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Hangzhou Dingyan Chem Co., Ltd

Items Standard Result Appearance Colorless or pale yellow liquid Clear liquid Assay 98.0%min

Top purity 3,3-Dimethylacryloyl chloride with high quality and best price cas:3350-78-5

Cas:3350-78-5

Min.Order:1 Kilogram

FOB Price: $3.0 / 10.0

Type:Manufacturers

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Dayang Chem (Hangzhou) Co.,Ltd.

As a leading manufacturer and supplier of chemicals in China, DayangChem not only supply popular chemicals, but also DayangChem's R&D center offer custom synthesis services. DayangChem can provide different quantities of custom synthesis ch

3,3-Dimethylacryloyl chloride Manufacturer/High quality/Best price/In stock

Cas:3350-78-5

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

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Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

3-Methyl-2-butenoyl chloride

Cas:3350-78-5

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

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Henan Tianfu Chemical Co., Ltd.

Our advantage:Our company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scient

TIANFU-CHEM 3-Methylcrotonoyl chloride

Cas:3350-78-5

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Hebei Nengqian Chemical Import and Export Co., LTD

With our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin

3-Methylcrotonoyl chloride

Cas:3350-78-5

Min.Order:1 Kilogram

FOB Price: $1.0 / 10.0

Type:Trading Company

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Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Pharmaceutical Grade CAS 3350-78-5 with competitive price

Cas:3350-78-5

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

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Wuhan Han Sheng New Material Technology Co.,Ltd

Our Advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We

Fast delivery 3-Methylcrotonoyl chloride CAS 3350-78-5 with best price

Cas:3350-78-5

Min.Order:10 Kilogram

Negotiable

Type:Trading Company

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Hebei Sankai Chemical Technology Co., Ltd

1. Product advantages High purity, all above 98.5%, no impurities after dissolution We will test each batch to ensure quality OEM and private brand services designed for free Various cap colors available We can also provide MT1 peptide powd

3-Methylcrotonoyl chloride

Cas:3350-78-5

Min.Order:1 Kilogram

FOB Price: $50.0 / 100.0

Type:Trading Company

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Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

2-Butenoyl chloride,3-methyl- 3350-78-5

Cas:3350-78-5

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

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Changchun Artel lmport and Export trade company

Superiority We can customize and synthesize products that other suppliers may not be able to provide. Product Detail Minimum Order Q

China supplier 3,3-Dimethylacryloyl chloride CAS:3350-78-5

Cas:3350-78-5

Min.Order:100 Kilogram

Negotiable

Type:Trading Company

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Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

CAS NO.:3350-78-5

Cas:3350-78-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Xiamen Hisunny Chemical Co.,Ltd

Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia

3,3-Dimethylaclyloyl chloride

Cas:3350-78-5

Min.Order:0

Negotiable

Type:Manufacturers

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Triumph International Development Limilted

Appearance:off-white to white solid Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application:Used for Synthesis API and Research Transportation:As customer request Port:Qingda

3-Methylcrotonoyl chloride 3350-78-5

Cas:3350-78-5

Min.Order:1 Kilogram

FOB Price: $18.0 / 20.0

Type:Lab/Research institutions

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Afine Chemicals Limited

Company Introduction 1. Established in 2005, with two independent business divisions: Fine chemicals division; Pharmaceutical division. 2. Main product: Optical brightener Textile auxiliary Dye stuff Pigments

3,3-DIMETHYLACRYLOYL CHLORIDE

Cas:3350-78-5

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

SHANGHAI T&W PHARMACEUTICAL CO., LTD.

