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bis(benzylthio)methane
A
monochloromethanesulfonyl chloride
B
Benzyl acetate
C
benzyl chloride
Conditions | Yield |
---|---|
With water; chlorine; acetic acid In water at 20 - 30℃; for 2h; | A 53.6% B 9.8% C 73.9% |
bis(benzylthio)methane
A
monochloromethanesulfonyl chloride
B
Benzyl acetate
C
benzyl chloride
D
benzenesulfonyl chloride
Conditions | Yield |
---|---|
With water; chlorine In acetic acid Product distribution; other methyl substituted bis(thiobenzyl) methane derivatives; other products; | A 53.6% B 9.8% C 73.9% D 38% |
Conditions | Yield |
---|---|
With potassium chlorate In hydrogenchloride for 5h; Ambient temperature; | 62% |
With chlorine; acetic acid | |
With hydrogenchloride; potassium chlorate |
benzyl chloromethyl sulfide
A
monochloromethanesulfonyl chloride
B
Benzyl acetate
C
benzyl chloride
D
benzenesulfonyl chloride
Conditions | Yield |
---|---|
With water; chlorine; acetic acid at 20 - 30℃; for 2h; | A 54% B 16% C 38% D 9.4% |
benzyl chloromethyl sulfide
acetic acid
A
monochloromethanesulfonyl chloride
B
Benzyl acetate
C
benzyl chloride
D
benzenesulfonyl chloride
Conditions | Yield |
---|---|
With chlorine In water at 20 - 30℃; for 2h; | A 54% B 16% C 38% D 9.4% |
Conditions | Yield |
---|---|
With hydrogenchloride; chlorine; sodium thiosulfate In water at -10℃; for 1.5h; | 28% |
With hydrogenchloride; formaldehyd; hydrogen sulfide 2.) glacial acetic acid, water, 30 deg C, 3-4 h; Yield given. Multistep reaction; | |
With hydrogenchloride; formaldehyd; hydrogen sulfide; water anschliessendes Behandeln bei -15grad mit Chlor; |
chloromethanesulfenyl chloride
monochloromethanesulfonyl chloride
Conditions | Yield |
---|---|
With dihydrogen peroxide; acetic acid | |
With chlorine |
methane
monochloromethanesulfonyl chloride
Conditions | Yield |
---|---|
With sulfur dioxide; chlorine bei der Einwirkung von hochfrequenten elektrischen Entladungen; |
chloromethyl sodium sulfonate
monochloromethanesulfonyl chloride
Conditions | Yield |
---|---|
With phosphorus pentachloride; trichlorophosphate | |
With phosphorus pentachloride (heating); | |
Stage #1: sodium chloromethanesulfonate With phosphorus pentachloride at 130℃; for 1.25h; Cooling with ice; Stage #2: With water for 1h; Cooling with ice; |
Conditions | Yield |
---|---|
With pyridine; sulfuryl dichloride In tetrachloromethane |
water
chlorine
[1,3,5]trithiane
monochloromethanesulfonyl chloride
monochloromethanesulfonyl chloride
Conditions | Yield |
---|---|
With water; chlorine unter Kuehlung; | |
With chlorine; acetic acid |
chloromethanesulfenyl chloride
water
chlorine
monochloromethanesulfonyl chloride
monochloromethanesulfonyl chloride
(4aS,5S)-4,4a,5,6,7,8-hexahydro-5-hydroxy-4a-methylnaphthalen-2(3H)-one
Chloro-methanesulfonic acid (1S,8aS)-8a-methyl-6-oxo-1,2,3,4,6,7,8,8a-octahydro-naphthalen-1-yl ester
Conditions | Yield |
---|---|
With pyridine at 0 - 20℃; for 0.333333h; | 100% |
monochloromethanesulfonyl chloride
testosterone
Chloro-methanesulfonic acid (8R,9S,10R,13S,14S,17S)-10,13-dimethyl-3-oxo-2,3,6,7,8,9,10,11,12,13,14,15,16,17-tetradecahydro-1H-cyclopenta[a]phenanthren-17-yl ester
