Products

Refine

Country

Business Type

Certificate

Display

Dayang Chem (Hangzhou) Co.,Ltd.

Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities

4-Aminophenylboronic acid pinacol ester Manufacturer/High quality/Best price/In stock

Cas:214360-73-3

Min.Order:1 Kilogram

FOB Price: $3.0

Type:Lab/Research institutions

inquiry

Simagchem Corporation

Welcome to Simagchem, your partner in China as a premier supply of bulk specialty chemicals for industry and life science. We introduce experienced quality product and exceptional JIT service with instant market intelligence in China to benefit our

High quality 4-Aminophenylboronic Acid Pinacol Ester supplier in China

Cas:214360-73-3

Min.Order:1 Kilogram

Negotiable

Type:Manufacturers

inquiry

Henan Allgreen Chemical Co.,Ltd

high quality Appearance:Yellow to Brown solid Storage:Sealed, dry, microtherm , avoid light and smell Package:According to the demand of customer Application:Pharmaceutical intermediates Transportation:by air or by sea Port:shanghai

4-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)aniline(4-Aminophenylboronic acid pinacol ester)

Cas:214360-73-3

Min.Order:1 Kilogram

Negotiable

Type:Manufacturers

inquiry

Xi'an Xszo Chem Co., Ltd.

1. Factory price and high quality must be guaranteed, base on 8 years of production and R&D experience2. Free samples will be provided,ensure specifications and quality are right for customer3. Customers will receive the most professional technical s

Factory Price OLED 99% 214360-73-3 4-Aminophenylboronic acid pinacol ester Manufacturer

Cas:214360-73-3

Min.Order:1 Gram

FOB Price: $0.1

Type:Manufacturers

inquiry

Chemwill Asia Co., Ltd.

Our main production base is located in Xuzhou industry park. We are certified both to the ISO 9001 and ISO 14001 Standards, have a safety management system in place.Our R&D team masters core technology for process-design of target building block

4-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)-aniline

Cas:214360-73-3

Min.Order:5 Kiloliter

FOB Price: $1.2 / 5.0

Type:Manufacturers

inquiry

Henan Tianfu Chemical Co., Ltd.

Best service ,quality & low price 4-Aminophenylboronic acid pinacol ester Basic information Product Name: 4-Aminophenylboronic acid pinacol ester Synonyms: 2-(4-AMINOPHENYL)-4,

CAS:214360-73-3 4-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)aniline(4-Aminophenylboronic acid pinacol ester)

Cas:214360-73-3

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Jinan Finer Chemical Co., Ltd

Product Description Product website: http://www.finerchem.com/pro01en/id/125.html Product Name 4-Aminophenylboronic acid pinacol ester CAS No. 214360-73-

4-Aminophenylboronic acid pinacol ester

Cas:214360-73-3

Min.Order:1 Gram

FOB Price: $62.0

Type:Lab/Research institutions

inquiry

Hebei Nengqian Chemical Import and Export Co., LTD

With our good experience, we offer detailed technical support and advice to assist customers. We communicate closely with customers to establish their quality requirements. Consistent Quality Our plant has strict quality control in each manufacturin

4-Aminophenylboronic Acid Pinacol Ester CAS 214360-73-3

Cas:214360-73-3

Min.Order:1 Kilogram

FOB Price: $1.0 / 10.0

Type:Trading Company

inquiry

Zhuozhou Wenxi import and Export Co., Ltd

WITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et

Top Purity CAS 214360-73-3 with fast shipping

Cas:214360-73-3

Min.Order:1 Kilogram

FOB Price: $139.0 / 210.0

Type:Trading Company

inquiry

Henan Sinotech Import&Export Corporation

Product name 4-Aminophenylboronic acid pinacol ester Cas number 214360-73-3 Molecular formula C12H18BNO2 Molecular weight 219.09

4-Aminophenylboronic acid pinacol ester CAS: 214360-73-3

Cas:214360-73-3

Min.Order:5 Metric Ton

FOB Price: $1.0 / 2.0

Type:Other

inquiry

Shanghai Upbio Tech Co.,Ltd

1.No Less 8 years exporting experience. Clients can 100% received goods 2.Lower Price with higher quality 3,Free sample 4,We are sincerely responsible for the "product quality" and "After Service" Upbio is Specialized

Benzenamine,4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)- 214360-73-3

Cas:214360-73-3

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Baoji Guokang Healthchem co.,ltd

Our company has been in existence for 10 years since its establishment. We have our own unique team. The company integrates independent research and development, production and sales. We have established famous brands at home and abroad. At prese

4-Aminophenylboronic acid pinacol ester

Cas:214360-73-3

Min.Order:1 Kilogram

FOB Price: $76.0 / 85.0

Type:Trading Company

inquiry

Qingdao Beluga Import and Export Co., LTD

4-Aminophenylboronic acid pinacol ester CAS:214360-73-3 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high

4-Aminophenylboronic acid pinacol ester CAS:214360-73-3

Cas:214360-73-3

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

Shandong Hanjiang Chemical Co., Ltd.

Hello, dear friend! I'm Hansen and Allen from China. Welcome to my lookchem mall! The following is a brief introduction of our company's products and services. If you are interested in our products, please contact us by emai

Benzenamine,4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-

Cas:214360-73-3

Min.Order:1 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Henan Wentao Chemical Product Co., Ltd.

