Dayangchem's R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. DayangChem can provide different quantities
Cas:3424-93-9
Min.Order:1 Kilogram
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Type:Lab/Research institutions
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Cas:3424-93-9
Min.Order:5 Kiloliter
FOB Price: $1.2 / 5.0
Type:Manufacturers
inquiryWITH US,YOUR MONEY IN SAFE,YOUR BUSINESS IN SAFE 1)Quick Response Within 12 hours; 2)Quality Guarantee: All products are strictly tested by our QC, confirmed by QA and approved by third party lab in China, USA, Canada, Germany, UK, Italy, France et
Cas:3424-93-9
Min.Order:1 Kilogram
FOB Price: $139.0 / 210.0
Type:Trading Company
inquiryProduct Name: 4-Methoxybenzamide CAS: 3424-93-9 MF: C8H9NO2 MW: 151.16 EINECS: 222-319-6 Mol File: 3424-93-9.mol 4-Methoxybenzamide Structure 4-Methoxybenzamide Chemical Properties Melting point 164-167 °C (lit.) Boiling p
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Cas:3424-93-9
Min.Order:1 Gram
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Type:Lab/Research institutions
inquiry4-Methoxybenzamide CAS:3424-93-9 Qingdao Belugas Import and Export Co., Ltd. is a scientific and technological company integrating research and development, production and trade of chemical intermediates, specializing in high quality organic interme
Cas:3424-93-9
Min.Order:1 Gram
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Type:Lab/Research institutions
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Cas:3424-93-9
Min.Order:1 Kilogram
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Type:Lab/Research institutions
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Cas:3424-93-9
Min.Order:10 Kilogram
Negotiable
Type:Trading Company
inquiryHenan Wentao Chemical Product Co.,Ltd is Located in Zhengzhou High-tech Development Zone with import and export license, We passed ISO 9001:2008 as well, Henan Wentao has developed more than 1000 compounds, which are widely used in the fields of prod
J&H CHEM R&D center can offer custom synthesis according to the contract research and development services for the fine chemicals, pharmaceutical, biotechnique and some of the other chemicals. J&H CHEM has some Manufacturing base in Jia
The above product is Ality Chemical's strong item with best price, good quality and fast supply. Ality Chemical has been focusing on the research and production of this field for over 14 years. At the same time, we are always committed to providi
Cas:3424-93-9
Min.Order:0 Metric Ton
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Type:Other
inquiryZibo Hangyu Biotechnology Development Co., Ltd is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemi
Cas:3424-93-9
Min.Order:10 Gram
FOB Price: $100.0
Type:Lab/Research institutions
inquiryWe are one of a few suppliers that can offer custom synthesis service of this product We are specialized in custom synthesis, chemical/pharmaceutical/ pesticides outsourcing and contract research. We are committed to prov
Cas:3424-93-9
Min.Order:100 Gram
FOB Price: $100.0 / 2000.0
Type:Lab/Research institutions
inquiryOur company was built in 2009 with an ISO certificate.In the past 5 years, we have grown up as a famous fine chemicals supplier in China and we had established stable business relationships with Samsung,LG,Merck,Thermo Fisher Scientific and so on.O
