Maufacturer supply 4,4''-Diamino-p-terphenyl CAS 3365-85-3 at reasonable price Company profile Wuhan Fortuna Chemical Co.,Ltd established in 2006, is a big integrative chemical enterprise being engaged in Pharmaceutical & its interme
Cas:3365-85-3
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inquiryhigh quality Appearance:solid Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:OLED Intermediate Transportation:by air or by sea Port:Shanghai, Qingdao
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inquiry4,4''-DIAMINO-P-TERPHENYL CAS:3365-85-3 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality
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Cas:3365-85-3
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inquiryProduct name: 4-[4-(4-Aminophenyl)Phenyl]Aniline CAS No.:3365-85-3 Molecule Formula:C18H16N2 Molecule Weight:260.33 Purity: 99% Package: 25kg/drum Description:Gray powder Manufacture Standards:Enterprise Standard TESTING ITEMS
Cas:3365-85-3
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inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
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Cas:3365-85-3
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inquiry4,4''-Diamino-p-terphenyl CAS NO.3365-85-3 Application:4,4''-Diamino-p-terphenyl CAS NO.3365-85-3
good quality, competitive price, thoughtful after sale serviceAppearance:white powder Storage:Keep it in dry,shady and cool place Package:25kg,50kg,180kg,200kg,250kg,1000kg,customization Application:Pharma;Industry;Agricultural;chemical reaserch Tran
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inquiryConditions | Yield |
---|---|
With palladium 10% on activated carbon; hydrazine In ethanol for 6h; Inert atmosphere; Reflux; | 100% |
With hydrogen; palladium on activated charcoal In tetrahydrofuran for 18h; | 99% |
With 3% Pd/C; hydrazine In ethanol Heating; | 77% |
1.4-dibromobenzene
4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline
4,4''-diamino-p-terphenyl
Conditions | Yield |
---|---|
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In water; toluene for 24h; Schlenk technique; Inert atmosphere; Heating; | 52% |
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In water; toluene for 24h; Schlenk technique; Inert atmosphere; Heating; | 52% |
With tetrakis(triphenylphosphine) palladium(0); sodium carbonate In 1,4-dioxane; water at 110℃; for 48h; Inert atmosphere; | 48% |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 76 percent / K2CO3 / tetrakis(triphenylphosphine)palladium(0) / tetrahydrofuran / 18 h / Heating 2: 99 percent / H2 / Pd/C / tetrahydrofuran / 18 h View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 76 percent / K2CO3 / tetrakis(triphenylphosphine)palladium(0) / tetrahydrofuran / 18 h / Heating 2: 99 percent / H2 / Pd/C / tetrahydrofuran / 18 h View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: fuming HNO3 / acetic acid 2: SnCl2, aq. HCl View Scheme | |
Multi-step reaction with 2 steps 1: HNO3 / acetic acid 2: H2, Py / Raney-Ni / 100 °C / 60800 - 65360 Torr View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: N-Bromosuccinimide; sulfuric acid / 60 °C 2: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / tetrahydrofuran / 48 h / Reflux; Inert atmosphere 3: palladium 10% on activated carbon; hydrazine / ethanol / 6 h / Inert atmosphere; Reflux View Scheme |
3,5-dinitrobromobenzene
4,4''-diamino-p-terphenyl
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / tetrahydrofuran / 48 h / Reflux; Inert atmosphere 2: palladium 10% on activated carbon; hydrazine / ethanol / 6 h / Inert atmosphere; Reflux View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: triethylamine; bis-triphenylphosphine-palladium(II) chloride / 1,4-dioxane / 12 h / 120 °C / Schlenk technique; Inert atmosphere 2: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / water; toluene / 24 h / Schlenk technique; Inert atmosphere; Heating View Scheme | |
Multi-step reaction with 2 steps 1: bis-triphenylphosphine-palladium(II) chloride; triethylamine / 1,4-dioxane / 12 h / 120 °C / Schlenk technique; Inert atmosphere 2: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / water; toluene / 24 h / Schlenk technique; Inert atmosphere; Heating View Scheme |
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: bis(dibenzylideneacetone)-palladium(0); tricyclohexylphosphine; potassium acetate / 1,4-dioxane / Heating 2: potassium carbonate; tetrakis(triphenylphosphine) palladium(0) / tetrahydrofuran; water / Heating 3: hydrazine; 3% Pd/C / ethanol / Heating View Scheme | |
Multi-step reaction with 3 steps 1.1: potassium acetate; bis(dibenzylideneacetone)-palladium(0); tricyclohexylphosphine / 1,4-dioxane / 4.33 h / 110 °C 2.1: potassium carbonate / tetrahydrofuran; water / 0.33 h / 100 °C 2.2: 5 h / 100 °C 3.1: hydrazine; 3% Pd/C / ethanol / 12 h / 100 °C View Scheme |
benzene-1,4-diboronic acid bispinacol ester
4,4''-diamino-p-terphenyl