Henan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod

CAS NO.:214360-73-3

Cas:214360-73-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Xiamen Hisunny Chemical Co.,Ltd

Best quality & Attractive price & Professional service; Trial & Pilot & Commercial Hisunny Chemical is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality intermediates, specia

4-Aminophenylboronic Acid Pinacol Ester

Cas:214360-73-3

Min.Order:0

Negotiable

Type:Manufacturers

inquiry

Triumph International Development Limilted

Appearance:white or light yellow crystalline powder Storage:Store in a cool,dry place and keep away from direct strong light Package:As customer request Application:Used for research and industrial manufacture. Transportation:By Se

4-Aminophenylboronic acid pinacol ester

Cas:214360-73-3

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Wuhan Han Sheng New Material Technology Co.,Ltd

Our advantage: high quality with competitive price High quality standard: BP/USP/EP Enterprise standard All purity customized Fast and safe delivery We have reliable forwarder who can help us deliver our goods more fast and safe. We have s

4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzenamine

Cas:214360-73-3

Min.Order:10 Kilogram

Negotiable

Type:Trading Company

inquiry

SHANGHAI T&W PHARMACEUTICAL CO., LTD.

A substitute for perfluorooctanoic acid, mainly used as a surfactant, dispersant, additive, etc Appearance:White solid or Colorless liquid Purity:99.3 % We will ship the goods in a timely manner as required We can provide relevant documents acc

4-Aminophenylboronic acid pinacol ester

Cas:214360-73-3

Min.Order:4 Kilogram

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou Keyingchem Co.,Ltd

Hangzhou KeyingChem Co., Ltd. exported this product to many countries and regions at best price. If you are looking for the material’s manufacturer or supplier in China, KeyingChem is your best choice. Pls contact with us freely for getting det

4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzenamine

Cas:214360-73-3

Min.Order:0 Metric Ton

Negotiable

Type:Lab/Research institutions

inquiry

Hangzhou J&H Chemical Co., Ltd.

J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia

4-(4,4 ,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzenamine

Cas:214360-73-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Afine Chemicals Limited

Our Services 1. New Molecules R&D 2. Own test center HPLC NMR GC LC-MS 3. API and Intermediates from China reputed manufacturers 4. Documents support COA MOA MSDS DMF open part Our advantages 1. Government awarded company. Top 100 enter

4-AMINOPHENYLBORONIC ACID PINACOL ESTER

Cas:214360-73-3

Min.Order:0

Negotiable

Type:Lab/Research institutions

inquiry

Shanghai Massive Chemical Technology Co., Ltd.

Massive Chemical is certified with ISO9001 and ISO14001 manufacturer for this product. We will offer all documents as requirement for the materials which includes, Certificate of Analysis, Material Safety Data Sheet, and Method of Analysis and

4-Aminophenylboronic acid pinacol ester/High quality/Best price

Cas:214360-73-3

Min.Order:1 Gram

FOB Price: $1.0

Type:Lab/Research institutions

inquiry

Zibo Hangyu Biotechnology Development Co., Ltd

Zibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi

High quality 4-Aminophenylboronic Acid Pinacol Ester

Cas:214360-73-3

Min.Order:10 Gram

FOB Price: $100.0

Type:Lab/Research institutions

inquiry

HANGZHOU YUNUO CHEMICAL CO.,LTD

Superior quality, moderate price & quick delivery. Appearance:white to brown solid Storage:Low temperature dry and shady Package:1kg/bag,or as your request Application:For medicine , pesticide intermediates Transportation:as your request Po

4-Aminophenylboronic acid pinacol ester

Cas:214360-73-3

Min.Order:1 Gram

Negotiable

Type:Trading Company

inquiry

AllyChem Co., Ltd., Dalian, China(BBChem)

AllyChem Co., Ltd., Dalian, China was founded in 2004 with a registered capital of 66 million yuan and is located in dagushan peninsula chemical industrial park, jinzhou new district, dalian.It is a pharmaceutical intermediates based on the research

4-Aminophenylboronic Acid Pinacol Ester AC081010 manufacturer in China

Cas:214360-73-3

Min.Order:1 Kilogram

Negotiable

Type:Trading Company

inquiry

Xiamen Jenny Chemical Technology Co., Ltd.

GMP standard, high purity, competitive price, in stock 1. Quick Response: within 6 hours after receiving your email. 2. Quality Guarantee: All products are strictly tested by our QC, confirmed by QA, and approved by a third-party lab in China, USA,

4-Aminophenylboronicacidpinacolester

Cas:214360-73-3

Min.Order:1 Milligram

Negotiable

Type:Trading Company

inquiry

Shanghai Minstar Chemical Co., Ltd

4-Aminophenylboronic acid pinacol ester Basic information Product Name: 4-Aminophenylboronic acid pinacol ester Synonyms: 2-(4-AMINOPHENYL)-4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLANE;4-Aminophenylboronic acid pinacol ester 97%;4-Aminophenylboroni

4-Aminophenylboronic acid pinacol ester

Cas:214360-73-3

Min.Order:1 Gram

Negotiable

Type:Lab/Research institutions

inquiry

EAST CHEMSOURCES LIMITED

factory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B

4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzenamine

Cas:214360-73-3

Min.Order:1 Kilogram

FOB Price: $18.0 / 20.0

Type:Trading Company

inquiry

HUNAN CHEMAPI BIOLOGICAL TECHNOLOGY CO.,LTD.