Cas:3424-93-9
Min.Order:1 Kilogram
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Type:Lab/Research institutions
inquiryfactory?direct?saleAppearance:White Powder Storage:Store In Dry, Cool And Ventilated Place Package:25kg/drum, also according to the clients requirement Application:It is widely used as a thickener, emulsifier and stabilizer Transportation:By Sea Or B
Cas:3424-93-9
Min.Order:1 Kilogram
FOB Price: $18.0 / 20.0
Type:Trading Company
inquiryShandong Mopai Biotechnology Co., LTD is a leading manufacturer and supplier of chemicals in China. We develop produce and distribute high quality pharmaceuticals, intermediates, special chemicals and OLED intermediates and other fine chemicals. W
Cas:3424-93-9
Min.Order:1 Gram
Negotiable
Type:Lab/Research institutions
inquiry1.Applied in food field.it can improve the immune system and prolong life. 2.Appliedin cosmetic field.it can improve the skin care. 3.Applied in pharmaceutical field.it can treat various dieases. 4.Our product quality assurance will make our customer
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Min.Order:1 Metric Ton
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Type:Trading Company
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Triumph has the complete production of G- KG - MT service chain,we can make the new technology into productivity quickly in the research and development of new products. Main Business Custom Synthesis:
We are a Union of chemistry in China, consists of chemists,engineers, laboratories,factories in China. We organize surplus capacity of R&D and production as well as custom synthesis for chemical products and chemical business project. We are supp
Cas:3424-93-9
Min.Order:1 Metric Ton
FOB Price: $1.0
Type:Trading Company
inquiryWe produce carbomer by our own factory,carbomer 940 is our best seller.It is used for cosmetic and medical.And we also become agent for lubrizol.Our carbomer 940 get high viscosity and good transparency.The price will depond on the market,surely supp
Lower price, sample is available,SDS test documents are available,large stock in warehouseAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:Fine chemical intermediates, used as the main raw material for the synthe
Cas:3424-93-9
Min.Order:0
Negotiable
Type:Lab/Research institutions
inquiryhigh purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:drum and bag Application:for pharma use Transportation:by sea or air Port:Beijing or Guangzhou
1.High quality : the purity is 99% min . through multiple producing procedures. 2.Competitive price : low price because of our skilled production technolpgy ,save the production cost at most , and give big profit room to our customers 27.Safe and fa
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high quality Storage:Sealed, dry, microtherm , avoid light and smell. Package:According to the demand of customer Application:Organic synthesis Transportation:by air or by sea
Ansciep Chemical is a professional enterprise manufacturing and distributing fine chemicals and speciality chemicals. We have been dedicated to heterocycle compounds and phenyl rings for tens of years. This is our mature product for export. Our quali