A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc

3-Methylcrotonoyl chloride

Cas:3350-78-5

Min.Order:4 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

2-Butenoyl chloride,3-methyl-

Cas:3350-78-5

Min.Order:0

Negotiable

Type:Lab/Research institutions

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Chemlyte Solutions

Chemlyte Solutions believe that customers and suppliers deserve much more than what traditional distributors can offer. To grow in today s fast-paced and increasingly competitive market it is essential to be able to quickly adapt to market forces eff

Featured products 3,3-Dimethylacryloyl chloride

Cas:3350-78-5

Min.Order:100 Gram

Negotiable

Type:Other

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SHANGHAI SYSTEAM BIOCHEM CO., LTD

We are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov

Fast delivery 3-Methylcrotonoyl chloride CAS 3350-78-5 with best price

Cas:3350-78-5

Min.Order:100 Gram

FOB Price: $100.0 / 2000.0

Type:Lab/Research institutions

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Siwei Development Group Ltd.

Product name: 3,3-Dimethylacryloyl Chloride CAS No.:3350-78-5 Molecule Formula:C5H7ClO Molecule Weight:118.56 Purity: 97% Package: 25kg/drum Description:Colorless liquid Manufacture Standards:Enterprise Standard TESTING ITEMS

High Quality 3,3-Dimethylacryloyl Chloride in stock

Cas:3350-78-5

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Xiamen Jenny Chemical Technology Co., Ltd.

GMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,

3-Methylcrotonoylchloride

Cas:3350-78-5

Min.Order:1 Milligram

Negotiable

Type:Trading Company

inquiry

Shanghai Minstar Chemical Co., Ltd

Product Name: 3-Methylcrotonoyl chloride Synonyms: 3-methyl-2-butenoylchlorid;3-METHYL-2-BUTENOYL CHLORIDE;3-METHYL-BUT-2-ENOYL CHLORIDE;3-METHYLCROTONOYL CHLORIDE;3,3-DIMETHYLACRYLOYL CHLORIDE;SENECIOYL CHLORIDE;3,3-Dimethylaclyloyl chloride;M

3,3-Dimethylacryloyl chloride 3350-78-5 C5H7ClO

Cas:3350-78-5

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

EAST CHEMSOURCES LIMITED

factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B

Fast delivery 3-Methylcrotonoyl chloride CAS 3350-78-5 with best price

Cas:3350-78-5

Min.Order:1 Kilogram

FOB Price: $18.0 / 20.0

Type:Trading Company

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TAIZHOU ZHENYU BIOTECHNOLOGY CO., LTD

Zhenyu biotech exported this product to many countries and regions at best price. if you are looking for the material's manufacturer or supplier in china, zhenyu biotech is your best choice. pls contact with us freely for getting detailed

3-Methylcrotonoyl chloride

Cas:3350-78-5

Min.Order:1 Kilogram

FOB Price: $2.0

Type:Lab/Research institutions

inquiry

Shandong Mopai Biotechnology Co., LTD

Shandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W

Fast delivery 3-Methylcrotonoyl chloride CAS 3350-78-5 with best price

Cas:3350-78-5

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

KAISA GROUP INC

1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer

China supplier 3,3-Dimethylacryloyl chloride CAS:3350-78-5 CAS NO.3350-78-5

Cas:3350-78-5

Min.Order:1 Metric Ton

FOB Price: $7.0 / 8.0

Type:Trading Company

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Hangzhou Zhongqi chem Co.,Ltd.

located in hangzhou national hi-tech industrial development zone, zhongqichem is a technical company mainly focus on the custom synthesis, manufacturing, sales of chemicals to various industries. benefiting from the outstanding customer service and h

Quality Factory Supply 3350-78-5 In Bulk Supply

Cas:3350-78-5

Min.Order:0

Negotiable

Type:Other

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Hunan chemfish Pharmaceutical co.,Ltd

Appearance:95%+ Package:R&D,Pilot run Transportation:per client require Port:Express ,Air, Sea

3,3-Dimethylaclyloyl chloride

Cas:3350-78-5

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Bluecrystal chem-union

We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp

Fast delivery 3-Methylcrotonoyl chloride CAS 3350-78-5 with best price

Cas:3350-78-5

Min.Order:1 Metric Ton

FOB Price: $1.0

Type:Trading Company

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Hebei Mojin Biotechnology Co.,Ltd

