobis-4,4'-(1,1,3,3-tetramethylbutyl)phenol
[TaCp*Cl2(κ3-2,2'-thiobis(6-tert-octylphenolato)]
Conditions | Yield |
---|---|
With triethylamine In toluene byproducts: triethylammonium chloride; (N2); addn. of amine to a soln. of Ta complex and ligand in toluene, stirring at 100°C for 12 h, cooling to room temp.; filtration, extn. with toluene, evapn., washing with cold pentane, crystn. (pentane); elem. anal.; | 79% |
2,2'-thiobis-4,4'-(1,1,3,3-tetramethylbutyl)phenol
zirconium(IV) chloride
[Zr2(μ-2,2'-thiobis(4-(1,1,3,3-tetramethyl-butyl)phenolate)-κ3O,S,O)2Cl4]
Conditions | Yield |
---|---|
In toluene byproducts: HCl; (N2); to suspn. of ZrCl4 in toluene was added thiobisphenol, stirred at room temp. for 48 h; evapd. in vac., elem. anal.; | 73% |
2,2'-thiobis-4,4'-(1,1,3,3-tetramethylbutyl)phenol
zirconium(IV) chloride
[Zr(2,2'-thiobis(4-(1,1,3,3-tetramethylbutyl)phenolato)-κ3O,S,O)2]
Conditions | Yield |
---|---|
In toluene byproducts: HCl; (N2); addn. of ligand to a suspn. of metal salt in toluene, reflux for 48 h; filtration, evapn. in vac.; elem. anal.; | 55% |
2,2'-thiobis-4,4'-(1,1,3,3-tetramethylbutyl)phenol
bis(2,2'-thiobis[4-(1,1,3,3-tetramethylbutyl)phenolato]-κ3O,S,O)titanium(IV)
Conditions | Yield |
---|---|
In hexane under N2; S compd. added to soln. of Ti complex in hexane, mixt. refluxed for 6 h; volatiles removed under vac., residue dissolved in hexane, stored at room temp. for several d, crysts. sepd.; elem. anal.; | 15.8% |
In not given |
bis(2-isopropyl-5-methylphenyl)phosphorochloridite
2,2'-thiobis-4,4'-(1,1,3,3-tetramethylbutyl)phenol
Conditions | Yield |
---|---|
With triethylamine In toluene at -10 - 25℃; for 18h; |
2,2'-thiobis-4,4'-(1,1,3,3-tetramethylbutyl)phenol
Conditions | Yield |
---|---|
Stage #1: ortho-cresol With triethylamine; phosphorus trichloride In toluene at -15℃; for 2h; Stage #2: 2,2'-thiobis-4,4'-(1,1,3,3-tetramethylbutyl)phenol In toluene at -15 - 25℃; for 18h; |
2,2'-thiobis-4,4'-(1,1,3,3-tetramethylbutyl)phenol
aluminum ethoxide
[Al2(μ-ethoxo)2(κ3-O,S,O-2,2'-thiobis(4-(1,1,3,3-tetramethylbutyl)phenolato))2]
Conditions | Yield |
---|---|
In toluene under N2; |
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