Hunan Kaimir Biotechnology Co., Ltd. is a professional technology company specializing in the research and production of raw materials and intermediates. In 2017, it was recognized as a high-tech enterprise and a small technological innovation giant

4-Aminophenylboronic acid pinacol ester

Cas:214360-73-3

Min.Order:1 Metric Ton

Negotiable

Type:Other

inquiry

Synthetic route

4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)nitrobenzene
171364-83-3

4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)nitrobenzene

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline
214360-73-3

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline

Conditions
ConditionsYield
With C36H56Cl3CrN2O; magnesium; 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane In tetrahydrofuran at 60℃; for 24h; Inert atmosphere;99%
With 5%-palladium/activated carbon; hydrogen In methanol at 20℃; under 760.051 Torr; for 4h;98%
With palladium 10% on activated carbon; hydrogen In methanol at 20℃; for 4h;97%
4-bromo-aniline
106-40-1

4-bromo-aniline

bis(pinacol)diborane
73183-34-3

bis(pinacol)diborane

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline
214360-73-3

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline

Conditions
ConditionsYield
With 10H-phenothiazine; caesium carbonate In acetonitrile for 48h; Irradiation; Sealed tube; Inert atmosphere;97%
With potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride In dimethyl sulfoxide at 150℃; for 0.366667h; microwave irradiation;85%
With bis(tri-t-butylphosphine)palladium(0); potassium acetate In water at 20℃; for 24h; Reagent/catalyst; Miyaura Borylation Reaction; Inert atmosphere;85%
bis(pinacol)diborane
73183-34-3

bis(pinacol)diborane

p-aminoiodobenzene
540-37-4

p-aminoiodobenzene

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline
214360-73-3

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline

Conditions
ConditionsYield
With caesium carbonate In methanol for 60h; Reflux; Inert atmosphere;96%
With pyridine; C50H44CuN4OP2(1+)*F6P(1-); N-ethyl-N,N-diisopropylamine In water; acetonitrile at 20℃; for 12h; Inert atmosphere; Irradiation;87%
With 10H-phenothiazine; caesium carbonate In acetonitrile for 48h; Irradiation; Sealed tube; Inert atmosphere;80%
C18H34BNO2Si2

C18H34BNO2Si2

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline
214360-73-3

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline

Conditions
ConditionsYield
With hydrogenchloride; water In methanol at 20℃; for 1h;91%
4-bromo-aniline
106-40-1

4-bromo-aniline

4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane
25015-63-8

4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline
214360-73-3

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline

Conditions
ConditionsYield
With bis-triphenylphosphine-palladium(II) chloride; triethylamine In 1,4-dioxane at 120℃; for 12h; Time; Schlenk technique; Inert atmosphere;90%
With bis-triphenylphosphine-palladium(II) chloride; triethylamine In 1,4-dioxane at 120℃; for 12h; Schlenk technique; Inert atmosphere;90%
With bis-triphenylphosphine-palladium(II) chloride; triethylamine In 1,4-dioxane at 120℃; for 12h; Inert atmosphere;89%
2,2,2-trifluoro-N-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]acetamide
864754-08-5

2,2,2-trifluoro-N-[4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]acetamide

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline
214360-73-3

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline

Conditions
ConditionsYield
87.1%
p-aminoiodobenzene
540-37-4

p-aminoiodobenzene

4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane
25015-63-8

4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline
214360-73-3

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline

Conditions
ConditionsYield
With dichlorobis(chlorodi-tert-butylphosphine) palladium(II); triethylamine In toluene for 2h; Inert atmosphere; Reflux;83%
With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; triethylamine In 1,4-dioxane at 90℃; for 1.5h; Inert atmosphere;80%
With triethylamine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride In 1,4-dioxane at 80℃; for 8h;75 %Chromat.
2-(4-iodophenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
73852-88-7

2-(4-iodophenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline
214360-73-3

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline

Conditions
ConditionsYield
With bis(triphenylphosphine)nickel(II) chloride; lithium hexamethyldisilazane In toluene at 100℃; for 2h; Glovebox; Sealed tube;80%
Multi-step reaction with 2 steps
1: chlorotris(triphenylphosphine)cobalt(I); bis[2-(diphenylphosphino)phenyl] ether / toluene / 12 h / 100 °C
2: hydrogenchloride; water / methanol / 1 h / 20 °C
View Scheme
Triisopropyl borate
5419-55-6

Triisopropyl borate

2-(4-bromophenyl)-1,1,1,3,3,3-hexamethyldisilazane
5089-33-8

2-(4-bromophenyl)-1,1,1,3,3,3-hexamethyldisilazane

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline
214360-73-3

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline

Conditions
ConditionsYield
Stage #1: 2-(4-bromophenyl)-1,1,1,3,3,3-hexamethyldisilazane With n-butyllithium In tetrahydrofuran at -78℃; for 1h; Inert atmosphere;
Stage #2: Triisopropyl borate In tetrahydrofuran at -78 - 25℃; for 4.5h; Inert atmosphere;
Stage #3: With 2,3-dimethyl-2,3-butane diol; acetic acid In tetrahydrofuran at 20℃; for 0.75h; pH=5; Inert atmosphere;
79%
(4-aminophenyl)boronic acid hydrochloride