We produce carbomer by our own factory,carbomer 940 is our best seller.It is used for cosmetic and medical.And we also become agent for lubrizol.Our carbomer 940 get high viscosity and good transparency.The price will depond on the market,surely supp

2-Butenoyl chloride,3-methyl-

Cas:3350-78-5

Min.Order:0

Negotiable

Type:Trading Company

inquiry

Kono Chem Co.,Ltd

high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou

3,3-Dimethylacryloyl chloride

Cas:3350-78-5

Min.Order:0

Negotiable

Type:Other

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Synthetic route

3-Methylbutenoic acid
541-47-9

3-Methylbutenoic acid

3,3-Dimethylacryloyl chloride
3350-78-5

3,3-Dimethylacryloyl chloride

Conditions
ConditionsYield
With oxalyl dichloride In dichloromethane at 20℃;99%
With thionyl chloride at 0℃; for 3h;96%
With thionyl chloride 1.) reflux, 1.3 h, 2.) room temperature, 2.5 h, 3.) reflux, 1 h;92%
4,4-dimethyloxetan-2-one
1823-52-5

4,4-dimethyloxetan-2-one

3,3-Dimethylacryloyl chloride
3350-78-5

3,3-Dimethylacryloyl chloride

Conditions
ConditionsYield
With thionyl chloride Erhitzen des Reaktionsgemisches mit wenig Schwefelsaeure;
3,3-Dimethylacryloyl chloride
3350-78-5

3,3-Dimethylacryloyl chloride

i-Amyl alcohol
123-51-3

i-Amyl alcohol

3-methyl-1-butyl 3-methyl-2-butenoate
56922-73-7

3-methyl-1-butyl 3-methyl-2-butenoate

Conditions
ConditionsYield
With pyridine; dmap; dicyclohexyl-carbodiimide In dichloromethane at 0 - 20℃; for 3.5h;100%
In benzene at 30℃; Kinetics; Activation energy; Further Variations:; Temperatures; Acylation; alcoholysis;
With pyridine; benzene
3,3-Dimethylacryloyl chloride
3350-78-5

3,3-Dimethylacryloyl chloride

aniline
62-53-3

aniline

N-phenyl-3-methyl-2-butenamide
13209-80-8

N-phenyl-3-methyl-2-butenamide

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 2h;100%
With N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 2h;100%
With pyridine97%
3,3-Dimethylacryloyl chloride
3350-78-5

3,3-Dimethylacryloyl chloride

diphenylphosphinous acid methyl ester
4020-99-9

diphenylphosphinous acid methyl ester

(3-Methyl-2-butenoyl)diphenylphosphanoxid
87951-17-5

(3-Methyl-2-butenoyl)diphenylphosphanoxid

Conditions
ConditionsYield
1) -196 deg C to r.t., 2) 2 h, r.t.;100%
3,3-Dimethylacryloyl chloride
3350-78-5

3,3-Dimethylacryloyl chloride

monohydroxymethyl-alpha-terthiophene
13059-93-3

monohydroxymethyl-alpha-terthiophene

5-(3-methyl-2-butenoyloxy)methyl-2,2':5',2''-terthiophene
26905-76-0

5-(3-methyl-2-butenoyloxy)methyl-2,2':5',2''-terthiophene

Conditions
ConditionsYield
With pyridine In dichloromethane100%
With pyridine In tetrahydrofuran 1.) 0 deg C, 3 h, 2.) reflux, 2h;
3,3-Dimethylacryloyl chloride
3350-78-5

