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inquiryMethyl 5-chloro-2-methoxybenzoateAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air
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inquiryAppearance & Physical State White to light yellow crystal powder Density 1.259 Boiling Point 235-240ºC Melting Point 150-152ºC Flash P
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inquiryMethyl 5-chloro-2-methoxybenzoateAppearance:detailed see specifications Storage:Keep away of light, cool place Package:25kg/drum;200kg/drum Application:Used in Synthesis, Pharmaceuticals and other fields Transportation:Sea/air/courier
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inquiry2-methoxybenzoic acid methyl ester
methyl 5-chloro-2-methoxybenzoate
Conditions | Yield |
---|---|
With N-chloro-succinimide; silver hexafluoroantimonate; 1-methylthiotriptycene In 1,2-dichloro-ethane at 20℃; for 2h; Inert atmosphere; Schlenk technique; | 91% |
With sodium persulfate; tris(bipyridine)ruthenium(II) dichloride hexahydrate; sodium chloride In water; acetonitrile at 25℃; for 15h; Irradiation; | 73 %Spectr. |
5-chloro-2-hydroxybenzoic acid
dimethyl sulfate
methyl 5-chloro-2-methoxybenzoate
Conditions | Yield |
---|---|
With sodium hydroxide; tetra-(n-butyl)ammonium iodide In dichloromethane; water at 20℃; for 4h; | 46% |
With sodium hydroxide | |
With sodium hydroxide; tetrabutylammomium bromide In dichloromethane; water for 4h; Ambient temperature; | |
Stage #1: 5-chloro-2-hydroxybenzoic acid With sodium hydroxide In water at 37℃; for 0.5h; pH=10; Stage #2: dimethyl sulfate In water for 3h; pH=10; |
methanol
5-chloro-2-methoxybenzoic acid
methyl 5-chloro-2-methoxybenzoate
Conditions | Yield |
---|---|
With hydrogenchloride |
2-methoxy-5-chlorobenzonitrile
methyl 5-chloro-2-methoxybenzoate
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: aqueous-alcoholic KOH-solution 2: hydrogen chloride View Scheme |
5-chloro-2-hydroxybenzoic acid
methyl 5-chloro-2-methoxybenzoate
Conditions | Yield |
---|---|
With potassium carbonate; dimethyl sulfate In acetone | 23.10 g (99%) |
methyl 5-chloro-2-methoxybenzoate
Conditions | Yield |
---|---|
With thionyl chloride In N-methyl-acetamide; benzene |
5-chloro-2-hydroxybenzoic acid
methyl iodide
methyl 5-chloro-2-methoxybenzoate
Conditions | Yield |
---|---|
With potassium carbonate In acetone at 20℃; Reflux; Darkness; |
4-chloromethoxybenzene
methyl 5-chloro-2-methoxybenzoate
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: triisobutylaluminum; 2,2,6,6-tetramethyl-piperidine; n-butyllithium / tetrahydrofuran; hexane / 3 h / -78 - 20 °C 1.2: 3 h / -78 - 20 °C / 760.05 Torr 2.1: toluene; methanol / Inert atmosphere View Scheme |
5-chloro-2-methoxybenzoic acid
diazomethyl-trimethyl-silane
methyl 5-chloro-2-methoxybenzoate
Conditions | Yield |
---|---|
In methanol; toluene Inert atmosphere; | 86.3 mg |
methyl 5-chloro-2-methoxybenzoate
methyl 2-methoxy-5-sulfamoyl-benzoate
Conditions | Yield |
---|---|
With sodium sulfamate; copper(I) bromide In tetrahydrofuran at 50℃; for 10h; Temperature; Reflux; | 96.55% |
With sodium aminosulfinate; copper(I) bromide In tetrahydrofuran at 40℃; for 18h; Concentration; Temperature; | 96.55% |
With sodium aminosulfinate; copper(l) chloride In tetrahydrofuran at 40℃; for 8h; Temperature; | 96.55% |