(4-aminophenyl)boronic acid hydrochloride

2,3-dimethyl-2,3-butane diol
76-09-5

2,3-dimethyl-2,3-butane diol

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline
214360-73-3

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline

Conditions
ConditionsYield
With magnesium sulfate In tetrahydrofuran at 20℃; for 5h;76%
2,3-dimethyl-2,3-butane diol
76-09-5

2,3-dimethyl-2,3-butane diol

4-bromo-N-(diphenylmethylidene)aniline
53847-33-9

4-bromo-N-(diphenylmethylidene)aniline

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline
214360-73-3

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline

Conditions
ConditionsYield
Stage #1: 4-bromo-N-(diphenylmethylidene)aniline With C12H27Mg(1-)*Li(1+) In tetrahydrofuran at -20℃; for 1h; Inert atmosphere; Green chemistry; Large scale;
Stage #2: With Trimethyl borate In tetrahydrofuran at -20 - 25℃; for 2.5h; Inert atmosphere; Green chemistry; Large scale;
Stage #3: 2,3-dimethyl-2,3-butane diol Reagent/catalyst; Temperature; Green chemistry; Large scale; Further stages;
70%
4-fluoroaniline
371-40-4

4-fluoroaniline

bis(pinacol)diborane
73183-34-3

bis(pinacol)diborane

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline
214360-73-3

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline

Conditions
ConditionsYield
With tris-(dibenzylideneacetone)dipalladium(0); lithium hexamethyldisilazane In toluene at 80℃; for 12h; Inert atmosphere; Schlenk technique;68%
With tetramethylammonium fluoride; 2-mercaptopyridine sodium salt In acetonitrile at 30 - 35℃; for 24h; Irradiation; Inert atmosphere;52%
1,4-phenylenediamine
106-50-3

1,4-phenylenediamine

bis(pinacol)diborane
73183-34-3

bis(pinacol)diborane

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline
214360-73-3

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline

Conditions
ConditionsYield
With tert.-butylnitrite In acetonitrile at 80℃; for 2h;62%
With tert.-butylnitrite In acetonitrile at 80℃; for 2h;62%
With tert.-butylnitrite In acetonitrile at 80℃; for 2h;62%
With tert.-butylnitrite In acetonitrile at 80℃; for 2h;62%
Stage #1: 1,4-phenylenediamine With hydrogenchloride; methanol; sodium nitrite In water at 0 - 5℃; for 0.5h; Sandmeyer Reaction; Green chemistry;
Stage #2: bis(pinacol)diborane In water at 20℃; for 1h; Sandmeyer Reaction; Green chemistry;
53%
4-amino-N,N,N-trimethylbenzenaminium trifluoromethanesulfonate

4-amino-N,N,N-trimethylbenzenaminium trifluoromethanesulfonate

bis(pinacol)diborane
73183-34-3

bis(pinacol)diborane

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline
214360-73-3

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline

Conditions
ConditionsYield
With bis(1,5-cyclooctadiene)nickel(0); potassium tert-butylate; 1,3-dicyclohexyl-1H-imidazol-3-ium chloride In 2-ethoxy-ethanol; toluene at 50℃; for 24h; Schlenk technique; Inert atmosphere;62%
4-chloro-aniline
106-47-8

4-chloro-aniline

bis(pinacol)diborane
73183-34-3

bis(pinacol)diborane

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline
214360-73-3

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline

Conditions
ConditionsYield
With Co(1,3-bis(2,4,6-trimethylphenyl)imidazol-2-ylidene)2Cl2; potassium methanolate In tert-butyl methyl ether at 50℃; for 8h;60%
With potassium acetate In isopropyl alcohol at 82℃; for 2h; Suzuki-Miyaura Coupling;75 %Chromat.
2,3-dimethyl-2,3-butane diol
76-09-5

2,3-dimethyl-2,3-butane diol

Triisopropyl borate
5419-55-6

Triisopropyl borate

(4-(bis(trimethylsilyl)amino)phenyl)magnesium bromide
756822-47-6

(4-(bis(trimethylsilyl)amino)phenyl)magnesium bromide

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline
214360-73-3

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline

Conditions
ConditionsYield
Stage #1: Triisopropyl borate; (4-(bis(trimethylsilyl)amino)phenyl)magnesium bromide In tetrahydrofuran at -70 - -60℃; for 5h; Inert atmosphere;
Stage #2: With tetrabutyl ammonium fluoride In tetrahydrofuran at 20℃; for 2h;
Stage #3: 2,3-dimethyl-2,3-butane diol In tetrahydrofuran at 20℃;
59%
6-methyl-1-oxo-2-[4-(4,4,5,5-tetramethyl[1,3,2]dioxaborolan-2-yl)phenyl]-1,2-dihydrobenzo[b][1,6]naphthyridine-4-carboxylic acid
627093-70-3