4-Methoxybenzamide CAS NO.3424-93-9 Application:4-Methoxybenzamide CAS NO.3424-93-9
We product this chemical more than 10 years . We are very experience to export it to many countries, Our superior & stable quality , competitive price gain warm reception from our customers. Application:Pharm intermediate
4-Methoxybenzamide cas 3424-93-9Appearance:white crystalline powder Storage:Store in dry, dark and ventilated place Package:25KG drum Application:intermediate Transportation:by air, by sea, by express
Conditions | Yield |
---|---|
With C18H57O3P6Ru2(1+)*C6H5O(1-)*C6H6O; water In 1,4-dioxane for 6h; Time; Sealed tube; Inert atmosphere; Schlenk technique; | 100% |
With [bis(2-methylallyl)cycloocta-1,5-diene]ruthenium(II); water; 2-(diphenylphosphino)-N,N-dimethylpyridine-4-amine In 1,2-dimethoxyethane at 80℃; for 5h; | 99% |
With C12H24O16Ru3*2H2O In water at 110℃; for 13h; Catalytic behavior; Schlenk technique; Inert atmosphere; | 99% |
Conditions | Yield |
---|---|
With hydroxylamine; C33H28F3N5O3Ru(1+)*Cl(1-) In water at 60℃; for 0.5h; Catalytic behavior; Sonication; | 99% |
Stage #1: 4-methoxy-benzaldehyde With hydroxylamine hydrochloride; caesium carbonate In water; dimethyl sulfoxide at 100℃; Stage #2: With palladium diacetate In water; dimethyl sulfoxide at 125℃; chemoselective reaction; | 97% |
With copper(ll) sulfate pentahydrate; hydroxylamine hydrochloride; sodium acetate at 110℃; for 2h; Neat (no solvent); | 97% |
Conditions | Yield |
---|---|
Stage #1: 4-methoxybenzoic acid With 1,3,5-trichloro-2,4,6-triazine; potassium carbonate In tetrahydrofuran for 0.0166667h; Milling; Stage #2: With ammonium thiocyanate In tetrahydrofuran for 0.0833333h; Milling; | 99% |
With pyridine; urea for 0.00833333h; microwave irradiation; | 90% |
Stage #1: 4-methoxybenzoic acid With thionyl chloride In tetrahydrofuran at 50℃; for 1h; Stage #2: With ammonium hydroxide In tetrahydrofuran at 0℃; for 0.0833333h; | 84% |
N-tert-butyl-4-methoxybenzamide
4-methoxyphenylacetamide
Conditions | Yield |
---|---|
scandium tris(trifluoromethanesulfonate) In nitromethane at 170℃; for 1h; Irradiation; | 99% |
With t-butyldimethylsiyl triflate In toluene at 100℃; for 8h; | 74% |
p-hydroxybenzamide
carbonic acid dimethyl ester
4-methoxyphenylacetamide
Conditions | Yield |
---|---|
With dmap at 135℃; under 3000.3 Torr; for 7h; Pressure; Temperature; Reagent/catalyst; | 99% |
Conditions | Yield |
---|---|
With ammonia Inert atmosphere; | 98% |
With ammonia at -10 - 20℃; for 1h; Temperature; | 96.3% |
With ammonia In water at 20℃; for 1h; | 79% |
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; ammonia; oxygen In water; N,N-dimethyl-formamide at 80℃; under 1520.1 Torr; for 5h; Green chemistry; | 98% |
Stage #1: 4-Methoxybenzyl alcohol With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; ammonia; oxygen; copper(II) nitrate In water; dimethyl sulfoxide at 80℃; under 760.051 Torr; for 5h; Stage #2: With Acetaldehyde oxime In water; dimethyl sulfoxide at 110℃; for 24h; Inert atmosphere; | 97% |
With ammonia; oxygen In water at 150℃; under 22502.3 Torr; for 3h; | 96.5% |
Conditions | Yield |
---|---|
With manganese(IV) oxide at 130℃; under 4560.31 Torr; for 3h; | 98% |
With dihydrogen peroxide at 80℃; for 10h; Inert atmosphere; | 96% |