methyl 5-chloro-2-methoxybenzoate
acetonitrile
3-(5-chloro-2-methoxyphenyl)-3-oxopropanenitrile
Conditions | Yield |
---|---|
Stage #1: acetonitrile With n-butyllithium; diisopropylamine In tetrahydrofuran; hexane at -78℃; for 0.5h; Inert atmosphere; Stage #2: methyl 5-chloro-2-methoxybenzoate In tetrahydrofuran; hexane at -78℃; for 0.666667h; | 94% |
methyl 5-chloro-2-methoxybenzoate
p-tolylzinc(II) chloride
methyl 2-methoxy-5-(p-methylphenyl)benzoate
Conditions | Yield |
---|---|
With Ni(Cl){2-(Ph2P)C6H4NCH(Ph)P(O)Ph2} In tetrahydrofuran; 1-methyl-pyrrolidin-2-one at 25℃; for 24h; Negishi coupling reaction; Inert atmosphere; | 93% |
methyl 5-chloro-2-methoxybenzoate
bis(pinacol)diborane
3-chloro-6-methoxy-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzoic acid methyl ester
Conditions | Yield |
---|---|
With silica-SMAP-Ir(OCH3)(C8H12) In hexane ligand reacted with B-compound in hexane in presence of Ir-complex as catalyst at 25°C for 4 h; | 85% |
With Silica-SMAP-Ir(OMe)(cod) In hexane at 25℃; for 4h; Autoclave; regioselective reaction; | 85% |
methyl 5-chloro-2-methoxybenzoate
5-chloro-2-methoxybenzoic acid
Conditions | Yield |
---|---|
With sodium hydroxide In water at 20℃; | 83% |
With water; sodium hydroxide In ethanol at 15 - 30℃; for 4h; | 74.9% |
With sodium hydroxide for 16h; Ambient temperature; Yield given; | |
With sodium hydroxide In 1,4-dioxane | |
With water at 80℃; for 0.25h; |
methyl 5-chloro-2-methoxybenzoate
(5-chloro-2-methoxyphenyl)methanol
Conditions | Yield |
---|---|
With lithium aluminium tetrahydride In tetrahydrofuran at 0℃; for 2h; | 73.5% |
In tetrahydrofuran | |
In tetrahydrofuran | |
With lithium aluminium tetrahydride In tetrahydrofuran for 2h; Heating / reflux; | |
With lithium aluminium tetrahydride In diethyl ether for 2h; Cooling with ice; |
1-Chlorooctane
methyl 5-chloro-2-methoxybenzoate
Conditions | Yield |
---|---|
With nickel(II) bromide dimethoxyethane; pyridine-2,6-bis(N-cyanocarboxamidine); lithium chloride; zinc In 1-methyl-pyrrolidin-2-one at 80℃; for 23h; Inert atmosphere; | 59% |
pyrrolidine
methyl 5-chloro-2-methoxybenzoate
Conditions | Yield |
---|---|
With sodium hexamethyldisilazane In tetrahydrofuran at 0 - 20℃; for 2h; | 56% |
methyl 5-chloro-2-methoxybenzoate
cyclooctylguanidine sulfate
N-(5-Chloro-2-methoxy-benzoyl)-N'-cyclooctyl-guanidine; hydrochloride
Conditions | Yield |
---|---|
With hydrogenchloride; sodium In methanol for 5h; Ambient temperature; | 55.4% |
4-methoxyphenyl triflate
methyl 5-chloro-2-methoxybenzoate
Conditions | Yield |
---|---|
With nickel(II) chloride2-methoxyethyl ether; 1,4-di(diphenylphosphino)-butane; 4,4'-di-tert-butyl-2,2'-bipyridine; lithium chloride; palladium dichloride; zinc In 1-methyl-pyrrolidin-2-one; N,N-dimethyl-formamide at 20 - 80℃; for 24h; Ullmann Condensation; Inert atmosphere; | 45% |
methyl 5-chloro-2-methoxybenzoate
4-(4-methylpiperazin-1-yl)-6-(3-chloro-6-methoxyphenyl)-1,3,5-triazin-2-amine
Conditions | Yield |
---|---|
With methanol; sodium Reflux; | 31% |
methyl 5-chloro-2-methoxybenzoate
N-BENZO[1,3]DIOXOL-5-YL-6-(5-CHLORO-2-METHOXYPHENYL)-[1,3,5]TRIAZINE-2,4-DIAMINE
Conditions | Yield |
---|---|
28% |
methyl 5-chloro-2-methoxybenzoate
6-(5-chloro-2-methoxy-phenyl)-N-phenyl-[1,3,5]triazine-2,4-diamine
Conditions | Yield |