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: potassium carbonate / tetrahydrofuran; water / 0.33 h / 100 °C 1.2: 5 h / 100 °C 2.1: hydrazine; 3% Pd/C / ethanol / 12 h / 100 °C View Scheme |
4,4''-diamino-p-terphenyl
2-hydroxynaphthalene-1-carbaldehyde
1,1'-[(4,4''-p-terphenylene)bis(iminomethyl)]bis(2-naphthol)
Conditions | Yield |
---|---|
With formic acid In methanol; dichloromethane Reflux; | 98% |
Conditions | Yield |
---|---|
With tri-tert-butyl phosphine; potassium tert-butylate; bis(dibenzylideneacetone)-palladium(0) In toluene at 80℃; for 69.5h; Inert atmosphere; | 97% |
3,5-di-tert-butyl-2-hydroxybenzaldehyde
4,4''-diamino-p-terphenyl
Conditions | Yield |
---|---|
With formic acid In methanol; dichloromethane Reflux; | 93% |
3-tert-butyl-2-hydroxybenzaldehyde
4,4''-diamino-p-terphenyl
Conditions | Yield |
---|---|
With formic acid In methanol; dichloromethane Reflux; | 91% |
4,4''-diamino-p-terphenyl
Ethoxycarbonyl isothiocyanate
4,4''-bis(N'-ethoxycarbonylthiourea)-[1,1';4',1'']terphenyl
Conditions | Yield |
---|---|
In dichloromethane at 20℃; for 24h; | 89% |
4,4''-diamino-p-terphenyl
4,4''-bis(N'-ethoxycarbonylthiourea)-[1,1';4',1'']terphenyl
Conditions | Yield |
---|---|
With Ethoxycarbonyl isothiocyanate In dichloromethane at 20℃; for 24h; | 89% |
Conditions | Yield |
---|---|
With formic acid In methanol; dichloromethane Reflux; | 84% |
Conditions | Yield |
---|---|
With tris-(dibenzylideneacetone)dipalladium(0); tri-tert-butyl phosphine; sodium t-butanolate In toluene for 5h; Inert atmosphere; Reflux; | 83.6% |
4,4''-diamino-p-terphenyl
N,N'-bis-Boc-S-methyl-isothiourea
Conditions | Yield |
---|---|
With triethylamine; mercury dichloride In N,N-dimethyl-formamide at 20℃; for 24h; | 79% |
With triethylamine; mercury dichloride In N,N-dimethyl-formamide at 20℃; for 24h; | 79% |
4,4''-diamino-p-terphenyl
Conditions | Yield |
---|---|
Stage #1: 4,4''-diamino-p-terphenyl With hydrogenchloride; sodium nitrite In water at 0℃; for 0.5h; Cooling with ice; Stage #2: With sodium azide In water at 0℃; for 2h; Cooling with ice; | 78.1% |
Stage #1: 4,4''-diamino-p-terphenyl With sodium nitrite In water for 2h; Stage #2: With sodium azide In water for 2h; | 45.6% |
4,4''-diamino-p-terphenyl
Conditions | Yield |
---|---|
With tetra-(n-butyl)ammonium iodide; triethylamine In tetrahydrofuran at 20℃; for 6h; | 75% |
4,4''-diamino-p-terphenyl
ethyl iodide
N,N-dimethyl-formamide
p,p"-bis-diethylamino-p-terphenyl
Conditions | Yield |
---|---|
With calcium carbonate In N-methyl-acetamide; water | 70% |
Conditions | Yield |
---|---|
With propionic acid at 150℃; for 10h; | 70% |
4,4''-diamino-p-terphenyl
Conditions | Yield |
---|---|
With potassium dichromate; perchloric acid; acetic acid In water | 55.5% |
4,4''-diamino-p-terphenyl
Conditions | Yield |
---|---|
In tetrahydrofuran Schlenk techniques used, 7c (0.32 mmol) added to THF soln. of 5a (0.16 mmol) in THF under Ar, stirred for 2 h at room temp.; solvent removed under vac., chromd. (SiO2, hexane/AcOEt) under Ar pressure; elem. anal.; | 47% |
Conditions | Yield |
---|---|
With sodium t-butanolate; bis-triphenylphosphine-palladium(II) chloride In xylene at 130℃; for 24h; | 41% |
2'-bromo(spiro[cyclohexane-1,9'[9H]fluoren])
4,4''-diamino-p-terphenyl
Conditions | Yield |
---|---|
With sodium t-butanolate; bis-triphenylphosphine-palladium(II) chloride In xylene at 130℃; for 24h; | 36% |
Conditions | Yield |
---|---|
In N,N-dimethyl-formamide tren (2 mmol) added to soln. of Cu(ClO4)2*6H2O (2 mmol) under stirring, NH2(C6H4)3NH2 (1 mmol) soln. added dropwise; soln. filtered off, Et2O slow diffused into soln., crystd. for one week at room temp., collected, air dried; elem. anal.; | 31% |
Conditions | Yield |
---|---|
In various solvent(s) for 3h; Condensation; Heating; | 20% |
Conditions | Yield |
---|---|
Stage #1: 4,4''-diamino-p-terphenyl; α-chlorobenzaldehyde phenylhydrazone With triethylamine In tetrahydrofuran for 24h; Reflux; Stage #2: With palladium 10% on activated carbon; 1,8-diazabicyclo[5.4.0]undec-7-ene In dichloromethane for 24h; | 14% |
4,4''-diamino-p-terphenyl
Conditions | Yield |
---|---|
With Na In toluene soln. of Mo-complex and ligand in toluene contg. Na was heated under reflux, stirred for 18 h under N2, cooled; filtered, solvent was removed in vacuo, sepd. by column chromy. with CH2Cl2/hexane; elem. anal.; | 2% |
Conditions | Yield |
---|---|
With acetic acid In toluene for 48h; Knorr Pyrazole Synthesis; Inert atmosphere; Reflux; | |
In acetic acid; toluene at 130℃; for 72h; Inert atmosphere; | 0.24% |
Conditions | Yield |
---|---|
With hydrogenchloride Diazotization.Einleiten von Wasserdampf; |
4,4''-diamino-p-terphenyl
phenyl Salicylate
N,N'-p-terphenyl-4,4''-diyl-bis-salicylamide
Conditions | Yield |
---|---|
With 1-Methylnaphthalene |
4,4''-diamino-p-terphenyl
2-Methoxybenzoyl chloride
4,4''-Bis-(2-methoxy-benzoylamino)-p-terphenyl
Conditions | Yield |
---|---|
With pyridine |
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