With (carbonyl)(chloro)(hydrido)tris(triphenylphosphine)ruthenium(II); potassium tert-butylate In tert-butyl alcohol at 70℃; for 12h; | 95% |
Conditions | Yield |
---|---|
With (1,4-diazabicyclo{2.2.2}-octane)zinc(II) tetrahydoborate In tetrahydrofuran for 48h; Ambient temperature; | 97% |
With 1,3-diadamantane-4,5-dihydroimidazole chloride; potassium tert-butylate; bis(pinacol)diborane; copper(l) chloride In toluene at 25℃; for 4h; Schlenk technique; Inert atmosphere; | 94% |
With sodium tetrahydroborate; copper(II) sulfate In methanol at 0 - 5℃; for 1h; | 92% |
4-methoxybenzonitrile
A
4-methoxyphenylacetamide
B
4-methoxybenzamidoxime
Conditions | Yield |
---|---|
With hydroxylamine In ethanol for 3h; Reagent/catalyst; Reflux; | A 97% B n/a |
With hydroxylamine hydrochloride; sodium hydroxide In ethanol; water Reflux; |
Conditions | Yield |
---|---|
With 2-(2'-pyridyl)(di(1-adamantyl)phosphino)benzene; ammonia; palladium diacetate In 1,4-dioxane at 120℃; under 1500.15 Torr; for 16h; Autoclave; | 96% |
With tris-(dibenzylideneacetone)dipalladium(0); (2R)-1-[(1R)-1-[bis(1,1-dimethylethyl)phosphino]ethyl]-2-(diphenylphosphino)ferrocene; ammonium carbamate; sodium hydrogencarbonate In 1,4-dioxane at 100℃; for 20h; Inert atmosphere; | 93% |
With dmap; bis-triphenylphosphine-palladium(II) chloride; formamide In 1,4-dioxane at 120℃; under 3750.38 Torr; for 18h; | 69% |
4-methoxyphenylacetamide
Conditions | Yield |
---|---|
With lithium hydroxide monohydrate In water at 20℃; for 2h; | 96% |
tert-butyl (4-methoxybenzoyl)carbamate
4-methoxyphenylacetamide
Conditions | Yield |
---|---|
With trifluoroacetic acid In dichloromethane for 1h; Ambient temperature; | 95% |
With trifluoroacetic acid In dichloromethane at 20℃; for 1h; Reagent/catalyst; |
Conditions | Yield |
---|---|
With ammonium hydroxide; 1,3,5,7-tetramethyl-2,4,8-trioxa-6-phenyl-6-phosphaadamantane; palladium diacetate In toluene at 130℃; under 5171.62 Torr; Temperature; Autoclave; | 95% |
With 1,4-diaza-bicyclo[2.2.2]octane; N-methoxylamine hydrochloride; sodium iodide; palladium dichloride In acetonitrile at 90℃; under 3800.26 Torr; for 8h; Autoclave; Inert atmosphere; | 93% |
With 1,4-diaza-bicyclo[2.2.2]octane; palladium 10% on activated carbon; ammonium carbamate; potassium iodide In acetonitrile at 90℃; for 8h; Autoclave; Green chemistry; | 90% |
p-methoxyl benzaldoxime
4-methoxyphenylacetamide
Conditions | Yield |
---|---|
With silver tetrafluoroborate; chloro(1,3-bis(2,6-di-i-propylphenyl)imidazol-2-ylidene)gold(I) at 100℃; for 20h; Beckmann rearrangement; Sealed tube; Neat (no solvent); | 95% |
With C55H45ClN5P2Ru(1+)*Cl(1-) In water at 110℃; for 12h; Sealed tube; | 94% |
With C82H80N4O6; mercury dichloride In tetrahydrofuran; water; toluene at 20℃; for 5h; Beckmann Rearrangement; | 93% |
Conditions | Yield |
---|---|
With toluene-4-sulfonic acid; 1,2-bis-(diphenylphosphino)ethane; carbonyl(dihydro)tris(triphenylphosphine)ruthenium(II) In toluene Heating; | 93% |
With cerium(III) chloride; silica gel; sodium iodide for 0.0666667h; Beckmann rearrangement; microwave irradiation; | 80% |
1-bromo-4-methoxy-benzene
dicobalt octacarbonyl
4-methoxyphenylacetamide
Conditions | Yield |
---|---|
With 1H-imidazole; 1,1'-bis-(diphenylphosphino)ferrocene; palladium diacetate; ammonium chloride; N-ethyl-N,N-diisopropylamine In 1,4-dioxane at 90℃; for 3h; Catalytic behavior; Reagent/catalyst; Solvent; Temperature; Sealed tube; | 93% |