---|---|
With sodium ethanolate In ethanol; water | 27% |
2-acetyl-1-tetralone
methyl 5-chloro-2-methoxybenzoate
1-(5-Chloro-2-methoxyphenyl)-3-(1,2,3,4-tetrahydro-1-oxo-2-naphthalenyl)-1,3-propanedione
Conditions | Yield |
---|---|
With sodium hydride In 1,2-dimethoxyethane for 6h; Heating; |
2-acetyl-6-allylphenol
methyl 5-chloro-2-methoxybenzoate
8-Allyl-2-(5-chloro-2-methoxy-phenyl)-chromen-4-one
Conditions | Yield |
---|---|
With sulfuric acid; sodium hydride 1) THF, reflux, 5 h, 2) THF, MeOH, reflux, 3 h; Yield given. Multistep reaction; |
methyl 5-chloro-2-methoxybenzoate
Conditions | Yield |
---|---|
With diethyl ether |
ortho-methylbenzoic acid
methyl 5-chloro-2-methoxybenzoate
Conditions | Yield |
---|---|
With lithium diisopropyl amide 1) THF, 0 deg C, 60 min, 2) THF; Yield given. Multistep reaction; |
tert-butyl phenylcarbamate
methyl 5-chloro-2-methoxybenzoate
Conditions | Yield |
---|---|
Stage #1: tert-butyl phenylcarbamate With tert.-butyl lithium In tetrahydrofuran at -78 - -40℃; Stage #2: methyl 5-chloro-2-methoxybenzoate In tetrahydrofuran at -40 - 0℃; |
methyl 5-chloro-2-methoxybenzoate
N-(t-butoxycarbonyl)-4-chloroaniline
Conditions | Yield |
---|---|
Stage #1: N-(t-butoxycarbonyl)-4-chloroaniline With tert.-butyl lithium In tetrahydrofuran at -78 - -40℃; Stage #2: methyl 5-chloro-2-methoxybenzoate In tetrahydrofuran at -40 - 0℃; |
methyl 5-chloro-2-methoxybenzoate
t-butyl<3-(trifluoromethyl)phenyl>-carbamate
Conditions | Yield |
---|---|
Stage #1: t-butyl<3-(trifluoromethyl)phenyl>-carbamate With tert.-butyl lithium In tetrahydrofuran at -78 - -40℃; Stage #2: methyl 5-chloro-2-methoxybenzoate In tetrahydrofuran at -40 - 0℃; |
methyl 5-chloro-2-methoxybenzoate
tert-butyl (4-(trifluoromethyl)phenyl)carbamate
N-[2-[(5-chloro-2-methoxyphenyl) carbonyl]-4-(trifluoromethyl) phenyl]aminocarboxylic acid, 1,1-dimethylethyl ester
Conditions | Yield |
---|---|
Stage #1: tert-butyl (4-(trifluoromethyl)phenyl)carbamate With tert.-butyl lithium In tetrahydrofuran at -78 - -40℃; Stage #2: methyl 5-chloro-2-methoxybenzoate In tetrahydrofuran at -40 - 0℃; |
methyl 5-chloro-2-methoxybenzoate
tert-butyl (2-(trifluoromethyl)phenylamino)formate
Conditions | Yield |
---|---|
Stage #1: tert-butyl (2-(trifluoromethyl)phenylamino)formate With tert.-butyl lithium In tetrahydrofuran at -78 - -40℃; Stage #2: methyl 5-chloro-2-methoxybenzoate In tetrahydrofuran at -40 - 0℃; |
methyl 5-chloro-2-methoxybenzoate
(2-amino-phenyl)-(5-chloro-2-methoxy-phenyl)-methanone
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: t-BuLi / tetrahydrofuran / -78 - -40 °C 1.2: tetrahydrofuran / -40 - 0 °C 2.1: 3 N HCl / ethanol / Heating View Scheme |
methyl 5-chloro-2-methoxybenzoate
(2-amino-5-chloro-phenyl)-(5-chloro-2-methoxy-phenyl)-methanone
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1.1: t-BuLi / tetrahydrofuran / -78 - -40 °C 1.2: tetrahydrofuran / -40 - 0 °C 2.1: 3 N HCl / ethanol / Heating View Scheme |
methyl 5-chloro-2-methoxybenzoate
2-chloro-N-[2-(5-chloro-2-methoxy-benzoyl)-phenyl]-acetamide
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1.1: t-BuLi / tetrahydrofuran / -78 - -40 °C 1.2: tetrahydrofuran / -40 - 0 °C 2.1: 3 N HCl / ethanol / Heating 3.1: pyridine / CH2Cl2 View Scheme |
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