6-methyl-1-oxo-2-[4-(4,4,5,5-tetramethyl[1,3,2]dioxaborolan-2-yl)phenyl]-1,2-dihydrobenzo[b][1,6]naphthyridine-4-carboxylic acid

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline
214360-73-3

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline

Conditions
ConditionsYield
With triethylamine In DMF (N,N-dimethyl-formamide); toluene Reduced pressure;45%
2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
61676-62-8

2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

4-bromo-aniline
106-40-1

4-bromo-aniline

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline
214360-73-3

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline

Conditions
ConditionsYield
Stage #1: 4-bromo-aniline With n-butyllithium In tetrahydrofuran at -78℃; for 1h;
Stage #2: 2-Isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane In tetrahydrofuran at 20℃; for 24h;
42.2%
4-Amino-thiobenzoesaeure-S-ethylester
102879-36-7

4-Amino-thiobenzoesaeure-S-ethylester

bis(pinacol)diborane
73183-34-3

bis(pinacol)diborane

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline
214360-73-3

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline

Conditions
ConditionsYield
With [Rh(OH)(cod)]2; tributylphosphine; potassium acetate at 80℃; for 24h; Inert atmosphere; Glovebox;32.4%
4-bromo-aniline
106-40-1

4-bromo-aniline

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline
214360-73-3

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: n-butyllithium / tetrahydrofuran; hexane / 2.5 h / 0 °C / Inert atmosphere
1.2: 20 °C / Inert atmosphere
2.1: n-butyllithium / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere
2.2: 4.5 h / -78 - 25 °C / Inert atmosphere
2.3: 0.75 h / 20 °C / pH 5 / Inert atmosphere
View Scheme
Multi-step reaction with 3 steps
1.1: triethylamine / tetrahydrofuran / 0 - 60 °C / Inert atmosphere
1.2: -10 - 0 °C
2.1: magnesium; iodine / tetrahydrofuran / 2 h / 50 °C / Inert atmosphere; Reflux
3.1: tetrahydrofuran / 5 h / -70 - -60 °C / Inert atmosphere
3.2: 2 h / 20 °C
3.3: 20 °C
View Scheme
aniline
62-53-3

aniline

4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane
25015-63-8

4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

A

2-anilineboronic acid pinacol ester
191171-55-8

2-anilineboronic acid pinacol ester

B

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline
214360-73-3

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline

C

3-aminophenylboronic acid pinacolate
210907-84-9

3-aminophenylboronic acid pinacolate

Conditions
ConditionsYield
With (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; 3,4,7,8-Tetramethyl-o-phenanthrolin; 1,2,3,4,5,6,7,8,9,10,11,12-dodecahydrotriphenylene In tetrahydrofuran at 80℃; for 16h; Inert atmosphere; Glovebox; regioselective reaction;
4-nitro-aniline
100-01-6

4-nitro-aniline

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline
214360-73-3

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 2-(4-biphenylyl)-5-phenyloxazole; tert.-butylnitrite / acetonitrile / 4 h / 20 °C
2: 5%-palladium/activated carbon; hydrogen / methanol / 4 h / 20 °C / 760.05 Torr
View Scheme
bis(pinacol)diborane
73183-34-3

bis(pinacol)diborane

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline
214360-73-3

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 2-(4-biphenylyl)-5-phenyloxazole; tert.-butylnitrite / acetonitrile / 4 h / 20 °C
2: 5%-palladium/activated carbon; hydrogen / methanol / 4 h / 20 °C / 760.05 Torr
View Scheme
(4-tert-butoxycarbonylaminophenyl)boronic acid pinacol ester
330793-01-6

(4-tert-butoxycarbonylaminophenyl)boronic acid pinacol ester

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline
214360-73-3

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline

Conditions
ConditionsYield
With hydrogenchloride In ethyl acetate at 20℃; for 4h;
2,3-dimethyl-2,3-butane diol
76-09-5

2,3-dimethyl-2,3-butane diol

(4-aminophenyl)boronic acid
89415-43-0

(4-aminophenyl)boronic acid

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline
214360-73-3

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline

Conditions
ConditionsYield
With magnesium sulfate In tetrahydrofuran at 20℃; for 5h;
1,4-phenylenediamine
106-50-3

1,4-phenylenediamine

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline
214360-73-3

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: formic acid; sodium cyanoborohydride / methanol / 16 h / 0 - 20 °C / pH 3 - 4 / Inert atmosphere
1.2: 0 °C / Inert atmosphere
2.1: bis(1,5-cyclooctadiene)nickel(0); 1,3-dicyclohexyl-1H-imidazol-3-ium chloride; potassium tert-butylate / toluene; 2-ethoxy-ethanol / 24 h / 50 °C / Schlenk technique; Inert atmosphere
View Scheme
S-(p-nitrobenzoyl)mercaptoethane
24524-95-6

S-(p-nitrobenzoyl)mercaptoethane

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline
214360-73-3

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: tin(II) chloride dihdyrate / ethyl acetate / 4 h / Inert atmosphere; Reflux
2: [Rh(OH)(cod)]2; tributylphosphine; potassium acetate / 24 h / 80 °C / Inert atmosphere; Glovebox
View Scheme
acetic anhydride
108-24-7

acetic anhydride

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline
214360-73-3

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline

N-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)acetamide
214360-60-8

N-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)acetamide

Conditions
ConditionsYield
at 20℃; for 1h;100%
In dichloromethane at 20℃; for 10h;87%
for 1h;
1-bromo-4-(2,2,2-trifluoroethyl)benzene
155820-88-5