2-(4-methoxybenzoylamino)-2-methylpropionic acid
4-methoxyphenylacetamide
Conditions | Yield |
---|---|
With copper dichloride In dimethyl sulfoxide at 120℃; for 11h; | 93% |
With copper dichloride In dimethyl sulfoxide at 120℃; for 11h; | 93% |
(E)-4-methoxybenzaldoxime
4-methoxyphenylacetamide
Conditions | Yield |
---|---|
bis[dichloro(pentamethylcyclopentadienyl)iridium(III)] In toluene at 111℃; for 6h; | 92% |
With indium(III) chloride; 4-methoxybenzonitrile In toluene for 18h; Reflux; | 91% |
In ethanol for 20h; Quantum yield; Irradiation; |
Conditions | Yield |
---|---|
Stage #1: p-Methoxybenzyl bromide With ammonia; iodine In water at 60℃; for 4h; Stage #2: With ammonia; dihydrogen peroxide In water at 0 - 20℃; | 92% |
Conditions | Yield |
---|---|
Stage #1: benzylamine With N-chloro-succinimide In acetonitrile at 20℃; for 3h; Green chemistry; Stage #2: p-methylanizole With tert.-butylhydroperoxide; iron(II) acetate In decane; acetonitrile at 82℃; for 22h; Green chemistry; Stage #3: With palladium 10% on activated carbon; hydrogen In methanol at 20℃; for 12h; Green chemistry; | 92% |
Conditions | Yield |
---|---|
With tert.-butylhydroperoxide; iron(III) chloride hexahydrate; tetrabutylammonium iodide; ammonium hydroxide In water at 80℃; for 18h; Sealed tube; | 91% |
With tert.-butylhydroperoxide; ammonium chloride; calcium carbonate In dihydrogen peroxide; acetonitrile at 80℃; for 10h; Catalytic behavior; Inert atmosphere; | 60% |
Conditions | Yield |
---|---|
bis[dichloro(pentamethylcyclopentadienyl)iridium(III)] In toluene at 111℃; for 6h; | 90% |
4-methoxy-benzaldehyde
A
4-methoxyphenylacetamide
B
4-methoxybenzonitrile
C
4-methoxybenzoic acid
Conditions | Yield |
---|---|
With H2SO4*2NH2OH; Rh(OH)x/Al2O3 In water for 7h; Heating; | A 90% B 5 % Chromat. C 9 % Chromat. |
Stage #1: 4-methoxy-benzaldehyde With pyridine; sodium persulfate; tris(2,2-bipyridine)ruthenium(II) hexafluorophosphate; 4-acetylamino-2,2,6,6-tetramethyl-1-piperidinoxy; 1,1,1,3,3,3-hexamethyl-disilazane In acetonitrile at 0.2℃; for 24h; Molecular sieve; Sealed tube; Irradiation; Stage #2: With tetrabutyl ammonium fluoride In tetrahydrofuran; acetonitrile for 1h; Molecular sieve; |
Conditions | Yield |
---|---|
With sodium azide; iodine; sodium hydrogencarbonate In water at 100℃; for 2h; Reagent/catalyst; Temperature; Solvent; | 90% |
With ammonia; iodine In water at 60℃; for 1h; Lieben-Haller-Bauer reaction; | 83% |
With ammonia; water; iodine In tetrahydrofuran at 20℃; for 24h; Haller-Bauer reaction; | 83% |
With sodium azide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; oxygen; copper dichloride In water; N,N-dimethyl-formamide at 120℃; under 760.051 Torr; for 15h; Schlenk technique; chemoselective reaction; | 67% |
With tert.-butylhydroperoxide; ammonia; tetra-(n-butyl)ammonium iodide In water at 100℃; for 16h; Green chemistry; | 53% |
Conditions | Yield |
---|---|
With [{Au(SIPr)}2(μ-OH)][BF4] In tetrahydrofuran at 140℃; for 2h; Reagent/catalyst; Concentration; Microwave irradiation; | 90% |
Conditions | Yield |
---|---|
With water; potassium carbonate In dimethyl sulfoxide at 110℃; for 12h; | 90% |
Conditions | Yield |
---|---|