3,3-Dimethylacryloyl chloride

(E)-trimethyl[2-(4-methylphenyl)ethenyl]silane
73839-45-9

(E)-trimethyl[2-(4-methylphenyl)ethenyl]silane

(E)-1-(4-methylphenyl)-3-oxo-5-methyl-1,4-hexadiene
73839-46-0

(E)-1-(4-methylphenyl)-3-oxo-5-methyl-1,4-hexadiene

Conditions
ConditionsYield
With aluminium trichloride In dichloromethane at -78℃; for 0.5h;100%
3,3-Dimethylacryloyl chloride
3350-78-5

3,3-Dimethylacryloyl chloride

2-methoxy-4,4,5,5-tetramethyl-1,3,2-dioxaphospholane
14812-60-3

2-methoxy-4,4,5,5-tetramethyl-1,3,2-dioxaphospholane

3-Methyl-1-(4,4,5,5-tetramethyl-2-oxo-2λ5-[1,3,2]dioxaphospholan-2-yl)-but-2-en-1-one

3-Methyl-1-(4,4,5,5-tetramethyl-2-oxo-2λ5-[1,3,2]dioxaphospholan-2-yl)-but-2-en-1-one

Conditions
ConditionsYield
at 0 - 35℃; for 4h;100%
for 1h; Yield given;
3,3-Dimethylacryloyl chloride
3350-78-5

3,3-Dimethylacryloyl chloride

4-bromo-aniline
106-40-1

4-bromo-aniline

N-(3,3'-dimethylacryoloyl)-4-bromoaniline
135631-89-9

N-(3,3'-dimethylacryoloyl)-4-bromoaniline

Conditions
ConditionsYield
With triethylamine In dichloromethane at 20℃; for 3.33333h;100%
Stage #1: 3,3-Dimethylacryloyl chloride; 4-bromo-aniline In dichloromethane at 20℃; for 0.333333h;
Stage #2: With triethylamine In dichloromethane at 20℃; for 3h;
100%
With pyridine at 0 - 20℃; for 5h; Inert atmosphere;99%
3,3-Dimethylacryloyl chloride
3350-78-5

3,3-Dimethylacryloyl chloride

(R)-3-benzyloxy-1,2-propanediol
56552-80-8

(R)-3-benzyloxy-1,2-propanediol

1,2-di(3-methylbut-2-enoyl)-3-benzyl-sn-glycerol
349123-42-8

1,2-di(3-methylbut-2-enoyl)-3-benzyl-sn-glycerol

Conditions
ConditionsYield
With pyridine; dmap In dichloromethane at 0 - 20℃;100%
3,3-Dimethylacryloyl chloride
3350-78-5

3,3-Dimethylacryloyl chloride

4-bromo-N-methylaniline
6911-87-1

4-bromo-N-methylaniline

N-(4-bromophenyl)-N-methyl-3-methyl-2-butenamide
345964-72-9

N-(4-bromophenyl)-N-methyl-3-methyl-2-butenamide

Conditions
ConditionsYield
With triethylamine In dichloromethane at 20℃; for 2.5h;100%
With triethylamine In dichloromethane
With triethylamine In dichloromethane at 20℃; for 2.5h;
With triethylamine In dichloromethane for 2.58333h;
3,3-Dimethylacryloyl chloride
3350-78-5

3,3-Dimethylacryloyl chloride

(+/-)-2-methyl-1-butanol
137-32-6

(+/-)-2-methyl-1-butanol

2-methylbutyl 3-methyl-2-butenoate

2-methylbutyl 3-methyl-2-butenoate

Conditions
ConditionsYield
With pyridine; dmap; dicyclohexyl-carbodiimide In dichloromethane at 0 - 20℃; for 3.5h;100%
3,3-Dimethylacryloyl chloride
3350-78-5

3,3-Dimethylacryloyl chloride

pentan-1-ol
71-41-0

pentan-1-ol

pentyl 3-methyl-2-butenoate

pentyl 3-methyl-2-butenoate

Conditions
ConditionsYield
With pyridine; dmap; dicyclohexyl-carbodiimide In dichloromethane at 0 - 20℃; for 3.5h;99.7%
In benzene at 30℃; Kinetics; Activation energy; Further Variations:; Temperatures; Acylation; alcoholysis;
3,3-Dimethylacryloyl chloride
3350-78-5