Conditions | Yield |
---|---|
With pyridine at 0 - 20℃; for 0.25h; | 100% |
With pyridine at 0℃; Substitution; |
Conditions | Yield |
---|---|
With pyridine at 0 - 20℃; for 0.75h; | 100% |
monochloromethanesulfonyl chloride
Cholestanol
Chloro-methanesulfonic acid (3S,5S,8R,9S,10S,13R,14S,17R)-17-((R)-1,5-dimethyl-hexyl)-10,13-dimethyl-hexadecahydro-cyclopenta[a]phenanthren-3-yl ester
Conditions | Yield |
---|---|
With pyridine at 0 - 20℃; for 0.0833333h; | 100% |
With pyridine at 0℃; Substitution; |
Conditions | Yield |
---|---|
With pyridine at 0 - 30℃; for 0.166667h; | 100% |
monochloromethanesulfonyl chloride
Conditions | Yield |
---|---|
With pyridine at 0 - 20℃; for 1h; | 100% |
monochloromethanesulfonyl chloride
(2S,3R)-1-Benzyloxymethoxy-2,4-dimethyl-pentan-3-ol
Conditions | Yield |
---|---|
With pyridine at 0 - 20℃; for 0.166667h; | 100% |
monochloromethanesulfonyl chloride
(4R,5S,6S)-1-tert-butyldimethylsilyloxy-4,5,7-tribenzyloxy-2(E)-hepten-6-ol
(4R,5S,6S)-1-tert-butyldimethylsilyloxy-6-[(chloro-methylsulfonyl)-oxy]-4,5,7-tribenzyloxy-2(E)-heptene
Conditions | Yield |
---|---|
With pyridine at 20℃; for 0.5h; Substitution; | 100% |
monochloromethanesulfonyl chloride
[(2R,4S,5R)-2-Phenyl-5-((4R,5S)-2-phenyl-4-vinyl-[1,3,2]dioxaborinan-5-yloxy)-[1,3]dioxan-4-yl]-methanol
Chloro-methanesulfonic acid (2R,4S,5R)-2-phenyl-5-((4R,5S)-2-phenyl-4-vinyl-[1,3,2]dioxaborinan-5-yloxy)-[1,3]dioxan-4-ylmethyl ester
Conditions | Yield |
---|---|
With 2,6-dimethylpyridine In dichloromethane at 21 - 23℃; | 100% |
monochloromethanesulfonyl chloride
Conditions | Yield |
---|---|
With lutidine In dichloromethane for 12h; | 100% |
monochloromethanesulfonyl chloride
Conditions | Yield |
---|---|
Stage #1: (R)-3-(7-amino-1,1-dioxo-1,4-dihydro-1λ6-benzo[1,2,4]thiadiazin-3-yl)-4-hydroxy-1-methyl-1-(3-methyl-butyl)-1H-naphthalen-2-one hydrochloride; monochloromethanesulfonyl chloride With pyridine In acetone at 20℃; for 24h; Stage #2: With citric acid In water; ethyl acetate; acetone | 100% |
monochloromethanesulfonyl chloride
2-azido-N,N-diethyl-4,5-O-isopropylidene-3-O-triisopropylsilyl-7-O-trityl-D-glycero-D-allo-heptonamide
C43H61ClN4O8SSi
Conditions | Yield |
---|---|
With pyridine at 0℃; for 0.75h; | 100% |
Conditions | Yield |
---|---|
With pyridine at 0℃; for 0.166667h; | 100% |
monochloromethanesulfonyl chloride
Conditions | Yield |
---|---|
With 2,6-dimethylpyridine In dichloromethane at 0 - 20℃; Inert atmosphere; | 100% |
With 2,6-dimethylpyridine In dichloromethane at 0 - 20℃; |
Conditions | Yield |
---|---|
With 2,6-dimethylpyridine In dichloromethane at 0℃; for 1h; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
With 2,6-dimethylpyridine In dichloromethane at 0℃; for 1h; Inert atmosphere; | 100% |
Conditions | Yield |
---|---|
With 2,6-dimethylpyridine In dichloromethane at 0℃; for 1.5h; Inert atmosphere; | 100% |
monochloromethanesulfonyl chloride
(R)-4-benzyl-3-((2R,3S,6R)-6-((2R,5S)-5-((S)-((tert-butyldimethylsilyl)oxy)((2R,4S,5R)-5-(((tert-butyldimethylsilyl)oxy)methyl)-4-((4-methoxybenzyl)oxy)-2-methyltetrahydrofuran-2-yl)methyl)tetrahydrofuran-2-yl)-6-hydroxy-2-methyl-3-((triethylsilyl)oxy)hexanoyl)oxazolidin-2-one