1-bromo-4-(2,2,2-trifluoroethyl)benzene

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline
214360-73-3

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline

4-[4'-(2,2,2-trifluoroethyl)-4-biphenylyl]amine

4-[4'-(2,2,2-trifluoroethyl)-4-biphenylyl]amine

Conditions
ConditionsYield
With potassium carbonate; tetrakis(triphenylphosphine) palladium(0) In N,N-dimethyl-formamide at 100℃; for 17h; Suzuki coupling;100%
dichlorobenzenesulfonyl chloride
82417-45-6

dichlorobenzenesulfonyl chloride

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline
214360-73-3

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline

2,3-dichloro-N-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-benzenesulfonamide
912675-28-6

2,3-dichloro-N-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-benzenesulfonamide

Conditions
ConditionsYield
With pyridine at 20℃; for 15h;100%
With pyridine In dichloromethane at 20 - 25℃; for 20h;77%
With pyridine In dichloromethane at 20 - 25℃; for 20h;77%
6-chloro-2-ethoxy-N-methylnicotinamide

6-chloro-2-ethoxy-N-methylnicotinamide

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline
214360-73-3

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline

6-(4-aminophenyl)-2-ethoxy-N-methylnicotinamide
1138322-13-0

6-(4-aminophenyl)-2-ethoxy-N-methylnicotinamide

Conditions
ConditionsYield
With sodium hydrogencarbonate; tetrakis(triphenylphosphine) palladium(0) In 1,2-dimethoxyethane; ethanol; water for 16h; Inert atmosphere; Reflux;100%
7-bromo-2-chloroquinoxaline
89891-65-6

7-bromo-2-chloroquinoxaline

4-(piperazin-1-yl)pyridine
1008-91-9

4-(piperazin-1-yl)pyridine

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline
214360-73-3

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline

4-[3-(4-pyridin-4-yl-piperazin-1-yl)-quinoxalin-6-yl]-phenlamine
1271847-04-1

4-[3-(4-pyridin-4-yl-piperazin-1-yl)-quinoxalin-6-yl]-phenlamine

Conditions
ConditionsYield
Stage #1: 7-bromo-2-chloroquinoxaline; 4-(piperazin-1-yl)pyridine With N-ethyl-N,N-diisopropylamine In 1-methyl-pyrrolidin-2-one at 20 - 160℃; Microwave irradiation;
Stage #2: 4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline With potassium carbonate; tris-(o-tolyl)phosphine; palladium diacetate In 1-methyl-pyrrolidin-2-one at 140℃; Microwave irradiation;
100%
C11H13BrN4O
1252598-01-8

C11H13BrN4O

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline
214360-73-3

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline

C17H19N5O
1252597-72-0

C17H19N5O

Conditions
ConditionsYield
dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2 In dimethyl ether, 1,2- at 130℃; for 1h; Microwave irradiation;100%
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate In 1,2-dimethoxyethane at 130℃; for 1h; Microwave irradiation;100%
methyl chloroformate
79-22-1

methyl chloroformate

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline
214360-73-3

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline

methyl (4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)carbamate
844500-75-0

methyl (4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)carbamate

Conditions
ConditionsYield
With pyridine In 1,2-dichloro-ethane at 0 - 60℃;100%
6-(2-((tert-butyldimethylsilyl)oxy)ethoxy)-2-chloroquinoxaline
1437281-38-3

6-(2-((tert-butyldimethylsilyl)oxy)ethoxy)-2-chloroquinoxaline

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline
214360-73-3

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline

4-(6-(2-((tert-butyldimethylsilyl)oxy)ethoxy)quinoxalin-2-yl)aniline
1437281-40-7

4-(6-(2-((tert-butyldimethylsilyl)oxy)ethoxy)quinoxalin-2-yl)aniline

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In ethanol; water; toluene for 4h; Reflux;100%
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In ethanol; toluene for 4h; Reflux;100%
2-methylphenyl aldehyde
529-20-4

2-methylphenyl aldehyde

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline
214360-73-3

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline

(E)-N-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-1-(o-tolyl)methanimine

(E)-N-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)-1-(o-tolyl)methanimine

Conditions
ConditionsYield
In dichloromethane at 20℃; for 18h; Inert atmosphere; Molecular sieve;100%
glycolic Acid
79-14-1

glycolic Acid

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline
214360-73-3

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline

C14H20BNO4

C14H20BNO4

Conditions
ConditionsYield
With N-ethyl-N,N-diisopropylamine; HATU In N,N-dimethyl-formamide at 20℃; for 36h;100%
2,4,6-trimethylphenyl bromide
576-83-0