3,3-Dimethylacryloyl chloride

Geraniol
106-24-1

Geraniol

(E)-geranyl 3-methyl-3-butenoate
84825-22-9

(E)-geranyl 3-methyl-3-butenoate

Conditions
ConditionsYield
With triethylamine In dichloromethane at -78℃; for 3h;99%
3,3-Dimethylacryloyl chloride
3350-78-5

3,3-Dimethylacryloyl chloride

tert-butyl pyrrolidine-1-carboxylate
86953-79-9

tert-butyl pyrrolidine-1-carboxylate

N-(tert-butoxycarbonyl)-2-(1-oxopropyl)pyrrolidine

N-(tert-butoxycarbonyl)-2-(1-oxopropyl)pyrrolidine

Conditions
ConditionsYield
With sec.-butyllithium; (-)-sparteine In tetrahydrofuran at -78℃; for 2h; Product distribution; other reag.;99%
3,3-Dimethylacryloyl chloride
3350-78-5

3,3-Dimethylacryloyl chloride

tert-butyl pyrrolidine-1-carboxylate
86953-79-9

tert-butyl pyrrolidine-1-carboxylate

N-(tert-butoxycarbonyl)-2-[3-methyl-1-oxo-2-butenyl]pyrrolidine

N-(tert-butoxycarbonyl)-2-[3-methyl-1-oxo-2-butenyl]pyrrolidine

Conditions
ConditionsYield
Stage #1: tert-butyl pyrrolidine-1-carboxylate With sec.-butyllithium; (-)-sparteine In tetrahydrofuran at -78℃; for 1h;
Stage #2: With lithium chloride In tetrahydrofuran at -55℃; for 1h;
Stage #3: 3,3-Dimethylacryloyl chloride In tetrahydrofuran at -50 - 20℃;
99%
With sec.-butyllithium; (-)-sparteine 1.) THF, -78 deg C; Yield given;
3,3-Dimethylacryloyl chloride
3350-78-5

3,3-Dimethylacryloyl chloride

(S)-4-phenyl-2-oxazolidinone
99395-88-7

(S)-4-phenyl-2-oxazolidinone

(S)-3-(3-Methyl-but-2-enoyl)-4-phenyl-oxazolidin-2-one
294176-63-9

(S)-3-(3-Methyl-but-2-enoyl)-4-phenyl-oxazolidin-2-one

Conditions
ConditionsYield
Stage #1: (S)-4-phenyl-2-oxazolidinone With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 0.5h; Metallation;
Stage #2: 3,3-Dimethylacryloyl chloride In tetrahydrofuran; hexane at -78 - 0℃; for 3.5h; Acylation;
99%
3,3-Dimethylacryloyl chloride
3350-78-5

3,3-Dimethylacryloyl chloride

2-Bromo-4-(5-hydroxy-3-methyl-pyrazol-1-yl)-benzonitrile
1008520-71-5

2-Bromo-4-(5-hydroxy-3-methyl-pyrazol-1-yl)-benzonitrile

2-Bromo-4-[5-hydroxy-3-methyl-4-(3-methyl-but-2-enoyl)-pyrazol-1-yl]-benzonitrile
1008520-72-6

2-Bromo-4-[5-hydroxy-3-methyl-4-(3-methyl-but-2-enoyl)-pyrazol-1-yl]-benzonitrile

Conditions
ConditionsYield
Stage #1: 2-Bromo-4-(5-hydroxy-3-methyl-pyrazol-1-yl)-benzonitrile With magnesium ethylate In tetrahydrofuran for 4h; Heating / reflux;
Stage #2: 3,3-Dimethylacryloyl chloride In tetrahydrofuran at 0 - 20℃;
Stage #3: With hydrogenchloride; water In tetrahydrofuran at 0℃; for 0.25h;
99%
3,3-Dimethylacryloyl chloride
3350-78-5