(1R,4S,5R)-6-((R)-4-benzyl-2-oxooxazolidin-3-yl)-1-((2R,5S)-5-((S)-((tert-butyldimethylsilyl)oxy)((2R,4S,5R)-5-(((tert-butyldimethylsilyl)oxy)methyl)-4-((4-methoxybenzyl)oxy)-2-methyltetrahydrofuran-2-yl)methyl)tetrahydrofuran-2-yl)-5-methyl-6-oxo-4-((triethylsilyl)oxy)hexyl chloromethanesulfonate
Conditions | Yield |
---|---|
With pyridine at 0 - 20℃; for 2.5h; | 99% |
monochloromethanesulfonyl chloride
(4R,5R,6R)-1-<(tert-butyldimethylsilyl)oxy>-4,5,7-tris(benzyloxy)-2(E)-hepten-6-ol
(4R,5R,6R)-1-<(tert-butyldimethylsilyl)oxy>-6-<((chloromethyl)sulfonyl)oxy>-4,5,7-tris(benzyloxy)-2(E)-heptene
Conditions | Yield |
---|---|
In pyridine for 0.5h; Ambient temperature; | 98% |
With pyridine at 20℃; for 0.5h; | 98% |
With pyridine for 0.5h; Ambient temperature; |
monochloromethanesulfonyl chloride
Methanesulfonic acid (1S,2R)-3-(tert-butyl-diphenyl-silanyloxy)-1-[2-(tert-butyl-diphenyl-silanyloxy)-ethyl]-2-methyl-propyl ester
Chloro-methanesulfonic acid (1S,2R)-3-(tert-butyl-diphenyl-silanyloxy)-1-[2-(tert-butyl-diphenyl-silanyloxy)-ethyl]-2-methyl-propyl ester
Conditions | Yield |
---|---|
With pyridine at 0 - 20℃; for 0.5h; | 98% |
monochloromethanesulfonyl chloride
(R)-Pantolacton
Chloro-methanesulfonic acid (R)-4,4-dimethyl-2-oxo-tetrahydro-furan-3-yl ester
Conditions | Yield |
---|---|
With pyridine at 0 - 20℃; for 0.166667h; | 98% |
monochloromethanesulfonyl chloride
[(2R,4S,5R)-5-((4R,5S)-4-Allyl-2-phenyl-[1,3,2]dioxaborinan-5-yloxy)-2-phenyl-[1,3]dioxan-4-yl]-methanol
Chloro-methanesulfonic acid (2R,4S,5R)-5-((4R,5S)-4-allyl-2-phenyl-[1,3,2]dioxaborinan-5-yloxy)-2-phenyl-[1,3]dioxan-4-ylmethyl ester
Conditions | Yield |
---|---|
With 2,6-dimethylpyridine In dichloromethane at 21 - 23℃; | 98% |
monochloromethanesulfonyl chloride
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran at 5 - 25℃; for 2h; | 98% |
monochloromethanesulfonyl chloride
3-{1-[(chloromethyl)sulfonyl]2,3-dihydro-1H-indol-5-yl}-5-vinyl-3H-imidazo[4,5-b]pyridine
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 0.333333h; | 98% |
monochloromethanesulfonyl chloride
(S)-2-(aminomethyl)pyrrolidine-1-carboxylic acid tert-butyl ester
C11H21ClN2O4S
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; for 17h; | 98% |
Conditions | Yield |
---|---|
Stage #1: C31H46O10Si With pyridine; tetra-(n-butyl)ammonium iodide; pyridine hydrogenfluoride In dichloromethane at 0℃; Stage #2: monochloromethanesulfonyl chloride In dichloromethane at -30℃; | 98% |
Conditions | Yield |
---|---|
With 2,6-dimethylpyridine In dichloromethane at 0℃; for 1h; Inert atmosphere; | 98% |
monochloromethanesulfonyl chloride
(4R,5S,6R)-1-tert-butyldimethylsilyloxy-4,5,7-tribenzyloxy-2(E)-hepten-6-ol
(4R,5S,6R)-1-tert-butyldimethylsilyloxy-6-[(chloromethylsulfonyl)-oxy]-4,5,7-tribenzyloxy-2(E)-heptene
Conditions | Yield |
---|---|
With pyridine at 20℃; for 0.5h; Substitution; | 97% |
monochloromethanesulfonyl chloride
Conditions | Yield |
---|---|
With pyridine; dmap at 0 - 20℃; for 1.5h; | 97% |
monochloromethanesulfonyl chloride
Conditions | Yield |
---|---|
With pyridine at -10℃; for 4h; | 95% |
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