2,4,6-trimethylphenyl bromide

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline
214360-73-3

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline

2′,4′,6′-trimethylbiphenyl-4-amine
66818-61-9

2′,4′,6′-trimethylbiphenyl-4-amine

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In 1,4-dioxane for 17h; Suzuki-Miyaura Coupling; Inert atmosphere; Reflux;100%
methyl 4-iodobenzoate
619-44-3

methyl 4-iodobenzoate

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline
214360-73-3

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline

methyl 4’-amino-[1,1’-biphenyl]-4-carboxylate
5730-76-7

methyl 4’-amino-[1,1’-biphenyl]-4-carboxylate

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In 1,4-dioxane; water at 100℃; for 10h;100%
methanesulfonyl chloride
124-63-0

methanesulfonyl chloride

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline
214360-73-3

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline

4-(methylsulfonylamino)phenyl boronic acid
380430-57-9

4-(methylsulfonylamino)phenyl boronic acid

Conditions
ConditionsYield
Stage #1: methanesulfonyl chloride; 4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline With pyridine In dichloromethane at 0 - 20℃;
Stage #2: With water In dichloromethane
99%
1-fluoro-2-isocyanato-4-(trifluoromethyl)benzene
69922-27-6

1-fluoro-2-isocyanato-4-(trifluoromethyl)benzene

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline
214360-73-3

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline

N-(2-fluoro-5-trifluoromethylphenyl)-N'-[4-(4,4,5,5-tetramethyl-[1,3,2]-dioxaborolan-2-yl)phenyl]urea
796967-62-9

N-(2-fluoro-5-trifluoromethylphenyl)-N'-[4-(4,4,5,5-tetramethyl-[1,3,2]-dioxaborolan-2-yl)phenyl]urea

Conditions
ConditionsYield
In 1,2-dichloro-ethane at 20℃;98.8%
In tetrahydrofuran at 20℃; for 0.5h;85%
In dichloromethane at 20℃;
1-isocyanato-3-trifluoromethyl-benzene
329-01-1

1-isocyanato-3-trifluoromethyl-benzene

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline
214360-73-3

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline

N-[4-(4,4,5,5-tetramethyl-[1,3,2]-dioxaborolan-2-yl)phenyl]-N'-(3-trifluoromethylphenyl)urea
796967-48-1

N-[4-(4,4,5,5-tetramethyl-[1,3,2]-dioxaborolan-2-yl)phenyl]-N'-(3-trifluoromethylphenyl)urea

Conditions
ConditionsYield
In tetrahydrofuran at 20℃;98%
In dichloromethane at 20℃;
With triethylamine In dichloromethane at 20℃;
2,5-dichlorobenzenesulphonyl chloride
5402-73-3

2,5-dichlorobenzenesulphonyl chloride

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline
214360-73-3

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline

2,5-dichloro-N-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-benzenesulfonamide
1426214-54-1

2,5-dichloro-N-[4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-phenyl]-benzenesulfonamide

Conditions
ConditionsYield
With pyridine In dichloromethane at 20℃; for 1h;98%
With pyridine In dichloromethane at 20 - 25℃; for 16h;17.9 g
With pyridine In dichloromethane at 20 - 25℃; for 16h;17.9 g
1,3,6,8-tetrabromopyrene
128-63-2

1,3,6,8-tetrabromopyrene

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline
214360-73-3

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline

4,4’,4’’,4’’’-(pyrene-1,3,6,8-tetrayl) tetra aniline
1610471-69-6

4,4’,4’’,4’’’-(pyrene-1,3,6,8-tetrayl) tetra aniline

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In 1,4-dioxane; water at 115℃; Inert atmosphere;98%
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In 1,4-dioxane; water for 72h; Schlenk technique; Inert atmosphere; Reflux;94%
With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In 1,4-dioxane; water at 115℃; for 72h; Inert atmosphere;90%
succinic acid anhydride
108-30-5

succinic acid anhydride

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline
214360-73-3

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline

4-oxo-4-[(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)amino]butanoic acid
480424-98-4

4-oxo-4-[(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)amino]butanoic acid

Conditions
ConditionsYield
In chloroform at 20℃; for 4h;98%
3-oxobenzo[d]isothiazole-2(3H)-carbaldehyde 1,1-dioxide
50978-45-5

3-oxobenzo[d]isothiazole-2(3H)-carbaldehyde 1,1-dioxide

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline
214360-73-3

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline

N-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)formamide

N-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)formamide

Conditions
ConditionsYield
In dichloromethane at 20℃; for 0.166667h; Solvent; Time;98%
5-bromo-2-(2-fluorophenyl)thiazole

5-bromo-2-(2-fluorophenyl)thiazole

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline
214360-73-3

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline

4-[2-(2-fluorophenyl)thiazol-5-yl]phenylamine

4-[2-(2-fluorophenyl)thiazol-5-yl]phenylamine

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); sodium carbonate In 1,4-dioxane at 100℃; for 2h; Inert atmosphere;98%
[5,15-dibromo-10,20-bis(2,6-dioctoxyphenyl)porphinato]zinc(II)

[5,15-dibromo-10,20-bis(2,6-dioctoxyphenyl)porphinato]zinc(II)

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline
214360-73-3

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline

C91H124N6O4Zn

C91H124N6O4Zn

Conditions
ConditionsYield
Stage #1: [5,15-dibromo-10,20-bis(2,6-dioctoxyphenyl)porphinato]zinc(II) With tetrakis(triphenylphosphine) palladium(0) In toluene at 20℃; for 0.5h; Sonogashira Cross-Coupling;
Stage #2: 4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline With sodium carbonate In ethanol; water; toluene at 100℃; for 5h; Sonogashira Cross-Coupling;
97.22%
phenyl isocyanate
103-71-9

phenyl isocyanate

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline
214360-73-3

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline

N-phenyl-N'-[4-(4,4,5,5-tetramethyl-[1,3,2]-dioxaborolan-2-yl)phenyl]urea
819056-67-2