3,3-Dimethylacryloyl chloride

(R)-4-(phenylmethyl)-2-oxazolidinone
40217-17-2, 90719-32-7, 120574-96-1, 102029-44-7

(R)-4-(phenylmethyl)-2-oxazolidinone

(R)-4-Benzyl-3-(3-methyl-but-2-enoyl)-oxazolidin-2-one

(R)-4-Benzyl-3-(3-methyl-but-2-enoyl)-oxazolidin-2-one

Conditions
ConditionsYield
Stage #1: (R)-4-(phenylmethyl)-2-oxazolidinone With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 0.166667h; Inert atmosphere;
Stage #2: 3,3-Dimethylacryloyl chloride In tetrahydrofuran; hexane at -78 - 0℃; for 0.5h; Inert atmosphere;
99%
Stage #1: (R)-4-(phenylmethyl)-2-oxazolidinone With n-butyllithium In tetrahydrofuran for 0.166667h; Inert atmosphere; Cooling;
Stage #2: 3,3-Dimethylacryloyl chloride In tetrahydrofuran at 0℃; for 0.5h; Inert atmosphere; Cooling;
51.1 g
3,3-Dimethylacryloyl chloride
3350-78-5

3,3-Dimethylacryloyl chloride

amino-5-bromo-2-toluene
6933-10-4

amino-5-bromo-2-toluene

N-(4-bromo-2-methylphenyl)-3-methyl-2-butenamide
203856-43-3

N-(4-bromo-2-methylphenyl)-3-methyl-2-butenamide

Conditions
ConditionsYield
With sodium hydroxide In dichloromethane; water98.6%
With sodium hydroxide In dichloromethane at 20℃; for 16h; Acylation;65%
3,3-Dimethylacryloyl chloride
3350-78-5

3,3-Dimethylacryloyl chloride

p-cresol
106-44-5

p-cresol

4'-methylphenyl 3-methylbut-2-enoate
24700-20-7

4'-methylphenyl 3-methylbut-2-enoate

Conditions
ConditionsYield
Stage #1: p-cresol With sodium hydride In tetrahydrofuran at 0℃; for 0.25h;
Stage #2: 3,3-Dimethylacryloyl chloride In tetrahydrofuran at 0 - 20℃; for 3h;
98%
3,3-Dimethylacryloyl chloride
3350-78-5

3,3-Dimethylacryloyl chloride

1,2-dimethoxybenzene
91-16-7

1,2-dimethoxybenzene

1-(3,4-dimethoxyphenyl)-3-methylbut-2-en-1-one

1-(3,4-dimethoxyphenyl)-3-methylbut-2-en-1-one

Conditions
ConditionsYield
With aluminum (III) chloride In dichloromethane at 0℃; for 3h; Inert atmosphere;98%
With aluminium trichloride; diethyl ether
With aluminum (III) chloride In dichloromethane
3,3-Dimethylacryloyl chloride
3350-78-5

3,3-Dimethylacryloyl chloride

4,6-dimethoxyindole
23659-87-2

4,6-dimethoxyindole

1-(4',6'-dimethoxyindol-1'-yl)-3-methylbut-2-en-1-one
151290-63-0

1-(4',6'-dimethoxyindol-1'-yl)-3-methylbut-2-en-1-one

Conditions
ConditionsYield
With sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate for 2h; Ambient temperature;98%
3,3-Dimethylacryloyl chloride
3350-78-5

3,3-Dimethylacryloyl chloride

diallylamine
124-02-7

diallylamine

3-methylbut-2-enoic acid diallylamide
82799-51-7

3-methylbut-2-enoic acid diallylamide

Conditions
ConditionsYield
With triethylamine In benzene98%
3,3-Dimethylacryloyl chloride
3350-78-5