With ammonia; dihydrogen peroxide; iodine In water; dimethyl sulfoxide at 20℃; for 3h; Irradiation; | 90% |
4-methoxy-benzylamine
A
4-methoxyphenylacetamide
B
4-methoxybenzonitrile
Conditions | Yield |
---|---|
With water; oxygen at 140℃; under 3800.26 Torr; for 10h; | A 89% B n/a |
With ammonium hydroxide; oxygen In tert-Amyl alcohol at 110℃; under 1500.15 Torr; for 16h; | A 13.6% B 79.3% |
Conditions | Yield |
---|---|
With tetraphosphorus decasulfide In 1,4-dioxane at 50 - 68℃; for 3h; Temperature; | 100% |
With pyridin-1-ium-1-yl[pyridin-1-ium-1-yl(sulfido)phosphinothioyl]sulfanyl-sulfido-thioxo-phosphane In acetonitrile for 0.5h; Reflux; | 88% |
With Lawessons reagent In tetrahydrofuran at 20℃; Reflux; | 80% |
Conditions | Yield |
---|---|
With barium trifluoromethanesulfonate In toluene for 18h; Reflux; Inert atmosphere; | 100% |
With C23H24ClIrN3OS(1+)*F6P(1-); caesium carbonate In toluene at 120℃; | 96% |
With bis[dichloro(pentamethylcyclopentadienyl)iridium(III)]; caesium carbonate In toluene at 140℃; for 12h; | 84% |
Conditions | Yield |
---|---|
With thionyl chloride; carbonic acid dimethyl ester at 80℃; for 7h; Temperature; | 99.2% |
With trichloromethyl chloroformate In various solvent(s) 0-5 deg C then heated to 60 deg C, 5 min; | 97% |
With ((1,3,5-triazine-2,4,6-triyl)tris(oxy))tris(triphenylphosphonium) chloride at 140 - 150℃; for 2h; | 97% |
Conditions | Yield |
---|---|
With chloro-trimethyl-silane In acetonitrile at 10 - 20℃; for 24h; Inert atmosphere; | 99% |
With chloro-trimethyl-silane In acetonitrile at 23℃; | |
With chloro-trimethyl-silane In acetonitrile at 0 - 20℃; Inert atmosphere; |
Conditions | Yield |
---|---|
With copper(l) iodide; 1,10-Phenanthroline In benzene at 60℃; for 11h; Inert atmosphere; | 99% |
With copper(l) iodide; 1,10-Phenanthroline In benzene at 60℃; for 11h; Inert atmosphere; | 99% |
4-methoxyphenylacetamide
4-methoxy-benzaldehyde
4-methoxy-N-(4-methoxybenzyl)benzamide
Conditions | Yield |
---|---|
With carbon monoxide In diethyl ether at 150 - 160℃; under 30003 Torr; Sealed tube; | 99% |
With carbon monoxide; C14H10*Ru(2+)*C11H17O(1-)*F6P(1-) In diethyl ether at 150℃; under 22801.5 Torr; for 22h; Autoclave; | 70% |
Conditions | Yield |
---|---|
With [bis(acetoxy)iodo]benzene; ammonia In methanol at 0 - 20℃; for 2h; Temperature; Hofmann Rearrangement; Inert atmosphere; | 99% |
4-methoxyphenylacetamide
4-tolyl iodide
N-(p-methylphenyl)-p-methoxybenzamide
Conditions | Yield |
---|---|
With 2-Phenyl-1,3,2-dioxaborinane In 1,4-dioxane at 115℃; for 30h; Inert atmosphere; | 99% |
4-methoxyphenylacetamide
sodium methylate
methyl N-(4-methoxyphenyl)carbamate
Conditions | Yield |
---|---|
Stage #1: 4-methoxyphenylacetamide; sodium methylate In methanol at 20℃; for 0.25h; Stage #2: With bis(1,3-dimethyl-2-imidazolidinone) hydrotribromide In methanol for 4h; Hofmann Rearrangement; Reflux; | 98% |
With N-Bromosuccinimide In methanol for 0.166667h; Heating; | 87% |
Conditions | Yield |
---|---|
With copper; potassium carbonate; N,N`-dimethylethylenediamine In toluene at 135℃; for 2h; Ullmann type reaction; Inert atmosphere; | 98% |
With caesium carbonate; palladium diacetate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene In 1,4-dioxane at 100℃; for 10h; | 95% |
With palladium diacetate; caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene In 1,4-dioxane at 100℃; | |