N-phenyl-N'-[4-(4,4,5,5-tetramethyl-[1,3,2]-dioxaborolan-2-yl)phenyl]urea

Conditions
ConditionsYield
In toluene at 50℃; for 16h;97%
With triethylamine In dichloromethane at 20℃;70%
With 4-methyl-morpholine In tetrahydrofuran
5-chloro-3-cyclopropyl-7-morpholin-4-yl-3H-[1,2,3]triazolo[4,5-d]pyrimidine
1173205-24-7

5-chloro-3-cyclopropyl-7-morpholin-4-yl-3H-[1,2,3]triazolo[4,5-d]pyrimidine

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline
214360-73-3

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline

4-(3-cyclopropyl-7-morpholin-4-yl-3H-[1,2,3]triazolo[4,5-d]pyrimidin-5-yl)aniline
1173205-23-6

4-(3-cyclopropyl-7-morpholin-4-yl-3H-[1,2,3]triazolo[4,5-d]pyrimidin-5-yl)aniline

Conditions
ConditionsYield
With tetrakis(triphenylphosphine) palladium(0); sodium carbonate In 1,2-dimethoxyethane; water at 140℃; for 0.75h; Suzuki coupling; Microwave irradiation;97%
2-chloro-7-(2,2-dimethoxyethyl)-4-morpholin-4-yl-7H-pyrrolo[2,3-d]pyrimidine
1202885-77-5

2-chloro-7-(2,2-dimethoxyethyl)-4-morpholin-4-yl-7H-pyrrolo[2,3-d]pyrimidine

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline
214360-73-3

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline

4-[7-(2,2-dimethoxyethyl)-4-morpholin-4-yl-7H-pyrrolo[2,3-d]pyrimidin-2-yl]aniline
1202885-78-6

4-[7-(2,2-dimethoxyethyl)-4-morpholin-4-yl-7H-pyrrolo[2,3-d]pyrimidin-2-yl]aniline

Conditions
ConditionsYield
With sodium carbonate; tetrakis(triphenylphosphine) palladium(0) In 1,2-dimethoxyethane; water at 130℃; for 0.5h; Suzuki Coupling; Microwave irradiation;97%
With tetrakis(triphenylphosphine) palladium(0); sodium carbonate In 1,2-dimethoxyethane; water at 130℃; for 0.5h; Suzuki coupling; Microwave irradiation;97%
4-[1-(benzenesulfonyl)cyclopropyl]-2-chloro-6-[(3S)-3-methylmorpholin-4-yl]pyrimidine
1101819-64-0

4-[1-(benzenesulfonyl)cyclopropyl]-2-chloro-6-[(3S)-3-methylmorpholin-4-yl]pyrimidine

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline
214360-73-3

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline

4-[4-[1-(benzenesulfonyl)cyclopropyl]-6-[(3S)-3-methylmorpholin-4-yl]pyrimidin-2-yl]aniline
1101819-63-9

4-[4-[1-(benzenesulfonyl)cyclopropyl]-6-[(3S)-3-methylmorpholin-4-yl]pyrimidin-2-yl]aniline

Conditions
ConditionsYield
With bis-triphenylphosphine-palladium(II) chloride; sodium carbonate In 1,2-dimethoxyethane; ethanol; water; N,N-dimethyl-formamide at 80 - 95℃; for 5h; Inert atmosphere;97%
3-chloro-5-(3,4-dimethoxyphenyl)pyrazin-2-amine

3-chloro-5-(3,4-dimethoxyphenyl)pyrazin-2-amine

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline
214360-73-3

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline

3-(4-aminophenyl)-5-(3,4-dimethoxyphenyl) pyrazin-2-amine

3-(4-aminophenyl)-5-(3,4-dimethoxyphenyl) pyrazin-2-amine

Conditions
ConditionsYield
With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; caesium carbonate In 1,4-dioxane; water at 100℃; for 4h;96.8%
para-fluorophenyl isocyanate
1195-45-5

para-fluorophenyl isocyanate

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline
214360-73-3

4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline

N-(4-fluorophenyl)-N'-[4-(4,4,5,5-tetramethyl-[1,3,2]-dioxaborolan-2-yl)phenyl]urea
819056-61-6

N-(4-fluorophenyl)-N'-[4-(4,4,5,5-tetramethyl-[1,3,2]-dioxaborolan-2-yl)phenyl]urea

Conditions
ConditionsYield
at 20℃;96%
In dichloromethane at 20℃;
In dichloromethane Alkaline conditions;
In dichloromethane at 0 - 20℃; Alkaline conditions;

Hot Products

Post buying leads

About|Contact|Cas|Product Name|Molecular|Country|Encyclopedia

Message|New Cas|MSDS|Service|Advertisement|CAS DataBase|Article Data|Manufacturers | Chemical Catalog

©2008 LookChem.com,License: ICP

NO.:Zhejiang16009103

complaints:service@lookchem.com Desktop View