3,3-Dimethylacryloyl chloride

3-Methyl-6-nitro-2,3,4,5-tetrahydro-1H-benzo[b][1,4]diazepine
189939-48-8

3-Methyl-6-nitro-2,3,4,5-tetrahydro-1H-benzo[b][1,4]diazepine

3-Methyl-1-(3-methyl-6-nitro-2,3,4,5-tetrahydro-benzo[b][1,4]diazepin-1-yl)-but-2-en-1-one
189939-49-9

3-Methyl-1-(3-methyl-6-nitro-2,3,4,5-tetrahydro-benzo[b][1,4]diazepin-1-yl)-but-2-en-1-one

Conditions
ConditionsYield
With dmap; sodium hydrogencarbonate for 3h;98%
3,3-Dimethylacryloyl chloride
3350-78-5

3,3-Dimethylacryloyl chloride

benzyl-(2-tert-butyl-phenyl)-amine
205242-33-7

benzyl-(2-tert-butyl-phenyl)-amine

N-benzyl-N-(2-tert-butylphenyl)-3,3-dimethylacrylamide
205242-34-8

N-benzyl-N-(2-tert-butylphenyl)-3,3-dimethylacrylamide

Conditions
ConditionsYield
In benzene for 24h;98%
3,3-Dimethylacryloyl chloride
3350-78-5

3,3-Dimethylacryloyl chloride

2,2,2-trifluoroethanol
75-89-8

2,2,2-trifluoroethanol

2,2,2-trifluoroethyl 3-methylbut-2-enoate
796850-91-4

2,2,2-trifluoroethyl 3-methylbut-2-enoate

Conditions
ConditionsYield
With triethylamine In diethyl ether at 0℃; for 4h;98%
3,3-Dimethylacryloyl chloride
3350-78-5

3,3-Dimethylacryloyl chloride

3-methyl-2-buten-1-ol
556-82-1

3-methyl-2-buten-1-ol

3-methyl-2-buten-1-yl 3-methyl-2-butenoate
72779-06-7

3-methyl-2-buten-1-yl 3-methyl-2-butenoate

Conditions
ConditionsYield
With pyridine; dmap; dicyclohexyl-carbodiimide In dichloromethane at 0 - 20℃; for 3.5h;97.9%
With pyridine; benzene
3,3-Dimethylacryloyl chloride
3350-78-5

3,3-Dimethylacryloyl chloride

tryptamine
61-54-1

tryptamine

N-(2-(1H-indol-3-yl)-ethyl)-3-methylbut-2-enamide
87078-46-4

N-(2-(1H-indol-3-yl)-ethyl)-3-methylbut-2-enamide

Conditions
ConditionsYield
With 1,1,1,3,3,3-hexamethyl-disilazane In tetrahydrofuran for 48h; Inert atmosphere;97.4%
3,3-Dimethylacryloyl chloride
3350-78-5

3,3-Dimethylacryloyl chloride

3-methyl-phenol
108-39-4

3-methyl-phenol

3'-methylphenyl 3-methylbut-2-enoate
133532-17-9

3'-methylphenyl 3-methylbut-2-enoate

Conditions
ConditionsYield
Stage #1: 3-methyl-phenol With sodium hydride In tetrahydrofuran at 0℃; for 0.25h;
Stage #2: 3,3-Dimethylacryloyl chloride In tetrahydrofuran at 0 - 20℃; for 3h;
97%
3,3-Dimethylacryloyl chloride
3350-78-5

3,3-Dimethylacryloyl chloride

copper(I) cyanide
544-92-3

copper(I) cyanide

senecioyl cyanide
38576-60-2

senecioyl cyanide

Conditions
ConditionsYield
In acetone for 0.416667h; Heating;97%
In acetonitrile at 90℃; for 1.5h;59%
With phosphorus pentoxide In benzene for 6h; Heating;51%
In acetonitrile
In acetonitrile for 0.5h; Heating;

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