With palladium diacetate; caesium carbonate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene In 1,4-dioxane at 100℃; for 10h; Inert atmosphere; Sealed tube; |
Conditions | Yield |
---|---|
With 3-[4-(diacetoxyiodo)phenoxy]-1-propyl-N,N,N-trimethylammonium 4-methylbenzenesulfonate; potassium hydroxide In chloroform at 0 - 20℃; Hofmann Rearrangement; Inert atmosphere; | 98% |
Conditions | Yield |
---|---|
With samarium diiodide; water In tetrahydrofuran at 23℃; for 0.0833333h; Reagent/catalyst; Inert atmosphere; Schlenk technique; chemoselective reaction; | 98% |
With samarium diiodide; water; triethylamine In tetrahydrofuran at 23℃; for 18h; Inert atmosphere; chemoselective reaction; | 92% |
With C24H20ClN2OPRu; potassium tert-butylate; hydrogen In tetrahydrofuran at 110℃; under 10640.7 Torr; for 36h; Inert atmosphere; Schlenk technique; | 82% |
4-methoxyphenylacetamide
3-bromo-butanone
2-(4-methoxy-phenyl)-4,5-dimethyl-oxazole
Conditions | Yield |
---|---|
With silver(I) trifluoromethoxide In ethyl acetate at 50℃; for 4h; Darkness; | 98% |
Conditions | Yield |
---|---|
With dmap; triethylamine In dichloromethane at 20℃; | 98% |
4-methoxyphenylacetamide
α-bromoacetophenone
2-(4-methoxyphenyl)-4-phenyloxazole
Conditions | Yield |
---|---|
With silver(I) trifluoromethoxide In ethyl acetate at 50℃; for 4h; Reagent/catalyst; Temperature; Darkness; | 97% |
at 140℃; for 1h; | 80% |
With silver trifluoromethanesulfonate In ethyl acetate at 50℃; Inert atmosphere; | 64% |
Heating; |
ethyl Bromopyruvate
4-methoxyphenylacetamide
ethyl 2-(4-methoxyphenyl)-1,3-oxazole-4-carboxylate
Conditions | Yield |
---|---|
With silver hexafluoroantimonate In 1,2-dichloro-ethane at 90℃; for 2h; Inert atmosphere; Microwave irradiation; | 97% |
With silver hexafluoroantimonate In dichloromethane at 90℃; under 3750.38 Torr; for 1h; Sealed tube; Microwave irradiation; | |
In ethanol at 70℃; for 5h; | |
Stage #1: ethyl Bromopyruvate; 4-methoxyphenylacetamide With sodium hydrogencarbonate In tetrahydrofuran at 60℃; for 23h; Stage #2: With trifluoroacetic anhydride In tetrahydrofuran at 20℃; for 12h; |
4-methoxyphenylacetamide
di-tert-butyl dicarbonate
Conditions | Yield |
---|---|
With dmap In neat (no solvent) for 4h; Milling; chemoselective reaction; | 97% |
With dmap In acetonitrile at 20℃; for 15h; Inert atmosphere; Sealed tube; | 90% |
With dmap In acetonitrile at 20℃; for 15h; | 86% |
formaldehyd
4-methoxyphenylacetamide
5-(4-methoxy)phenyl-1,3,4-oxadiazol-2(3H)-one
Conditions | Yield |
---|---|
With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; ammonium cerium (IV) nitrate; nickel diethyldithiocarbamate; N-fluorobis(benzenesulfon)imide; 1-butyl-methylpyrrolidinium bis(trifluoromethylsulfonyl)amide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione In dimethyl sulfoxide at 60℃; for 10h; | 96.8% |
4-methyleneoxetan-2-one
4-methoxyphenylacetamide
4-Methoxy-N-(3-oxo-butyryl)-benzamide
Conditions | Yield |
---|---|
With Aliquat 336 In toluene for 10h; Heating; | 96% |
With chloro-trimethyl-silane; sodium iodide In acetonitrile for 2h; Ambient temperature; | 90% |
With chloro-trimethyl-silane; sodium iodide In acetonitrile for 2h; Ambient temperature; | 89.5% |
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